DTA measure 1program_3_Pb_updown Date: 2026923:918 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.15 s Mass = 1124.000 mg data_number = 1340 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3045 -1.2253 221.5679 222.7931 249.7010 2.1323 -1.2214 221.7010 222.9224 249.7006 2.8980 -1.2177 221.8283 223.0461 249.6978 3.7465 -1.2136 221.9705 223.1841 249.7029 4.5233 -1.2101 222.1214 223.3315 249.7009 5.3400 -1.2065 222.2858 223.4923 249.7080 6.1270 -1.2025 222.4559 223.6584 249.7162 6.9345 -1.1997 222.6260 223.8258 249.7263 7.7515 -1.1962 222.7862 223.9824 249.7460 8.5178 -1.1940 222.9140 224.1080 249.7650 9.3150 -1.1916 223.0631 224.2547 249.7933 10.1628 -1.1889 223.2320 224.4209 249.8142 10.9393 -1.1849 223.3739 224.5588 249.8533 11.7570 -1.1829 223.5248 224.7077 249.9013 12.5540 -1.1781 223.6915 224.8696 249.9403 13.3505 -1.1749 223.8422 225.0172 249.9964 14.1785 -1.1725 224.0046 225.1771 250.0408 14.9448 -1.1693 224.1544 225.3237 250.0614 15.7925 -1.1660 224.3281 225.4941 250.1120 16.5385 -1.1633 224.4628 225.6262 250.1574 17.3870 -1.1598 224.6230 225.7829 250.2217 18.1525 -1.1570 224.7749 225.9319 250.2983 18.9908 -1.1537 224.9245 226.0782 250.3589 19.7675 -1.1532 225.0875 226.2406 250.4172 20.5948 -1.1492 225.2444 226.3936 250.4732 21.3918 -1.1442 225.3763 226.5205 250.5513 22.1890 -1.1392 225.5125 226.6517 250.6268 22.9755 -1.1367 225.6570 226.7937 250.7160 23.7723 -1.1339 225.8027 226.9365 250.8122 24.6003 -1.1294 225.9536 227.0831 250.9193 25.3560 -1.1245 226.0974 227.2219 251.0078 26.2245 -1.1209 226.2650 227.3859 251.1220 26.9808 -1.1188 226.3918 227.5106 251.2173 27.8080 -1.1144 226.5412 227.6556 251.3296 28.6050 -1.1125 226.6852 227.7977 251.4323 29.4125 -1.1130 226.8235 227.9365 251.5512 30.1885 -1.1110 226.9749 228.0859 251.6609 31.0163 -1.1066 227.1449 228.2514 251.7767 31.8443 -1.1007 227.2933 228.3940 251.8867 32.6000 -1.0980 227.4206 228.5185 251.9917 33.4685 -1.0921 227.5954 228.6875 252.1086 34.1940 -1.0874 227.7440 228.8314 252.2108 35.0523 -1.0835 227.9091 228.9926 252.3546 35.8183 -1.0828 228.0404 229.1232 252.4574 36.6463 -1.0793 228.1891 229.2684 252.5769 37.4433 -1.0769 228.3220 229.3989 252.6927 38.2295 -1.0744 228.4519 229.5263 252.8037 39.0575 -1.0685 228.5937 229.6622 252.9318 39.8343 -1.0662 228.7306 229.7968 253.0541 40.6820 -1.0650 228.8820 229.9470 253.2127 41.4380 -1.0642 229.0161 230.0803 253.3292 42.2865 -1.0619 229.1602 230.2220 253.4654 43.0625 -1.0608 229.2969 230.3577 253.6109 43.8800 -1.0593 229.4377 230.4970 253.7274 44.6773 -1.0590 229.5840 230.6430 253.8448 45.4740 -1.0569 229.7301 230.7870 253.9561 46.3015 -1.0549 229.8757 230.9306 254.0867 47.0680 -1.0539 230.0093 231.0632 254.2005 47.9165 -1.0520 230.1713 231.2233 254.3566 48.6615 -1.0501 230.3015 231.3516 254.4877 49.5100 -1.0487 230.4748 231.5235 254.6288 50.2765 -1.0455 230.6196 231.6651 254.7572 51.1243 -1.0436 230.7683 231.8119 254.8956 51.8905 -1.0413 230.9191 231.9604 255.0050 52.7185 -1.0378 231.0465 232.0843 255.1311 53.5148 -1.0363 231.1952 232.2315 255.2630 54.3120 -1.0349 231.3302 232.3652 255.4062 55.1298 -1.0343 231.4737 232.5081 255.5367 55.9055 -1.0332 231.6071 232.6404 255.6710 56.7540 -1.0353 231.7516 232.7869 255.8104 57.5205 -1.0340 231.8775 232.9115 255.9401 58.3478 -1.0312 232.0238 233.0550 256.0698 59.1448 -1.0295 232.1818 233.2114 256.2011 59.9420 -1.0279 232.3093 233.3372 256.3351 60.7285 -1.0246 232.4478 233.4724 256.4595 61.5560 -1.0223 232.5922 233.6145 256.5944 62.3430 -1.0214 232.7239 233.7453 256.7184 63.1500 -1.0209 232.8731 233.8940 256.8649 63.9673 -1.0189 233.0153 234.0342 256.9933 64.7235 -1.0167 233.1465 234.1632 257.1245 65.5923 -1.0168 233.3087 234.3255 257.2544 66.3478 -1.0163 233.4297 234.4460 257.3914 67.1758 -1.0143 233.5865 234.6008 257.5243 67.9728 -1.0139 233.7248 234.7387 257.6493 68.7693 -1.0116 233.8674 234.8790 257.7953 69.5870 -1.0125 234.0347 235.0472 257.9391 70.3843 -1.0114 234.1865 235.1979 258.0898 71.2113 -1.0096 234.3295 235.3390 258.2216 71.9675 -1.0091 234.4482 235.4573 258.3308 72.8365 -1.0080 234.6091 235.6171 258.4518 73.5920 -1.0074 234.7587 235.7661 258.5824 74.4198 -1.0068 234.9012 235.9081 258.7205 75.2170 -1.0060 235.0274 236.0334 258.8466 76.0138 -1.0058 235.1644 236.1703 258.9532 76.8105 -1.0070 235.3064 236.3134 259.0834 77.5975 -1.0060 235.4480 236.4540 259.1964 78.4663 -1.0046 235.6154 236.6200 259.3061 79.1910 -1.0038 235.7430 236.7468 259.4023 80.0395 -1.0040 235.8998 236.9038 259.5306 80.8058 -1.0028 236.0379 237.0406 259.6582 81.6638 -1.0053 236.1895 237.1948 259.8001 82.4303 -1.0052 236.3428 237.3480 259.9309 83.2583 -1.0041 236.4965 237.5005 260.0478 84.0135 -1.0033 236.6171 237.6204 260.1580 84.8415 -1.0021 236.7655 237.7675 260.2739 85.6388 -0.9998 236.9270 237.9268 260.4229 86.4355 -0.9998 237.0571 238.0569 260.5449 87.2528 -0.9993 237.1926 238.1918 260.6706 88.0295 -0.9974 237.3252 238.3226 260.7813 88.8780 -0.9975 237.4812 238.4787 260.9059 89.6435 -0.9987 237.6161 238.6148 261.0220 90.4715 -1.0001 237.7610 238.7611 261.1470 91.2380 -0.9987 237.8897 238.8885 261.2734 92.0855 -0.9999 238.0263 239.0262 261.3903 92.8623 -1.0029 238.1521 239.1550 261.5025 93.6798 -1.0039 238.3099 239.3138 261.6317 94.4455 -1.0041 238.4398 239.4439 261.7346 95.2735 -1.0041 238.5901 239.5942 261.8543 96.0605 -1.0050 238.7445 239.7495 261.9459 96.8568 -1.0042 238.8869 239.8911 262.0545 97.6848 -1.0029 239.0354 240.0384 262.1848 98.4513 -1.0025 239.1651 240.1676 262.3037 99.2993 -1.0027 239.3081 240.3108 262.4261 100.0653 -1.0004 239.4383 240.4388 262.5485 100.9138 -1.0001 239.5917 240.5918 262.6846 101.6493 -0.9990 239.7128 240.7119 262.8170 102.5175 -0.9923 239.8543 240.8466 262.9545 103.2738 -0.9912 239.9947 240.9859 263.0707 104.1018 -0.9960 240.1650 241.1610 263.2030 104.8983 -0.9981 240.3013 241.2995 263.3477 105.6850 -1.0011 240.4414 241.4425 263.4868 106.5130 -1.0011 240.5811 241.5822 263.6255 107.2793 -1.0011 240.7104 241.7115 263.7561 108.1065 -1.0026 240.8541 241.8567 263.9006 108.8730 -1.0026 240.9887 241.9914 264.0368 109.7215 -1.0010 241.1482 242.1492 264.1831 110.4973 -0.9978 241.2910 