DTA measure 1program_4_Pb_updown Date: 2026923:1021 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.50 s Mass = 1124.000 mg data_number = 1071 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5115 -0.9279 224.8842 225.8121 201.2521 4.1318 -0.9238 224.7815 225.7054 201.1527 5.7519 -0.9195 224.6914 225.6109 201.0573 7.5316 -0.9173 224.5914 225.5087 200.9656 9.1366 -0.9169 224.5011 225.4180 200.8820 10.7414 -0.9127 224.4199 225.3326 200.8038 12.3314 -0.9102 224.2986 225.2088 200.7308 13.9519 -0.9078 224.1980 225.1058 200.6586 15.5515 -0.9027 224.1174 225.0201 200.6389 17.1616 -0.8982 224.0276 224.9258 200.5857 18.7620 -0.8930 223.9316 224.8245 200.5450 20.3668 -0.8928 223.8505 224.7433 200.5248 21.9766 -0.8920 223.7487 224.6406 200.5233 23.5664 -0.8882 223.6571 224.5453 200.5214 25.1769 -0.8876 223.5626 224.4502 200.5600 26.7919 -0.8862 223.4560 224.3422 200.5748 28.3970 -0.8825 223.3677 224.2501 200.5710 30.0075 -0.8760 223.2487 224.1246 200.5743 31.6071 -0.8731 223.1597 224.0328 200.6166 33.2119 -0.8727 223.0833 223.9560 200.6858 34.8176 -0.8736 222.9961 223.8696 200.7441 36.4070 -0.8748 222.8918 223.7665 200.8059 38.0119 -0.8707 222.7951 223.6658 200.8781 39.6329 -0.8676 222.7091 223.5767 200.9596 41.2325 -0.8675 222.6213 223.4888 201.0449 42.8428 -0.8678 222.5166 223.3844 201.1368 44.4430 -0.8695 222.4359 223.3054 201.2487 46.0478 -0.8710 222.3167 223.1877 201.3637 47.6525 -0.8658 222.1928 223.0586 201.4740 49.2581 -0.8646 222.1014 222.9661 201.5960 50.8733 -0.8649 222.0354 222.9003 201.7067 52.4678 -0.8603 221.9485 222.8088 201.8419 54.0725 -0.8588 221.8825 222.7413 201.9657 55.6779 -0.8584 221.7851 222.6436 202.0955 57.2779 -0.8578 221.7037 222.5614 202.2372 58.8826 -0.8578 221.5911 222.4489 202.3732 60.4874 -0.8588 221.5032 222.3620 202.5108 62.1085 -0.8587 221.4159 222.2745 202.6424 63.7286 -0.8581 221.3370 222.1951 202.7926 65.3334 -0.8583 221.2480 222.1062 202.9414 66.9230 -0.8571 221.1453 222.0024 203.1084 68.5336 -0.8612 221.0462 221.9074 203.2496 70.1333 -0.8621 220.9511 221.8132 203.3891 71.7380 -0.8632 220.8723 221.7355 203.5515 73.3483 -0.8654 220.7744 221.6398 203.7064 74.9639 -0.8659 220.6942 221.5601 203.8513 76.5686 -0.8727 220.6276 221.5003 203.9795 78.1788 -0.8735 220.5615 221.4350 204.1405 79.7791 -0.8729 220.5158 221.3887 204.3089 81.3839 -0.8750 220.4329 221.3079 204.4751 82.9886 -0.8791 220.3750 221.2541 204.6380 84.6200 -0.8784 220.2921 221.1705 204.8041 86.2299 -0.8810 220.2468 221.1278 204.9869 87.8193 -0.8861 220.1628 221.0488 205.1614 89.4244 -0.8881 220.0845 220.9726 205.3218 91.0298 -0.8868 220.0101 220.8969 205.4817 92.6345 -0.8888 219.9311 220.8198 205.6352 94.2444 -0.8923 219.8497 220.7420 205.7929 95.8496 -0.8982 219.8048 220.7030 205.9457 97.4651 -0.8991 219.7281 220.6272 206.1064 99.2544 -0.9014 219.6580 220.5594 206.2708 100.8701 -0.9035 219.6081 220.5116 206.4199 102.4700 -0.9099 219.5492 220.4590 206.5827 104.0799 -0.9093 219.4783 220.3875 206.7708 105.6805 -0.9113 219.4077 220.3190 206.9324 107.2904 -0.9120 219.3396 220.2517 207.0977 108.8951 -0.9148 219.2954 220.2101 207.2703 110.5108 -0.9155 219.2341 220.1495 207.4475 112.1056 -0.9157 219.1707 220.0864 207.6261 113.7104 -0.9178 219.1302 220.0480 207.8017 115.3100 -0.9186 219.0803 219.9989 207.9825 116.9205 -0.9228 219.0198 219.9426 208.1569 118.5205 -0.9252 218.9756 219.9008 208.3255 120.1304 -0.9280 218.9521 219.8801 208.5117 121.7300 -0.9314 218.9232 219.8546 208.6914 123.3358 -0.9319 218.8785 219.8105 208.8969 124.9456 -0.9356 218.8464 219.7820 209.0785 126.5403 -0.9396 218.8190 219.7586 209.2687 128.1459 -0.9422 218.7761 219.7184 209.4566 129.7558 -0.9425 218.7399 219.6823 209.6431 131.3608 -0.9429 218.7197 219.6625 209.8389 132.9560 -0.9415 218.6875 219.6290 210.0249 134.5556 -0.9444 218.6627 219.6071 210.2176 136.1606 -0.9434 218.6187 219.5621 210.4255 137.7866 -0.9456 218.5799 219.5255 210.6102 139.3863 -0.9476 218.5517 219.4993 210.7992 140.9859 -0.9488 218.5308 219.4797 210.9797 142.5810 -0.9519 218.5077 219.4596 211.1672 144.1861 -0.9510 218.4918 219.4427 211.3453 145.7858 -0.9540 218.4712 219.4252 211.5174 147.3964 -0.9567 218.4417 219.3984 211.7061 148.9963 -0.9577 218.4241 219.3818 211.9005 150.6010 -0.9594 218.4320 219.3914 212.0636 152.2110 -0.9588 218.4058 219.3647 212.2618 153.8269 -0.9597 218.3732 219.3329 212.4429 155.4316 -0.9623 218.3625 219.3248 212.6010 157.0415 -0.9650 218.3770 219.3420 212.7631 158.6416 -0.9664 218.3845 219.3509 212.9204 160.2366 -0.9673 218.4004 219.3677 213.0901 161.8568 -0.9702 218.3936 219.3638 213.2557 163.4564 -0.9686 218.3796 219.3482 213.4344 165.0568 -0.9686 218.3653 219.3339 213.5943 166.6669 -0.9699 218.3843 219.3542 213.7698 168.2870 -0.9707 218.3963 219.3670 213.9578 169.8665 -0.9707 218.3537 219.3244 214.1429 171.5026 -0.9724 218.3444 219.3168 214.3589 173.1023 -0.9730 218.3592 219.3322 214.5459 174.7019 -0.9738 218.3887 219.3625 214.7057 176.3119 -0.9735 218.3894 219.3629 214.8923 177.9175 -0.9740 218.3857 219.3597 215.0764 179.5171 -0.9766 218.3855 219.3620 215.2592 181.1219 -0.9784 218.4168 219.3952 215.4448 182.7271 -0.9791 218.4367 219.4157 215.6183 184.3324 -0.9811 218.4517 219.4327 215.8021 185.9525 -0.9804 218.4675 219.4479 215.9839 187.5526 -0.9812 218.4805 219.4617 216.1587 189.1579 -0.9821 218.5053 219.4874 216.3541 190.7524 -0.9834 218.5126 219.4960 216.5328 192.3725 -0.9843 218.5580 219.5423 216.7318 193.9781 -0.9837 