DTA measure 1lassu Date: 2025318:1149 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1232.85 s Mass = 936.800 mg data_number = 1533 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2215 0.7127 254.0793 253.3666 242.7646 2.0433 0.7132 254.0374 253.3242 242.7160 2.8055 0.7146 253.9777 253.2631 242.6608 3.6580 0.7148 253.9400 253.2252 242.6244 4.4495 0.7109 253.8776 253.1667 242.5998 5.2415 0.7176 253.8306 253.1130 242.5526 6.0648 0.7155 253.7723 253.0567 242.5144 6.8265 0.7159 253.7306 253.0146 242.4679 7.6633 0.7166 253.6703 252.9538 242.4566 8.4545 0.7181 253.6185 252.9005 242.4273 9.2765 0.7211 253.5785 252.8574 242.3878 10.0690 0.7259 253.5377 252.8118 242.3936 10.8625 0.7271 253.4912 252.7641 242.3863 11.6845 0.7301 253.4435 252.7133 242.4003 12.4765 0.7305 253.3884 252.6579 242.4026 13.2985 0.7266 253.3464 252.6197 242.3817 14.0910 0.7181 253.3017 252.5836 242.3816 14.8845 0.7104 253.2258 252.5154 242.4096 15.7065 0.7066 253.2111 252.5045 242.4313 16.4985 0.7063 253.1659 252.4596 242.4422 17.3205 0.7087 253.0879 252.3792 242.4653 18.1125 0.7124 253.0428 252.3304 242.4921 18.9045 0.7145 252.9993 252.2849 242.5061 19.7273 0.7137 252.9538 252.2401 242.5264 20.5165 0.7136 252.8987 252.1851 242.6065 21.3335 0.7096 252.8736 252.1641 242.6425 22.1235 0.7074 252.8077 252.1002 242.7104 22.9133 0.7015 252.7579 252.0563 242.7359 23.7330 0.6993 252.7206 252.0212 242.7987 24.5220 0.7021 252.6824 251.9803 242.8723 25.3400 0.7057 252.6419 251.9362 242.9387 26.1285 0.7013 252.5996 251.8983 243.0163 26.9180 0.6993 252.5551 251.8559 243.0934 27.7498 0.6988 252.5004 251.8016 243.1818 28.5230 0.6973 252.4491 251.7518 243.2820 29.3428 0.7010 252.4225 251.7214 243.3754 30.1330 0.6950 252.3698 251.6748 243.4735 30.9543 0.6932 252.3254 251.6322 243.5686 31.7448 0.6979 252.2872 251.5894 243.6639 32.5365 0.7005 252.2359 251.5355 243.7671 33.3588 0.7014 252.2044 251.5030 243.8588 34.1505 0.6982 252.1591 251.4609 243.9747 34.9725 0.6911 252.1174 251.4264 244.0977 35.7658 0.6928 252.0773 251.3845 244.2075 36.5585 0.6912 252.0430 251.3518 244.3275 37.3805 0.6872 251.9957 251.3085 244.4452 38.1425 0.6839 251.9443 251.2604 244.5709 38.9955 0.6856 251.8921 251.2065 244.7138 39.7875 0.6815 251.8834 251.2019 244.8429 40.5795 0.6780 251.8531 251.1751 244.9721 41.4015 0.6739 251.7998 251.1259 245.0947 42.1635 0.6767 251.7623 251.0856 245.2076 43.0168 0.6731 251.7234 251.0504 245.3544 43.8085 0.6730 251.6881 251.0151 245.4822 44.6005 0.6677 251.6604 250.9927 245.6365 45.4225 0.6630 251.6206 250.9576 245.7735 46.1845 0.6623 251.5791 250.9168 245.8939 47.0383 0.6607 251.5458 250.8850 246.0454 47.8303 0.6622 251.5103 250.8482 246.1793 48.6435 0.6632 251.4878 250.8246 246.3135 49.4365 0.6574 251.4507 250.7933 246.4581 50.2285 0.6537 251.4340 250.7803 246.5814 51.0510 0.6488 251.3909 250.7420 246.7095 51.8125 0.6459 251.3500 250.7041 246.8428 