DTA measure 1GYORS Date: 2025318:110 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 893.07 s Mass = 936.800 mg data_number = 1108 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2168 -0.6589 201.9613 202.6202 260.7727 2.0700 -0.6549 202.2292 202.8841 260.7799 2.9045 -0.6478 202.4909 203.1387 260.7813 3.8593 -0.6369 202.8137 203.4506 260.7906 4.6505 -0.6316 203.0588 203.6904 260.8115 5.4708 -0.6311 203.3123 203.9435 260.8465 6.2605 -0.6270 203.5443 204.1713 260.8431 7.0785 -0.6188 203.7890 204.4078 260.8997 7.8665 -0.6165 204.0368 204.6533 260.9354 8.6550 -0.6121 204.3072 204.9193 260.9701 9.4730 -0.6109 204.5507 205.1616 261.0093 10.2610 -0.6059 204.7809 205.3867 261.0738 11.0808 -0.6012 205.0438 205.6450 261.1168 11.8693 -0.5928 205.2654 205.8582 261.1902 12.6590 -0.5936 205.5026 206.0962 261.2682 13.6210 -0.5904 205.8037 206.3941 261.3645 14.5015 -0.5865 206.0824 206.6688 261.4618 15.2913 -0.5828 206.3272 206.9100 261.5597 16.0818 -0.5798 206.5488 207.1285 261.6786 16.9045 -0.5751 206.8102 207.3853 261.7876 17.6665 -0.5741 207.0244 207.5985 261.8999 18.5185 -0.5691 207.2844 207.8535 262.0062 19.2810 -0.5683 207.5126 208.0809 262.1278 20.1035 -0.5650 207.7668 208.3318 262.2913 20.9255 -0.5595 208.0105 208.5701 262.4467 21.6873 -0.5565 208.2113 208.7678 262.5817 22.5395 -0.5543 208.4563 209.0106 262.7373 23.3020 -0.5510 208.6885 209.2395 262.8767 24.1243 -0.5492 208.9312 209.4804 263.0521 24.9465 -0.5474 209.1764 209.7238 263.2386 25.7080 -0.5480 209.4051 209.9531 263.3957 26.5600 -0.5463 209.6356 210.1818 263.5726 27.3520 -0.5407 209.8713 210.4120 263.7334 28.1435 -0.5412 210.1095 210.6507 263.9242 28.9675 -0.5415 210.3510 210.8925 264.1133 29.7295 -0.5424 210.5635 211.1059 264.2913 30.5820 -0.5487 210.8223 211.3710 264.5073 31.3740 -0.6035 211.0443 211.6478 264.6737 32.1655 -0.6382 211.2762 211.9143 264.8675 32.9883 -0.6065 211.5114 212.1179 265.0610 33.7585 -0.5426 211.7652 212.3078 265.2740 34.5900 -0.5371 211.9835 212.5206 265.4456 35.3818 -0.5482 212.2116 212.7598 265.6438 36.2038 -0.5618 212.4421 213.0038 265.8403 36.9955 -0.5613 212.6497 213.2111 266.0266 37.7840 -0.5635 212.8764 213.4399 266.1898 38.6025 -0.5644 213.1121 213.6765 266.3731 39.3923 -0.5648 213.3466 213.9113 266.5594 40.2100 -0.5642 213.5872 214.1514 266.7486 40.9988 -0.5619 213.8102 214.3721 266.9470 41.7880 -0.5463 214.0366 214.5829 267.0941 42.6080 -0.5418 214.2700 214.8118 267.2933 43.3970 -0.5409 214.5002 215.0411 267.4491 44.2353 -0.5325 214.7220 215.2545 267.6217 44.9995 -0.5362 214.9259 215.4622 267.7900 45.8183 -0.5345 215.1666 215.7011 267.9578 46.6368 -0.5374 215.4163 215.9537 268.1445 47.3970 -0.5409 215.5985 216.1394 268.2796 48.2480 -0.5421 215.8641 216.4062 268.4583 49.0098 -0.5353 216.0355 216.5708 268.6046 49.8318 -0.5234 216.2739 216.7972 268.7619 50.6238 -0.5209 216.4938 217.0147 