242.2889 264.3119 111.3253 -0.9975 241.4491 242.4466 264.4551 112.0815 -1.0004 241.5883 242.5887 264.5883 112.9398 -1.0026 241.7568 242.7593 264.7466 113.6955 -1.0008 241.8850 242.8859 264.8889 114.5235 -1.0022 242.0285 243.0307 265.0360 115.3205 -0.9971 242.1763 243.1734 265.1875 116.1170 -0.9951 242.3188 243.3139 265.3257 116.9348 -0.9963 242.4737 243.4700 265.4700 117.7113 -0.9967 242.5877 243.5844 265.6083 118.5590 -0.9981 242.7282 243.7263 265.7740 119.3255 -1.0002 242.8487 243.8490 265.9051 120.1535 -1.0027 242.9858 243.9885 266.0500 120.9395 -1.0024 243.1283 244.1307 266.1858 121.7573 -1.0016 243.2583 244.2599 266.3146 122.5340 -1.0040 243.3879 244.3919 266.4412 123.3615 -1.0035 243.5389 244.5424 266.5842 124.1480 -1.0041 243.6764 244.6804 266.7181 124.9453 -1.0083 243.8136 244.8220 266.8466 125.7733 -1.0114 243.9543 244.9656 266.9964 126.5285 -1.0136 244.0915 245.1052 267.1366 127.3975 -1.0150 244.2316 245.2465 267.2963 128.1230 -1.0155 244.3546 245.3702 267.4389 128.9810 -1.0167 244.5170 245.5337 267.5905 129.7473 -1.0172 244.6582 245.6754 267.7108 130.5753 -1.0162 244.7994 245.8156 267.8401 131.3720 -1.0163 244.9544 245.9706 267.9785 132.1995 -1.0197 245.1085 246.1281 268.1249 132.9558 -1.0211 245.2329 246.2539 268.2524 133.7835 -1.0215 245.3970 246.4186 268.4029 134.5800 -1.0222 245.5341 246.5564 268.5358 135.3773 -1.0237 245.6654 246.6890 268.6739 136.1950 -1.0258 245.8057 246.8315 268.8199 136.9608 -1.0241 245.9472 246.9713 268.9463 137.8193 -1.0260 246.0977 247.1238 269.0873 138.5755 -1.0267 246.2273 247.2540 269.2128 139.4033 -1.0266 246.3743 247.4009 269.3380 140.1998 -1.0268 246.5030 247.5298 269.4758 140.9970 -1.0254 246.6433 247.6687 269.6102 141.8250 -1.0248 246.7760 247.8008 269.7489 142.6213 -1.0253 246.9093 247.9346 269.8876 143.4185 -1.0265 247.0387 248.0652 270.0244 144.2055 -1.0295 247.1893 248.2188 270.1553 145.0430 -1.0294 247.3589 248.3883 270.2867 145.7990 -1.0301 247.4841 248.5142 270.4115 146.6578 -1.0308 247.6377 248.6685 270.5557 147.4235 -1.0328 247.7772 248.8100 270.6940 148.2410 -1.0338 247.9389 248.9727 270.8363 149.0383 -1.0363 248.0734 249.1097 270.9727 149.8350 -1.0379 248.2065 249.2444 271.1142 150.6625 -1.0401 248.3316 249.3717 271.2565 151.4290 -1.0435 248.4693 249.5128 271.3837 152.2870 -1.0422 248.6215 249.6637 271.5261 153.0430 -1.0414 248.7653 249.8067 271.6546 153.8915 -1.0412 248.9305 249.9717 271.8122 154.6680 -1.0397 249.0705 250.1102 271.9244 155.4850 -1.0392 249.2052 250.2444 272.0600 156.2823 -1.0397 249.3352 250.3749 272.1987 157.0795 -1.0420 249.4644 250.5064 272.3248 157.9065 -1.0410 249.6217 250.6627 272.4640 158.6628 -1.0403 249.7655 250.8058 272.5796 159.5215 -1.0415 249.9304 250.9719 272.7196 160.2870 -1.0415 250.0588 251.1003 272.8554 161.1150 -1.0422 250.2147 251.2569 272.9925 161.9020 -1.0439 250.3459 251.3899 273.1242 162.7295 -1.0464 250.4885 251.5348 273.2454 163.4955 -1.0440 250.6151 251.6591 273.3682 164.3235 -1.0444 250.7468 251.7912 273.4948 165.1205 -1.0463 250.8858 251.9321 273.6092 165.9170 -1.0477 251.0252 