DTA measure 1lassu Date: 2025225:1148 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1251.47 s Mass = 956.200 mg data_number = 1557 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3130 -1.3948 240.9643 242.3591 228.6641 2.0698 -1.3940 240.9469 242.3409 228.6511 2.9200 -1.3943 240.9328 242.3271 228.6344 3.6770 -1.3942 240.9149 242.3091 228.6136 4.5270 -1.3930 240.8953 242.2884 228.5898 5.2943 -1.3925 240.8773 242.2698 228.5650 6.1138 -1.3916 240.8597 242.2513 228.5295 6.9223 -1.3901 240.8450 242.2351 228.4943 7.7103 -1.3891 240.8268 242.2160 228.4650 8.5295 -1.3883 240.8097 242.1980 228.4224 9.2968 -1.3872 240.7975 242.1847 228.3845 10.1468 -1.3866 240.7799 242.1665 228.3364 10.9243 -1.3848 240.7687 242.1536 228.2924 11.7433 -1.3836 240.7514 242.1349 228.2448 12.5003 -1.3820 240.7382 242.1202 228.2046 13.3503 -1.3813 240.7271 242.1083 228.1495 14.1278 -1.3803 240.7141 242.0944 228.0930 14.9470 -1.3782 240.6952 242.0734 228.0330 15.7453 -1.3769 240.6790 242.0558 227.9754 16.5335 -1.3753 240.6596 242.0349 227.9136 17.3733 -1.3745 240.6422 242.0167 227.8427 18.1303 -1.3732 240.6338 242.0070 227.7824 18.9800 -1.3718 240.6198 241.9916 227.7148 19.7578 -1.3698 240.6053 241.9751 227.6430 20.5768 -1.3673 240.5888 241.9561 227.5689 21.3753 -1.3656 240.5761 241.9417 227.4937 22.1738 -1.3642 240.5612 241.9253 227.4140 22.9720 -1.3626 240.5466 241.9092 227.3379 23.7598 -1.3609 240.5290 241.8899 227.2612 24.5993 -1.3583 240.5129 241.8712 227.1725 25.3563 -1.3566 240.4969 241.8535 227.0924 26.2060 -1.3543 240.4869 241.8412 226.9990 26.9838 -1.3524 240.4732 241.8256 226.9102 27.8028 -1.3506 240.4582 241.8088 226.8262 28.6010 -1.3492 240.4427 241.7919 226.7359 29.3995 -1.3468 240.4286 241.7754 226.6484 30.2285 -1.3443 240.4064 241.7508 226.5557 30.9858 -1.3422 240.3937 241.7359 226.4689 31.8253 -1.3399 240.3788 241.7186 226.3681 32.6028 -1.3376 240.3665 241.7041 226.2855 33.4320 -1.3354 240.3476 241.6830 226.1906 34.2200 -1.3331 240.3318 241.6649 226.0958 35.0390 -1.3303 240.3164 241.6466 226.0003 35.8168 -1.3277 240.3050 241.6327 225.9049 36.6668 -1.3254 240.2871 241.6125 225.8065 37.4033 -1.3235 240.2736 241.5971 225.7152 38.2533 -1.3201 240.2551 241.5752 225.6076 39.0310 -1.3178 240.2394 241.5572 225.5140 39.8503 -1.3157 240.2214 241.5372 225.4169 40.6380 -1.3134 240.2028 241.5162 225.3178 41.4468 -1.3110 240.1864 241.4974 225.2128 42.2658 -1.3081 240.1674 241.4755 225.1083 43.0640 -1.3051 240.1555 241.4605 225.0092 43.8933 -1.3026 240.1360 241.4385 224.9077 44.6605 -1.2989 240.1203 241.4191 224.8163 45.5208 -1.2957 240.1011 241.3968 224.7116 46.2778 -1.2931 240.0823 241.3755 224.6220 47.1070 -1.2907 240.0617 241.3524 224.5191 47.9050 -1.2883 240.0490 