52.6660 0.6457 251.3153 250.6696 247.0087 53.4578 0.6413 251.2984 250.6571 247.1281 54.2460 0.6422 251.2557 250.6135 247.2379 55.0645 0.6364 251.2246 250.5882 247.3692 55.8223 0.6349 251.1984 250.5635 247.4789 56.6708 0.6325 251.1608 250.5283 247.6326 57.4588 0.6265 251.1316 250.5051 247.7714 58.2480 0.6225 251.0955 250.4730 247.9100 59.0660 0.6202 251.0805 250.4603 248.0008 59.8540 0.6130 251.0642 250.4512 248.1344 60.6728 0.6102 251.0180 250.4079 248.2425 61.4618 0.6047 250.9874 250.3828 248.3625 62.2520 0.5976 250.9734 250.3759 248.4705 63.0710 0.5958 250.9313 250.3355 248.5797 63.8625 0.5936 250.9110 250.3173 248.6919 64.6845 0.5955 250.8962 250.3008 248.8096 65.4768 0.5987 250.8548 250.2561 248.9122 66.2695 0.5982 250.8410 250.2429 249.0211 67.0948 0.6096 250.8143 250.2048 249.1360 67.8573 0.6104 250.7996 250.1892 249.2147 68.7095 0.6015 250.7739 250.1723 249.3209 69.4715 0.5949 250.7426 250.1477 249.4258 70.2933 0.5893 250.7267 250.1374 249.5457 71.1153 0.5867 250.6865 250.0998 249.6411 71.8765 0.5770 250.6817 250.1047 249.7203 72.7290 0.5675 250.6632 250.0956 249.8170 73.4913 0.5657 250.6511 250.0854 249.9054 74.3138 0.5658 250.6136 250.0478 250.0151 75.1360 0.5623 250.5980 250.0357 250.1010 75.8975 0.5539 250.5853 250.0314 250.1836 76.7500 0.5490 250.5573 250.0083 250.2897 77.5120 0.5457 250.5520 250.0063 250.3805 78.3358 0.5381 250.5362 249.9981 250.4600 79.1353 0.5312 250.5210 249.9899 250.5243 79.9295 0.5284 250.5006 249.9723 250.6198 80.7820 0.5223 250.4709 249.9486 250.7339 81.5440 0.5227 250.4760 249.9533 250.8122 82.3668 0.5220 250.4367 249.9147 250.8945 83.1588 0.5134 250.4273 249.9139 250.9770 83.9505 0.5078 250.4238 249.9159 251.0532 84.8028 0.5062 250.3960 249.8898 251.1452 85.5625 0.5122 250.3652 249.8530 251.2257 86.3830 0.5156 250.3520 249.8364 251.2986 87.1715 0.5113 250.3656 249.8542 251.3771 87.9600 0.5105 250.3580 249.8475 251.4564 88.7823 0.5040 250.3441 249.8401 251.5413 89.5703 0.5056 250.3178 249.8122 251.6261 90.3883 0.4978 250.3070 249.8092 251.6954 91.1770 0.4974 250.3180 249.8207 251.7744 91.9660 0.4948 250.2981 249.8033 251.8636 92.7850 0.4958 250.2851 249.7893 251.9532 93.5743 0.4907 250.2624 249.7717 252.0454 94.3930 0.4928 250.2629 249.7701 252.1211 95.1818 0.4838 250.2288 249.7450 252.2000 95.9718 0.4766 250.2150 249.7383 252.2860 96.8210 0.4742 250.2183 249.7441 252.3717 97.5820 0.4726 250.2132 249.7407 252.4474 98.4048 0.4732 250.2316 249.7584 252.5367 99.2013 0.4690 250.1963 249.7273 252.6203 100.0065 0.4689 250.1897 249.7208 252.7082 100.7990 0.4649 250.1868 249.7219 252.7970 101.5905 0.4623 250.1844 249.7222 252.8883 102.4430 0.4616 250.1812 249.7196 252.9824 103.2048 0.4556 250.1837 249.7280 253.0802 104.0285 0.4575 250.1890 249.7315 253.1676 104.8210 0.4502 250.1657 249.7155 253.2599 105.6125 0.4429 250.1439 249.7011 253.3339 106.4650 0.4382 250.1549 249.7167 253.4486 