DTA measure 1olomlassu1 Date: 2026916:918 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.05 s Mass = 100.000 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1580 -5.6712 186.4394 192.1106 246.5833 1.9655 -5.6453 186.7149 192.3601 246.6728 2.7620 -5.6213 186.9242 192.5456 246.9827 3.5898 -5.6124 187.2010 192.8134 246.8800 4.3663 -5.5880 187.3698 192.9578 246.6701 5.1935 -5.5840 187.6653 193.2493 246.4108 5.9600 -5.5883 187.9169 193.5052 246.3217 6.7773 -5.5638 188.3661 193.9299 246.1935 7.5535 -5.5515 188.6229 194.1744 245.9585 8.3918 -5.5390 188.8660 194.4049 245.8207 9.1575 -5.5428 188.9973 194.5401 245.8517 10.0673 -5.5112 189.2257 194.7369 245.8046 10.8645 -5.5212 189.3568 194.8780 245.6925 11.7328 -5.4967 189.5668 195.0635 245.5890 12.4888 -5.4912 189.8056 195.2968 245.7567 13.3168 -5.4782 190.0111 195.4893 245.9740 14.0825 -5.4913 190.5250 196.0163 245.8995 14.9103 -5.4511 190.8132 196.2642 246.0968 15.7075 -5.4349 191.1045 196.5394 246.0369 16.4935 -5.4356 191.2474 196.6830 246.0112 17.3318 -5.4019 191.4198 196.8217 245.8638 18.0983 -5.3437 191.6559 196.9996 246.1399 18.9560 -5.2852 191.9216 197.2068 246.0023 19.7123 -5.2799 192.2480 197.5279 246.1261 20.5503 -5.2293 192.5548 197.7840 246.1583 21.3365 -5.1968 192.8799 198.0767 245.9003 22.1440 -5.2072 193.1702 198.3774 245.8401 22.9405 -5.2050 193.2242 198.4292 245.7748 23.7375 -5.1706 193.2301 198.4007 245.6238 24.5655 -5.1618 193.4301 198.5919 245.5788 25.3418 -5.1530 193.7673 198.9204 245.6448 26.1590 -5.1320 194.0513 199.1833 245.6534 26.9460 -5.0978 194.3878 199.4856 245.5289 27.7730 -5.1066 194.4815 199.5881 245.6699 28.5395 -5.1089 194.6806 199.7895 245.8381 29.3983 -5.1134 195.0992 200.2126 245.7820 30.1638 -5.0955 195.3664 200.4619 245.8945 31.0020 -5.0900 195.7020 200.7919 245.9602 31.7888 -5.0693 196.0404 201.1097 246.1065 32.5955 -5.0274 196.2540 201.2813 246.1651 33.3928 -4.9750 196.4495 201.4244 246.1157 34.1898 -4.9626 196.6232 201.5858 246.2211 35.0068 -4.9466 196.8279 201.7746 246.1767 35.7835 -4.9370 197.0992 202.0362 246.0770 36.6420 -4.9214 197.5073 202.4287 246.2635 37.3975 -4.8859 197.8262 202.7121 246.4454 38.2255 -4.8886 197.9037 202.7923 246.5169 39.0220 -4.8891 197.8713 202.7604 246.7027 39.8190 -4.9005 198.0483 202.9488 246.7632 40.6060 -4.8952 198.1834 203.0786 246.8512 41.4023 -4.8894 198.3387 203.2281 247.1118 42.2303 -4.8620 198.4878 203.3498 247.1460 42.9863 -4.8181 198.7174 203.5356 247.1354 43.8545 -4.7504 199.1579 203.9082 247.4199 44.6108 -4.7163 199.6196 204.3359 247.5186 45.4380 -4.7247 199.9892 204.7140 247.7798 46.2350 -4.7518 200.3842 205.1360 247.8904 47.0218 -4.7330 200.6602 205.3932 248.1466 47.8285 -4.7326 201.0612 205.7938 248.3381 48.6258 -4.6985 201.3204 206.0189 248.6557 49.4535 -4.6576 201.5629 206.2206 248.6815 50.2193 -4.6740 201.6624 206.3365 248.6741 51.0780 -4.6699 201.7777 206.4476 248.7674 51.8338 -4.6372 202.0870 206.7242 248.9482 52.6715 -4.6182 202.1885 206.8067 249.0549 53.4585 -4.6081 202.2431 206.8512 249.2219 54.2553 -4.5932 202.3713 206.9645 249.4035 55.0828 -4.5912 202.5773 207.1686 249.4844 55.8595 -4.5764 202.7615 207.3379 249.5269 56.7073 -4.5528 203.0271 207.5799 250.0195 57.4838 -4.5617 203.2286 207.7903 250.2626 58.3015 -4.5332 203.2605 207.7937 250.5848 59.1080 -4.5298 203.3844 207.9141 250.8711 59.8950 -4.5503 203.4800 208.0302 251.0604 60.7328 -4.5576 203.7421 208.2997 251.2432 61.4885 -4.5668 203.9279 208.4948 251.3883 62.3575 -4.5602 204.1002 208.6604 251.6178 63.1130 -4.5306 204.3727 208.9033 251.9144 63.9408 -4.5077 204.5604 209.0681 252.1055 64.7380 -4.4678 204.7535 209.2214 252.1822 65.5448 -4.4388 204.9570 209.3958 252.4285 66.3623 -4.4284 204.9731 209.4015 252.4710 67.1285 -4.3764 205.0739 209.4503 252.6659 67.9865 -4.3260 205.4484 209.7743 252.6651 68.7530 -4.3191 205.7196 210.0387 252.5471 69.5808 -4.3180 205.9617 210.2797 252.6800 70.3670 -4.3109 206.1749 210.4858 253.1086 71.1643 -4.2701 206.5099 210.7800 253.3061 71.9815 -4.2882 206.7686 211.0569 253.5914 72.7475 -4.2763 207.0290 211.3053 253.8035 73.5755 -4.2901 207.3838 211.6739 254.0034 74.3410 -4.2819 207.4454 211.7273 254.0823 75.1895 -4.2812 207.5711 211.8523 254.2926 75.9660 -4.2450 207.8212 212.0662 254.7741 76.7830 -4.2420 208.0234 212.2653 255.2154 77.5700 -4.2512 208.1835 212.4346 255.2788 78.3773 -4.2578 208.3826 212.6405 255.3623 79.1943 -4.2502 208.4432 212.6933 255.7209 79.9608 -4.2362 208.6997 212.9360 255.8796 80.7885 -4.2367 208.9501 213.1868 256.0073 81.5543 -4.2441 209.1684 213.4125 256.3658 82.4130 -4.2324 209.4846 213.7170 256.5120 83.1688 -4.2048 209.7325 213.9373 256.7873 84.0065 -4.1839 209.9100 214.0939 257.0883 84.7935 -4.2200 210.1203 214.3403 257.3462 85.5903 -4.2204 210.5594 214.7798 257.3688 86.4178 -4.2209 210.7438 214.9648 257.5106 87.1843 -4.2200 210.9724 215.1924 257.6618 88.0425 -4.1770 210.9927 215.1697 257.7386 88.7983 -4.1682 211.2373 215.4055 257.8787 89.6365 -4.1450 211.4268 215.5718 258.1116 90.4230 -4.1237 211.2871 215.4109 258.1724 91.2198 -4.1528 211.5121 215.6649 258.3867 92.0478 -4.1600 211.9578 216.1178 258.5381 92.8135 -4.1635 212.1709 216.3344 258.5365 93.6720 -4.1524 212.1312 216.2836 258.6378 94.4283 -4.1224 212.0215 216.1439 258.8062 95.2658 -4.1113 212.1856 216.2969 259.0174 96.0320 -4.1246 212.2447 216.3693 259.2603 96.8600 -4.1670 212.5856 216.7526 259.1327 97.6460 -4.1509 212.7290 216.8800 258.9943 98.4535 -4.0786 212.9372 217.0158 258.7499 99.2713 -4.1024 213.3771 217.4796 258.8784 100.0368 -4.0840 213.7160 217.8000 259.1070 100.8955 -4.0528 213.8274 217.8801 259.4107 101.6723 -4.0281 214.1072 218.1353 259.3371 102.4890 -4.0027 214.2946 218.2973 259.2856 103.2760 -3.9757 214.4571 218.4328 259.4631 