DTA measure 3program_3_Pb_updown Date: 2026923:949 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1645.74 s Mass = 1124.000 mg data_number = 1022 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5829 -4.3642 428.4969 432.8611 406.8329 4.1830 -4.3684 428.4703 432.8387 406.8580 5.7929 -4.3743 428.4209 432.7951 406.8983 7.4034 -4.3772 428.3665 432.7437 406.8817 8.9983 -4.3838 428.3282 432.7121 406.8747 10.6081 -4.3891 428.2973 432.6864 406.8534 12.2135 -4.3947 428.2453 432.6401 406.8140 13.8135 -4.4046 428.2109 432.6155 406.7573 15.4388 -4.4137 428.1612 432.5749 406.7174 17.0393 -4.4189 428.1144 432.5333 406.6270 18.6441 -4.4250 428.0499 432.4750 406.5732 20.2490 -4.4316 427.9935 432.4250 406.4635 21.8495 -4.4346 427.9655 432.4001 406.3481 23.4543 -4.4384 427.9378 432.3762 406.2321 25.0641 -4.4399 427.8953 432.3352 406.0891 26.6699 -4.4440 427.8435 432.2875 405.9594 28.2849 -4.4468 427.7958 432.2427 405.8250 29.8951 -4.4511 427.7430 432.1941 405.6737 31.5159 -4.4552 427.6994 432.1546 405.5336 33.1206 -4.4578 427.6621 432.1199 405.3747 34.7255 -4.4623 427.6058 432.0681 405.1818 36.3311 -4.4619 427.5459 432.0078 404.9923 37.9410 -4.4599 427.5053 431.9653 404.8155 39.5359 -4.4642 427.4549 431.9191 404.6152 41.1413 -4.4676 427.4071 431.8747 404.4145 42.7409 -4.4696 427.3361 431.8057 404.2202 44.3508 -4.4733 427.3008 431.7741 404.0267 45.9719 -4.4751 427.2418 431.7169 403.8279 47.5715 -4.4779 427.1758 431.6537 403.6477 49.1764 -4.4797 427.1175 431.5972 403.4723 50.7718 -4.4796 427.0728 431.5524 403.3069 52.3765 -4.4771 427.0120 431.4891 403.1216 53.9814 -4.4806 426.9479 431.4286 402.9356 55.5819 -4.4799 426.9001 431.3800 402.7610 57.1866 -4.4802 426.8283 431.3085 402.5917 58.8068 -4.4822 426.7569 431.2390 402.3979 60.3970 -4.4827 426.6864 431.1691 402.1889 62.0019 -4.4851 426.6132 431.0983 401.9881 63.6066 -4.4844 426.5396 431.0240 401.8102 65.2269 -4.4861 426.4670 430.9531 401.6011 66.8274 -4.4871 426.4055 430.8926 401.3986 68.4219 -4.4862 426.3245 430.8107 401.1824 70.0423 -4.4876 426.2507 430.7382 400.9895 71.6324 -4.4892 426.1668 430.6560 400.7980 73.2371 -4.4885 426.0897 430.5781 400.6012 74.8419 -4.4870 426.0161 430.5030 400.3845 76.4475 -4.4833 425.9309 430.4142 400.1802 78.0524 -4.4799 425.8471 430.3270 399.9812 79.8113 -4.4827 425.7597 430.2424 399.7723 81.4679 -4.4836 425.6876 430.1711 399.5491 83.0726 -4.4825 425.5924 430.0750 399.3477 84.6671 -4.4809 425.5041 429.9851 399.1473 86.2675 -4.4783 425.4400 429.9184 398.9487 87.8674 -4.4738 425.3748 429.8487 398.7449 89.4926 -4.4745 425.2954 429.7699 398.5647 91.0930 -4.4725 425.1959 429.6684 398.3802 92.6980 -4.4727 425.0986 429.5713 398.1978 94.3028 -4.4728 425.0042 429.4769 398.0014 