DTA measure 1pbupdown4_results Date: 2025312:105 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.94 s Mass = 924.400 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3950 -1.2135 220.7659 221.9795 209.0899 3.9980 -1.2104 220.7390 221.9494 209.0291 5.6115 -1.2071 220.7130 221.9201 208.9667 7.2299 -1.2042 220.6899 221.8941 208.9025 8.8228 -1.2012 220.6674 221.8687 208.8407 10.4310 -1.1987 220.6383 221.8370 208.7742 12.0338 -1.1953 220.6140 221.8093 208.7122 13.6471 -1.1929 220.5922 221.7851 208.6608 15.2501 -1.1895 220.5730 221.7626 208.6083 16.8634 -1.1854 220.5495 221.7348 208.5584 18.4663 -1.1817 220.5300 221.7117 208.5205 20.0590 -1.1790 220.5009 221.6799 208.4919 21.6826 -1.1769 220.4837 221.6606 208.4782 23.2856 -1.1744 220.4610 221.6355 208.4747 24.8988 -1.1712 220.4355 221.6066 208.4734 26.5068 -1.1687 220.4067 221.5753 208.4895 28.1150 -1.1643 220.3843 221.5486 208.5238 29.7023 -1.1598 220.3555 221.5153 208.5664 31.3155 -1.1583 220.3269 221.4853 208.6284 32.9233 -1.1564 220.3021 221.4585 208.7050 34.5471 -1.1539 220.2768 221.4308 208.7940 36.1553 -1.1513 220.2555 221.4068 208.8999 37.7480 -1.1492 220.2277 221.3769 209.0188 39.3613 -1.1467 220.2089 221.3555 209.1585 40.9695 -1.1454 220.1880 221.3334 209.3201 42.5775 -1.1439 220.1652 221.3091 209.4997 44.1909 -1.1426 220.1427 221.2853 209.6956 45.7938 -1.1416 220.1153 221.2569 209.9069 47.4120 -1.1415 220.0988 221.2403 210.1295 49.0201 -1.1411 220.0778 221.2188 210.3728 50.6281 -1.1417 220.0590 221.2007 210.6419 52.2310 -1.1425 220.0435 221.1860 210.9224 53.8340 -1.1434 220.0281 221.1716 211.2172 55.4264 -1.1446 220.0100 221.1546 211.5186 57.0294 -1.1463 219.9936 221.1399 211.8346 58.6476 -1.1475 219.9846 221.1321 212.1682 60.2556 -1.1495 219.9641 221.1136 212.5138 61.8534 -1.1520 219.9477 221.0996 212.8672 63.4666 -1.1531 219.9383 221.0914 213.2419 65.0695 -1.1549 219.9253 221.0802 213.6221 66.6724 -1.1568 219.9153 221.0720 214.0091 68.2804 -1.1600 219.9173 221.0773 214.4017 69.8936 -1.1638 219.9188 221.0826 214.8045 71.5070 -1.1678 219.9115 221.0793 215.2024 73.1099 -1.1707 219.9225 221.0932 215.5953 74.7074 -1.1739 219.9263 221.1003 215.9920 76.3158 -1.1776 219.9308 221.1084 216.3867 77.9183 -1.1815 219.9354 221.1168 216.7799 79.5316 -1.1859 219.9522 221.1381 217.1684 81.1346 -1.1895 219.9615 221.1510 217.5499 82.7581 -1.1945 219.9783 221.1728 217.9357 84.3716 -1.1991 220.0031 221.2023 218.3153 85.9744 -1.2032 220.0250 221.2282 218.6765 87.5876 -1.2072 220.0484 221.2556 219.0293 89.1906 -1.2100 220.0758 221.2858 219.3723 90.7831 -1.2140 220.1041 221.3180 219.7068 92.3964 -1.2185 220.1374 221.3559 220.0306 93.9994 -1.2222 220.1688 221.3910 220.3411 95.6229 -1.2266 220.2052 