241.3373 224.4274 48.7038 -1.2854 240.0339 241.3193 224.3322 49.5020 -1.2831 240.0128 241.2959 224.2422 50.3003 -1.2796 239.9930 241.2726 224.1585 51.1198 -1.2764 239.9731 241.2495 224.0649 51.8973 -1.2735 239.9559 241.2295 223.9827 52.7475 -1.2702 239.9364 241.2066 223.8970 53.4943 -1.2676 239.9181 241.1857 223.8250 54.3443 -1.2651 239.8936 241.1587 223.7411 55.1220 -1.2618 239.8721 241.1339 223.6737 55.9413 -1.2588 239.8546 241.1134 223.5970 56.7290 -1.2560 239.8368 241.0928 223.5279 57.5278 -1.2531 239.8135 241.0665 223.4624 58.3468 -1.2504 239.7892 241.0396 223.3929 59.1038 -1.2478 239.7684 241.0162 223.3423 59.9640 -1.2452 239.7441 240.9893 223.2816 60.7213 -1.2427 239.7217 240.9645 223.2306 61.5400 -1.2398 239.6976 240.9374 223.1825 62.3385 -1.2371 239.6771 240.9142 223.1402 63.1268 -1.2347 239.6599 240.8946 223.1013 63.9458 -1.2324 239.6385 240.8709 223.0637 64.7130 -1.2299 239.6227 240.8527 223.0315 65.5630 -1.2269 239.6030 240.8300 223.0038 66.3408 -1.2247 239.5816 240.8062 222.9852 67.1598 -1.2230 239.5595 240.7826 222.9681 67.9478 -1.2217 239.5390 240.7607 222.9623 68.7460 -1.2194 239.5186 240.7380 222.9589 69.5343 -1.2159 239.5020 240.7179 222.9620 70.3325 -1.2134 239.4866 240.7000 222.9740 71.1928 -1.2118 239.4638 240.6757 222.9986 71.9188 -1.2100 239.4406 240.6505 223.0251 72.7790 -1.2073 239.4191 240.6263 223.0559 73.5363 -1.2055 239.3953 240.6008 223.0908 74.3760 -1.2031 239.3682 240.5712 223.1412 75.1638 -1.2017 239.3459 240.5477 223.1910 75.9518 -1.2007 239.3266 240.5273 223.2471 76.7810 -1.1987 239.3020 240.5007 223.3114 77.5485 -1.1969 239.2760 240.4729 223.3793 78.4090 -1.1960 239.2556 240.4516 223.4648 79.1658 -1.1956 239.2332 240.4288 223.5494 79.9950 -1.1945 239.2066 240.4011 223.6422 80.7935 -1.1939 239.1803 240.3742 223.7384 81.5920 -1.1932 239.1570 240.3501 223.8439 82.3903 -1.1929 239.1287 240.3216 223.9553 83.1780 -1.1922 239.1028 240.2949 224.0716 84.0073 -1.1913 239.0766 240.2679 224.2000 84.7748 -1.1909 239.0526 240.2435 224.3243 85.6350 -1.1900 239.0298 240.2197 224.4744 86.3923 -1.1899 239.0120 240.2019 224.6144 87.2215 -1.1895 238.9916 240.1811 224.7698 88.0198 -1.1895 238.9655 240.1550 224.9233 88.8180 -1.1894 238.9455 240.1349 225.0906 89.6473 -1.1886 238.9254 240.1140 225.2741 90.4040 -1.1886 238.9048 240.0934 225.4451 91.2643 -1.1889 238.8906 240.0795 225.6405 92.0320 -1.1891 238.8714 240.0605 225.8215 92.8613 -1.1893 238.8486 240.0379 226.0261 93.6493 -1.1898 238.8314 240.0212 226.2232 94.4480 -1.1906 238.8117 240.0023 226.4277 95.2773 -1.1914 238.7911 239.9825 226.6426 96.0340 -1.1922 238.7753 239.9676 226.8399 96.8943 -1.1940 238.7594 239.9534 227.0753 97.6620 -1.1954 238.7404 239.9358 227.2861 98.4913 -1.1970 238.7244 239.9214 227.5125 99.2793 -1.1988 238.7053 239.9041 227.7347 100.0775 -1.2011 238.6884 239.8895 227.9633 100.9068 -1.2031 238.6733 239.8764 228.2065 101.6640 -1.2048 238.6603 239.8651 228.4295 102.5243 -1.2076 238.6495 239.8571 228.6957 103.2915 -1.2087 238.6403 239.8490 228.9282 104.1210 -1.2110 238.6205 239.8315 229.1822 104.9090 -1.2134 238.6071 239.8205 229.4253 105.7278 -1.2153 238.5945 239.8098 229.6818 106.5263 -1.2172 238.5799 239.7971 229.9261 107.3248 -1.2196 238.5720 239.7916 230.1718 108.1435 -1.2221 238.5626 239.7847 230.4281 108.9213 -1.2249 238.5521 239.7770 230.6763 109.7710 -1.2272 238.5379 239.7652 230.9384 110.5383 -1.2302 238.5281 239.7583 231.1764 111.3578 -1.2329 238.5211 239.7540 231.4327 112.1663 -1.2356 238.5151 239.7507 231.6819 112.9543 -1.2384 238.5153 239.7537 231.9243 113.7940 -1.2415 238.5091 239.7506 232.1786 114.5510 -1.2445 238.5030 239.7475 232.4092 115.4115 -1.2477 238.4949 239.7426 232.6670 116.1478 -1.2506 238.4877 239.7383 232.8834 116.9978 -1.2542 238.4866 239.7408 233.1325 117.7753 -1.2573 238.4820 239.7393 233.3546 118.5940 -1.2605 238.4756 239.7361 233.5897 119.3925 -1.2636 238.4728 239.7363 233.8109 120.1908 -1.2670 238.4746 239.7416 234.0360 121.0203 -1.2705 238.4778 239.7482 234.2673 121.7773 -1.2738 238.4771 239.7510 234.4808 122.6270 -1.2783 238.4808 239.7592 234.7079 123.3943 -1.2821 238.4868 239.7689 234.9022 124.2138 -1.2859 238.4894 239.7754 235.1109 125.0018 -1.2890 238.4927 239.7817 235.3085 125.8000 -1.2927 238.4987 239.7914 235.5104 126.5878 -1.2965 238.5087 239.8052 235.7080 127.3760 -1.2990 238.5194 239.8184 235.8983 128.2053 -1.3023 238.5267 239.8289 236.0878 128.9623 -1.3055 238.5399 239.8454 236.2609 129.8230 -1.3096 238.5524 239.8620 236.4486 130.5903 -1.3132 238.5627 239.8760 236.6111 131.4090 -1.3171 238.5770 239.8941 236.7812 132.2073 -1.3205 238.5890 239.9095 236.9457 132.9955 -1.3242 238.5959 239.9201 237.1038 133.8353 -1.3276 238.6083 239.9360 237.2625 134.5923 -1.3307 238.6251 239.9558 237.4050 135.4420 -1.3339 238.6315 239.9654 237.5586 136.2098 -1.3373 238.6450 239.9824 237.6875 137.0288 -1.3407 238.6587 239.9994 237.8272 137.8373 -1.3433 238.6724 240.0157 237.9569 138.6253 -1.3456 238.6833 240.0289 238.0801 139.4448 -1.3483 238.7029 240.0511 238.2022 140.2120 -1.3506 238.7166 240.0672 238.3188 141.0308 -1.3527 238.7317 240.0844 238.4367 141.8085 -1.3550 238.7459 240.1009 238.5456 142.6585 -1.3578 238.7655 240.1233 238.6571 143.4158 -1.3602 238.7815 240.1418 238.7588 144.2553 -1.3630 238.8034 240.1664 238.8666 145.0430 -1.3655 238.8275 240.1930 238.9581 145.8413 -1.3682 238.8486 240.2168 239.0457 146.6605 -1.3719 238.8718 240.2437 239.1316 147.4383 -1.3745 