252.0729 273.7350 166.7348 -1.0490 251.1740 252.2229 273.8786 167.5113 -1.0496 251.3025 252.3521 274.0074 168.3590 -1.0514 251.4462 252.4975 274.1477 169.1255 -1.0518 251.5848 252.6366 274.2707 169.9535 -1.0505 251.7352 252.7857 274.4222 170.7395 -1.0504 251.8665 252.9169 274.5435 171.5368 -1.0508 252.0088 253.0596 274.6716 172.3648 -1.0540 252.1604 253.2144 274.8045 173.1615 -1.0562 252.2984 253.3546 274.9116 173.9480 -1.0544 252.4433 253.4977 275.0412 174.7555 -1.0543 252.6028 253.6570 275.1764 175.5728 -1.0548 252.7599 253.8147 275.3156 176.3388 -1.0548 252.8978 253.9526 275.4210 177.1975 -1.0557 253.0260 254.0818 275.5613 177.9533 -1.0565 253.1571 254.2136 275.6743 178.7808 -1.0574 253.2994 254.3568 275.8137 179.5780 -1.0557 253.4408 254.4965 275.9445 180.3745 -1.0565 253.5919 254.6485 276.0687 181.2023 -1.0569 253.7403 254.7972 276.1943 181.9585 -1.0556 253.8659 254.9216 276.3222 182.8373 -1.0558 254.0198 255.0756 276.4487 183.5725 -1.0548 254.1401 255.1950 276.5430 184.4108 -1.0559 254.2859 255.3417 276.6681 185.1665 -1.0541 254.4492 255.5033 276.7834 186.0248 -1.0548 254.5992 255.6540 276.9155 186.7913 -1.0534 254.7351 255.7886 277.0206 187.6193 -1.0527 254.8872 255.9400 277.1235 188.4053 -1.0528 255.0246 256.0775 277.2269 189.2025 -1.0532 255.1686 256.2218 277.3279 189.9998 -1.0520 255.2919 256.3440 277.4390 190.7963 -1.0532 255.4218 256.4749 277.5671 191.6138 -1.0513 255.5634 256.6148 277.7037 192.3905 -1.0498 255.7229 256.7727 277.8320 193.2485 -1.0503 255.8809 256.9311 277.9675 194.0045 -1.0512 256.0210 257.0722 278.0709 194.8325 -1.0510 256.1596 257.2106 278.1975 195.5983 -1.0505 256.3045 257.3549 278.3197 196.4465 -1.0484 256.4610 257.5094 278.4473 197.2233 -1.0476 256.6068 257.6544 278.5413 198.0405 -1.0460 256.7555 257.8015 278.6631 198.8065 -1.0452 256.9017 257.9468 278.7597 199.6345 -1.0458 257.0695 258.1153 278.8697 200.4310 -1.0479 257.1973 258.2452 278.9759 201.2178 -1.0475 257.3389 258.3864 279.0877 202.0458 -1.0454 257.4900 258.5354 279.2178 202.8118 -1.0425 257.6213 258.6638 279.3286 203.7725 -1.0427 257.7989 258.8416 279.4615 204.6620 -1.0405 257.9417 258.9822 279.5715 205.4285 -1.0390 258.0751 259.1141 279.6696 206.2560 -1.0371 258.2215 259.2587 279.7840 207.0528 -1.0374 258.3661 259.4035 279.8899 207.8500 -1.0375 258.5153 259.5527 279.9782 208.6675 -1.0381 258.6706 259.7086 280.0803 209.4435 -1.0404 258.7950 259.8353 280.1695 210.2613 -1.0413 258.9230 259.9644 280.2713 211.0275 -1.0401 259.0820 260.1221 280.3872 211.8855 -1.0383 259.2618 260.3000 280.5073 212.6418 -1.0384 259.4071 260.4455 280.6230 213.4698 -1.0356 259.5604 260.5960 280.7640 214.2660 -1.0334 259.7024 260.7358 280.8954 215.0633 -1.0296 259.8397 260.8693 280.9987 215.8810 -1.0288 259.9794 261.0082 281.1126 216.6468 -1.0260 260.1314 261.1575 281.2398 217.5053 -1.0233 260.2881 261.3114 281.3705 218.2718 -1.0232 260.4129 261.4361 281.4998 219.0888 -1.0199 260.5702 261.5902 281.6664 219.8858 -1.0180 260.7055 261.7235 281.8015 220.6830 -1.0162 260.8302 261.8465 281.9368 221.5003 -1.0144 260.9769 