DTA measure 4pbupdown3_results Date: 2025312:929 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.76 s Mass = 924.400 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5881 -5.2720 436.4646 441.7366 419.7352 4.1848 -5.2777 436.5153 441.7930 419.7707 5.7971 -5.2844 436.5627 441.8470 419.8429 7.3990 -5.2912 436.6005 441.8918 419.9455 9.0061 -5.2988 436.6358 441.9346 420.0783 10.6131 -5.3078 436.6717 441.9795 420.2423 12.2358 -5.3182 436.7083 442.0265 420.4390 13.8429 -5.3284 436.7415 442.0699 420.6626 15.4449 -5.3391 436.7677 442.1068 420.8951 17.0575 -5.3505 436.7960 442.1465 421.1493 18.6696 -5.3629 436.8183 442.1812 421.4091 20.2565 -5.3740 436.8409 442.2149 421.6623 21.8793 -5.3874 436.8687 442.2562 421.9306 23.5020 -5.4003 436.8878 442.2882 422.2063 25.1091 -5.4132 436.9076 442.3208 422.4640 26.7216 -5.4274 436.9407 442.3680 422.7176 28.3133 -5.4411 436.9707 442.4118 422.9501 29.9153 -5.4550 436.9974 442.4524 423.1666 31.5123 -5.4688 437.0179 442.4867 423.3647 33.1194 -5.4825 437.0372 442.5198 423.5471 34.7109 -5.4954 437.0689 442.5643 423.7057 36.3129 -5.5091 437.1102 442.6193 423.8437 37.9356 -5.5214 437.1386 442.6601 423.9615 39.5426 -5.5332 437.1686 442.7017 424.0507 41.1445 -5.5457 437.1971 442.7428 424.1145 42.7466 -5.5573 437.2291 442.7864 424.1541 44.3593 -5.5687 437.2663 442.8351 424.1625 45.9613 -5.5785 437.2985 442.8770 424.1361 47.5685 -5.5881 437.3324 442.9206 424.0849 49.1964 -5.5977 437.3629 442.9606 424.0099 50.8036 -5.6064 437.3952 443.0016 423.9114 52.4055 -5.6154 437.4213 443.0366 423.7884 54.0181 -5.6227 437.4510 443.0737 423.6378 55.6151 -5.6292 437.4859 443.1151 423.4664 57.2170 -5.6355 437.5199 443.1555 423.2720 58.8293 -5.6413 437.5438 443.1850 423.0527 60.4315 -5.6465 437.5736 443.2201 422.8171 62.0544 -5.6515 437.6023 443.2538 422.5573 63.6510 -5.6558 437.6244 443.2802 422.2790 65.2530 -5.6598 437.6379 443.2977 421.9800 66.8498 -5.6627 437.6545 443.3172 421.6609 68.4466 -5.6673 437.6645 443.3318 421.3321 70.0591 -5.6695 437.6770 443.3464 420.9877 71.6611 -5.6706 437.6888 443.3594 420.6287 73.2684 -5.6720 437.6963 443.3683 420.2445 74.8601 -5.6735 437.7019 443.3754 419.8564 76.4828 -5.6733 437.7097 443.3829 419.4485 78.0899 -5.6733 437.7138 443.3871 419.0437 79.6919 -5.6723 437.7078 443.3801 418.6178 81.3041 -5.6714 437.7048 443.3763 418.1870 82.9064 -5.6712 437.6982 443.3693 417.7604 84.5138 -5.6692 437.6829 443.3520 417.3302 86.1211 -5.6669 437.6678 443.3347 416.8875 87.7283 -5.6649 437.6513 443.3162 416.4406 89.3460 -5.6624 437.6274 443.2899 415.9913 90.9533 -5.6593 437.6037 443.2629 415.5420 92.5604 -5.6561 437.5701 443.2262 415.0927 94.1629 -5.6538 437.5329 443.1866 414.6408 95.7648 -5.6502 437.4886 