268.9421 51.4155 -0.5212 216.7215 217.2427 269.0761 52.2680 -0.5203 216.9709 217.4911 269.2094 53.0303 -0.5282 217.2001 217.7283 269.3464 53.8538 -0.5343 217.4094 217.9437 269.4933 54.6380 -0.5348 217.6308 218.1656 269.6232 55.4608 -0.5269 217.8418 218.3687 269.7765 56.2530 -0.5195 218.0671 218.5865 269.9044 57.0445 -0.5203 218.2867 218.8070 270.0186 57.8670 -0.5168 218.4994 219.0162 270.1656 58.6588 -0.5250 218.6992 219.2243 270.2833 59.4808 -0.5309 218.9442 219.4751 270.4191 60.2733 -0.5459 219.1632 219.7091 270.5347 61.0665 -0.5572 219.3660 219.9232 270.6584 61.8890 -0.5604 219.5831 220.1435 270.8026 62.6808 -0.5549 219.8068 220.3617 270.9243 63.5028 -0.5559 220.0493 220.6052 271.0399 64.3035 -0.5562 220.2571 220.8133 271.1567 65.1055 -0.5561 220.4903 221.0464 271.2419 65.8978 -0.5573 220.6940 221.2513 271.3905 66.7195 -0.5511 220.9044 221.4555 271.5172 67.5418 -0.5509 221.1505 221.7013 271.6181 68.3635 -0.5533 221.3477 221.9010 271.7490 69.2155 -0.5536 221.5662 222.1198 271.8908 69.9768 -0.5578 221.7584 222.3162 272.0092 70.8240 -0.5574 221.9890 222.5464 272.1254 71.6130 -0.5587 222.2112 222.7699 272.2194 72.4010 -0.5568 222.4134 222.9703 272.3168 73.2205 -0.5526 222.6222 223.1748 272.4494 73.9790 -0.5505 222.8349 223.3855 272.5462 74.8273 -0.5645 223.0570 223.6214 272.6691 75.6150 -0.5716 223.2634 223.8350 272.7849 76.4030 -0.5716 223.4749 224.0465 272.9140 77.2220 -0.5602 223.6987 224.2589 273.0129 77.9810 -0.5521 223.8964 224.4485 273.1187 78.8305 -0.5503 224.1297 224.6801 273.2464 79.6198 -0.5515 224.3319 224.8834 273.3651 80.4105 -0.5533 224.5406 225.0939 273.4484 81.2313 -0.5612 224.7541 225.3153 273.5436 81.9918 -0.5643 224.9550 225.5193 273.6726 82.8450 -0.5631 225.1613 225.7244 273.7817 83.6363 -0.5642 225.3607 225.9250 273.9206 84.4275 -0.5629 225.5536 226.1165 274.0394 85.2500 -0.5592 225.7684 226.3275 274.1596 86.0115 -0.5591 225.9610 226.5201 274.2749 86.8640 -0.5591 226.1703 226.7294 274.3898 87.6558 -0.5615 226.3948 226.9563 274.5171 88.4475 -0.5641 226.6286 227.1926 274.6257 89.2713 -0.5623 226.8316 227.3939 274.7345 90.0335 -0.5616 227.0300 227.5917 274.8634 90.8878 -0.5670 227.2360 227.8030 275.0198 91.6505 -0.5685 227.4196 227.9881 275.1268 92.4728 -0.5687 227.6524 228.2211 275.2591 93.2948 -0.5689 227.8662 228.4351 275.3645 94.0565 -0.5683 228.0251 228.5934 275.4871 94.9133 -0.5533 228.2621 228.8154 275.6359 95.6825 -0.5422 228.4475 228.9897 275.7566 96.5045 -0.5420 228.6559 229.1979 275.8812 97.2965 -0.5403 228.8640 229.4043 276.0288 98.1485 -0.5365 229.0533 229.5898 276.1920 98.9705 -0.5366 229.2467 229.7833 276.3215 99.7925 -0.5362 229.4835 230.0197 276.4539 100.6183 -0.5390 229.7103 230.2493 276.5870 101.4425 -0.5401 229.8858 230.4259 276.7188 102.2388 -0.5356 230.0788 230.6144 276.8841 103.0588 -0.5422 230.2949 230.8370 277.0182 103.8220 -0.5479 230.4870 