261.9913 282.0802 222.2765 -1.0124 261.1285 262.1409 282.2264 223.1250 -1.0096 261.2674 262.2770 282.3710 223.8605 -1.0086 261.4061 262.4147 282.5035 224.7185 -1.0061 261.5583 262.5644 282.6641 225.4850 -1.0055 261.6954 262.7009 282.7934 226.3130 -1.0056 261.8337 262.8393 282.9321 227.0990 -1.0049 261.9724 262.9772 283.0564 227.9065 -1.0056 262.1099 263.1155 283.1954 228.7243 -1.0032 262.2629 263.2661 283.3376 229.4798 -1.0006 262.4027 263.4033 283.4645 230.3485 -1.0001 262.5690 263.5691 283.6016 231.1048 -0.9996 262.7075 263.7072 283.7406 231.9218 -0.9964 262.8490 263.8454 283.8841 232.7290 -0.9941 263.0133 264.0075 284.0091 233.5160 -0.9919 263.1450 264.1369 284.1477 234.3435 -0.9880 263.2860 264.2740 284.2825 235.1095 -0.9862 263.4125 264.3987 284.4143 235.9683 -0.9854 263.5765 264.5619 284.5617 236.7343 -0.9848 263.7140 264.6987 284.7036 237.5515 -0.9854 263.8620 264.8474 284.8475 238.3590 -0.9830 263.9967 264.9797 284.9799 239.1458 -0.9790 264.1337 265.1127 285.1101 239.9730 -0.9783 264.2796 265.2579 285.2518 240.7395 -0.9762 264.4252 265.4015 285.3794 241.5880 -0.9742 264.5769 265.5511 285.5134 242.3538 -0.9739 264.7083 265.6823 285.6410 243.1815 -0.9734 264.8512 265.8247 285.7907 243.9788 -0.9725 265.0072 265.9796 285.9191 244.9605 -0.9695 265.1714 266.1409 286.0826 245.7875 -0.9692 265.3255 266.2947 286.2211 246.5540 -0.9683 265.4675 266.4358 286.3586 247.4025 -0.9660 265.6228 266.5888 286.4885 248.1785 -0.9640 265.7424 266.7065 286.6230 248.9960 -0.9615 265.8897 266.8512 286.7654 249.7830 -0.9567 266.0248 266.9815 286.8867 250.5898 -0.9549 266.1707 267.1256 287.0295 251.4073 -0.9523 266.3215 267.2738 287.1716 252.1635 -0.9502 266.4616 267.4118 287.2974 253.0323 -0.9492 266.6171 267.5663 287.4571 253.7878 -0.9480 266.7456 267.6936 287.5820 254.6158 -0.9475 266.9030 267.8505 287.7189 255.4130 -0.9438 267.0424 267.9861 287.8458 256.2093 -0.9405 267.1872 268.1278 287.9756 257.0270 -0.9384 267.3370 268.2755 288.0941 257.7935 -0.9372 267.4791 268.4162 288.2107 258.6518 -0.9350 267.6421 268.5771 288.3459 259.4178 -0.9342 267.7839 268.7181 288.4840 260.2355 -0.9318 267.9241 268.8559 288.6318 261.0430 -0.9286 268.0739 269.0025 288.7746 261.8290 -0.9271 268.2132 269.1403 288.8943 262.6570 -0.9259 268.3729 269.2988 289.0330 263.4235 -0.9231 268.5145 269.4376 289.1567 264.2710 -0.9202 268.6575 269.5776 289.3034 265.0375 -0.9172 268.7899 269.7071 289.4236 265.8655 -0.9174 268.9410 269.8585 289.5374 266.6620 -0.9150 269.0947 270.0097 289.6791 267.4590 -0.9123 269.2558 270.1682 289.8040 268.2768 -0.9103 269.4191 270.3295 289.9370 269.0528 -0.9096 269.5654 270.4750 290.0550 269.9010 -0.9072 269.7174 270.6246 290.1846 270.6880 -0.9048 269.8577 270.7626 290.3222 271.4955 -0.9023 269.9973 270.8996 290.4458 272.3125 -0.9026 270.1642 271.0668 290.5675 273.0788 -0.9002 270.3023 271.2024 290.6954 273.9375 -0.8985 270.4652 271.3637 290.8357 274.7035 -0.8971 270.5863 271.4833 290.9654 275.6745 -0.8945 270.7603 271.6549 291.1157 276.5435 -0.8934 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