107.2270 0.4347 250.1518 249.7170 253.5509 108.0498 0.4370 250.1414 249.7044 253.6378 108.8418 0.4382 250.1510 249.7128 253.7293 109.6335 0.4378 250.1443 249.7066 253.8247 110.4858 0.4343 250.1369 249.7026 253.9305 111.2475 0.4345 250.1431 249.7086 254.0196 112.0718 0.4346 250.1634 249.7287 254.1264 112.8638 0.4305 250.1492 249.7186 254.2212 113.6555 0.4292 250.1550 249.7258 254.3214 114.5075 0.4261 250.1566 249.7305 254.4118 115.2695 0.4265 250.1516 249.7251 254.4995 116.0935 0.4238 250.1585 249.7347 254.6138 116.8908 0.4207 250.1523 249.7316 254.7128 117.6800 0.4180 250.1546 249.7366 254.7912 118.4983 0.4158 250.1561 249.7403 254.8968 119.2860 0.4102 250.1621 249.7520 254.9961 120.1245 0.4076 250.1534 249.7457 255.0905 120.8900 0.4068 250.1498 249.7431 255.1782 121.7080 0.4051 250.1792 249.7741 255.3037 122.4968 0.4019 250.1799 249.7781 255.3989 123.2860 0.3974 250.1734 249.7760 255.5111 124.1053 0.3821 250.1783 249.7961 255.6063 124.8945 0.3621 250.1902 249.8281 255.7159 125.7153 0.3505 250.1907 249.8402 255.8087 126.5043 0.3490 250.1960 249.8470 255.9117 127.2933 0.3439 250.2084 249.8644 256.0184 128.1448 0.3435 250.2092 249.8657 256.1560 128.9060 0.3387 250.1989 249.8602 256.2399 129.7268 0.3361 250.2353 249.8992 256.3525 130.5190 0.3357 250.2439 249.9082 256.4608 131.3125 0.3331 250.2583 249.9252 256.5637 132.1648 0.3303 250.2523 249.9221 256.6801 132.9270 0.3250 250.2546 249.9296 256.7852 133.7498 0.3249 250.2702 249.9453 256.8821 134.5420 0.3201 250.2826 249.9625 256.9960 135.3335 0.3154 250.2892 249.9738 257.0978 136.1858 0.3188 250.3148 249.9960 257.2107 136.9480 0.3157 250.3155 249.9998 257.3257 137.7705 0.3111 250.3188 250.0077 257.4209 138.5625 0.3099 250.3529 250.0430 257.5099 139.3545 0.3068 250.3506 250.0438 257.6156 140.2065 0.2974 250.3537 250.0563 257.7295 140.9685 0.2985 250.3588 250.0603 257.8358 141.7925 0.3022 250.3853 250.0831 257.9425 142.5845 0.3052 250.3973 250.0921 258.0518 143.3765 0.3115 250.4304 250.1188 258.1420 144.2285 0.3155 250.4279 250.1124 258.2593 144.9908 0.3117 250.4577 250.1460 258.3490 145.8135 0.3113 250.4555 250.1442 258.4422 146.6055 0.3066 250.4646 250.1580 258.5722 147.3975 0.2998 250.4884 250.1886 258.6683 148.2495 0.3013 250.5140 250.2127 258.7731 149.0115 0.3004 250.5342 250.2338 258.8610 149.8328 0.2983 250.5557 250.2573 258.9601 150.5973 0.2963 250.5539 250.2577 259.0531 151.4238 0.2912 250.5861 250.2949 259.1802 152.2423 0.2860 250.6093 250.3233 259.2707 153.0010 0.2869 250.6130 250.3262 259.3797 153.8495 0.2871 250.6521 250.3650 259.4945 154.6085 0.2851 250.6687 250.3836 259.5917 155.4288 0.2807 250.6955 250.4148 259.6890 156.2473 0.2779 250.7078 250.4299 259.8063 157.0060 0.2715 250.7240 250.4524 259.8877 157.8545 0.2709 250.7357 250.4647 259.9870 158.6448 0.2669 250.7772 250.5103 260.0834 159.4355 0.2665 250.7819 250.5154 260.1833 160.2548 0.2641 250.8075 