443.1389 414.2018 97.3565 -5.6462 437.4482 443.0944 413.7724 98.9585 -5.6426 437.3988 443.0414 413.3428 100.5659 -5.6389 437.3451 442.9840 412.9193 102.1835 -5.6360 437.2870 442.9230 412.5037 103.7906 -5.6332 437.2356 442.8688 412.0911 105.3926 -5.6301 437.1739 442.8040 411.6858 107.0050 -5.6277 437.1059 442.7336 411.2951 108.6070 -5.6250 437.0352 442.6602 410.9246 110.2193 -5.6225 436.9569 442.5793 410.5560 111.8216 -5.6193 436.8776 442.4970 410.2066 113.4494 -5.6162 436.7833 442.3995 409.8614 115.0563 -5.6136 436.6917 442.3053 409.5300 116.6635 -5.6119 436.5998 442.2118 409.2125 118.2655 -5.6097 436.5042 442.1139 408.9021 119.8776 -5.6075 436.4067 442.0142 408.6134 121.4848 -5.6064 436.3052 441.9115 408.3418 123.0918 -5.6047 436.2024 441.8071 408.0877 124.7196 -5.6039 436.0926 441.6966 407.8526 126.3214 -5.6025 435.9829 441.5854 407.6284 127.9286 -5.6013 435.8654 441.4667 407.4218 129.5253 -5.6007 435.7470 441.3477 407.2264 131.1118 -5.6009 435.6276 441.2285 407.0512 132.7244 -5.6019 435.5073 441.1093 406.8823 134.3211 -5.6032 435.3833 440.9865 406.7279 135.9283 -5.6053 435.2515 440.8569 406.5834 137.5460 -5.6068 435.1167 440.7235 406.4616 139.1583 -5.6082 434.9794 440.5876 406.3429 140.7605 -5.6102 434.8509 440.4611 406.2360 142.3730 -5.6122 434.7172 440.3294 406.1477 143.9801 -5.6141 434.5793 440.1934 406.0637 145.5871 -5.6165 434.4389 440.0554 405.9845 147.1944 -5.6197 434.3006 439.9203 405.9012 148.8015 -5.6217 434.1637 439.7854 405.8301 150.4035 -5.6244 434.0321 439.6565 405.7611 152.0315 -5.6259 433.8929 439.5188 405.7048 153.6336 -5.6276 433.7604 439.3881 405.6527 155.2461 -5.6300 433.6145 439.2445 405.6020 156.8481 -5.6329 433.4717 439.1046 405.5491 158.4554 -5.6361 433.3318 438.9679 405.4891 160.0365 -5.6392 433.1976 438.8368 405.4271 161.6540 -5.6420 433.0577 438.6997 405.3611 163.2611 -5.6451 432.9182 438.5633 405.2925 164.8634 -5.6479 432.7844 438.4322 405.2271 166.4653 -5.6503 432.6425 438.2928 405.1479 168.0569 -5.6527 432.5003 438.1530 405.0670 169.6693 -5.6544 432.3531 438.0075 404.9814 171.2711 -5.6568 432.2157 437.8725 404.8823 172.8835 -5.6597 432.0817 437.7414 404.7894 174.5009 -5.6618 431.9515 437.6133 404.6814 176.1083 -5.6624 431.8220 437.4844 404.5644 177.7051 -5.6648 431.6823 437.3471 404.4410 179.3125 -5.6662 431.5424 437.2086 404.3038 180.9145 -5.6682 431.4081 437.0763 404.1586 182.5269 -5.6691 431.2728 436.9419 404.0056 184.1341 -5.6698 431.1295 436.7993 403.8385 185.7413 -5.6686 430.9858 436.6544 403.6740 187.3485 -5.6682 430.8515 436.5197 403.4931 188.9608 -5.6682 430.7151 436.3834 403.3066 190.5629 -5.6677 430.5629 436.2306 403.1109 192.1596 -5.6670 430.4215 436.0885 402.9068 193.7619 -5.6664 430.2767 435.9431 