DTA measure 2pbupdown3_results Date: 2025312:90 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.62 s Mass = 924.400 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1958 0.0090 224.0073 223.9983 271.0407 2.0148 0.0096 224.2981 224.2885 270.9051 2.7928 0.0108 224.5760 224.5652 270.7798 3.6428 0.0119 224.8813 224.8694 270.6400 4.4103 0.0130 225.1550 225.1420 270.5088 5.2293 0.0141 225.4461 225.4320 270.3641 6.0383 0.0150 225.7285 225.7134 270.2251 6.8263 0.0158 226.0032 225.9874 270.0820 7.6453 0.0171 226.2859 226.2688 269.9326 8.4233 0.0186 226.5597 226.5411 269.7884 9.2730 0.0210 226.8568 226.8358 269.6321 10.0408 0.0228 227.1248 227.1020 269.4884 10.8598 0.0244 227.4037 227.3793 269.3308 11.6168 0.0262 227.6650 227.6388 269.1850 12.4878 0.0288 227.9630 227.9342 269.0129 13.2448 0.0315 228.2204 228.1889 268.8616 14.0638 0.0332 228.4944 228.4612 268.7045 14.8623 0.0352 228.7633 228.7281 268.5544 15.6608 0.0384 229.0323 228.9940 268.4045 16.4900 0.0406 229.3102 229.2696 268.2483 17.2473 0.0434 229.5645 229.5211 268.1034 18.0970 0.0457 229.8447 229.7990 267.9390 18.8645 0.0478 230.0980 230.0502 267.7993 19.6838 0.0499 230.3653 230.3154 267.6540 20.4928 0.0529 230.6271 230.5742 267.5134 21.2808 0.0553 230.8839 230.8286 267.3732 22.0893 0.0573 231.1431 231.0858 267.2345 22.8773 0.0597 231.3926 231.3330 267.1082 23.7170 0.0615 231.6629 231.6014 266.9790 24.4743 0.0629 231.9003 231.8374 266.8664 25.3240 0.0650 232.1637 232.0987 266.7467 26.1018 0.0672 232.4089 232.3417 266.6365 26.9208 0.0695 232.6686 232.5991 266.5302 27.7190 0.0718 232.9205 232.8486 266.4298 28.5070 0.0749 233.1713 233.0964 266.3417 29.3470 0.0774 233.4340 233.3566 266.2510 30.1038 0.0795 233.6675 233.5880 266.1757 30.9640 0.0814 233.9310 233.8495 266.1046 31.7313 0.0832 234.1667 234.0835 266.0437 32.5503 0.0852 234.4172 234.3320 265.9867 33.3490 0.0864 234.6542 234.5677 265.9435 34.1470 0.0877 234.8904 234.8026 265.9157 34.9763 0.0894 235.1450 235.0556 265.8910 35.7438 0.0914 235.3696 235.2782 265.8727 36.6040 0.0929 235.6186 235.5257 265.8663 37.3608 0.0947 235.8375 235.7428 265.8734 38.1905 0.0966 236.0735 235.9769 265.8911 38.9888 0.0973 236.3011 236.2039 265.9213 39.7768 0.0979 236.5271 236.4293 265.9570 40.6060 0.0980 236.7664 236.6684 266.0090 41.3738 0.0990 236.9850 236.8860 266.0693 42.2340 0.0997 237.2292 237.1295 266.1484 42.9913 0.0997 237.4433 237.3436 266.2315 43.8310 0.0997 237.6794 237.5798 266.3344 44.6188 0.0991 237.8981 237.7991 266.4428 45.4068 0.0992 238.1152 238.0160 266.5621 46.2363 0.0983 238.3387 238.2403 266.7019 46.9933 0.0970 238.5485 238.4515 266.8462 47.8535 0.0962 238.7850 238.6888 267.0098 48.6210 0.0949 238.9935 238.8986 267.1682 49.4400 0.0932 239.2158 239.1226 267.3520 50.2383 0.0926 239.4318 239.3392 267.5498 51.0263 0.0909 239.6414 239.5505 267.7477 51.8660 0.0886 239.8651 239.7765 267.9667 52.6233 0.0865 240.0706 239.9841 268.1693 53.4730 0.0832 240.2949 240.2117 268.4118 54.2510 0.0807 240.5034 240.4227 268.6469 55.0700 0.0774 240.7173 240.6399 268.9031 55.8683 0.0745 