104.0725 -3.9641 214.7050 218.6691 259.7129 104.9003 -3.9911 215.0258 219.0169 259.8460 105.6565 -4.0105 215.2269 219.2375 259.9855 106.4835 -4.0268 215.5689 219.5957 260.1759 107.2500 -4.0385 215.8106 219.8491 260.2155 108.0983 -4.0422 215.9689 220.0111 260.4618 108.8743 -4.0355 216.1031 220.1386 260.3777 109.6920 -4.0575 216.3975 220.4550 260.4778 110.4890 -4.0346 216.4250 220.4596 260.4208 111.2855 -4.0331 216.6006 220.6336 260.4991 112.1135 -4.0140 216.7251 220.7391 260.8291 112.8795 -3.9935 216.9748 220.9683 261.1201 113.6968 -3.9759 217.3455 221.3214 261.2998 114.4633 -3.9882 217.7763 221.7645 261.5065 115.3215 -4.0144 217.8647 221.8791 261.6079 116.0773 -3.9799 218.0743 222.0543 261.7224 116.9155 -3.9778 218.1556 222.1334 261.9535 117.7020 -3.9711 218.2193 222.1904 262.2106 118.5090 -3.9553 218.5571 222.5124 262.4016 119.3268 -3.9478 218.7612 222.7090 262.5499 120.1028 -3.9655 218.8876 222.8531 262.6474 120.9510 -3.9989 219.2643 223.2632 262.6704 121.7173 -4.0101 219.4594 223.4695 262.6341 122.5445 -3.9883 219.6414 223.6297 262.9301 123.3418 -3.9417 219.8878 223.8295 263.0468 124.1385 -3.9183 220.1711 224.0893 262.9744 124.9558 -3.8896 220.0465 223.9361 262.9222 125.7325 -3.9040 220.2935 224.1975 263.0863 126.5603 -3.8703 220.3662 224.2365 263.1804 127.3260 -3.8332 220.5141 224.3473 263.4011 128.1745 -3.8382 220.6440 224.4822 263.6877 128.9505 -3.8077 220.8535 224.6613 263.8006 129.7680 -3.8199 221.0816 224.9016 263.7469 130.5653 -3.8253 221.3565 225.1818 264.1030 131.3615 -3.8354 221.5819 225.4174 264.2862 132.1998 -3.8127 221.7178 225.5305 264.4929 132.9558 -3.8142 221.8119 225.6261 264.4509 133.8138 -3.8253 222.1514 225.9767 264.4354 134.5803 -3.8386 222.4024 226.2410 264.5009 135.3975 -3.8457 222.4744 226.3201 264.7241 136.1943 -3.8168 222.7201 226.5369 264.7938 136.9915 -3.8132 222.7245 226.5377 264.9752 137.8083 -3.8144 222.7004 226.5148 265.2933 138.5748 -3.8114 223.1130 226.9245 265.5459 139.4335 -3.7979 223.3672 227.1651 265.6034 140.1990 -3.7923 223.5006 227.2928 265.5759 141.0168 -3.7960 223.7455 227.5416 265.6621 141.8140 -3.7398 223.7020 227.4418 265.5829 142.6103 -3.7180 223.7773 227.4953 265.5646 143.4075 -3.7104 224.1854 227.8958 265.4707 144.1943 -3.7232 224.3492 228.0724 265.8035 145.0318 -3.6735 224.5514 228.2250 266.1167 145.7880 -3.6673 224.5951 228.2625 266.3028 146.6463 -3.6910 224.7066 228.3976 266.6635 147.4123 -3.6765 224.6918 228.3683 266.7262 148.2403 -3.6950 224.9099 228.6048 266.7319 149.0368 -3.6929 225.2287 228.9216 266.8893 149.8235 -3.6695 225.3880 229.0575 266.8566 150.6618 -3.6422 225.7684 229.4106 267.3312 151.4170 -3.6605 225.9632 229.6237 267.3930 152.2758 -3.6506 226.2564 229.9069 267.5595 153.0423 -3.6671 226.3089 229.9760 267.9580 153.8693 -3.6957 226.5758 230.2715 267.9811 154.6665 -3.7038 226.9133 230.6171 268.0611 155.4533 -3.6732 