238.8974 240.2719 239.2065 148.2883 -1.3754 238.9235 240.2989 239.2885 149.0450 -1.3774 238.9486 240.3260 239.3627 149.8850 -1.3788 238.9719 240.3507 239.4371 150.6730 -1.3804 238.9915 240.3719 239.5027 151.4713 -1.3818 239.0100 240.3919 239.5660 152.2903 -1.3834 239.0356 240.4190 239.6288 153.0683 -1.3853 239.0606 240.4459 239.6840 153.9183 -1.3865 239.0901 240.4765 239.7453 154.6750 -1.3878 239.1182 240.5060 239.7909 155.5148 -1.3889 239.1470 240.5358 239.8405 156.3030 -1.3899 239.1737 240.5636 239.8794 157.1013 -1.3902 239.2046 240.5948 239.9169 157.9203 -1.3915 239.2275 240.6190 239.9560 158.6980 -1.3919 239.2509 240.6428 239.9881 159.5483 -1.3924 239.2830 240.6753 240.0236 160.3050 -1.3935 239.3130 240.7065 240.0536 161.1450 -1.3942 239.3500 240.7443 240.0845 161.9330 -1.3950 239.3787 240.7737 240.1070 162.7418 -1.3955 239.4051 240.8007 240.1239 163.5300 -1.3960 239.4335 240.8295 240.1401 164.3283 -1.3963 239.4624 240.8587 240.1539 165.1473 -1.3966 239.4956 240.8922 240.1669 165.9253 -1.3973 239.5299 240.9271 240.1794 166.7753 -1.3977 239.5676 240.9653 240.1886 167.5530 -1.3971 239.6036 241.0007 240.1981 168.3723 -1.3970 239.6380 241.0350 240.2077 169.1600 -1.3968 239.6717 241.0685 240.2209 169.9690 -1.3967 239.7034 241.1001 240.2242 170.7888 -1.3962 239.7353 241.1316 240.2274 171.5568 -1.3954 239.7638 241.1593 240.2325 172.4070 -1.3942 239.8014 241.1957 240.2374 173.1853 -1.3929 239.8359 241.2288 240.2401 174.0050 -1.3926 239.8749 241.2675 240.2441 174.7935 -1.3921 239.9098 241.3019 240.2495 175.6030 -1.3915 239.9477 241.3392 240.2532 176.4225 -1.3909 239.9845 241.3754 240.2557 177.1903 -1.3897 240.0154 241.4051 240.2615 178.0408 -1.3891 240.0535 241.4426 240.2629 178.8190 -1.3874 240.0919 241.4793 240.2644 179.6388 -1.3855 240.1286 241.5141 240.2697 180.4375 -1.3841 240.1616 241.5458 240.2745 181.2360 -1.3830 240.1957 241.5787 240.2802 182.0553 -1.3814 240.2307 241.6121 240.2815 182.8335 -1.3798 240.2651 241.6449 240.2854 183.6843 -1.3784 240.3031 241.6815 240.2879 184.4520 -1.3771 240.3437 241.7207 240.2981 185.2715 -1.3759 240.3839 241.7598 240.3134 186.0290 -1.3741 240.4252 241.7993 240.3241 186.8588 -1.3729 240.4643 241.8373 240.3361 187.6475 -1.3709 240.4995 241.8703 240.3500 188.4360 -1.3689 240.5337 241.9026 240.3729 189.2660 -1.3675 240.5745 241.9420 240.3956 190.0235 -1.3656 240.6076 241.9733 240.4116 190.8740 -1.3639 240.6493 242.0133 240.4321 191.6520 -1.3625 240.6876 242.0501 240.4578 192.4615 -1.3614 240.7293 242.0908 240.4877 193.2708 -1.3594 240.7692 242.1285 240.5260 194.0593 -1.3580 240.8078 242.1658 240.5587 194.8790 -1.3566 240.8492 242.2058 240.5946 195.6468 -1.3549 240.8833 242.2382 240.6381 196.4970 -1.3536 240.9248 242.2784 