231.0349 277.1458 104.6695 -0.5494 230.7031 231.2525 277.3089 105.4590 -0.5440 230.8923 231.4363 277.4554 106.2470 -0.5436 231.0768 231.6204 277.5910 107.0650 -0.5488 231.2928 231.8416 277.7475 107.8230 -0.5505 231.4878 232.0383 277.8874 108.6730 -0.5569 231.7057 232.2626 278.0281 109.4610 -0.5656 231.8866 232.4522 278.1989 110.2500 -0.5834 232.0557 232.6390 278.3358 111.0683 -0.5865 232.2672 232.8537 278.4799 111.8578 -0.5838 232.4752 233.0591 278.6375 112.6783 -0.5885 232.6601 233.2485 278.7923 113.4693 -0.5907 232.8516 233.4423 278.9217 114.2615 -0.5915 233.0655 233.6570 279.0641 115.0828 -0.5928 233.2711 233.8639 279.2135 115.8610 -0.5939 233.4431 234.0370 279.3808 116.6895 -0.5940 233.6429 234.2369 279.4967 117.4515 -0.5961 233.8496 234.4457 279.6437 118.3055 -0.6021 234.0357 234.6377 279.7913 119.0978 -0.6018 234.2255 234.8273 279.9392 119.8895 -0.6089 234.4266 235.0354 280.0711 120.7125 -0.6080 234.6331 235.2412 280.2016 121.4745 -0.6106 234.7955 235.4061 280.3324 122.3265 -0.6091 234.9915 235.6007 280.4849 123.0885 -0.6028 235.1824 235.7852 280.6256 123.9105 -0.6052 235.4064 236.0116 280.7362 124.7365 -0.6000 235.6236 236.2237 280.8959 125.4995 -0.6017 235.7772 236.3788 281.0361 126.3515 -0.6039 235.9760 236.5799 281.1657 127.1135 -0.6086 236.1629 236.7715 281.3000 127.9355 -0.6108 236.3573 236.9681 281.4405 128.7275 -0.6096 236.5361 237.1456 281.5739 129.5195 -0.6117 236.7583 237.3700 281.6901 130.3715 -0.6269 236.9544 237.5813 281.8353 131.1335 -0.6445 237.1038 237.7484 281.9726 131.9553 -0.6532 237.2947 237.9479 282.1229 132.7785 -0.6570 237.4890 238.1460 282.2538 133.6013 -0.6596 237.6771 238.3367 282.3954 134.3905 -0.6624 237.8614 238.5238 282.5224 135.2375 -0.6652 238.0745 238.7397 282.6501 135.9718 -0.6680 238.2549 238.9229 282.7648 136.8373 -0.6738 238.4510 239.1249 282.9054 137.5970 -0.6726 238.6394 239.3120 283.0233 138.4150 -0.6742 238.8272 239.5014 283.1699 139.2030 -0.6810 239.0077 239.6887 283.2983 139.9910 -0.6814 239.1979 239.8793 283.4323 140.8100 -0.6820 239.3980 240.0800 283.5622 141.5983 -0.6886 239.5661 240.2546 283.6947 142.4178 -0.6883 239.7585 240.4468 283.8110 143.2060 -0.6766 239.9526 240.6292 283.9438 143.9958 -0.6734 240.1285 240.8019 284.0800 144.8455 -0.6692 240.3250 240.9942 284.2225 145.6663 -0.6688 240.5281 241.1969 284.3652 146.4568 -0.6650 240.7078 241.3727 284.4852 147.2775 -0.6750 240.8938 241.5688 284.6045 148.0688 -0.6809 241.0760 241.7569 284.7384 148.8605 -0.6833 241.2584 241.9418 284.8590 149.6828 -0.6846 241.4379 242.1225 284.9958 150.4745 -0.6837 241.6002 242.2839 285.1211 151.2965 -0.6672 241.8104 242.4776 285.2632 152.0885 -0.6543 242.0019 242.6562 285.4156 152.8805 -0.6499 242.1730 242.8229 285.5181 153.7025 -0.6553 242.3512 243.0065 285.6601 154.4945 -0.6583 242.5432 243.2015 285.7897 155.3188 -0.6580 242.7189 243.3769 285.9085 156.1425 -0.6574 242.9293 243.5867 286.0494 156.9345 -0.6600 243.1233 243.7833 286.1729 157.7565 -0.6599 243.3202 243.9801 286.3087 158.5793 -0.6624 243.4873 244.1497 286.4241 159.4015 -0.6640 243.6828 244.3467 286.5461 160.3155 -0.6673 243.8903 244.5575 286.7041 161.1700 -0.6684 244.0726 244.7410 286.8274 161.9323 -0.6706 244.2415 244.9121 286.9324 162.7560 -0.6767 244.4172 245.0939 287.0728 163.5808 -0.6746 244.6016 245.2762 287.1960 164.3748 -0.6753 244.7783 245.4536 287.3216 165.2273 -0.6853 244.9577 245.6430 287.4512 166.0508 -0.6871 245.1490 245.8362 287.5772 166.8415 -0.6870 245.3337 246.0207 287.7116 167.6310 -0.6846 245.5004 246.1850 287.8669 168.4495 -0.6897 245.7060 246.3957 287.9840 169.2378 -0.6970 245.8868 246.5838 288.1089 170.0558 -0.7121 246.0492 246.7613 288.2143 170.8443 -0.7158 246.2342 246.9500 288.3338 171.6350 -0.7285 246.3880 247.1164 288.4565 172.4530 -0.7343 246.5858 247.3201 288.5831 173.2410 -0.7338 246.7666 247.5005 288.6838 174.0598 -0.7336 246.9562 247.6898 288.8008 174.8480 -0.7359 247.1383 247.8743 288.9463 175.6393 -0.7402 247.3007 248.0408 289.0757 176.4885 -0.7434 247.4989 248.2423 289.1933 177.2498 -0.7505 247.6405 248.3910 289.3076 178.0723 -0.7540 247.8505 248.6045 289.4314 178.8628 -0.7515 248.0306 248.7821 289.5611 179.6543 -0.7549 248.1936 248.9485 289.6938 180.4773 -0.7605 248.3675 249.1280 289.8230 181.2695 -0.7614 248.5562 249.3176 289.9450 182.0915 -0.7602 248.7522 249.5123 290.0806 182.8835 -0.7637 248.9207 249.6844 290.2273 183.6750 -0.7623 249.0915 249.8538 290.3833 184.4975 -0.7657 249.2651 250.0308 290.5228 185.2890 -0.7674 249.4434 250.2108 290.6592 186.1108 -0.7675 249.6258 250.3933 290.7760 186.9030 -0.7706 249.7725 250.5432 290.9357 187.7193 -0.7650 249.9621 250.7272 291.0595 188.5110 -0.7547 250.1400 250.8947 291.2029 189.3025 -0.7478 250.3186 251.0664 291.3372 190.1550 -0.7397 250.5127 251.2523 291.4983 190.9170 -0.7457 250.6714 251.4170 291.6513 191.7398 -0.7403 250.8455 251.5858 291.7835 192.5320 -0.7463 251.0009 251.7472 291.9056 193.3235 -0.7513 251.1949 251.9462 292.0355 194.1760 -0.7529 251.3684 252.1213 292.2128 194.9380 -0.7498 251.5411 252.2909 292.3421 195.7608 -0.7398 251.7143 252.4541 292.4901 196.5530 -0.7450 251.8761 252.6211 292.6344 197.3458 -0.7529 252.0580 252.8108 292.7663 198.1730 -0.7520 252.2271 252.9791 292.9101 198.9615 -0.7635 252.3909 253.1544 293.0644 199.7810 -0.7663 252.5681 253.3343 293.2035 200.5698 -0.7663 252.7389 253.5052 293.3563 201.3580 -0.7656 252.9075 253.6731 293.5138 202.1763 -0.7679 253.0908 253.8587 293.6431 202.9643 -0.7729 253.2675 254.0404 293.7861 203.7830 -0.7728 253.4487 254.2215 293.9431 204.5713 -0.7777 253.6004 254.3781 294.0665 205.3590 -0.7830 253.7800 254.5631 294.1936 206.2080 -0.7793 253.9629 254.7423 294.3444 206.9663 -0.7817 254.1095 254.8912 294.4744 207.7878 -0.7851 254.2841 