221.4318 220.6503 97.2361 -1.2313 220.2383 221.4697 220.9554 98.8390 -1.2358 220.2719 221.5076 221.2314 100.4525 -1.2396 220.3166 221.5562 221.5018 102.0659 -1.2423 220.3555 221.5978 221.7628 103.6686 -1.2450 220.3974 221.6423 221.9942 105.2769 -1.2479 220.4422 221.6901 222.2266 106.8903 -1.2504 220.4849 221.7353 222.4467 108.4983 -1.2528 220.5293 221.7820 222.6542 110.1011 -1.2551 220.5736 221.8288 222.8483 111.7145 -1.2567 220.6288 221.8854 223.0301 113.3019 -1.2581 220.6829 221.9411 223.1976 114.8995 -1.2589 220.7432 222.0021 223.3515 116.5128 -1.2605 220.8032 222.0638 223.4986 118.1104 -1.2619 220.8641 222.1260 223.6329 119.6979 -1.2626 220.9210 222.1836 223.7639 121.2959 -1.2627 220.9815 222.2442 223.8877 122.9095 -1.2626 221.0479 222.3105 224.0009 124.5226 -1.2636 221.1178 222.3814 224.1101 126.1254 -1.2629 221.1836 222.4466 224.2084 127.7234 -1.2621 221.2509 222.5130 224.3012 129.3209 -1.2614 221.3274 222.5887 224.3871 130.9343 -1.2597 221.4000 222.6597 224.4688 132.5320 -1.2560 221.4710 222.7270 224.5423 134.1400 -1.2548 221.5485 222.8033 224.6156 135.7636 -1.2535 221.6273 222.8808 224.6917 137.3665 -1.2518 221.7065 222.9583 224.7642 138.9746 -1.2493 221.7833 223.0327 224.8376 140.5829 -1.2474 221.8612 223.1086 224.9023 142.1856 -1.2448 221.9398 223.1845 224.9753 143.7989 -1.2427 222.0252 223.2678 225.0469 145.4019 -1.2402 222.1121 223.3523 225.1202 147.0099 -1.2368 222.1983 223.4351 225.1990 148.6338 -1.2344 222.2854 223.5198 225.2786 150.2419 -1.2319 222.3708 223.6027 225.3628 151.8345 -1.2286 222.4497 223.6783 225.4510 153.4376 -1.2254 222.5329 223.7583 225.5537 155.0508 -1.2226 222.6191 223.8417 225.6653 156.6536 -1.2198 222.7108 223.9305 225.7623 158.2670 -1.2169 222.8074 224.0243 225.8785 159.8751 -1.2141 222.8955 224.1097 226.0013 161.4990 -1.2106 222.9917 224.2023 226.1312 163.1070 -1.2072 223.0755 224.2828 226.2729 164.7153 -1.2033 223.1639 224.3672 226.4329 166.3181 -1.1996 223.2530 224.4526 226.5988 167.9313 -1.1944 223.3453 224.5397 226.7731 169.5343 -1.1903 223.4416 224.6319 226.9528 171.1426 -1.1871 223.5325 224.7196 227.1447 172.7660 -1.1838 223.6273 224.8111 227.3519 174.3739 -1.1803 223.7169 224.8973 227.5664 175.9769 -1.1781 223.8092 224.9873 227.7865 177.5849 -1.1748 223.9088 225.0836 228.0173 179.1670 -1.1720 224.0101 225.1821 228.2535 180.7800 -1.1698 224.1012 225.2710 228.5123 182.3830 -1.1675 224.1978 225.3653 228.7728 183.9809 -1.1655 224.2941 225.4596 229.0429 185.5941 -1.1632 224.3926 225.5558 229.3190 187.1919 -1.1613 224.4945 225.6558 229.5928 188.7999 -1.1599 224.5984 225.7583 229.8834 190.4079 -1.1583 224.7072 225.8655 230.1690 192.0054 -1.1562 224.8182 225.9744 230.4600 193.6189 -1.1550 224.9264 226.0814 