240.9272 240.8526 269.1587 56.6563 0.0718 241.1388 241.0670 269.4186 57.4963 0.0686 241.3532 241.2846 269.7103 58.2533 0.0659 241.5495 241.4835 269.9798 59.0725 0.0623 241.7643 241.7020 270.2795 59.8500 0.0579 241.9640 241.9060 270.5717 60.7000 0.0523 242.1840 242.1317 270.8978 61.4673 0.0469 242.3848 242.3379 271.1991 62.2863 0.0421 242.5949 242.5528 271.5294 63.0848 0.0368 242.7969 242.7601 271.8554 63.9143 0.0309 243.0050 242.9742 272.2004 64.7023 0.0254 243.2025 243.1772 272.5344 65.5005 0.0198 243.4050 243.3852 272.8793 66.3300 0.0134 243.6212 243.6077 273.2370 67.0870 0.0078 243.8097 243.8018 273.5687 67.9163 0.0010 244.0218 244.0208 273.9386 68.6840 -0.0062 244.2194 244.2255 274.2830 69.5440 -0.0135 244.4401 244.4535 274.6724 70.3115 -0.0212 244.6354 244.6566 275.0247 71.1408 -0.0288 244.8434 244.8722 275.4042 71.9288 -0.0361 245.0393 245.0754 275.7648 72.7270 -0.0445 245.2364 245.2809 276.1269 73.5563 -0.0531 245.4463 245.4994 276.5034 74.3235 -0.0607 245.6371 245.6978 276.8615 75.1838 -0.0699 245.8496 245.9195 277.2558 75.9098 -0.0780 246.0305 246.1085 277.5802 76.7700 -0.0877 246.2492 246.3370 277.9628 77.5273 -0.0967 246.4451 246.5417 278.2970 78.3460 -0.1055 246.6533 246.7587 278.6557 79.1448 -0.1146 246.8531 246.9678 278.9966 79.9430 -0.1242 247.0557 247.1799 279.3390 80.7723 -0.1350 247.2674 247.4024 279.6884 81.5293 -0.1442 247.4611 247.6053 280.0025 82.3790 -0.1547 247.6815 247.8362 280.3558 83.1568 -0.1646 247.8797 248.0443 280.6675 83.9758 -0.1752 248.0878 248.2630 280.9948 84.7740 -0.1848 248.2972 248.4819 281.3095 85.5620 -0.1947 248.4999 248.6946 281.6144 86.3710 -0.2057 248.7056 248.9112 281.9166 87.1588 -0.2162 248.9128 249.1289 282.2086 87.9778 -0.2268 249.1250 249.3518 282.5052 88.7558 -0.2369 249.3301 249.5670 282.7798 89.6058 -0.2482 249.5468 249.7950 283.0706 90.3730 -0.2584 249.7413 249.9997 283.3236 91.1920 -0.2690 249.9449 250.2139 283.5847 92.0008 -0.2805 250.1500 250.4304 283.8405 92.7888 -0.2915 250.3490 250.6405 284.0830 93.6078 -0.3029 250.5561 250.8590 284.3252 94.3858 -0.3132 250.7537 251.0669 284.5476 95.2358 -0.3238 250.9737 251.2975 284.7781 96.0033 -0.3333 251.1701 251.5034 284.9782 96.8223 -0.3441 251.3826 251.7267 285.1841 97.6310 -0.3539 251.5869 251.9408 285.3836 98.4188 -0.3643 251.7871 252.1514 285.5675 99.2273 -0.3747 251.9894 252.3641 285.7479 100.0153 -0.3845 252.1916 252.5762 285.9157 100.8345 -0.3947 252.3984 252.7931 286.0822 101.6123 -0.4048 252.5960 253.0008 286.2344 102.4620 -0.4154 252.8219 253.2373 286.3885 103.2398 -0.4251 253.0259 253.4510 286.5219 104.0588 -0.4348 253.2404 253.6752 286.6552 104.8573 -0.4444 253.4452 253.8896 286.7796 105.6453 -0.4539 253.6503 254.1042 286.8945 106.4850 -0.4633 253.8682 254.3315 287.0103 107.2423 -0.4714 254.0647 254.5362 287.1044 108.0920 -0.4816 254.2845 254.7660 287.2041 108.8598 -0.4901 254.4838 254.9739 287.2945 109.6788 -0.4989 254.6925 255.1914 287.3783 110.4668 -0.5077 254.8951 255.4028 287.4548 111.2650 -0.5164 255.0980 255.6144 287.5304 112.0840 -0.5251 255.3020 255.8271 