255.0692 294.6262 208.5773 -0.7864 254.4553 255.2416 294.7752 209.3670 -0.7911 254.6235 255.4146 294.8771 210.2175 -0.7948 254.8133 255.6081 295.0420 210.9788 -0.7944 254.9765 255.7708 295.1659 211.8008 -0.7943 255.1454 255.9397 295.3048 212.5940 -0.7964 255.3116 256.1080 295.4263 213.3865 -0.7971 255.4683 256.2654 295.5464 214.2390 -0.7962 255.6568 256.4530 295.6969 215.0008 -0.8017 255.8236 256.6253 295.7967 215.8248 -0.8022 256.0195 256.8216 295.9312 216.6170 -0.8044 256.1720 256.9764 296.0608 217.4085 -0.8063 256.3471 257.1534 296.1937 218.2683 -0.8097 256.5140 257.3236 296.3243 219.0015 -0.8095 256.6718 257.4812 296.4300 219.8560 -0.8116 256.8591 257.6707 296.5514 220.6480 -0.8147 257.0149 257.8296 296.6718 221.4395 -0.8123 257.1842 257.9964 296.7917 222.2628 -0.8145 257.3398 258.1543 296.9226 223.0255 -0.8187 257.5156 258.3343 297.0439 223.8780 -0.8186 257.7174 258.5360 297.1720 224.6698 -0.8243 257.8686 258.6929 297.2980 225.4615 -0.8272 258.0230 258.8502 297.4194 226.2855 -0.8330 258.1987 259.0316 297.5481 227.0475 -0.8338 258.3425 259.1763 297.6571 227.8995 -0.8336 258.5469 259.3805 297.7572 228.6620 -0.8354 258.6869 259.5223 297.8936 229.4845 -0.8358 258.8659 259.7017 298.0269 230.3065 -0.8416 259.0418 259.8835 298.1338 231.0663 -0.8430 259.2090 260.0520 298.2638 231.9115 -0.8481 259.3774 260.2255 298.3923 232.6710 -0.8261 259.5232 260.3493 298.5192 233.4890 -0.8156 259.6929 260.5085 298.6554 234.3070 -0.8213 259.8688 260.6901 298.7667 235.0650 -0.8345 260.0265 260.8610 298.8673 235.9155 -0.9545 260.1912 261.1457 299.0260 236.6743 -0.9945 260.3616 261.3561 299.1534 237.4940 -1.0243 260.5373 261.5615 299.2695 238.3185 -1.0256 260.7110 261.7366 299.4046 239.0990 -1.0241 260.8760 261.9001 299.5523 239.9173 -1.0343 261.0349 262.0692 299.6961 240.6763 -1.0377 261.1869 262.2246 299.7930 241.5270 -1.0453 261.3529 262.3982 299.9319 242.2888 -1.0476 261.5098 262.5574 300.0648 243.1118 -1.0573 261.6890 262.7463 300.2189 243.9338 -1.0604 261.8562 262.9166 300.3681 244.6955 -1.0668 261.9943 263.0610 300.4868 245.5490 -1.0722 262.1846 263.2568 300.6419 246.3105 -1.0865 262.3411 263.4275 300.7759 247.1325 -1.0920 262.4984 263.5904 300.9308 247.9260 -1.0832 262.6942 263.7773 301.0413 248.7185 -1.1109 262.8265 263.9374 301.1683 249.5708 -1.1281 262.9913 264.1194 301.3277 250.3325 -1.1428 263.1397 264.2825 301.4631 251.1545 -1.0871 263.3147 264.4017 301.6115 251.9480 -1.1015 263.4906 264.5921 301.7529 252.7405 -1.1309 263.6598 264.7907 301.8896 253.5928 -1.1172 263.8218 264.9389 302.0261 254.3545 -1.1076 263.9796 265.0872 302.1605 255.1765 -1.1042 264.1541 265.2582 302.2996 255.9690 -1.1028 264.3303 265.4331 302.4520 256.7615 -1.1210 264.4753 265.5963 302.5966 257.6135 -1.1093 264.6462 265.7555 302.7461 258.3755 -1.0791 264.8260 265.9051 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