230.7642 195.2166 -1.1536 225.0352 226.1888 231.0727 196.8093 -1.1520 225.1409 226.2930 231.3786 198.4174 -1.1498 225.2577 226.4075 231.6880 200.0358 -1.1485 225.3803 226.5288 232.0003 201.6438 -1.1477 225.4944 226.6421 232.3095 203.2418 -1.1470 225.6019 226.7488 232.6245 204.8551 -1.1466 225.7156 226.8622 232.9410 206.4579 -1.1451 225.8300 226.9752 233.2476 208.0711 -1.1444 225.9552 227.0996 233.5594 209.6585 -1.1448 226.0761 227.2210 233.8648 211.2663 -1.1452 226.2011 227.3464 234.1717 212.8900 -1.1452 226.3359 227.4812 234.4814 214.4930 -1.1447 226.4651 227.6099 234.7803 216.1065 -1.1449 226.5885 227.7334 235.0734 217.7094 -1.1458 226.7139 227.8597 235.3569 219.3070 -1.1471 226.8448 227.9919 235.6283 220.9203 -1.1481 226.9875 228.1357 235.9011 222.5230 -1.1482 227.1310 228.2792 236.1676 224.1311 -1.1468 227.2697 228.4165 236.4305 225.7549 -1.1464 227.4053 228.5516 236.6878 227.3420 -1.1473 227.5470 228.6943 236.9361 228.9450 -1.1473 227.6772 228.8245 237.1816 230.5684 -1.1474 227.8130 228.9604 237.4212 232.1765 -1.1476 227.9535 229.1011 237.6460 233.7794 -1.1477 228.0904 229.2381 237.8602 235.3926 -1.1474 228.2373 229.3847 238.0727 236.9954 -1.1449 228.3834 229.5282 238.2798 238.6086 -1.1436 228.5299 229.6735 238.4837 240.2064 -1.1424 228.6828 229.8252 238.6759 241.8040 -1.1425 228.8366 229.9791 238.8550 243.4120 -1.1425 228.9923 230.1348 239.0332 245.0048 -1.1426 229.1434 230.2860 239.2040 246.6024 -1.1418 229.2873 230.4291 239.3727 248.2156 -1.1411 229.4326 230.5737 239.5410 249.8186 -1.1407 229.5883 230.7290 239.6946 251.4161 -1.1401 229.7335 230.8736 239.8439 253.0398 -1.1402 229.8854 231.0256 239.9883 254.6428 -1.1395 230.0480 231.1875 240.1382 256.2459 -1.1386 230.2078 231.3464 240.2800 257.8435 -1.1367 230.3648 231.5014 240.4172 259.4466 -1.1346 230.5201 231.6547 240.5572 261.0599 -1.1321 230.6734 231.8055 240.6920 262.6676 -1.1297 230.8351 231.9648 240.8225 264.2758 -1.1265 230.9969 232.1234 240.9559 265.8940 -1.1264 231.1565 232.2829 241.0886 267.5071 -1.1241 231.3197 232.4438 241.2206 269.0945 -1.1231 231.4877 232.6108 241.3508 270.7183 -1.1213 231.6573 232.7786 241.4837 272.3110 -1.1204 231.8212 232.9416 241.6173 273.9191 -1.1179 231.9853 233.1031 241.7495 275.5325 -1.1152 232.1489 233.2641 241.8838 277.1354 -1.1135 232.3106 233.4241 242.0279 278.7589 -1.1115 232.4782 233.5897 242.1803 280.3670 -1.1094 232.6498 233.7592 242.3367 281.9751 -1.1079 232.8120 233.9199 242.4934 283.5829 -1.1060 232.9703 234.0763 242.6487 285.1860 -1.1050 233.1380 234.2430 242.8125 286.7990 -1.1034 233.3112 234.4146 242.9802 288.4019 -1.1020 233.4829 234.5850 243.1497 290.0153 -1.1016 233.6499 234.7515 243.3207 291.6231 -1.1001 233.8166 234.9167 243.4951 