287.5878 112.8515 -0.5325 255.4948 256.0273 287.6353 113.7118 -0.5409 255.7150 256.2559 287.6872 114.4690 -0.5482 255.9118 256.4599 287.7306 115.2983 -0.5564 256.1236 256.6800 287.7713 116.0658 -0.5641 256.3203 256.8844 287.7972 116.8950 -0.5723 256.5353 257.1076 287.8218 117.6833 -0.5792 256.7347 257.3139 287.8424 118.4710 -0.5867 256.9356 257.5224 287.8553 119.3008 -0.5947 257.1466 257.7413 287.8658 120.0680 -0.6010 257.3446 257.9456 287.8736 120.9283 -0.6092 257.5659 258.1750 287.8779 121.6853 -0.6159 257.7589 258.3748 287.8770 122.5250 -0.6232 257.9685 258.5918 287.8764 123.3128 -0.6301 258.1672 258.7973 287.8682 124.1113 -0.6369 258.3764 259.0133 287.8538 124.9405 -0.6433 258.5867 259.2300 287.8405 125.6978 -0.6490 258.7779 259.4269 287.8218 126.5580 -0.6557 258.9882 259.6439 287.7988 127.3253 -0.6610 259.1840 259.8450 287.7730 128.1548 -0.6673 259.3888 260.0561 287.7455 128.9428 -0.6719 259.5849 260.2568 287.7146 129.7410 -0.6764 259.7813 260.4578 287.6905 130.5703 -0.6821 259.9829 260.6651 287.6582 131.3375 -0.6865 260.1697 260.8562 287.6255 132.1978 -0.6920 260.3800 261.0720 287.5820 132.9550 -0.6971 260.5690 261.2661 287.5467 133.7843 -0.7028 260.7739 261.4767 287.5090 134.5518 -0.7074 260.9599 261.6673 287.4733 135.4223 -0.7123 261.1651 261.8774 287.4292 136.1793 -0.7159 261.3508 262.0667 287.3967 137.0088 -0.7207 261.5553 262.2760 287.3599 137.8073 -0.7257 261.7493 262.4749 287.3283 138.5950 -0.7302 261.9438 262.6740 287.2969 139.4243 -0.7343 262.1471 262.8815 287.2673 140.1918 -0.7381 262.3328 263.0709 287.2375 141.0523 -0.7422 262.5371 263.2793 287.2035 141.8093 -0.7463 262.7127 263.4590 287.1777 142.6280 -0.7505 262.9026 263.6531 287.1521 143.4263 -0.7546 263.0939 263.8486 287.1384 144.2248 -0.7580 263.2832 264.0412 287.1258 145.0023 -0.7613 263.4742 264.2355 287.1154 145.8320 -0.7647 263.6695 264.4341 287.1047 146.6303 -0.7686 263.8551 264.6237 287.0997 147.4180 -0.7717 264.0379 264.8095 287.0950 148.2478 -0.7754 264.2314 265.0068 287.0981 149.0048 -0.7784 264.4071 265.1855 287.1055 149.8650 -0.7819 264.6038 265.3857 287.1296 150.6323 -0.7855 264.7795 265.5650 287.1475 151.4515 -0.7889 264.9723 265.7612 287.1663 152.2500 -0.7930 265.1554 265.9484 287.1878 153.0480 -0.7969 265.3401 266.1370 287.2198 153.8773 -0.8005 265.5268 266.3273 287.2619 154.6348 -0.8032 265.6961 266.4993 287.3050 155.4950 -0.8064 265.8856 266.6920 287.3578 156.2623 -0.8100 266.0533 266.8633 287.4091 157.0810 -0.8137 266.2343 267.0480 287.4684 157.8793 -0.8173 266.4089 267.2262 287.5335 158.6780 -0.8209 266.5813 267.4023 287.6015 159.5073 -0.8242 266.7635 267.5877 287.6849 160.2643 -0.8275 266.9304 267.7579 287.7705 161.1245 -0.8312 267.1131 267.9443 287.8710 161.8918 -0.8343 267.2783 268.1125 287.9681 162.7210 -0.8374 267.4618 268.2992 288.0832 163.5193 -0.8412 267.6328 268.4741 288.1985 164.3073 -0.8459 267.7988 268.6446 288.3218 165.1473 -0.8506 267.9822 268.8328 288.4647 165.9040 -0.8544 268.1497 269.0041 288.5961 166.7643 -0.8589 268.3364 269.1953 288.7457 167.5318 -0.8630 268.5008 269.3638 