DTA measure 1gyors2 Date: 2025225:1249 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 637.53 s Mass = 956.200 mg data_number = 1587 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.6080 -1.8779 269.2406 271.1185 276.5038 0.9655 -1.8780 269.2711 271.1491 276.4906 1.4065 -1.8782 269.3040 271.1822 276.4723 1.8270 -1.8785 269.3367 271.2152 276.4544 2.2050 -1.8788 269.3662 271.2450 276.4380 2.5635 -1.8788 269.3957 271.2744 276.4196 3.0665 -1.8787 269.4360 271.3148 276.3922 3.4240 -1.8793 269.4701 271.3494 276.3738 3.7825 -1.8792 269.5093 271.3885 276.3540 4.2235 -1.8792 269.5463 271.4256 276.3272 4.6430 -1.8797 269.5822 271.4619 276.2996 5.0015 -1.8800 269.6103 271.4903 276.2761 5.3805 -1.8798 269.6435 271.5233 276.2515 5.8620 -1.8795 269.6898 271.5693 276.2162 6.2410 -1.8797 269.7240 271.6037 276.1869 6.5995 -1.8801 269.7534 271.6335 276.1602 7.0400 -1.8800 269.7924 271.6725 276.1252 7.4600 -1.8798 269.8266 271.7064 276.0889 7.8180 -1.8790 269.8593 271.7383 276.0555 8.1970 -1.8784 269.8929 271.7713 276.0220 8.6790 -1.8772 269.9338 271.8110 275.9772 9.0580 -1.8766 269.9658 271.8424 275.9420 9.4155 -1.8760 269.9943 271.8703 275.9060 9.8565 -1.8755 270.0348 271.9102 275.8589 10.2770 -1.8754 270.0692 271.9446 275.8167 10.6345 -1.8749 270.0984 271.9733 275.7805 11.0135 -1.8748 270.1311 272.0059 275.7396 11.4960 -1.8740 270.1755 272.0495 275.6929 11.8740 -1.8731 270.2062 272.0793 275.6521 12.2325 -1.8721 270.2348 272.1069 275.6118 12.6115 -1.8714 270.2679 272.1394 275.5691 13.0930 -1.8706 270.3087 272.1793 275.5152 13.4515 -1.8703 270.3391 272.2095 275.4703 13.8305 -1.8700 270.3723 272.2422 275.4233 14.2710 -1.8696 270.4094 272.2789 275.3632 14.6910 -1.8687 270.4471 272.3159 275.3139 15.0490 -1.8676 270.4823 272.3499 275.2697 15.4275 -1.8668 270.5141 272.3809 275.2177 15.9100 -1.8657 270.5584 272.4241 275.1508 16.2680 -1.8649 270.5931 272.4579 275.1035 16.6470 -1.8638 270.6246 272.4884 275.0498 17.0875 -1.8623 270.6636 272.5258 274.9852 17.5080 -1.8614 270.7002 272.5615 274.9236 17.8660 -1.8603 270.7340 272.5944 274.8724 18.2445 -1.8595 270.7669 272.6264 274.8157 18.7270 -1.8577 270.8123 272.6700 274.7500 19.0850 -1.8568 270.8433 272.7000 274.6969 19.4635 -1.8558 270.8772 272.7329 274.6381 19.8425 -1.8545 270.9186 272.7731 274.5798 20.3250 -1.8525 270.9641 272.8165 274.5063 20.6825 -1.8515 270.9963 272.8478 274.4490 21.0615 -1.8506 271.0305 272.8811 274.3884 21.4820 -1.8488 271.0672 272.9160 274.3191 21.9015 -1.8476 271.1023 272.9499 274.2547 22.2805 -1.8466 271.1347 272.9813 274.1917 22.6590 -1.8455 271.1676 273.0132 274.1288 23.1410 -1.8435 271.2094 273.0528 274.0510 23.4995 -1.8422 271.2379 273.0801 273.9919 23.8780 -1.8411 271.2691 273.1102 273.9297 24.2985 -1.8392 271.3059 273.1451 273.8572 24.7185 -1.8379 271.3425 273.1804 273.7831 25.0975 -1.8356 271.3765 273.2121 273.7207 25.4760 -1.8334 271.4108 273.2442 273.6580 25.9580 -1.8308 271.4534 273.2842 273.5757 26.3165 -1.8289 271.4847 273.3137 273.5176 26.6955 -1.8265 271.5158 273.3423 273.4533 27.1150 -1.8245 271.5486 273.3730 273.3843 27.5355 -1.8216 271.5833 273.4049 273.3112 27.9140 -1.8199 271.6151 273.4351 273.2448 28.2925 -1.8184 271.6501 273.4685 273.1775 28.7750 -1.8157 271.6940 273.5098 273.0936 29.1330 -1.8142 271.7246 273.5388 273.0287 29.5120 -1.8124 271.7540 273.5664 272.9598 29.8700 -1.8107 271.7858 273.5965 272.8942 30.3730 -1.8080 271.8275 273.6355 272.8064 30.7305 -1.8066 271.8583 273.6648 272.7445 31.1095 -1.8050 271.8914 273.6964 272.6758 31.5295 -1.8031 271.9274 273.7305 272.6003 31.9495 -1.8015 271.9584 273.7599 272.5257 32.3285 -1.7992 271.9835 273.7828 272.4605 32.7070 -1.7972 272.0118 273.8090 272.3954 33.1890 -1.7946 272.0495 273.8441 272.3112 33.5475 -1.7921 272.0807 273.8728 272.2415 33.9260 -1.7903 272.1084 273.8987 272.1725 34.3460 -1.7882 272.1405 273.9287 272.0993 34.7660 -1.7858 272.1728 273.9587 272.0319 35.1450 -1.7837 272.2052 273.9889 271.9692 35.5235 -1.7819 272.2322 274.0141 271.9069 36.0060 -1.7790 272.2701 274.0492 271.8267 36.3635 -1.7779 272.2974 274.0753 271.7702 36.7425 -1.7760 272.3265 274.1025 271.7084 37.1630 -1.7734 272.3597 274.1330 271.6406 37.5830 -1.7702 272.3897 274.1599 271.5721 37.9615 -1.7677 272.4215 274.1892 271.5063 38.3405 -1.7654 272.4523 274.2177 271.4452 38.8220 -1.7630 272.4908 274.2538 271.3708 39.1805 -1.7611 272.5199 274.2809 271.3154 39.5595 -1.7595 272.5494 274.3089 271.2572 39.9795 -1.7569 272.5856 274.3425 271.1901 40.3995 -1.7552 272.6152 274.3704 271.1255 40.7785 -1.7532 272.6427 274.3960 271.0680 41.1575 -1.7509 272.6755 274.4264 271.0112 41.6390 -1.7479 272.7082 274.4561 270.9436 41.9975 -1.7457 272.7314 274.4771 270.8914 42.3760 -1.7439 272.7613 274.5052 270.8343 42.7340 -1.7422 272.7858 274.5280 270.7844 43.2165 -1.7395 272.8252 274.5648 270.7188 43.5950 -1.7377 272.8544 274.5921 270.6677 43.9530 -1.7360 272.8807 274.6167 270.6254 44.3730 -1.7333 272.9147 274.6480 270.5721 44.8135 -1.7308 272.9439 274.6747 270.5170 45.1720 -1.7286 272.9644 274.6931 270.4732 45.5510 -1.7265 272.9919 274.7184 270.4285 46.0330 -1.7236 273.0262 274.7498 270.3783 46.3910 -1.7216 273.0557 274.7773 270.3410 46.7700 -1.7195 273.0840 274.8035 270.3040 47.1900 -1.7171 273.1121 274.8292 270.2626 47.6305 -1.7144 273.1395 274.8539 270.2194 47.9890 -1.7127 273.1613 274.8740 270.1895 48.3465 -1.7110 273.1872 274.8983 270.1548 48.8495 -1.7082 273.2231 274.9313 270.1096 49.2080 -1.7063 273.2493 274.9556 270.0802 49.5655 -1.7042 273.2757 274.9799 270.0530 49.9445 -1.7013 273.2996 275.0008 270.0265 50.4270 -1.6986 273.3351 275.0337 269.9938 50.8050 -1.6966 273.3600 275.0566 269.9721 51.1635 -1.6949 273.3864 275.0813 269.9559 51.6045 -1.6928 273.4178 275.1106 269.9364 52.0240 -1.6902 273.4462 275.1364 269.9179 52.3825 -1.6887 273.4676 275.1563 269.9031 52.7615 -1.6867 273.4911 275.1778 269.8918 53.2430 -1.6835 273.5266 275.2101 269.8890 53.6015 -1.6813 273.5542 275.2355 269.8848 53.9805 -1.6796 273.5804 275.2599 269.8777 54.4000 -1.6778 273.6066 275.2843 269.8752 54.8205 -1.6757 273.6359 275.3116 269.8698 55.1995 -1.6735 273.6596 275.3331 269.8732 55.5780 -1.6715 273.6838 275.3553 269.8765 56.0600 -1.6692 273.7131 275.3823 269.8798 56.4185 -1.6674 273.7335 275.4009 269.8864 56.7970 -1.6653 273.7561 275.4214 269.8926 57.2170 -1.6632 273.7844 275.4476 269.9050 57.6370 -1.6612 273.8104 275.4716 269.9150 58.0155 -1.6597 273.8320 275.4917 269.9278 58.3740 -1.6565 273.8557 275.5122 269.9447 58.8560 -1.6539 273.8926 275.5465 269.9703 59.2345 -1.6526 273.9172 275.5698 269.9921 59.6135 -1.6510 273.9431 275.5941 270.0159 60.0335 -1.6493 273.9679 275.6172 270.0484 60.4535 -1.6474 273.9932 275.6406 270.0817 60.8325 -1.6455 274.0179 275.6634 270.1148 61.1900 -1.6441 274.0402 275.6843 270.1456 61.6725 -1.6422 274.0673 275.7095 270.1956 62.0515 -1.6410 274.0872 275.7282 270.2341 62.4090 -1.6400 274.1070 275.7470 270.2711 62.8295 -1.6382 274.1338 275.7720 270.3207 63.2705 -1.6362 274.1624 275.7986 270.3760 63.6485 -1.6349 274.1847 275.8196 270.4277 64.0070 -1.6336 274.2088 275.8424 270.4801 64.4890 -1.6323 274.2372 275.8695 270.5539 64.8675 -1.6313 274.2581 275.8893 270.6143 65.2260 -1.6303 274.2776 275.9078 270.6740 65.6050 -1.6286 274.3037 275.9323 270.7388 66.0865 -1.6270 274.3347 275.9616 270.8181 66.4655 -1.6256 274.3534 275.9791 270.8849 66.8240 -1.6244 274.3762 276.0006 270.9511 67.2435 -1.6235 274.4084 276.0320 271.0305 67.6845 -1.6221 274.4372 276.0594 271.1178 68.0420 -1.6215 274.4607 276.0823 271.1924 68.4005 -1.6205 274.4816 276.1021 271.2655 68.9035 -1.6197 274.5182 276.1379 271.3789 69.2615 -1.6189 274.5380 276.1568 271.4598 69.6400 -1.6184 274.5595 276.1779 271.5465 70.0605 -1.6179 274.5873 276.2052 271.6413 70.5010 -1.6167 274.6158 276.2325 271.7460 70.8590 -1.6160 274.6415 276.2575 271.8341 71.2175 -1.6154 274.6606 276.2760 271.9238 71.7200 -1.6137 274.6920 276.3058 272.0583 72.0780 -1.6136 274.7117 276.3253 272.1511 72.4570 -1.6127 274.7316 276.3443 272.2526 72.8775 -1.6118 274.7596 276.3714 272.3677 73.3180 -1.6115 274.7842 276.3957 272.4926 73.6760 -1.6114 274.8055 276.4169 272.5968 74.0345 -1.6108 274.8260 276.4368 272.7069 74.5375 -1.6110 274.8613 276.4724 272.8614 74.8950 -1.6112 274.8806 276.4918 272.9763 75.2740 -1.6108 274.9017 276.5126 273.0918 75.6945 -1.6102 274.9265 276.5367 273.2238 76.1350 -1.6098 274.9557 276.5655 273.3664 76.4930 -1.6093 274.9778 276.5871 273.4846 76.8510 -1.6094 275.0007 276.6100 273.6031 77.3540 -1.6093 275.0265 276.6358 273.7747 77.7120 -1.6093 275.0455 276.6547 273.8942 78.1115 -1.6093 275.0670 276.6763 274.0338 78.4700 -1.6093 275.0889 276.6982 274.1614 78.9515 -1.6089 275.1208 276.7297 274.3334 79.3305 -1.6095 275.1446 276.7541 274.4660 79.7095 -1.6099 275.1665 276.7765 274.6044 80.0670 -1.6101 275.1889 276.7990 274.7348 80.5495 -1.6106 275.2199 276.8304 274.9091 80.9280 -1.6105 275.2480 276.8586 275.0487 81.2860 -1.6112 275.2722 276.8834 275.1825 81.7065 -1.6121 275.3026 276.9147 275.3421 82.1470 -1.6132 275.3336 276.9469 275.5135 82.5255 -1.6138 275.3545 276.9683 275.6597 82.8840 -1.6140 275.3759 276.9900 275.7997 83.3660 -1.6147 275.4078 277.0225 275.9916 83.7445 -1.6155 275.4321 277.0476 276.1411 84.1030 -1.6167 275.4531 277.0698 276.2840 84.5230 -1.6178 275.4830 277.1008 276.4541 84.9635 -1.6191 275.5164 277.1355 276.6291 85.3425 -1.6201 275.5389 277.1590 276.7842 85.7000 -1.6213 275.5603 277.1816 276.9348 86.1825 -1.6226 275.5891 277.2117 277.1359 86.5615 -1.6235 275.6184 277.2419 277.2931 86.9190 -1.6249 275.6413 277.2662 277.4422 87.3395 -1.6267 275.6685 277.2952 277.6197 87.7805 -1.6279 275.6993 277.3273 277.8101 88.1595 -1.6294 275.7266 277.3560 277.9738 88.5170 -1.6302 275.7524 277.3827 278.1224 88.9375 -1.6314 275.7805 277.4119 278.2999 89.3780 -1.6327 275.8116 277.4443 278.4869 89.7360 -1.6340 275.8362 277.4701 278.6366 90.1150 -1.6357 275.8612 277.4969 278.7957 90.5970 -1.6376 275.8968 277.5344 278.9997 90.9755 -1.6392 275.9237 277.5629 279.1601 91.3340 -1.6405 275.9475 277.5880 279.3117 91.7540 -1.6423 275.9782 277.6204 279.4905 92.1945 -1.6441 276.0083 277.6524 279.6766 92.5530 -1.6453 276.0303 277.6757 279.8270 92.9320 -1.6467 276.0590 277.7057 279.9881 93.4140 -1.6490 276.0945 277.7435 280.1932 93.7925 -1.6511 276.1208 277.7719 280.3574 94.1510 -1.6531 276.1480 277.8011 280.5074 94.5705 -1.6553 276.1818 277.8371 280.6865 95.0115 -1.6575 276.2136 277.8711 280.8730 95.3700 -1.6589 276.2371 277.8960 281.0213 95.7480 -1.6600 276.2644 277.9245 281.1795 96.2305 -1.6621 276.2985 277.9606 281.3802 96.6095 -1.6638 276.3272 277.9910 281.5375 96.9670 -1.6652 276.3567 278.0219 281.6912 97.3875 -1.6674 276.3888 278.0562 281.8653 97.8285 -1.6699 276.4261 278.0960 282.0466 98.1860 -1.6715 276.4545 278.1260 282.1945 98.5650 -1.6736 276.4830 278.1566 282.3454 99.0475 -1.6764 276.5178 278.1942 282.5386 99.4260 -1.6791 276.5485 278.2275 282.6880 99.7840 -1.6812 276.5733 278.2545 282.8329 100.2045 -1.6833 276.6050 278.2883 283.0016 100.6450 -1.6859 276.6398 278.3258 283.1761 101.0235 -1.6875 276.6668 278.3543 283.3268 101.3820 -1.6891 276.6946 278.3837 283.4687 101.8015 -1.6917 276.7307 278.4224 283.6336 102.2425 -1.6941 276.7663 278.4604 283.8092 102.6010 -1.6962 276.7948 278.4910 283.9488 102.9800 -1.6986 276.8285 278.5271 284.0884 103.4615 -1.7011 276.8737 278.5748 284.2692 103.8405 -1.7033 276.9058 278.6091 284.4089 104.1980 -1.7051 276.9360 278.6411 284.5400 104.6185 -1.7077 276.9707 278.6783 