293.2363 -1.0991 233.9885 235.0876 243.6788 294.8394 -1.0970 234.1610 235.2580 243.8690 296.4526 -1.0948 234.3304 235.4251 244.0607 298.0555 -1.0931 234.4966 235.5897 244.2619 299.6636 -1.0931 234.6566 235.7498 244.4786 301.2718 -1.0919 234.8260 235.9179 244.6966 302.8900 -1.0906 234.9952 236.0858 244.9203 304.4929 -1.0899 235.1544 236.2442 245.1523 306.0751 -1.0898 235.3161 236.4059 245.3782 307.6881 -1.0890 235.4859 236.5749 245.6149 309.2860 -1.0881 235.6576 236.7457 245.8482 310.8734 -1.0875 235.8290 236.9165 246.0816 312.4763 -1.0877 235.9974 237.0851 246.3258 314.0843 -1.0882 236.1668 237.2551 246.5808 315.6816 -1.0881 236.3433 237.4313 246.8307 317.3053 -1.0881 236.5180 237.6061 247.0963 318.9133 -1.0888 236.6880 237.7769 247.3554 320.4954 -1.0899 236.8602 237.9501 247.6069 322.1035 -1.0916 237.0317 238.1233 247.8730 323.7061 -1.0919 237.2055 238.2973 248.1438 325.3091 -1.0917 237.3747 238.4664 248.4136 326.9173 -1.0933 237.5476 238.6409 248.6930 328.5203 -1.0952 237.7241 238.8193 248.9639 330.1335 -1.0967 237.9109 239.0076 249.2352 331.7520 -1.0974 238.0944 239.1918 249.5192 333.3441 -1.0989 238.2733 239.3722 249.8000 334.9525 -1.1007 238.4594 239.5600 250.0839 336.5555 -1.1008 238.6403 239.7411 250.3546 338.1686 -1.1022 238.8218 239.9239 250.6260 339.7719 -1.1034 239.0033 240.1067 250.8859 341.3850 -1.1049 239.1854 240.2904 251.1540 342.9828 -1.1063 239.3714 240.4777 251.4153 344.5858 -1.1076 239.5599 240.6674 251.6692 346.2095 -1.1085 239.7523 240.8608 251.9313 347.8176 -1.1100 239.9420 241.0520 252.1794 349.4205 -1.1121 240.1252 241.2373 252.4213 351.0339 -1.1130 240.3093 241.4223 252.6673 352.6370 -1.1141 240.4929 241.6070 252.9160 354.2503 -1.1156 240.6811 241.7968 253.1500 355.8530 -1.1167 240.8740 241.9908 253.3817 357.4766 -1.1181 241.0672 242.1853 253.6134 359.0896 -1.1206 241.2604 242.3810 253.8318 360.6978 -1.1225 241.4490 242.5715 254.0433 362.3006 -1.1242 241.6464 242.7706 254.2543 363.9140 -1.1256 241.8384 242.9640 254.4595 365.5169 -1.1273 242.0303 243.1576 254.6651 367.1299 -1.1286 242.2263 243.3549 254.8621 368.7381 -1.1303 242.4167 243.5470 255.0541 370.3410 -1.1323 242.6071 243.7395 255.2513 371.9386 -1.1339 242.7941 243.9281 255.4346 373.5419 -1.1351 242.9944 244.1296 255.6146 375.1395 -1.1357 243.1890 244.3248 255.7900 376.7476 -1.1374 243.3935 244.5309 255.9604 378.3453 -1.1397 243.5904 244.7301 256.1314 379.9533 -1.1408 243.7901 244.9309 256.2920 381.5561 -1.1424 243.9873 245.1297 256.4538 383.1641 -1.1430 244.1779 245.3209 256.6229 384.7619 -1.1429 244.3727 245.5157 256.7810 386.3750 -1.1432 244.5708 245.7140 256.9344 387.9779 -1.1431 244.7677 245.9108 257.0880 389.5809 -1.1441 244.9701 246.1143 257.2394 391.1886 -1.1451 245.1706 246.3157 257.3916 392.7968 -1.1460 245.3723 246.5183 257.5519 394.4151 -1.1464 245.5722 246.7186 257.7126 396.0281 -1.1463 245.7733 246.9195 257.8673 397.6313 -1.1467 245.9806 247.1273 258.0156 399.2291 -1.1461 246.1768 247.3229 258.1710 400.8371 -1.1468 246.3730 247.5198 258.3314 402.4399 -1.1460 246.5698 247.7159 258.4944 404.0530 -1.1453 246.7704 247.9157 258.6597 405.6558 -1.1458 246.9724 248.1181 258.8246 407.2795 -1.1459 247.1737 248.3196 258.9934 408.8875 -1.1445 247.3694 248.5139 259.1683 410.4956 -1.1436 247.5738 248.7174 259.3440 412.1035 -1.1443 247.7823 248.9266 259.5202 413.7115 -1.1453 247.9835 249.1288 259.7006 415.3196 -1.1460 248.1860 249.3319 259.8825 416.9280 -1.1466 248.3858 249.5324 260.0695 418.5204 -1.1478 248.5855 249.7333 260.2582 420.1439 -1.1482 248.7872 249.9354 260.4568 421.7519 -1.1475 248.9893 250.1368 260.6613 423.3601 -1.1474 249.1906 250.3379 260.8655 424.9734 -1.1478 249.3923 250.5401 261.0780 426.5763 -1.1484 249.5877 250.7361 261.2947 428.1845 -1.1500 249.7898 250.9398 261.5147 429.7925 -1.1505 249.9948 251.1453 261.7332 431.4211 -1.1508 250.1949 251.3456 261.9601 433.0241 -1.1513 250.3909 251.5422 262.1929 434.6116 -1.1521 250.5936 251.7457 262.4269 436.2093 -1.1534 250.7929 251.9463 262.6684 437.8174 -1.1538 250.9986 252.1525 262.9052 439.4201 -1.1546 251.2038 252.3584 263.1507 441.0230 -1.1555 251.4051 252.5606 263.4029 442.6209 -1.1574 251.6018 252.7592 263.6456 444.2341 -1.1598 251.8075 252.9672 263.9012 445.8475 -1.1612 252.0153 253.1765 264.1657 447.4504 -1.1632 252.2216 253.3849 264.4260 449.0585 -1.1648 252.4328 253.5976 264.6824 450.6613 -1.1675 252.6331 253.8005 264.9371 452.2643 -1.1695 252.8415 254.0111 265.1987 453.8724 -1.1714 253.0480 254.2194 265.4632 455.4650 -1.1729 253.2475 254.4205 265.7261 457.0884 -1.1745 253.4506 254.6250 265.9985 458.6859 -1.1761 253.6545 254.8306 266.2561 460.2993 -1.1790 253.8648 255.0438 266.5191 461.9023 -1.1819 254.0769 255.2588 266.7803 463.5103 -1.1848 254.2905 255.4753 267.0382 465.1183 -1.1873 254.5103 255.6975 267.2926 466.7263 -1.1904 254.7187 255.9091 267.5495 468.3496 -1.1922 254.9383 256.1305 267.8024 469.9526 -1.1952 255.1558 256.3510 268.0488 471.5661 -1.1976 255.3694 256.5670 268.2995 473.1690 -1.2006 255.5856 256.7863 268.5403 474.7771 -1.2034 255.8031 257.0065 268.7744 476.3853 -1.2063 256.0095 257.2158 269.0032 477.9934 -1.2097 256.2245 257.4342 269.2349 479.6173 -1.2128 256.4342 257.6471 269.4670 481.2301 -1.2156 256.6427 257.8582 269.6980 482.8331 -1.2186 256.8562 258.0748 269.9184 484.4464 -1.2220 257.0671 258.2892 270.1354 486.0494 -1.2256 257.2836 258.5092 270.3533 487.6574 -1.2287 257.5040 258.7327 270.5723 489.2658 -1.2324 257.7245 258.9569 270.7729 490.8891 -1.2349 257.9450 259.1799 270.9858 492.4970 -1.2387 258.1618 259.4004 271.1895 494.1000 -1.2414 258.3782 259.6196 271.3867 495.7133 -1.2438 258.5931 259.8369 271.5793 497.3111 -1.2452 258.8064 260.0516 271.7608 498.9140 -1.2475 259.0223 260.2698 271.9455 500.5221 -1.2505 259.2404 260.4909 272.1279 502.1145 -1.2540 259.4491 260.7031 272.3060 503.7228 -1.2567 259.6610 260.9177 272.4884 505.3259 -1.2600 259.8743 261.1343 272.6587 506.9235 -1.2627 260.0890 261.3517 272.8241 508.5368 -1.2650 260.3038 261.5689 272.9894 510.1346 -1.2681 260.5178 261.7859 273.1529 511.7428 -1.2704 260.7381 262.0085 273.3165 513.3509 -1.2723 260.9557 262.2280 273.4809 514.9589 -1.2739 261.1745 262.4484 273.6470 516.5670 -1.2757 261.3938 262.6695 273.8071 518.1751 -1.2774 261.6134 262.8908 273.9733 519.7728 -1.2799 261.8293 263.1092 274.1410 521.3861 -1.2830 262.0409 263.3238 274.3092 522.9893 -1.2847 262.2568 263.5415 274.4745 524.6025 -1.2879 262.4702 263.7581 274.6464 526.2055 -1.2910 262.6845 263.9755 274.8118 527.8291 -1.2939 262.9039 264.1978 274.9764 529.4373 -1.2966 263.1183 264.4149 275.1467 531.0401 -1.2990 263.3259 264.6249 275.3241 532.6535 -1.3010 263.5491 264.8502 275.4986 534.2565 -1.3029 263.7667 265.0696 275.6789 535.8699 -1.3063 263.9835 265.2898 275.8594 537.4730 -1.3094 264.2012 265.5106 276.0457 539.0965 -1.3117 264.4161 265.7279 276.2437 540.7045 -1.3137 264.6334 265.9471 276.4351 542.3078 -1.3164 264.8493 266.1657 276.6322 543.9211 -1.3183 265.0676 266.3859 276.8269 545.5243 -1.3217 265.2839 266.6056 277.0252 547.1375 -1.3260 265.5009 266.8268 277.2278 548.7405 -1.3285 265.7148 267.0433 277.4368 550.3641 -1.3323 265.9252 267.2575 277.6558 551.9721 -1.3344 266.1452 267.4797 277.8691 553.5751 -1.3370 266.3636 267.7006 278.0860 555.1885 -1.3404 266.5818 267.9221 278.3015 556.7914 -1.3431 266.8015 268.1445 278.5198 558.4049 -1.3457 267.0136 268.3593 278.7481 560.0080 -1.3486 267.2280 268.5766 278.9772 561.6316 -1.3501 267.4479 268.7981 279.2090 563.2291 -1.3525 267.6642 269.0167 279.4340 564.8321 -1.3569 267.8791 269.2361 279.6624 566.4298 -1.3607 268.0911 269.4518 279.8996 568.0378 -1.3635 268.3114 269.6750 280.1357 569.6356 -1.3677 268.5292 269.8969 280.3735 571.2435 -1.3725 268.7509 270.1234 280.6068 572.8259 -1.3766 268.9636 270.3401 280.8485 574.4443 -1.3797 269.1847 270.5644 281.0968 576.0523 -1.3834 269.4085 270.7919 281.3369 577.6551 -1.3877 269.6336 271.0213 281.5811 579.2631 -1.3921 269.8542 271.2463 281.8302 580.8661 -1.3966 270.0737 271.4704 282.0792 582.4794 -1.3999 270.2989 271.6988 282.3297 584.0669 -1.4031 270.5207 271.9238 282.5736 585.6905 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