227.3153 230.9885 268.1388 156.2908 -3.6826 227.5968 231.2793 268.0721 157.0573 -3.6462 227.6691 231.3153 268.1333 157.9155 -3.6699 227.5522 231.2221 268.1766 158.6713 -3.6754 227.5774 231.2529 268.3548 159.5095 -3.6695 227.4750 231.1446 268.4284 160.2958 -3.6992 227.5859 231.2852 268.2760 161.0928 -3.7162 227.8468 231.5630 268.2406 161.9208 -3.7264 228.1627 231.8891 268.3029 162.6968 -3.7348 228.6854 232.4202 268.2897 163.5450 -3.7006 228.7147 232.4153 268.5479 164.3113 -3.6571 228.9727 232.6298 268.6756 165.1385 -3.6290 229.2710 232.9000 268.8756 165.9358 -3.6295 229.3032 232.9327 269.1436 166.7220 -3.6094 229.4105 233.0199 269.2563 167.5498 -3.5868 229.5148 233.1017 269.4176 168.3163 -3.5624 229.6152 233.1776 269.4300 169.1640 -3.5659 229.6011 233.1670 269.6072 169.9303 -3.5872 229.7398 233.3269 269.8987 170.7480 -3.5687 229.9823 233.5510 270.0557 171.5443 -3.5925 230.2027 233.7953 269.9573 172.3415 -3.5902 230.4243 234.0144 270.0987 173.1693 -3.6181 230.6595 234.2776 270.2406 173.9350 -3.6192 230.8440 234.4632 270.4060 174.7528 -3.5852 231.1016 234.6868 270.6061 175.5290 -3.5697 231.2815 234.8513 270.7152 176.3770 -3.5635 231.1029 234.6663 270.6848 177.1435 -3.5218 231.0518 234.5736 270.6702 177.9708 -3.5185 231.3940 234.9125 270.6986 178.7678 -3.5141 231.6518 235.1659 270.8257 179.5650 -3.5060 231.8065 235.3125 271.0372 180.3818 -3.4856 231.9409 235.4265 271.1375 181.1585 -3.4895 232.3669 235.8564 271.3689 182.0068 -3.4787 232.5959 236.0746 271.3642 182.7725 -3.4593 232.9264 236.3857 271.3176 183.6005 -3.4363 232.8998 236.3361 271.4585 184.3970 -3.4598 233.0699 236.5297 271.7150 185.1940 -3.4724 233.2295 236.7020 271.8536 186.0118 -3.4677 233.5012 236.9689 272.0270 186.7878 -3.4443 233.5663 237.0106 272.1357 187.6360 -3.4742 233.6852 237.1594 272.4752 188.3820 -3.4797 233.6098 237.0895 272.7037 189.2295 -3.5244 233.8420 237.3664 273.0774 190.0063 -3.5298 233.9613 237.4911 273.4601 190.8240 -3.5358 233.9541 237.4899 273.7631 191.6203 -3.5386 234.1785 237.7171 273.7779 192.4175 -3.4980 234.4755 237.9736 273.9008 193.2455 -3.4826 234.8513 238.3340 274.0689 194.0110 -3.4830 234.9260 238.4090 274.3381 194.8698 -3.4916 235.1554 238.6471 274.2756 195.6363 -3.4661 235.2765 238.7425 274.2846 196.4633 -3.4475 235.3497 238.7973 274.2996 197.2605 -3.4214 235.5417 238.9631 274.3487 198.0575 -3.4335 235.7412 239.1747 274.2378 198.8848 -3.4185 235.9896 239.4082 274.2121 199.6410 -3.4359 236.3008 239.7367 274.3987 200.4993 -3.4599 236.3565 239.8164 274.7053 201.2345 -3.4176 236.4775 239.8951 274.6953 202.0830 -3.4157 236.7318 240.1475 274.9792 202.8488 -3.4057 236.9668 240.3725 275.2296 203.6765 -3.4284 237.1817 240.6101 275.5948 204.4635 -3.4364 237.1623 240.5987 275.5947 205.2598 -3.4307 237.1754 240.6061 275.4953 206.0878 -3.4339 237.5437 240.9775 275.6986 206.8438 -3.4136 237.8131 