95.9081 -4.4728 424.9100 429.3828 397.7767 97.5133 -4.4708 424.7988 429.2696 397.5732 99.1180 -4.4696 424.6915 429.1612 397.3797 100.7388 -4.4656 424.6157 429.0813 397.2109 102.3439 -4.4661 424.5059 428.9719 397.0373 103.9486 -4.4689 424.3816 428.8505 396.8865 105.5485 -4.4676 424.2874 428.7551 396.6895 107.1591 -4.4647 424.1904 428.6551 396.4917 108.7639 -4.4641 424.1032 428.5673 396.3181 110.5230 -4.4619 423.9937 428.4556 396.1239 112.1794 -4.4624 423.8890 428.3514 395.9400 113.7841 -4.4651 423.7714 428.2365 395.7610 115.3846 -4.4639 423.6604 428.1242 395.5887 116.9895 -4.4611 423.5330 427.9941 395.4026 118.6253 -4.4577 423.4031 427.8608 395.2015 120.2308 -4.4578 423.2788 427.7366 394.9852 121.8355 -4.4545 423.1774 427.6319 394.7815 123.4405 -4.4547 423.0688 427.5235 394.5871 125.0358 -4.4530 422.9798 427.4328 394.4109 126.6508 -4.4517 422.8463 427.2981 394.2313 128.2508 -4.4468 422.7219 427.1686 394.0462 129.8613 -4.4424 422.6112 427.0536 393.8425 131.4711 -4.4411 422.4944 426.9356 393.6347 133.0761 -4.4395 422.3819 426.8214 393.4500 134.6816 -4.4390 422.2820 426.7210 393.2567 136.2813 -4.4360 422.1507 426.5867 393.0454 137.8913 -4.4326 422.0391 426.4717 392.8409 139.4969 -4.4294 421.9124 426.3419 392.6474 141.2554 -4.4277 421.7861 426.2138 392.4535 142.9121 -4.4264 421.6555 426.0819 392.2818 144.5223 -4.4244 421.5320 425.9564 392.0990 146.1219 -4.4244 421.4033 425.8277 391.9217 147.7171 -4.4235 421.2736 425.6971 391.7252 149.3221 -4.4211 421.1454 425.5664 391.5299 150.9423 -4.4215 421.0044 425.4259 391.3660 152.5474 -4.4186 420.8696 425.2882 391.1977 154.1374 -4.4173 420.7517 425.1691 391.0034 155.7421 -4.4154 420.6034 425.0188 390.8120 157.3474 -4.4127 420.4808 424.8935 390.6328 158.9526 -4.4090 420.3385 424.7475 390.4524 160.5574 -4.4060 420.2225 424.6285 390.2572 162.1629 -4.4074 420.1161 424.5235 390.0462 163.7474 -4.4090 419.9607 424.3697 389.8447 165.3726 -4.4079 419.8059 424.2137 389.6509 166.9728 -4.4066 419.6677 424.0743 389.4597 168.5729 -4.4033 419.5425 423.9458 389.2809 170.1828 -4.4009 419.3840 423.7849 389.0819 171.7884 -4.3974 419.2528 423.6501 388.9136 173.3984 -4.3937 419.1143 423.5080 388.7338 174.9879 -4.3911 418.9703 423.3614 388.5097 176.5884 -4.3894 418.8185 423.2079 388.3001 178.2136 -4.3822 418.6688 423.0509 388.1034 179.8134 -4.3775 418.5280 422.9055 387.9097 181.4139 -4.3734 418.3944 422.7678 387.7115 183.0238 -4.3724 418.2602 422.6325 387.5366 184.6285 -4.3708 418.1283 422.4992 387.3495 186.2339 -4.3695 417.9892 422.3587 387.1696 187.8390 -4.3702 417.8406 422.2107 386.9961 189.4540 -4.3696 417.7026 422.0722 386.8122 191.0591 -4.3684 417.5463 421.9147 386.6508 192.6645 -4.3671 417.4146 421.7817 386.4645 194.2693 -4.3635 