284.6900 105.0595 -1.7102 277.0102 278.7203 284.8470 105.4170 -1.7121 277.0410 278.7531 284.9764 105.7960 -1.7144 277.0743 278.7887 285.1094 106.2785 -1.7172 277.1198 278.8370 285.2758 106.6575 -1.7197 277.1603 278.8799 285.4034 107.0150 -1.7211 277.1946 278.9157 285.5257 107.4355 -1.7230 277.2301 278.9531 285.6707 107.8760 -1.7253 277.2664 278.9918 285.8204 108.2340 -1.7274 277.2960 279.0234 285.9416 108.5925 -1.7295 277.3265 279.0560 286.0574 109.0950 -1.7330 277.3707 279.1036 286.2177 109.4530 -1.7353 277.4065 279.1417 286.3313 109.8115 -1.7373 277.4365 279.1737 286.4435 110.2520 -1.7399 277.4753 279.2153 286.5834 110.6720 -1.7429 277.5124 279.2553 286.7136 111.0305 -1.7448 277.5468 279.2916 286.8227 111.4095 -1.7466 277.5803 279.3269 286.9368 111.8910 -1.7494 277.6256 279.3751 287.0743 112.2495 -1.7511 277.6584 279.4095 287.1760 112.6285 -1.7533 277.6928 279.4461 287.2837 113.0690 -1.7561 277.7343 279.4904 287.4065 113.4890 -1.7589 277.7752 279.5342 287.5206 113.8470 -1.7607 277.8091 279.5698 287.6166 114.2260 -1.7632 277.8433 279.6065 287.7117 114.7080 -1.7666 277.8913 279.6579 287.8335 115.0660 -1.7687 277.9310 279.6997 287.9252 115.4445 -1.7708 277.9643 279.7351 288.0199 115.8650 -1.7730 278.0040 279.7770 288.1241 116.2850 -1.7754 278.0495 279.8249 288.2249 116.6635 -1.7780 278.0866 279.8646 288.3152 117.0220 -1.7802 278.1222 279.9024 288.3986 117.5040 -1.7829 278.1698 279.9527 288.5137 117.8825 -1.7854 278.2079 279.9933 288.5990 118.2410 -1.7874 278.2448 280.0321 288.6772 118.6605 -1.7893 278.2898 280.0792 288.7658 119.1015 -1.7912 278.3336 280.1248 288.8596 119.4805 -1.7936 278.3731 280.1667 288.9361 119.8380 -1.7953 278.4083 280.2036 289.0102 120.2585 -1.7976 278.4527 280.2502 289.0934 120.6995 -1.7997 278.4992 280.2989 289.1794 121.0570 -1.8020 278.5340 280.3359 289.2474 121.4360 -1.8040 278.5750 280.3790 289.3224 121.9185 -1.8066 278.6238 280.4304 289.4095 122.2765 -1.8084 278.6606 280.4690 289.4781 122.6550 -1.8103 278.6972 280.5075 289.5462 123.0755 -1.8123 278.7429 280.5552 289.6127 123.5160 -1.8138 278.7903 280.6041 289.6853 123.8740 -1.8155 278.8247 280.6403 289.7425 124.2325 -1.8174 278.8601 280.6775 289.8003 124.7350 -1.8199 278.9130 280.7329 289.8760 125.0930 -1.8216 278.9478 280.7694 289.9290 125.4510 -1.8234 278.9850 280.8084 289.9809 125.8920 -1.8261 279.0327 280.8587 290.0410 126.3120 -1.8281 279.0773 280.9054 290.0971 126.6910 -1.8290 279.1180 280.9469 290.1444 127.0490 -1.8304 279.1576 280.9880 290.1900 127.5515 -1.8332 279.2118 281.0449 290.2515 127.9100 -1.8344 279.2531 281.0875 290.2905 128.2675 -1.8358 279.2884 281.1242 290.3328 128.7085 -1.8380 279.3379 281.1759 290.3866 129.1290 -1.8399 279.3839 281.2238 290.4328 129.4865 -1.8413 279.4206 281.2619 290.4673 129.8655 -1.8428 279.4630 281.3058 290.5034 130.3480 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