240.6878 197.2345 -1.3528 240.9656 242.3183 240.7326 198.0950 -1.3518 241.0093 242.3611 240.7911 198.8528 -1.3506 241.0484 242.3990 240.8414 199.6828 -1.3491 241.0855 242.4346 240.9072 200.4710 -1.3475 241.1197 242.4672 240.9687 201.2705 -1.3463 241.1543 242.5006 241.0299 202.1000 -1.3451 241.1976 242.5427 241.1014 202.8578 -1.3435 241.2331 242.5766 241.1723 203.7188 -1.3416 241.2717 242.6134 241.2585 204.4863 -1.3393 241.3127 242.6520 241.3376 205.3058 -1.3377 241.3524 242.6902 241.4263 206.1048 -1.3362 241.3906 242.7268 241.5143 206.8933 -1.3344 241.4255 242.7600 241.6014 207.7230 -1.3327 241.4704 242.8032 241.6993 208.4805 -1.3317 241.5065 242.8382 241.7908 209.3415 -1.3303 241.5581 242.8885 241.9001 210.1093 -1.3293 241.6004 242.9297 242.0016 210.9290 -1.3277 241.6466 242.9744 242.1136 211.7278 -1.3267 241.6906 243.0173 242.2219 212.5270 -1.3266 241.7317 243.0583 242.3371 213.3568 -1.3268 241.7741 243.1009 242.4691 214.1143 -1.3254 241.8143 243.1396 242.5941 214.9755 -1.3247 241.8586 243.1833 242.7365 215.7430 -1.3244 241.8955 243.2199 242.8608 216.5625 -1.3240 241.9394 243.2634 242.9935 217.3615 -1.3234 241.9814 243.3048 243.1306 218.1603 -1.3227 242.0215 243.3441 243.2715 218.9590 -1.3219 242.0627 243.3846 243.4177 219.7478 -1.3211 242.1090 243.4302 243.5607 220.5878 -1.3198 242.1562 243.4760 243.7187 221.3455 -1.3192 242.2005 243.5196 243.8661 222.2065 -1.3184 242.2423 243.5607 244.0334 222.9743 -1.3184 242.2840 243.6023 244.1832 223.7938 -1.3180 242.3299 243.6479 244.3499 224.5928 -1.3181 242.3723 243.6904 244.5185 225.3913 -1.3176 242.4204 243.7380 244.6864 226.2213 -1.3174 242.4653 243.7827 244.8611 226.9788 -1.3176 242.5102 243.8278 245.0158 227.8395 -1.3177 242.5564 243.8740 245.2007 228.6075 -1.3176 242.6058 243.9234 245.3720 229.4270 -1.3175 242.6592 243.9767 245.5475 230.2258 -1.3175 242.7068 244.0243 245.7196 231.0250 -1.3175 242.7557 244.0732 245.8968 231.8548 -1.3181 242.8043 244.1225 246.0822 232.6123 -1.3182 242.8454 244.1636 246.2528 233.4735 -1.3185 242.8989 244.2174 246.4463 234.2410 -1.3188 242.9488 244.2676 246.6222 235.0605 -1.3186 243.0016 244.3202 246.8139 235.8593 -1.3196 243.0443 244.3639 246.9973 236.6583 -1.3193 243.0912 244.4105 247.1780 237.4880 -1.3195 243.1433 244.4628 247.3695 238.2458 -1.3194 243.1927 244.5121 247.5444 239.1065 -1.3197 243.2502 244.5698 247.7398 239.8743 -1.3200 243.2955 244.6155 247.9155 240.6943 -1.3204 243.3495 244.6699 248.1015 241.4930 -1.3209 243.4023 244.7231 248.2832 242.2920 -1.3208 243.4548 244.7755 248.4643 243.1218 -1.3223 243.5119 244.8343 248.6552 243.8793 -1.3231 243.5673 244.8904 248.8264 244.7405 -1.3244 243.6244 244.9488 249.0170 245.5083 -1.3261 243.6714 244.9975 249.1853 