250.5434 260.2972 161.0463 0.2652 250.8500 250.5848 260.3891 161.8665 0.2619 250.8682 250.6063 260.4824 162.6590 0.2573 250.9054 250.6482 260.5781 163.4515 0.2514 250.8951 250.6437 260.6824 164.2750 0.2498 250.9392 250.6895 260.7772 165.0385 0.2470 250.9601 250.7131 260.8802 165.8905 0.2453 251.0049 250.7596 260.9833 166.6825 0.2420 251.0210 250.7791 261.0681 167.4745 0.2380 251.0283 250.7903 261.1646 168.2980 0.2381 251.0606 250.8225 261.2618 169.0605 0.2343 251.0955 250.8612 261.3461 169.9125 0.2311 251.1130 250.8820 261.4422 170.7045 0.2273 251.1473 250.9200 261.5313 171.5200 0.2261 251.1803 250.9543 261.6295 172.3115 0.2243 251.2003 250.9760 261.7248 173.1035 0.2177 251.2273 251.0096 261.8211 173.9270 0.2189 251.2470 251.0280 261.9267 174.6895 0.2201 251.2646 251.0445 262.0191 175.5415 0.2170 251.3049 251.0879 262.1144 176.3335 0.2152 251.3367 251.1215 262.2080 177.1250 0.2145 251.3789 251.1643 262.3061 177.9480 0.2068 251.4052 251.1985 262.4123 178.7095 0.2028 251.4277 251.2250 262.4959 179.5620 0.2032 251.4510 251.2478 262.6057 180.3540 0.1948 251.4780 251.2832 262.7052 181.1455 0.1947 251.5146 251.3199 262.8196 181.9688 0.1883 251.5633 251.3750 262.9224 182.7320 0.1876 251.5690 251.3814 263.0314 183.5870 0.1874 251.6031 251.4157 263.1266 184.3188 0.1856 251.6501 251.4646 263.2248 185.1733 0.1830 251.6860 251.5029 263.3349 185.9615 0.1793 251.7342 251.5549 263.4257 186.7508 0.1762 251.7625 251.5863 263.5367 187.5693 0.1776 251.7812 251.6037 263.6365 188.3580 0.1743 251.8212 251.6469 263.7334 189.1768 0.1732 251.8638 251.6906 263.8366 189.9655 0.1671 251.8913 251.7242 263.9478 190.7560 0.1658 251.9249 251.7591 264.0491 191.5905 0.1681 251.9421 251.7740 264.1577 192.3643 0.1619 251.9838 251.8220 264.2604 193.1843 0.1616 251.9994 251.8379 264.3791 193.9765 0.1585 252.0371 251.8786 264.4848 194.7985 0.1549 252.0849 251.9300 264.5783 195.5955 0.1516 252.1190 251.9674 264.6813 196.3895 0.1478 252.1669 252.0191 264.7697 197.2118 0.1458 252.2008 252.0551 264.8839 197.9760 0.1443 252.2237 252.0795 264.9814 198.8328 0.1426 252.2835 252.1409 265.0961 199.5955 0.1378 252.3155 252.1777 265.2139 200.4175 0.1363 252.3390 252.2027 265.3024 201.2395 0.1334 252.3978 252.2645 265.4112 202.0010 0.1316 252.4450 252.3134 265.5152 202.8540 0.1303 252.4627 252.3324 265.6153 203.6158 0.1272 252.5022 252.3750 265.7252 204.4378 0.1271 252.5554 252.4283 265.8159 205.2600 0.1234 252.5936 252.4702 265.9026 206.0215 0.1212 252.6512 252.5300 266.0226 206.8755 0.1183 252.6881 252.5698 266.1339 207.6378 0.1158 252.7216 252.6058 266.2202 208.4598 0.1156 252.7766 252.6610 266.3260 209.2820 0.1131 252.8061 252.6929 266.4404 210.0435 0.1070 252.8589 252.7520 266.5407 210.8960 0.1041 252.8938 252.7897 266.6336 211.6880 0.1008 252.9357 252.8349 266.7054 212.5020 0.0991 252.9910 252.8919 266.8217 213.2950 0.0951 253.0269 252.9317 266.9155 214.0863 0.0945 