417.2773 421.6407 386.2653 195.8799 -4.3573 417.1276 421.4848 386.0946 197.4849 -4.3543 416.9799 421.3342 385.9004 199.0743 -4.3515 416.8391 421.1905 385.7058 200.6798 -4.3477 416.7091 421.0568 385.4988 202.2950 -4.3452 416.5399 420.8851 385.2885 203.8998 -4.3420 416.3800 420.7220 385.1031 205.5054 -4.3402 416.2177 420.5578 384.9101 207.1103 -4.3388 416.0530 420.3918 384.7125 208.7201 -4.3380 415.9124 420.2503 384.4887 210.3208 -4.3349 415.7711 420.1060 384.3075 211.9204 -4.3324 415.6255 419.9579 384.0887 213.5561 -4.3303 415.4634 419.7937 383.8639 215.1565 -4.3244 415.3102 419.6345 383.6551 216.7613 -4.3214 415.1610 419.4825 383.4347 218.3713 -4.3187 415.0392 419.3579 383.2398 219.9716 -4.3149 414.8823 419.1972 383.0409 221.5765 -4.3115 414.7264 419.0379 382.8364 223.3763 -4.3075 414.5617 418.8692 382.5857 225.0074 -4.3037 414.4128 418.7165 382.3974 226.6070 -4.2997 414.2544 418.5541 382.1906 228.2118 -4.2957 414.0629 418.3585 381.9880 229.8224 -4.2926 413.8936 418.1862 381.7815 231.4223 -4.2893 413.7429 418.0322 381.5699 233.0424 -4.2891 413.5775 417.8666 381.3760 234.6479 -4.2810 413.4352 417.7162 381.1772 236.2529 -4.2788 413.2745 417.5534 381.0064 237.8628 -4.2768 413.1082 417.3850 380.8276 239.4628 -4.2744 412.9709 417.2452 380.6239 241.0630 -4.2704 412.8200 417.0904 380.4242 242.6729 -4.2658 412.6409 416.9067 380.2335 244.2938 -4.2634 412.4628 416.7262 380.0234 245.8936 -4.2609 412.3095 416.5704 379.8494 247.4881 -4.2580 412.1517 416.4097 379.6652 249.0881 -4.2554 411.9909 416.2463 379.4922 250.6935 -4.2540 411.8307 416.0847 379.2914 252.2983 -4.2503 411.6725 415.9228 379.1131 253.9089 -4.2452 411.4967 415.7419 378.9122 255.5139 -4.2427 411.3168 415.5595 378.7196 257.1033 -4.2410 411.1570 415.3980 378.5556 258.7193 -4.2351 410.9855 415.2206 378.3630 260.3291 -4.2304 410.8179 415.0483 378.1836 261.9288 -4.2241 410.6505 414.8746 377.9863 263.5344 -4.2177 410.4655 414.6831 377.7975 265.1393 -4.2147 410.2882 414.5030 377.5873 266.7389 -4.2095 410.1368 414.3464 377.3817 268.3340 -4.2059 409.9681 414.1740 377.1888 269.9340 -4.2062 409.7962 414.0023 376.9876 271.5541 -4.2008 409.6248 413.8257 376.7793 273.1599 -4.1981 409.4466 413.6447 376.5838 274.7646 -4.1983 409.2799 413.4782 376.3490 276.3645 -4.1943 409.1208 413.3152 376.1350 277.9598 -4.1910 408.9791 413.1701 375.9283 279.5645 -4.1842 408.8023 412.9865 375.7242 281.1746 -4.1819 408.6189 412.8008 375.5204 282.7750 -4.1811 408.4427 412.6238 375.2929 284.3951 -4.1764 408.2751 412.4514 375.0717 286.0053 -4.1709 408.0978 412.2687 374.8869 287.6056 -4.1641 407.9279 412.0919 374.6712 289.1899 -4.1593 407.7684 411.9278 374.4676 290.8001 -4.1556 407.6116 411.7671 374.2844 292.4055 -4.1517 407.4208 