288.8857 168.3610 -0.8675 268.6735 269.5410 289.0474 169.1490 -0.8716 268.8375 269.7091 289.2107 169.9475 -0.8762 269.0032 269.8794 289.3771 170.7768 -0.8815 269.1777 270.0592 289.5600 171.5338 -0.8861 269.3343 270.2205 289.7292 172.4043 -0.8913 269.5155 270.4068 289.9387 173.1615 -0.8963 269.6714 270.5677 290.1254 173.9910 -0.9009 269.8421 270.7430 290.3336 174.7788 -0.9066 270.0020 270.9086 290.5429 175.5668 -0.9123 270.1635 271.0758 290.7541 176.3653 -0.9175 270.3341 271.2516 290.9741 177.1533 -0.9231 270.5024 271.4255 291.1920 177.9723 -0.9283 270.6725 271.6008 291.4264 178.7500 -0.9331 270.8279 271.7610 291.6529 179.6000 -0.9392 271.0006 271.9398 291.8987 180.3673 -0.9455 271.1617 272.1072 292.1295 181.1863 -0.9514 271.3325 272.2840 292.3821 181.9640 -0.9570 271.4911 272.4481 292.6243 182.7828 -0.9635 271.6599 272.6234 292.8803 183.5708 -0.9696 271.8208 272.7904 293.1308 184.3795 -0.9765 271.9877 272.9642 293.3865 185.1985 -0.9829 272.1534 273.1363 293.6521 185.9658 -0.9896 272.3082 273.2978 293.9098 186.8260 -0.9965 272.4891 273.4856 294.1934 187.5623 -1.0025 272.6346 273.6371 294.4366 188.4125 -1.0092 272.8081 273.8173 294.7245 189.1903 -1.0162 272.9697 273.9859 294.9869 190.0093 -1.0236 273.1393 274.1629 295.2620 190.7970 -1.0303 273.3011 274.3314 295.5293 191.6058 -1.0373 273.4648 274.5021 295.8069 192.4250 -1.0446 273.6317 274.6763 296.0858 193.1923 -1.0523 273.7901 274.8424 296.3453 194.0423 -1.0601 273.9617 275.0217 296.6297 194.8200 -1.0673 274.1224 275.1897 296.8936 195.6388 -1.0752 274.2907 275.3658 297.1729 196.4270 -1.0828 274.4495 275.5323 297.4357 197.2358 -1.0905 274.6131 275.7036 297.7041 198.0548 -1.0984 274.7842 275.8825 297.9741 198.8220 -1.1054 274.9435 276.0489 298.2222 199.6720 -1.1138 275.1189 276.2327 298.4981 200.4500 -1.1213 275.2790 276.4003 298.7442 201.2688 -1.1297 275.4445 276.5742 299.0036 202.0670 -1.1376 275.6090 276.7466 299.2508 202.8653 -1.1455 275.7736 276.9191 299.4977 203.6530 -1.1533 275.9358 277.0891 299.7417 204.4620 -1.1608 276.1051 277.2659 299.9815 205.2810 -1.1690 276.2741 277.4431 300.2258 206.0483 -1.1768 276.4339 277.6107 300.4461 206.8983 -1.1856 276.6119 277.7975 300.6853 207.6550 -1.1935 276.7702 277.9637 300.8922 208.4843 -1.2012 276.9490 278.1502 301.1183 209.2828 -1.2086 277.1178 278.3264 301.3288 210.0810 -1.2168 277.2824 278.4992 301.5333 210.9003 -1.2258 277.4579 278.6837 301.7422 211.6675 -1.2332 277.6194 278.8526 301.9364 212.4968 -1.2414 277.7941 279.0355 302.1307 213.2538 -1.2486 277.9486 279.1972 302.3069 214.1140 -1.2572 278.1263 279.3834 302.5090 214.8713 -1.2645 278.2786 279.5431 302.6743 215.7005 -1.2717 278.4546 279.7264 302.8564 216.4988 -1.2798 278.6241 279.9039 303.0275 217.2868 -1.2875 278.7933 280.0808 303.1917 218.1163 -1.2956 278.9771 280.2727 303.3548 218.8838 -1.3020 279.1431 280.4451 303.5017 219.7440 -1.3106 279.3209 280.6315 303.6616 220.5013 -1.3180 279.4848 280.8028 303.7997 221.3305 -1.3252 279.6680 280.9932 303.9457 222.1293 -1.3326 279.8397 281.1723 304.0755 222.9170 -1.3395 280.0110 