241.2267 275.8968 207.7018 -3.3861 237.9100 241.2961 276.2488 208.4683 -3.3566 237.9646 241.3213 276.5904 209.2960 -3.3688 238.1027 241.4716 276.6240 210.0925 -3.3981 238.2887 241.6868 276.6858 210.8795 -3.4194 238.4398 241.8592 276.7142 211.6865 -3.4029 238.5338 241.9367 277.0229 212.4730 -3.3911 238.6463 242.0374 277.3208 213.3010 -3.4172 238.9316 242.3487 277.3794 214.0668 -3.4194 239.0917 242.5111 277.5458 214.9253 -3.4268 239.4703 242.8971 277.7248 215.6918 -3.4150 239.7166 243.1316 277.9755 216.5088 -3.3906 239.7359 243.1265 278.2619 217.3160 -3.3727 239.6764 243.0491 278.5999 218.1028 -3.3446 239.8020 243.1466 278.8190 218.9300 -3.3695 239.9685 243.3380 278.7180 219.7068 -3.3522 240.0248 243.3770 278.6926 220.5345 -3.3346 240.1473 243.4819 278.9929 221.3310 -3.3552 240.2437 243.5989 279.0769 222.1180 -3.3567 240.3697 243.7264 279.2016 222.9253 -3.3492 240.5523 243.9015 279.5237 223.7423 -3.3430 240.7272 244.0702 279.7033 224.5190 -3.3428 241.0407 244.3835 279.6410 225.3673 -3.3693 241.2770 244.6463 279.5592 226.1433 -3.3280 241.3530 244.6810 279.6904 226.9610 -3.3259 241.5308 244.8568 279.8732 227.7580 -3.3245 241.7309 245.0554 279.9051 228.5545 -3.3345 241.7498 245.0843 279.8311 229.3825 -3.3780 241.7670 245.1451 280.2279 230.1590 -3.4155 241.9840 245.3995 280.4797 230.9658 -3.4131 242.2886 245.7017 280.7797 231.7528 -3.3928 242.5322 245.9250 281.0218 232.5803 -3.3767 242.6738 246.0505 281.1241 233.3360 -3.3750 242.7667 246.1416 281.2765 234.1948 -3.3432 242.9816 246.3248 281.3800 234.9608 -3.3599 243.2749 246.6347 281.6582 235.7780 -3.3648 243.3868 246.7516 281.9427 236.5753 -3.3358 243.5901 246.9258 282.0328 237.3720 -3.3101 243.7549 247.0650 281.8873 238.1995 -3.2774 243.8956 247.1730 282.0030 238.9660 -3.2605 244.0614 247.3219 281.9098 239.8140 -3.3006 244.2473 247.5480 281.9423 240.5698 -3.3378 244.5975 247.9353 281.9929 241.4285 -3.3116 244.8930 248.2047 282.1346 242.1633 -3.2933 245.0571 248.3504 282.2824 243.0220 -3.2936 244.9863 248.2799 282.1363 243.7778 -3.2911 245.0594 248.3505 282.2843 244.6155 -3.2859 245.4566 248.7425 282.5704 245.4025 -3.2641 245.5890 248.8531 282.6443 246.1988 -3.2640 245.6033 248.8673 282.8149 247.0268 -3.2545 245.5996 248.8541 282.8735 247.7933 -3.2525 245.7331 248.9856 283.1396 248.6510 -3.2684 245.8991 249.1675 283.4696 249.4073 -3.2602 245.8648 249.1250 283.4252 250.2453 -3.2610 246.0956 249.3565 283.5219 251.0008 -3.2805 246.6263 249.9068 283.7780 251.8595 -3.2823 246.9702 250.2525 283.8252 252.6255 -3.2812 247.0501 250.3313 283.9297 253.4530 -3.2556 247.1132 250.3689 284.0546 254.2708 -3.2777 247.2365 250.5142 284.1362 255.0470 -3.2750 247.2883 250.5633 284.3516 255.8745 -3.2542 247.4746 250.7289 284.3190 256.6410 -3.2503 247.6160 250.8663 284.7486 257.4885 -3.2593 247.7996 251.0589 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