411.5725 374.0833 294.0103 -4.1461 407.2520 411.3981 373.8565 295.6103 -4.1423 407.1016 411.2440 373.6436 297.2310 -4.1411 406.9150 411.0562 373.4352 298.8358 -4.1369 406.7171 410.8540 373.2432 300.4410 -4.1352 406.5256 410.6609 373.0682 302.0463 -4.1296 406.3526 410.4821 372.9005 303.6510 -4.1269 406.1988 410.3257 372.7014 305.2563 -4.1236 406.0245 410.1481 372.5464 306.8615 -4.1193 405.8747 409.9939 372.3327 308.4816 -4.1160 405.6571 409.7732 372.1401 310.0873 -4.1112 405.4756 409.5868 371.9229 311.6921 -4.1071 405.2902 409.3972 371.7438 313.2969 -4.1048 405.1008 409.2056 371.5389 314.8974 -4.1005 404.9172 409.0177 371.3581 316.5074 -4.0957 404.7480 408.8437 371.1759 318.1071 -4.0931 404.5910 408.6841 370.9910 319.7281 -4.0875 404.4314 408.5190 370.7958 321.3380 -4.0837 404.2535 408.3372 370.5990 322.9380 -4.0789 404.0683 408.1472 370.4238 324.5383 -4.0761 403.8727 407.9488 370.2617 326.1481 -4.0702 403.6890 407.7592 370.0715 327.7536 -4.0673 403.5146 407.5819 369.9059 329.3586 -4.0650 403.3336 407.3987 369.7288 330.9788 -4.0626 403.1401 407.2027 369.5185 332.5789 -4.0587 402.9614 407.0201 369.3196 334.1893 -4.0548 402.7970 406.8518 369.0916 335.7889 -4.0502 402.6126 406.6628 368.8777 337.3940 -4.0457 402.4165 406.4622 368.6675 338.9994 -4.0420 402.2375 406.2795 368.4588 340.6041 -4.0368 402.0694 406.1062 368.2474 342.2244 -4.0328 401.8783 405.9111 368.0334 343.8300 -4.0305 401.7012 405.7317 367.8357 345.4245 -4.0272 401.5342 405.5614 367.6353 347.0399 -4.0213 401.3627 405.3840 367.4192 348.6401 -4.0199 401.1887 405.2085 367.2248 350.2295 -4.0164 401.0270 405.0433 367.0193 351.8504 -4.0083 400.8373 404.8456 366.8019 353.4400 -4.0033 400.6668 404.6701 366.5982 355.0448 -3.9979 400.4757 404.4736 366.3758 356.6606 -3.9999 400.2789 404.2788 366.1776 358.2809 -3.9960 400.0926 404.0887 365.9843 359.8805 -3.9905 399.9043 403.8947 365.7912 361.4914 -3.9835 399.6956 403.6791 365.5836 363.0808 -3.9807 399.5084 403.4891 365.4026 364.6808 -3.9773 399.3245 403.3018 365.2210 366.2913 -3.9742 399.1591 403.1333 365.0246 367.8909 -3.9679 398.9646 402.9325 364.8418 369.4911 -3.9640 398.7956 402.7596 364.6423 371.1014 -3.9587 398.6121 402.5708 364.4437 372.7061 -3.9546 398.3999 402.3545 364.2418 374.3215 -3.9519 398.2272 402.1792 364.0396 375.9166 -3.9475 398.0623 402.0098 363.8612 377.5111 -3.9452 397.8762 401.8214 363.6722 379.1264 -3.9412 397.7015 401.6428 363.4669 380.7370 -3.9342 397.5324 401.4666 363.2811 382.3366 -3.9321 397.3268 401.2589 363.0721 383.9419 -3.9295 397.1380 401.0675 362.8877 385.5471 -3.9240 396.9557 400.8797 362.6950 387.1468 -3.9195 396.7700 400.6895 362.4891 388.7515 -3.9167 396.5986 400.5153 362.3094 390.3623 -3.9116 396.3972 400.3087 362.1251 