218.5868 219.5706 216.9283 195.5881 -0.9867 218.6294 219.6161 217.1000 197.1878 -0.9863 218.6427 219.6290 217.2914 198.7925 -0.9846 218.6518 219.6364 217.4949 200.3983 -0.9865 218.6858 219.6723 217.6967 202.0030 -0.9857 218.7347 219.7205 217.8997 203.6231 -0.9830 218.7803 219.7633 218.1190 205.2284 -0.9847 218.8066 219.7914 218.3570 206.8336 -0.9840 218.8448 219.8288 218.5558 208.4230 -0.9832 218.8637 219.8469 218.7348 210.0279 -0.9848 218.8787 219.8635 218.9016 211.6438 -0.9872 218.9023 219.8896 219.0809 213.2485 -0.9874 218.9382 219.9256 219.2847 214.8430 -0.9880 218.9918 219.9798 219.4884 216.4434 -0.9882 219.0500 220.0382 219.6714 218.0484 -0.9877 219.1052 220.0928 219.8690 219.6736 -0.9857 219.1582 220.1439 220.0486 221.2533 -0.9830 219.1835 220.1665 220.2379 222.8790 -0.9809 219.2169 220.1978 220.4244 224.4838 -0.9827 219.2788 220.2615 220.5848 226.0885 -0.9838 219.3420 220.3258 220.7748 227.6941 -0.9833 219.3874 220.3707 220.9847 229.2939 -0.9845 219.4394 220.4240 221.1573 230.8986 -0.9848 219.4981 220.4830 221.3332 232.5090 -0.9889 219.5443 220.5332 221.5116 234.1194 -0.9889 219.6359 220.6247 221.7060 235.7036 -0.9878 219.6872 220.6750 221.8919 237.3084 -0.9886 219.7337 220.7223 222.0740 238.9339 -0.9910 219.7813 220.7722 222.2561 240.5343 -0.9900 219.8368 220.8268 222.4815 242.1236 -0.9901 219.9005 220.8906 222.6780 243.7386 -0.9889 219.9636 220.9525 222.8827 245.3495 -0.9889 220.0376 221.0265 223.0747 246.9543 -0.9884 220.0940 221.0825 223.2947 248.5641 -0.9869 220.1536 221.1406 223.5125 250.1645 -0.9838 220.2161 221.1999 223.6966 251.7798 -0.9861 220.2728 221.2589 223.8886 253.3691 -0.9874 220.3361 221.3235 224.0846 254.9739 -0.9896 220.4075 221.3970 224.2851 256.5949 -0.9892 220.4812 221.4704 224.4775 258.1946 -0.9896 220.5756 221.5652 224.6791 259.8045 -0.9916 220.6458 221.6375 224.8611 261.3939 -0.9961 220.7263 221.7224 225.0763 262.9995 -0.9986 220.8188 221.8174 225.2837 264.6095 -0.9969 220.9078 221.9046 225.4717 266.2143 -0.9980 220.9732 221.9712 225.6679 267.8196 -1.0007 221.0388 222.0395 225.8458 269.4248 -1.0029 221.1188 222.1217 226.0070 271.0244 -1.0005 221.2021 222.2026 226.1867 272.6453 -0.9996 221.2899 222.2895 226.3755 274.2349 -1.0020 221.3719 222.3739 226.5516 275.8550 -1.0014 221.4593 222.4606 226.7269 277.4555 -1.0015 221.5664 222.5679 226.8998 279.0655 -0.9996 221.6446 222.6442 227.1051 280.6703 -1.0004 221.7491 222.7496 227.2876 282.2751 -1.0000 221.8457 222.8456 227.4757 283.8806 -1.0002 221.9212 222.9214 227.6725 285.4804 -1.0004 222.0153 223.0157 227.8785 287.1056 -0.9960 222.1197 223.1157 228.0979 288.7059 -0.9966 222.2117 223.2082 228.3094 290.3110 -0.9987 222.3224 223.3212 228.5022 291.9209 -0.9971 222.4374 