402.6945 195.3640 -5.6656 430.1343 435.7999 402.4692 196.9714 -5.6643 429.9948 435.6591 402.2382 198.5786 -5.6622 429.8617 435.5239 402.0089 200.1653 -5.6605 429.7204 435.3809 401.7743 201.7880 -5.6583 429.5744 435.2327 401.5239 203.3953 -5.6555 429.4392 435.0948 401.2735 205.0026 -5.6526 429.2918 434.9444 401.0117 206.6049 -5.6491 429.1471 434.7962 400.7475 208.2171 -5.6460 429.0038 434.6499 400.4760 209.8193 -5.6431 428.8613 434.5044 400.2026 211.4266 -5.6399 428.7099 434.3497 399.9235 213.0496 -5.6363 428.5638 434.2001 399.6420 214.6570 -5.6330 428.4186 434.0516 399.3557 216.2641 -5.6305 428.2667 433.8972 399.0668 217.8664 -5.6267 428.1140 433.7406 398.7806 219.4786 -5.6223 427.9637 433.5860 398.4947 221.0910 -5.6178 427.8122 433.4300 398.1999 222.6880 -5.6128 427.6589 433.2717 397.9142 224.3054 -5.6085 427.4956 433.1041 397.6204 225.9024 -5.6040 427.3321 432.9361 397.3296 227.4991 -5.5996 427.1704 432.7699 397.0421 229.1065 -5.5955 427.0015 432.5970 396.7500 230.7088 -5.5913 426.8392 432.4304 396.4613 232.3106 -5.5862 426.6843 432.2705 396.1768 233.9233 -5.5802 426.5232 432.1034 395.8929 235.5253 -5.5749 426.3697 431.9446 395.6113 237.1479 -5.5686 426.2077 431.7763 395.3343 238.7553 -5.5632 426.0404 431.6036 395.0520 240.3574 -5.5580 425.8773 431.4353 394.7718 241.9698 -5.5531 425.7193 431.2723 394.4994 243.5718 -5.5466 425.5483 431.0949 394.2314 245.1843 -5.5416 425.3774 430.9190 393.9765 246.7864 -5.5370 425.1990 430.7360 393.7268 248.4143 -5.5321 425.0248 430.5568 393.4719 250.0211 -5.5263 424.8508 430.3771 393.2283 251.6285 -5.5205 424.6750 430.1955 392.9789 253.2304 -5.5144 424.4973 430.0117 392.7369 254.8428 -5.5089 424.3185 429.8274 392.4990 256.4450 -5.5037 424.1384 429.6421 392.2716 258.0419 -5.4991 423.9545 429.4536 392.0527 259.6648 -5.4952 423.7688 429.2640 391.8349 261.2668 -5.4912 423.5782 429.0694 391.6244 262.8638 -5.4874 423.3884 428.8758 391.4192 264.4658 -5.4824 423.1982 428.6806 391.2127 266.0729 -5.4792 423.0046 428.4837 391.0095 267.6751 -5.4744 422.8162 428.2906 390.8196 269.2876 -5.4709 422.6360 428.1069 390.6328 270.8743 -5.4664 422.4507 427.9171 390.4485 272.4864 -5.4621 422.2625 427.7247 390.2646 274.1093 -5.4575 422.0752 427.5327 390.0916 275.7164 -5.4538 421.8939 427.3477 389.9248 277.3234 -5.4494 421.7028 427.1522 389.7497 278.9201 -5.4448 421.5073 426.9520 389.5818 280.5271 -5.4414 421.3186 426.7600 389.4142 282.1339 -5.4381 421.1317 426.5697 389.2507 283.7411 -5.4342 420.9415 426.3758 389.0885 285.3485 -5.4308 420.7467 426.1775 388.9285 286.9663 -5.4270 420.5564 425.9834 388.7717 288.5681 -5.4235 420.3634 425.7869 388.6112 290.1654 -5.4207 420.1719 425.5926 388.4586 291.7618 -5.4182 419.9903 425.4085 388.3026 