391.9620 -3.9066 396.2064 400.1130 361.9154 393.5823 -3.9024 396.0147 399.9171 361.7245 395.1776 -3.8963 395.8139 399.7102 361.5537 396.7824 -3.8923 395.6193 399.5116 361.3580 398.3976 -3.8885 395.4358 399.3243 361.1788 399.9980 -3.8827 395.2394 399.1222 360.9785 401.5925 -3.8785 395.0595 398.9380 360.7619 403.1975 -3.8739 394.8816 398.7555 360.5614 404.8081 -3.8717 394.7045 398.5762 360.3524 406.4129 -3.8670 394.5227 398.3897 360.1353 408.0228 -3.8612 394.3196 398.1808 359.9125 409.6284 -3.8573 394.1280 397.9853 359.6890 411.2486 -3.8539 393.9481 397.8019 359.4673 412.8534 -3.8496 393.7561 397.6057 359.2648 414.4533 -3.8431 393.5439 397.3870 359.0465 416.0639 -3.8382 393.3492 397.1874 358.8483 417.6584 -3.8344 393.1923 397.0266 358.6558 419.2683 -3.8295 393.0062 396.8357 358.4724 420.8788 -3.8267 392.8130 396.6398 358.2691 422.4788 -3.8250 392.6273 396.4524 358.1014 424.1091 -3.8209 392.4368 396.2576 357.8986 425.7200 -3.8159 392.2450 396.0609 357.7050 427.2991 -3.8114 392.0415 395.8529 357.5037 428.9301 -3.8057 391.8662 395.6719 357.2915 430.5353 -3.7993 391.6748 395.4741 357.0963 432.1349 -3.7973 391.4845 395.2819 356.8933 433.7399 -3.7916 391.3000 395.0916 356.6923 435.3505 -3.7881 391.1142 394.9023 356.4916 436.9501 -3.7847 390.9216 394.7063 356.2926 438.5554 -3.7807 390.7392 394.5199 356.1001 440.1914 -3.7746 390.5392 394.3138 355.8928 441.7961 -3.7696 390.3475 394.1171 355.7102 443.4014 -3.7638 390.1541 393.9179 355.5236 445.0066 -3.7627 389.9803 393.7430 355.3278 446.6063 -3.7581 389.7876 393.5457 355.1348 448.2118 -3.7528 389.6125 393.3653 354.9655 449.8168 -3.7497 389.3993 393.1490 354.7573 451.4369 -3.7442 389.2009 392.9450 354.5689 453.0420 -3.7384 389.0086 392.7470 354.4015 454.6474 -3.7338 388.8249 392.5587 354.2046 456.2521 -3.7275 388.6280 392.3555 354.0101 457.8730 -3.7207 388.4529 392.1736 353.8156 459.4626 -3.7177 388.2468 391.9645 353.6030 461.0623 -3.7167 388.0634 391.7801 353.4049 462.6881 -3.7140 387.8661 391.5802 353.1913 464.2881 -3.7115 387.6564 391.3678 352.9856 465.8929 -3.7068 387.4637 391.1705 352.7829 467.5034 -3.7005 387.2780 390.9784 352.5871 469.1136 -3.6921 387.0809 390.7730 352.3869 470.7184 -3.6894 386.8864 390.5759 352.1833 472.3395 -3.6848 386.6920 390.3768 352.0023 473.9289 -3.6815 386.4912 390.1727 351.7928 475.5336 -3.6748 386.3180 389.9927 351.5739 477.1439 -3.6698 386.1486 389.8184 351.3493 478.7493 -3.6634 385.9631 389.6265 351.1327 480.3591 -3.6609 385.7548 389.4157 350.9215 481.9641 -3.6600 385.5596 389.2196 350.7165 483.5696 -3.6558 385.3459 389.0017 350.5354 485.1898 -3.6529 385.1592 388.8121 350.3341 486.7954 -3.6509 384.9641 388.6150 350.1178 488.4003 -3.6452 384.7533 388.3985 349.8936 489.9900 -3.6393 384.5739 388.2133 349.6993 491.5903 -3.6357 384.4019 388.0377 349.4914 493.2001 -3.6303 384.2357 387.8660 349.2944 494.8054 -3.6246 384.0447 387.6694 349.0883 496.4106 -3.6190 383.8316 387.4506 348.8866 498.0308 -3.6128 383.6300 387.2428 348.6718 499.6363 -3.6090 383.4658 387.0748 348.4655 501.2413 -3.6030 383.2608 386.8638 348.2688 502.8460 -3.6004 383.0806 386.6810 348.0508 504.4514 -3.5965 382.8972 386.4937 347.8302 506.0565 -3.5874 382.7103 386.2977 347.6248 507.6613 -3.5831 382.4909 386.0740 347.4139 509.2769 -3.5810 382.2857 385.8667 347.2049 510.8871 -3.5765 382.0792 385.6557 346.9997 512.4868 -3.5691 381.8914 385.4606 346.7965 514.0920 -3.5660 381.7058 385.2718 346.6163 515.6973 -3.5634 381.5004 385.0638 346.4105 517.2970 -3.5579 381.2987 384.8566 346.1980 518.9078 -3.5519 381.1218 384.6738 346.0193 520.5279 -3.5486 380.9282 384.4768 345.8274 522.1326 -3.5458 380.7362 384.2820 345.6280 523.7378 -3.5421 380.5401 384.0822 345.4256 525.3431 -3.5358 380.3403 383.8761 345.2453 526.9479 -3.5318 380.1684 383.7002 345.0562 528.5534 -3.5251 379.9697 383.4948 344.8627 530.1533 -3.5202 379.7827 383.3029 344.6534 531.7785 -3.5160 379.5573 383.0733 344.4619 533.3786 -3.5100 379.3479 382.8579 344.2757 534.9685 -3.5041 379.1431 382.6473 344.0937 536.5784 -3.4987 378.9645 382.4631 343.9083 538.1788 -3.4962 378.7648 382.2610 343.7196 539.7786 -3.4914 378.5556 382.0470 343.5230 541.3885 -3.4824 378.3621 381.8445 343.3300 542.9889 -3.4775 378.1789 381.6564 343.1441 544.6246 -3.4755 377.9992 381.4747 342.9222 546.2294 -3.4722 377.8055 381.2776 342.7234 547.8193 -3.4657 377.6068 381.0726 342.5178 549.4245 -3.4621 377.3923 380.8544 342.3207 551.0446 -3.4589 377.1956 380.6545 342.1046 552.6346 -3.4553 377.0260 380.4813 341.9199 554.2449 -3.4507 376.8374 380.2881 341.7195 555.8599 -3.4455 376.6168 380.0623 341.5235 557.4650 -3.4408 376.4115 379.8523 341.3286 559.0755 -3.4371 376.2093 379.6464 341.1618 560.6751 -3.4305 376.0439 379.4744 340.9349 562.2856 -3.4271 375.8625 379.2896 340.7502 563.8856 -3.4215 375.6563 379.0779 340.5568 565.4904 -3.4181 375.4735 378.8916 340.3721 567.1106 -3.4130 375.2906 378.7035 340.1811 568.7111 -3.4072 375.0826 378.4898 339.9954 570.3159 -3.4038 374.9058 378.3096 339.8160 571.9259 -3.4007 374.6938 378.0945 339.6189 573.5264 -3.3928 374.5029 377.8957 339.4345 575.1260 -3.3874 374.3188 377.7062 339.2482 576.7316 -3.3823 374.1391 377.5213 339.0615 578.3519 -3.3777 373.9351 377.3128 338.8906 579.9566 -3.3728 373.7277 377.1005 338.7223 581.5620 -3.3689 373.5252 376.8942 338.5510 583.1671 -3.3679 373.3426 376.7105 338.3523 584.7719 -3.3658 373.1419 376.5077 338.1706 586.3774 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