281.3505 304.1979 223.7463 -1.3467 280.1855 281.5322 304.3220 224.5140 -1.3536 280.3516 281.7052 304.4357 225.3743 -1.3607 280.5391 281.8999 304.5555 226.1005 -1.3664 280.6937 282.0601 304.6511 226.9610 -1.3730 280.8777 282.2507 304.7629 227.7593 -1.3791 281.0527 282.4317 304.8610 228.5473 -1.3857 281.2194 282.6051 304.9545 229.3768 -1.3928 281.3955 282.7882 305.0460 230.1440 -1.3988 281.5596 282.9584 305.1282 231.0043 -1.4052 281.7430 283.1482 305.2216 231.7408 -1.4104 281.8967 283.3071 305.2940 232.6010 -1.4171 282.0812 283.4983 305.3742 233.3578 -1.4222 282.2417 283.6638 305.4401 234.1875 -1.4281 282.4199 283.8480 305.5119 234.9858 -1.4338 282.5904 284.0242 305.5715 235.7840 -1.4391 282.7574 284.1965 305.6298 236.6133 -1.4444 282.9328 284.3772 305.6817 237.3700 -1.4493 283.0936 284.5429 305.7244 238.2303 -1.4542 283.2801 284.7343 305.7723 238.9875 -1.4591 283.4436 284.9027 305.8172 239.8065 -1.4640 283.6208 285.0848 305.8562 240.6050 -1.4692 283.7900 285.2593 305.8967 241.4030 -1.4742 283.9568 285.4309 305.9337 242.2323 -1.4787 284.1373 285.6160 305.9680 242.9893 -1.4833 284.3005 285.7838 305.9962 243.8390 -1.4879 284.4793 285.9672 306.0311 244.6173 -1.4922 284.6510 286.1432 306.0612 245.4360 -1.4955 284.8301 286.3256 306.0922 246.2343 -1.4996 285.0025 286.5021 306.1217 247.0223 -1.5036 285.1651 286.6687 306.1447 247.8413 -1.5078 285.3375 286.8453 306.1678 248.6193 -1.5113 285.5041 287.0153 306.1894 249.4690 -1.5149 285.6842 287.1990 306.2103 250.2363 -1.5182 285.8460 287.3642 306.2318 251.0553 -1.5216 286.0179 287.5395 306.2578 251.8640 -1.5253 286.1823 287.7076 306.2784 252.6518 -1.5289 286.3439 287.8727 306.2960 253.4708 -1.5317 286.5147 288.0464 306.3169 254.2488 -1.5354 286.6737 288.2091 306.3406 255.0988 -1.5389 286.8476 288.3865 306.3669 255.8660 -1.5412 287.0045 288.5457 306.3904 256.6850 -1.5438 287.1786 288.7224 306.4211 257.4940 -1.5470 287.3444 288.8914 306.4468 258.2818 -1.5504 287.5055 289.0559 306.4748 259.1215 -1.5540 287.6778 289.2319 306.5099 259.8788 -1.5565 287.8378 289.3942 306.5419 260.7388 -1.5599 288.0122 289.5721 306.5778 261.4753 -1.5629 288.1695 289.7324 306.6129 262.3250 -1.5663 288.3422 289.9085 306.6565 263.1028 -1.5697 288.4982 290.0679 306.6988 263.9218 -1.5729 288.6613 290.2343 306.7411 264.7200 -1.5758 288.8227 290.3985 306.7923 265.5183 -1.5779 288.9822 290.5601 306.8428 266.3783 -1.5802 289.1535 290.7337 306.9038 267.1353 -1.5823 289.3049 290.8872 306.9609 267.9650 -1.5847 289.4700 291.0547 307.0271 268.7633 -1.5879 289.6269 291.2148 307.0960 269.5615 -1.5913 289.7864 291.3777 307.1636 270.3803 -1.5943 289.9530 291.5473 307.2392 271.1478 -1.5974 290.1020 291.6994 307.3150 271.9773 -1.6011 290.2671 291.8682 307.4053 272.7343 -1.6045 290.4145 292.0190 307.4874 273.5840 -1.6076 290.5775 292.1851 307.5803 274.3515 -1.6096 290.7279 292.3374 307.6679 275.1705 -1.6124 290.8872 292.4996 307.7649 275.9793 -1.6155 291.0397 292.6553 307.8724 276.7673 -1.6184 291.1890 292.8074 307.9800 277.5860 -1.6218 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