223.4345 228.7031 293.5206 -0.9966 222.5257 223.5223 228.9127 295.1416 -0.9962 222.6229 223.6192 229.1055 296.7413 -0.9963 222.7227 223.7190 229.3280 298.3511 -0.9980 222.8140 223.8120 229.5290 299.9564 -0.9994 222.9041 223.9035 229.7508 301.5668 -0.9991 223.0230 224.0221 229.9587 303.1818 -1.0004 223.1338 224.1342 230.1544 304.7711 -1.0030 223.2368 224.2398 230.3752 306.3916 -1.0022 223.3395 224.3417 230.5806 307.9970 -1.0023 223.4632 224.4656 230.7642 309.5864 -1.0016 223.5624 224.5640 230.9636 311.1864 -0.9989 223.6714 224.6703 231.1478 312.7969 -0.9953 223.7734 224.7688 231.3403 314.3965 -0.9938 223.8634 224.8572 231.5326 316.0013 -0.9930 223.9532 224.9462 231.7225 317.6115 -0.9925 224.0611 225.0536 231.9246 319.2169 -0.9900 224.1657 225.1557 232.1108 320.8268 -0.9909 224.3005 225.2913 232.2952 322.4315 -0.9918 224.4415 225.4333 232.4579 324.0313 -0.9903 224.5703 225.5607 232.6452 325.6471 -0.9899 224.6843 225.6742 232.8465 327.2519 -0.9898 224.8068 225.7966 233.0222 328.8566 -0.9891 224.9297 225.9188 233.1953 330.4415 -0.9875 225.0548 226.0423 233.3469 332.0518 -0.9902 225.1824 226.1726 233.5149 333.6616 -0.9896 225.3151 226.3047 233.6948 335.2613 -0.9886 225.4418 226.4304 233.8840 336.8718 -0.9896 225.5810 226.5706 234.0679 338.4718 -0.9908 225.6896 226.6803 234.2777 340.0765 -0.9917 225.8013 226.7929 234.5132 341.6974 -0.9875 225.9372 226.9247 234.7059 343.3024 -0.9855 226.0714 227.0570 234.9012 344.9071 -0.9882 226.1815 227.1697 235.1018 346.5121 -0.9889 226.3232 227.3121 235.3304 348.1125 -0.9884 226.4571 227.4455 235.5492 349.7173 -0.9864 226.5849 227.5713 235.7631 351.3118 -0.9859 226.7017 227.6876 235.9927 352.9171 -0.9836 226.8262 227.8098 236.2167 354.5376 -0.9853 226.9507 227.9360 236.4650 356.1270 -0.9864 227.0869 228.0733 236.6827 357.7270 -0.9852 227.2221 228.2074 236.9166 359.3324 -0.9882 227.3451 228.3334 237.1365 360.9525 -0.9870 227.4796 228.4666 237.3516 362.5524 -0.9888 227.6112 228.6000 237.5634 364.1630 -0.9892 227.7372 228.7264 237.7686 365.7678 -0.9870 227.8764 228.8634 237.9925 367.3726 -0.9883 228.0247 229.0130 238.2137 368.9783 -0.9900 228.1712 229.1612 238.4512 370.5881 -0.9882 228.3163 229.3045 238.6868 372.1929 -0.9860 228.4668 229.4528 238.9091 373.7983 -0.9875 228.6146 229.6021 239.1320 375.4188 -0.9872 228.7608 229.7480 239.3478 377.0030 -0.9903 228.8902 229.8805 239.5531 378.6180 -0.9911 229.0282 230.0192 239.7791 380.2231 -0.9899 229.1867 230.1766 239.9842 381.8285 -0.9904 229.3236 230.3140 240.1799 383.4333 -0.9910 229.4687 230.4597 240.3975 385.0534 -0.9931 229.6336 230.6267 240.6149 386.6489 -0.9964 229.7679 230.7644 240.8029 388.2485 -0.9952 229.9087 230.9039 241.0057 389.8584 -0.9935 230.0745 231.0680 241.1902 