246.3280 -1.3277 243.7272 245.0549 249.3668 247.1268 -1.3282 243.7806 245.1089 249.5424 247.9258 -1.3281 243.8374 245.1654 249.7158 248.7553 -1.3294 243.8949 245.2244 249.8949 249.5128 -1.3302 243.9491 245.2793 250.0591 250.3633 -1.3316 244.0181 245.3497 250.2383 251.1000 -1.3329 244.0691 245.4019 250.3969 251.9508 -1.3338 244.1298 245.4636 250.5688 252.7080 -1.3343 244.1888 245.5231 250.7210 253.5380 -1.3365 244.2510 245.5875 250.8876 254.3370 -1.3374 244.3148 245.6523 251.0503 255.1358 -1.3387 244.3771 245.7157 251.2095 255.9553 -1.3404 244.4364 245.7769 251.3669 256.7128 -1.3420 244.4898 245.8317 251.5072 257.5428 -1.3428 244.5488 245.8916 251.6638 258.3000 -1.3436 244.6046 245.9482 251.7995 259.1610 -1.3456 244.6713 246.0170 251.9497 259.9290 -1.3475 244.7338 246.0813 252.0842 260.7483 -1.3483 244.8033 246.1516 252.2284 261.5473 -1.3503 244.8676 246.2179 252.3633 262.3358 -1.3522 244.9342 246.2864 252.4940 263.1553 -1.3536 245.0048 246.3585 252.6250 263.9230 -1.3545 245.0754 246.4299 252.7439 264.7738 -1.3556 245.1410 246.4965 252.8763 265.5518 -1.3567 245.2017 246.5584 252.9927 266.3713 -1.3584 245.2743 246.6327 253.1113 267.1290 -1.3596 245.3450 246.7047 253.2214 267.9588 -1.3610 245.4198 246.7808 253.3320 268.7578 -1.3618 245.4915 246.8533 253.4380 269.5568 -1.3633 245.5618 246.9251 253.5469 270.3760 -1.3634 245.6363 246.9998 253.6591 271.1338 -1.3642 245.7001 247.0643 253.7580 271.9948 -1.3660 245.7689 247.1348 253.8654 272.7625 -1.3668 245.8307 247.1975 253.9567 273.5923 -1.3680 245.8986 247.2667 254.0528 274.3810 -1.3678 245.9694 247.3372 254.1453 275.1795 -1.3682 246.0376 247.4059 254.2342 276.0098 -1.3686 246.1087 247.4773 254.3183 276.7673 -1.3693 246.1750 247.5442 254.3946 277.5970 -1.3699 246.2519 247.6218 254.4752 278.3755 -1.3702 246.3210 247.6912 254.5440 279.2360 -1.3698 246.3947 247.7644 254.6289 279.9628 -1.3705 246.4597 247.8302 254.6938 280.8238 -1.3708 246.5406 247.9114 254.7741 281.6223 -1.3714 246.6121 247.9835 254.8418 282.4213 -1.3716 246.6815 248.0531 254.9119 283.2100 -1.3728 246.7544 248.1271 254.9757 284.0088 -1.3734 246.8309 248.2044 255.0386 284.8388 -1.3730 246.9112 248.2841 255.1027 285.5963 -1.3735 246.9832 248.3567 255.1570 286.4570 -1.3742 247.0681 248.4423 255.2147 287.2253 -1.3744 247.1383 248.5127 255.2644 288.0550 -1.3738 247.2125 248.5863 255.3226 288.8438 -1.3734 247.2819 248.6553 255.3752 289.6425 -1.3728 247.3516 248.7244 255.4289 290.4725 -1.3728 247.4314 248.8042 255.4777 291.2300 -1.3722 247.5019 248.8742 255.5213 292.0908 -1.3724 247.5841 248.9565 255.5779 292.8588 -1.3728 247.6546 249.0274 255.6263 293.6885 -1.3730 247.7343 249.1073 255.6732 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