293.3588 -5.4149 419.8016 425.2165 388.1516 294.9711 -5.4126 419.6039 425.0165 387.9901 296.5733 -5.4102 419.4077 424.8180 387.8288 298.1749 -5.4083 419.2205 424.6288 387.6703 299.7666 -5.4065 419.0373 424.4437 387.5086 301.3894 -5.4023 418.8477 424.2500 387.3428 302.9964 -5.3977 418.6535 424.0512 387.1748 304.6038 -5.3937 418.4616 423.8553 387.0093 306.2009 -5.3911 418.2685 423.6596 386.8478 307.8031 -5.3891 418.0854 423.4745 386.6864 309.4154 -5.3859 417.8942 423.2802 386.5191 311.0173 -5.3829 417.7037 423.0865 386.3514 312.6244 -5.3793 417.5128 422.8921 386.1823 314.2473 -5.3762 417.3248 422.7011 386.0082 315.8544 -5.3733 417.1378 422.5110 385.8307 317.4615 -5.3704 416.9506 422.3210 385.6534 319.0740 -5.3661 416.7586 422.1247 385.4692 320.6760 -5.3629 416.5675 421.9304 385.2751 322.2780 -5.3596 416.3779 421.7375 385.0972 323.8851 -5.3552 416.1850 421.5402 384.9040 325.4716 -5.3508 416.0036 421.3544 384.7038 327.0944 -5.3467 415.8190 421.1657 384.4975 328.7015 -5.3418 415.6307 420.9726 384.2915 330.3088 -5.3373 415.4328 420.7701 384.0842 331.9160 -5.3326 415.2316 420.5642 383.8771 333.5181 -5.3288 415.0392 420.3680 383.6722 335.1305 -5.3251 414.8539 420.1789 383.4594 336.7375 -5.3205 414.6636 419.9841 383.2456 338.3553 -5.3155 414.4747 419.7902 383.0192 339.9679 -5.3100 414.2882 419.5982 382.8020 341.5754 -5.3053 414.0969 419.4022 382.5841 343.1828 -5.2994 413.9102 419.2096 382.3655 344.7953 -5.2948 413.7213 419.0161 382.1355 346.3974 -5.2905 413.5407 418.8312 381.9067 348.0046 -5.2849 413.3569 418.6417 381.6773 349.6275 -5.2792 413.1707 418.4499 381.4568 351.2298 -5.2740 412.9871 418.2611 381.2299 352.8318 -5.2692 412.7940 418.0631 381.0045 354.4443 -5.2635 412.6055 417.8690 380.7673 356.0409 -5.2580 412.4186 417.6765 380.5312 357.6430 -5.2520 412.2246 417.4766 380.3010 359.2501 -5.2461 412.0297 417.2759 380.0715 360.8418 -5.2403 411.8411 417.0813 379.8428 362.4645 -5.2349 411.6551 416.8899 379.5999 364.0716 -5.2290 411.4693 416.6983 379.3633 365.6736 -5.2230 411.2804 416.5034 379.1292 367.2860 -5.2174 411.0920 416.3093 378.8887 368.8879 -5.2115 410.9076 416.1192 378.6555 370.4953 -5.2053 410.7173 415.9226 378.4179 372.1026 -5.1990 410.5194 415.7183 378.1836 373.7253 -5.1928 410.3198 415.5126 377.9476 375.3219 -5.1870 410.1279 415.3149 377.7133 376.9293 -5.1811 409.9350 415.1161 377.4775 378.5365 -5.1746 409.7448 414.9194 377.2445 380.1438 -5.1686 409.5492 414.7178 377.0126 381.7560 -5.1630 409.3558 414.5188 376.7828 383.3683 -5.1571 409.1640 414.3210 376.5515 384.9755 -5.1516 408.9683 414.1198 376.3264 386.5620 -5.1464 408.7705 413.9169 376.0980 388.1643 -5.1406 408.5763 413.7168 375.8715 389.7663 -5.1345 408.3763 413.5108 375.6405 391.3734 -5.1294 408.1780 413.3073 375.4178 392.9704 -5.1233 407.9796 413.1029 375.1988 394.5828 -5.1173 407.7793 412.8966 374.9763 396.1848 -5.1109 407.5774 412.6882 374.7532 397.7971 -5.1048 407.3777 412.4825 374.5279 399.3836 -5.0998 407.1679 412.2677 374.3152 400.9960 -5.0954 406.9604 412.0558 374.0963 402.6188 -5.0904 406.7684 411.8588 373.8805 404.2263 -5.0838 406.5694 411.6532 373.6668 405.8284 -5.0780 406.3731 411.4512 373.4518 407.4409 -5.0733 406.1653 411.2386 373.2356 409.0533 -5.0674 405.9613 411.0287 373.0214 410.6553 -5.0615 405.7579 410.8193 372.8069 412.2676 -5.0559 405.5544 410.6103 372.5949 413.8901 -5.0502 405.3511 410.4013 372.3767 415.4921 -5.0448 405.1548 410.1996 372.1631 417.0994 -5.0398 404.9520 409.9919 371.9449 418.6856 -5.0349 404.7545 409.7893 371.7329 420.2875 -5.0288 404.5530 409.5818 371.5276 421.8898 -5.0228 404.3504 409.3732 371.3285 423.4969 -5.0172 404.1487 409.1659 371.1263 425.1041 -5.0110 403.9425 408.9536 370.9210 426.7213 -5.0060 403.7404 408.7464 370.7231 428.3338 -4.9995 403.5392 408.5387 370.5319 429.9355 -4.9945 403.3359 408.3303 370.3404 431.5481 -4.9891 403.1288 408.1179 370.1549 433.1503 -4.9834 402.9246 407.9080 369.9645 434.7574 -4.9787 402.7264 407.7051 369.7717 436.3650 -4.9739 402.5227 407.4966 369.5882 437.9928 -4.9694 402.3140 407.2834 369.4091 439.5949 -4.9645 402.1116 407.0761 369.2271 441.2074 -4.9601 401.9098 406.8698 369.0352 442.8145 -4.9550 401.7089 406.6639 368.8450 444.4218 -4.9492 401.5060 406.4552 368.6606 446.0340 -4.9434 401.2987 406.2421 368.4761 447.6360 -4.9384 401.0968 406.0352 368.2930 449.2588 -4.9340 400.8823 405.8164 368.1026 450.8404 -4.9294 400.6742 405.6036 367.9184 452.4528 -4.9237 400.4706 405.3943 367.7289 454.0548 -4.9190 400.2653 405.1843 367.5350 455.6618 -4.9139 400.0572 404.9711 367.3471 457.2636 -4.9075 399.8521 404.7597 367.1578 458.8659 -4.9022 399.6494 404.5516 366.9747 460.4731 -4.8969 399.4496 404.3465 366.7881 462.0959 -4.8915 399.2562 404.1478 366.5945 463.7031 -4.8854 399.0537 403.9391 366.4038 465.3105 -4.8800 398.8608 403.7408 366.2153 466.9126 -4.8759 398.6611 403.5370 366.0264 468.5251 -4.8717 398.4594 403.3311 365.8322 470.1273 -4.8675 398.2607 403.1282 365.6345 471.7343 -4.8624 398.0627 402.9251 365.4319 473.3570 -4.8581 397.8554 402.7136 365.2266 474.9643 -4.8526 397.6512 402.5038 365.0260 476.5715 -4.8465 397.4535 402.3000 364.8206 478.1839 -4.8407 397.2541 402.0947 364.6132 479.7910 -4.8350 397.0556 401.8906 364.4084 481.3981 -4.8296 396.8529 401.6825 364.2004 482.9848 -4.8243 396.6576 401.4819 363.9913 484.5975 -4.8187 396.4681 401.2868 363.7842 486.2048 -4.8131 396.2692 401.0823 363.5732 487.8068 -4.8084 396.0734 400.8818 363.3595 489.3934 -4.8025 395.8707 400.6732 363.1469 491.0056 -4.7962 395.6698 400.4660 362.9376 492.6025 -4.7909 395.4694 400.2602 362.7284 494.2151 -4.7849 395.2587 400.0436 362.5099 495.8225 -4.7793 395.0534 399.8327 362.2998 497.4449 -4.7748 394.8491 399.6240 362.0799 499.0523 -4.7694 394.6444 399.4138 361.8645 500.6644 -4.7639 394.4454 399.2093 361.6454 502.2664 -4.7581 394.2497 399.0078 361.4248 503.8788 -4.7532 394.0478 398.8010 361.2042 505.4810 -4.7479 393.8405 398.5884 360.9887 507.0881 -4.7421 393.6297 398.3718 360.7648 508.7111 -4.7358 393.4318 398.1676 360.5397 510.3133 -4.7307 393.2303 397.9610 360.3182 511.9256 -4.7249 393.0257 397.7506 360.0963 513.5275 -4.7184 392.8222 397.5405 359.8759 515.1398 -4.7130 392.6154 397.3284 359.6436 516.7418 -4.7071 392.4090 397.1162 359.4243 518.3336 -4.6995 392.2072 396.9066 359.2011 519.9408 -4.6920 392.0063 396.6983 358.9787 521.5584 -4.6843 391.8064 396.4907 358.7677 523.1709 -4.6792 391.6010 396.2802 358.5578 524.7730 -4.6736 391.3960 396.0696 358.3411 526.3853 -4.6677 391.1948 395.8625 358.1182 527.9875 -4.6617 390.9897 395.6514 357.8983 529.5950 -4.6556 390.7831 395.4387 357.6839 531.2074 -4.6496 390.5734 395.2230 357.4725 532.8301 -4.6441 390.3654 395.0095 357.2588 534.4320 -4.6380 390.1712 394.8092 357.0406 536.0445 -4.6322 389.9714 394.6037 356.8241 537.6519 -4.6271 389.7705 394.3976 356.6072 539.2589 -4.6213 389.5747 394.1960 356.3865 540.8714 -4.6146 389.3792 393.9938 356.1765 542.4736 -4.6081 389.1799 393.7879 355.9650 544.0965 -4.6014 388.9780 393.5794 355.7480 545.6934 -4.5948 388.7810 393.3758 355.5365 547.3006 -4.5887 388.5780 393.1667 355.3185 548.9025 -4.5835 388.3754 392.9589 355.1041 550.5150 -4.5783 388.1703 392.7486 354.8953 552.1170 -4.5726 387.9857 392.5583 354.6815 553.7298 -4.5677 387.7823 392.3500 354.4731 555.3319 -4.5619 387.5815 392.1435 354.2628 556.9599 -4.5559 387.3744 391.9304 354.0482 558.5669 -4.5499 387.1711 391.7210 353.8416 560.1741 -4.5445 386.9753 391.5198 353.6401 561.7760 -4.5392 386.7737 391.3129 353.4317 563.3885 -4.5343 386.5718 391.1060 353.2304 564.9956 -4.5286 386.3674 390.8960 353.0297 566.6080 -4.5237 386.1620 390.6857 352.8255 568.2308 -4.5180 385.9509 390.4689 352.6161 569.8381 -4.5127 385.7507 390.2634 352.4052 571.4401 -4.5085 385.5459 390.0543 352.2002 573.0526 -4.5028 385.3399 389.8428 351.9932 574.6649 -4.4966 385.1301 389.6267 351.7895 576.2721 -4.4913 384.9172 389.4084 351.5860 577.8743 -4.4860 384.7141 389.2002 351.3812 579.4608 -4.4801 384.5130 388.9931 351.1774 581.0733 -4.4745 384.3024 388.7769 350.9796 582.6803 -4.4694 384.0975 388.5669 350.7734 584.2823 -4.4643 383.8847 388.3490 350.5726 585.8688 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