391.4635 -0.9907 230.2376 231.2283 241.3802 393.0791 -0.9882 230.3710 231.3592 241.5779 394.6890 -0.9895 230.4993 231.4888 241.7778 396.3040 -0.9894 230.6517 231.6412 241.9778 397.9096 -0.9886 230.8053 231.7938 242.1727 399.5094 -0.9904 230.9744 231.9648 242.3889 401.1193 -0.9922 231.1546 232.1468 242.5956 402.7191 -0.9916 231.3058 232.2975 242.7803 404.3298 -0.9912 231.4790 232.4702 242.9510 405.9499 -0.9917 231.6383 232.6300 243.1330 407.5393 -0.9885 231.7743 232.7629 243.3255 409.1549 -0.9893 231.9357 232.9250 243.5328 410.7498 -0.9915 232.0919 233.0834 243.7197 412.3545 -0.9908 232.2419 233.2327 243.9183 413.9596 -0.9937 232.4018 233.3955 244.1085 415.5701 -0.9945 232.5924 233.5869 244.2878 417.1698 -0.9939 232.7469 233.7409 244.4698 418.7643 -0.9936 232.8956 233.8892 244.6525 420.3903 -0.9959 233.0728 234.0687 244.8363 421.9799 -0.9954 233.2307 234.2261 245.0291 423.5795 -0.9963 233.3799 234.3762 245.2298 425.1999 -0.9973 233.5372 234.5344 245.4159 426.8054 -0.9955 233.7216 234.7171 245.5987 428.4153 -0.9937 233.8662 234.8599 245.7832 430.0251 -0.9937 234.0173 235.0110 245.9760 431.6251 -0.9959 234.1722 235.1681 246.1466 433.2356 -0.9967 234.3520 235.3487 246.3422 434.8353 -0.9965 234.5285 235.5250 246.5449 436.4605 -0.9955 234.7123 235.7078 246.7428 438.0456 -0.9972 234.8792 235.8764 246.9274 439.6556 -0.9946 235.0330 236.0276 247.1218 441.2553 -0.9942 235.2014 236.1956 247.3246 442.8764 -0.9932 235.3883 236.3815 247.5425 444.4811 -0.9900 235.5633 236.5533 247.7635 446.0910 -0.9888 235.7145 236.7033 247.9817 447.6858 -0.9884 235.8988 236.8872 248.1795 449.2964 -0.9859 236.0773 237.0632 248.4042 450.8960 -0.9867 236.2456 237.2323 248.6396 452.5008 -0.9886 236.4325 237.4211 248.8682 454.1111 -0.9887 236.6203 237.6090 249.0973 455.7113 -0.9852 236.7718 237.7570 249.3261 457.3416 -0.9866 236.9343 237.9209 249.5716 458.9211 -0.9876 237.1048 238.0924 249.8007 460.5419 -0.9864 237.2865 238.2729 250.0288 462.1466 -0.9858 237.4616 238.4474 250.2746 463.7569 -0.9890 237.6461 238.6351 250.4995 465.3571 -0.9903 237.8191 238.8094 250.7291 466.9568 -0.9900 237.9884 238.9784 250.9683 468.5666 -0.9898 238.1636 239.1533 251.1933 470.1719 -0.9938 238.3437 239.3375 251.4329 471.7720 -0.9962 238.5437 239.5399 251.6634 473.3819 -0.9969 238.7312 239.7282 251.8906 474.9969 -0.9963 238.8915 239.8877 252.0767 476.6023 -0.9986 239.0500 240.0486 252.2813 478.2074 -0.9993 239.2404 240.2397 252.4890 479.8121 -0.9988 239.3980 240.3968 252.7043 481.4171 -1.0003 239.5749 240.5752 252.9272 483.0278 -1.0023 239.7544 240.7567 253.1582 484.6274 -1.0016 239.9283 240.9298 253.3920 486.2321 -1.0018 240.1132 241.1149 253.6143 487.8580 -1.0039 240.3129 241.3169 253.8448 489.4426 -1.0072 240.5216 241.5288 254.0342 491.0474 -1.0080 240.6966 241.7046 254.2120 492.6728 -1.0090 240.8713 241.8803 254.4097 494.2733 -1.0075 241.0514 242.0589 254.6086 495.8780 -1.0080 241.2359 242.2439 254.8049 497.4831 -1.0085 241.4059 242.4144 254.9896 499.0885 -1.0125 241.6055 242.6180 255.2073 500.6984 -1.0123 241.7927 242.8050 255.4043 502.2980 -1.0135 241.9997 243.0131 255.5900 503.9184 -1.0134 242.1780 243.1914 255.7863 505.5239 -1.0158 242.3542 243.3700 255.9820 507.1286 -1.0195 242.5406 243.5601 256.1842 508.7231 -1.0197 242.7227 243.7424 256.3830 510.3391 -1.0187 242.9232 243.9419 256.5738 511.9593 -1.0197 243.1309 244.1506 256.7728 513.5486 -1.0208 243.3391 244.3599 256.9575 515.1490 -1.0201 243.5251 244.5452 257.1332 516.7591 -1.0179 243.6956 244.7135 257.3106 518.3741 -1.0185 243.8899 244.9084 257.4856 519.9791 -1.0214 244.0691 245.0905 257.6631 521.5898 -1.0230 244.2703 245.2933 257.8714 523.2048 -1.0265 244.4643 245.4907 258.0377 524.8098 -1.0265 244.6537 245.6802 258.2258 526.4153 -1.0266 244.8539 245.8805 258.4151 528.0251 -1.0253 245.0450 246.0703 258.6031 529.6248 -1.0265 245.2273 246.2538 258.7694 531.2251 -1.0274 245.4208 246.4481 258.9232 532.8353 -1.0285 245.6241 246.6526 259.0898 534.4349 -1.0315 245.8115 246.8430 259.2904 536.0448 -1.0334 246.0118 247.0452 259.4613 537.6659 -1.0364 246.2178 247.2542 259.6397 539.2604 -1.0383 246.4056 247.4439 259.8150 540.8754 -1.0405 246.6107 247.6512 259.9887 542.4804 -1.0408 246.8086 247.8495 260.1523 544.0859 -1.0412 246.9986 248.0398 260.3402 545.6906 -1.0441 247.1860 248.2301 260.5404 547.2954 -1.0441 247.3747 248.4189 260.7630 548.9111 -1.0423 247.5702 248.6125 260.9677 550.5264 -1.0448 247.7673 248.8122 261.1819 552.1260 -1.0495 247.9823 249.0318 261.4031 553.7464 -1.0494 248.1886 249.2380 261.6293 555.3519 -1.0502 248.3879 249.4382 261.8320 556.9515 -1.0521 248.6143 249.6664 262.0381 558.5566 -1.0535 248.7894 249.8429 262.2578 560.1569 -1.0538 248.9599 250.0137 262.4693 561.7668 -1.0561 249.1452 250.2013 262.6730 563.3869 -1.0593 249.3476 250.4069 262.8953 564.9925 -1.0606 249.5513 250.6119 263.1223 566.6076 -1.0603 249.7593 250.8196 263.3234 568.2124 -1.0619 249.9585 251.0204 263.5172 569.8071 -1.0665 250.1439 251.2104 263.7212 571.4229 -1.0651 250.3540 251.4190 263.9591 573.0276 -1.0650 250.5619 251.6269 264.1898 574.6278 -1.0662 250.7415 251.8076 264.4132 576.2381 -1.0679 250.9481 252.0159 264.6252 577.8429 -1.0668 251.1483 252.2152 264.8487 579.4581 -1.0676 251.3627 252.4303 265.0649 581.0534 -1.0721 251.5418 252.6139 265.2778 582.6581 -1.0772 251.7654 252.8426 265.4782 584.2733 -1.0816 251.9895 253.0710 265.6954 585.8840 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