253.0398 252.9453 267.0175 214.9035 0.0929 253.0826 252.9897 267.1140 215.6620 0.0923 253.1462 253.0539 267.2278 216.5100 0.0936 253.1889 253.0953 267.3390 217.2983 0.0951 253.2332 253.1381 267.4273 218.0870 0.0914 253.2708 253.1794 267.5239 218.9053 0.0823 253.3107 253.2284 267.6293 219.6933 0.0799 253.3658 253.2859 267.7057 220.5120 0.0745 253.4147 253.3402 267.8083 221.3005 0.0713 253.4400 253.3686 267.9224 222.0890 0.0655 253.4978 253.4323 267.9931 222.9098 0.0653 253.5401 253.4748 268.0996 223.6995 0.0604 253.5929 253.5325 268.2041 224.5193 0.0598 253.6471 253.5873 268.3031 225.3098 0.0612 253.7081 253.6468 268.3780 226.1000 0.0555 253.7548 253.6992 268.4963 226.9520 0.0585 253.8015 253.7430 268.6206 227.7138 0.0498 253.8434 253.7936 268.7234 228.5358 0.0477 253.8936 253.8460 268.8257 229.3280 0.0447 253.9290 253.8843 268.9336 230.1205 0.0414 253.9689 253.9275 269.0280 230.9430 0.0407 254.0257 253.9850 269.1380 231.7348 0.0383 254.0639 254.0256 269.2312 232.5670 0.0353 254.1467 254.1114 269.3663 233.3388 0.0353 254.1887 254.1534 269.4538 234.1638 0.0319 254.2457 254.2138 269.5638 234.9560 0.0287 254.2863 254.2576 269.6817 235.7475 0.0260 254.3458 254.3198 269.8027 236.5715 0.0224 254.3960 254.3736 269.9183 237.3638 0.0220 254.4419 254.4199 270.0171 238.1858 0.0181 254.4792 254.4610 270.1279 238.9805 0.0146 254.5411 254.5265 270.2291 239.7745 0.0142 254.5942 254.5800 270.3148 240.5968 0.0102 254.6638 254.6535 270.4439 241.3585 0.0072 254.7054 254.6982 270.5363 242.2120 0.0067 254.7537 254.7471 270.6609 243.0038 0.0025 254.7810 254.7785 270.7680 243.7955 0.0005 254.8445 254.8439 270.8699 244.6175 -0.0014 254.9044 254.9058 270.9880 245.4095 -0.0055 254.9628 254.9683 271.1002 246.2313 -0.0108 255.0205 255.0313 271.2125 247.0233 -0.0087 255.0817 255.0904 271.3111 247.8140 -0.0088 255.1461 255.1549 271.4300 248.6093 -0.0141 255.1759 255.1901 271.5194 249.3980 -0.0124 255.2390 255.2513 271.6415 250.2465 -0.0113 255.2849 255.2962 271.7613 251.0093 -0.0175 255.3452 255.3628 271.8634 251.8300 -0.0205 255.4020 255.4225 271.9528 252.6195 -0.0189 255.4624 255.4813 272.0658 253.4320 -0.0074 255.5242 255.5316 272.1760 254.2220 -0.0017 255.5814 255.5831 272.2599 255.0110 -0.0059 255.6504 255.6563 272.3742 255.8608 -0.0083 255.6950 255.7033 272.4688 256.6218 -0.0112 255.7504 255.7615 272.5821 257.4445 -0.0118 255.8115 255.8233 272.7028 258.2635 -0.0176 255.8640 255.8817 272.8030 259.0245 -0.0217 255.9002 255.9219 272.8942 259.8780 -0.0228 255.9617 255.9845 273.0109 260.6395 -0.0228 256.0233 256.0460 273.0989 261.4618 -0.0259 256.0834 256.1093 273.2046 262.2545 -0.0299 256.1473 256.1772 273.3218 263.0478 -0.0301 256.2042 256.2343 273.4270 263.8748 -0.0367 256.2620 256.2987 273.5265 264.6665 -0.0403 256.3476 256.3879 273.6279 265.4888 -0.0414 256.3878 256.4293 273.7347 266.2808 -0.0397 256.4426 256.4822 273.8282 267.0733 -0.0439 256.5113 256.5552 273.9454 267.8958 -0.0479 256.5797 256.6277 274.0435 268.6600 -0.0507 256.6404 256.6911 274.1425 269.5170 -0.0502 256.7000 256.7503 274.2509 270.2838 -0.0554 256.7688 256.8243 274.3412 271.1095 -0.0583 256.8256 256.8840 274.4380 271.9315 -0.0634 256.8874 256.9509 274.5380 272.6935 -0.0614 256.9565 257.0180 274.6553 273.5578 -0.0607 257.0351 257.0959 274.7466 274.3015 -0.0662 257.0649 257.1311 274.8304 275.1535 -0.0675 257.1354 257.2029 274.9345 275.9455 -0.0701 257.2216 257.2917 275.0345 276.7375 -0.0693 257.2677 257.3369 275.1397 277.5610 -0.0708 257.3457 257.4165 275.2335 278.3248 -0.0710 257.4032 257.4743 275.3301 279.1760 -0.0748 257.4591 257.5339 275.4543 279.9113 -0.0777 257.5081 257.5858 275.5366 280.7670 -0.0792 257.5831 257.6623 275.6411 281.5550 -0.0844 257.6502 257.7345 275.7229 282.3430 -0.0889 257.7101 257.7990 275.8271 283.1610 -0.0877 257.7817 257.8695 275.9228 283.9190 -0.0886 257.8351 257.9237 276.0258 284.7705 -0.0935 257.9005 257.9940 276.1261 285.5628 -0.0958 257.9774 258.0733 276.2113 286.3530 -0.0974 258.0319 258.1293 276.3011 287.1728 -0.1019 258.1114 258.2133 276.4163 287.9620 -0.1050 258.1717 258.2767 276.5087 288.7815 -0.1073 258.2361 258.3434 276.6166 289.5755 -0.1086 258.3127 258.4213 276.7100 290.3685 -0.1136 258.3711 258.4847 276.7986 291.1685 -0.1150 258.4238 258.5389 276.8952 291.9615 -0.1187 258.5008 258.6195 276.9858 292.8138 -0.1192 258.5665 258.6857 277.0912 293.5785 -0.1180 258.6317 258.7498 277.1799 294.4035 -0.1172 258.7119 258.8292 277.2751 295.1958 -0.1205 258.7693 258.8898 277.3505 295.9898 -0.1238 258.8296 258.9535 277.4386 296.8160 -0.1271 258.8969 259.0240 277.5491 297.5808 -0.1309 258.9728 259.1036 277.6490 298.4360 -0.1275 259.0422 259.1696 277.7707 299.2000 -0.1312 259.0949 259.2261 277.8494 300.0235 -0.1368 259.1935 259.3303 277.9777 300.8455 -0.1340 259.2463 259.3803 278.0631 301.6100 -0.1390 259.3149 259.4539 278.1482 302.4383 -0.1393 259.3861 259.5254 278.2363 303.2028 -0.1404 259.4659 259.6063 278.3405 304.0658 -0.1488 259.5342 259.6830 278.4588 304.8445 -0.1697 259.5927 259.7625 278.5681 305.6665 -0.1765 259.6828 259.8593 278.6522 306.4590 -0.1702 259.7244 259.8946 278.7547 307.2520 -0.1734 259.8018 259.9752 278.8666 308.0743 -0.1820 259.8861 260.0681 278.9797 308.8658 -0.1838 259.9543 260.1381 279.0996 309.6878 -0.1871 260.0310 260.2180 279.2172 310.4800 -0.1903 260.0811 260.2714 279.3101 311.2710 -0.1885 260.1604 260.3489 279.4094 312.0903 -0.1876 260.2360 260.4236 279.5261 312.8783 -0.1882 260.3040 260.4922 279.6075 313.6963 -0.1914 260.3587 260.5502 279.7358 314.4593 -0.1944 260.4337 260.6281 279.8432 315.2815 -0.1943 260.5101 260.7044 279.9597 316.1058 -0.1975 260.6039 260.8014 280.0661 316.8650 -0.1977 260.6823 260.8799 280.1601 317.7135 -0.1989 260.7346 260.9335 280.2725 318.4723 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