DTA measure 1olomleglassabb1 Date: 2026916:107 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1230.69 s Mass = 100.000 mg data_number = 1525 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3250 0.6316 253.7724 253.1408 252.8680 2.1733 0.6309 253.8698 253.2389 252.8197 2.9493 0.6338 253.8966 253.2628 252.9175 3.7670 0.6166 253.8794 253.2628 252.9930 4.5640 0.5926 253.8447 253.2521 252.9802 5.3605 0.5881 253.6923 253.1042 252.8968 6.1885 0.6003 253.7107 253.1104 252.8748 6.9545 0.5965 253.6601 253.0635 252.9622 7.8025 0.5731 253.6174 253.0443 252.9067 8.5485 0.5695 253.5819 253.0124 252.8997 9.3963 0.5720 253.5639 252.9919 252.9190 10.1933 0.5591 253.6095 253.0504 252.9673 10.9905 0.5628 253.6663 253.1035 252.9363 11.8178 0.5600 253.7039 253.1440 252.9442 12.5840 0.5540 253.7354 253.1815 252.8198 13.4325 0.5344 253.6549 253.1205 252.7099 14.2083 0.5146 253.5815 253.0669 252.7261 15.0363 0.5117 253.7054 253.1937 252.7417 15.8333 0.5027 253.6730 253.1703 252.6555 16.6195 0.4999 253.6615 253.1616 252.6637 17.4270 0.5038 253.6667 253.1629 252.5784 18.2135 0.5036 253.6054 253.1018 252.5594 19.0410 0.5015 253.5906 253.0892 252.5292 19.8075 0.4883 253.5970 253.1087 252.5823 20.6658 0.4916 253.6389 253.1473 252.6188 21.4318 0.4886 253.5466 253.0581 252.7022 22.2495 0.4758 253.5845 253.1087 252.7198 23.0873 0.4719 253.5617 253.0897 252.6304 23.8430 0.4583 253.4904 253.0321 252.5790 24.7018 0.4562 253.3861 252.9298 252.5983 25.4678 0.4599 253.2767 252.8168 252.5930 26.2953 0.4460 253.3518 252.9058 252.6131 27.0515 0.4425 253.4523 253.0099 252.6392 27.8788 0.4435 253.3973 252.9537 252.6038 28.6758 0.4531 253.3939 252.9408 252.5443 29.4628 0.4382 253.3776 252.9395 252.5055 30.2898 0.4327 253.3694 252.9367 252.4682 31.0563 0.4287 253.3439 252.9152 252.4971 31.9150 0.4297 253.3570 252.9273 252.5602 32.6703 0.4309 253.3869 252.9559 252.5614 33.5085 0.4291 253.3119 252.8828 252.5518 34.2648 0.4173 253.3469 252.9296 252.4199 35.0815 0.4151 253.3751 252.9600 252.4332 35.8890 0.4100 253.5425 253.1325 252.4428 36.6760 0.4095 253.5174 253.1080 252.4457 37.5030 0.4021 253.4623 253.0602 252.4192 38.2695 0.3992 253.4899 253.0907 252.4750 39.1278 0.3717 253.4277 253.0560 252.5894 39.8938 0.3613 253.3951 253.0338 252.6061 40.7115 0.3653 253.3974 253.0321 252.6145 41.5185 0.3793 253.3688 252.9895 252.6026 42.3050 0.3854 253.2711 252.8857 252.5379 43.1330 0.3886 253.2525 252.8639 252.5774 43.8990 0.3807 253.3067 252.9261 252.6178 44.7573 0.3766 253.3588 252.9822 252.7754 45.5238 0.3713 253.3580 252.9868 252.8689 46.3405 0.3714 253.4702 253.0988 252.9424 47.1480 0.3685 253.4886 253.1201 252.9417 47.9350 0.3668 253.4450 253.0782 252.9563 48.7620 0.3690 253.4399 253.0709 252.9713 49.5388 0.3689 253.4422 253.0733 253.0258 50.3668 0.3521 253.4604 253.1083 253.1116 51.1323 0.3388 253.3863 253.0474 253.1413 51.9910 0.3320 253.3699 253.0379 253.2620 52.7473 0.3177 253.3548 253.0371 253.3274 53.5848 0.3013 253.4052 253.1039 253.3575 54.3818 0.3056 253.3788 253.0732 253.4129 55.1783 0.3072 253.3221 253.0149 253.4655 55.9958 0.2950 253.3083 253.0133 253.4302 56.7725 0.2859 253.1457 252.8598 253.4535 57.6000 0.2792 252.9382 252.6590 253.5061 58.3660 0.2574 252.8591 252.6017 253.5586 59.2145 0.2485 252.8785 252.6300 253.6446 59.9703 0.2489 252.9851 252.7362 253.7419 60.7875 0.2439 252.9729 252.7289 253.8694 61.5848 0.2421 252.8666 252.6245 254.0318 62.3815 0.2402 252.9443 252.7041 254.2483 63.1988 0.2443 253.0438 252.7995 254.3624 63.9653 0.2477 253.1197 252.8720 254.4141 64.8235 0.2530 253.2028 252.9498 254.5237 65.5793 0.2439 253.1749 252.9310 254.6216 66.4073 0.2477 253.2429 252.9952 254.7057 67.2040 0.2602 253.2681 253.0079 254.8341 67.9905 0.2594 253.3038 253.0444 254.9720 68.8288 0.2366 253.3379 253.1012 255.1295 69.5943 0.2268 253.2592 253.0324 255.2005 70.3915 0.2381 253.2261 252.9879 255.2665 71.2193 0.2245 253.2801 253.0556 255.3121 72.0158 0.2111 253.2358 253.0247 255.3588 72.8130 0.1905 253.2423 253.0518 255.4247 73.6303 0.1857 253.3199 253.1341 255.5850 74.4065 0.1764 253.3873 253.2109 255.6991 75.2550 0.1576 253.4439 253.2862 255.8054 76.0210 0.1653 253.4567 253.2914 255.8849 76.8485 0.1755 253.5351 253.3596 255.9479 77.6458 0.1776 253.5231 253.3455 256.0529 78.4423 0.1822 253.4311 253.2489 256.2457 79.2598 0.1786 253.3838 253.2052 256.3457 80.0365 0.1835 253.3734 253.1899 256.4584 80.8845 0.1578 253.4721 253.3144 256.6372 81.6608 0.1579 253.4129 253.2550 256.7786 82.4785 0.1492 253.4265 253.2773 256.9546 83.2855 0.1472 253.4105 253.2633 257.0956 84.0720 0.1470 253.2775 253.1305 257.2216 84.9000 0.1340 253.2702 253.1362 257.3222 85.6658 0.1244 253.2525 253.1281 257.3783 86.5243 0.1111 253.2427 253.1316 257.5344 87.2908 0.0970 253.2666 253.1697 257.6788 88.1075 0.0893 253.3223 253.2331 257.7330 88.9150 0.0899 253.3017 253.2118 257.8056 89.7018 0.0829 253.2727 253.1898 257.9365 90.5290 0.0752 253.3447 253.2695 258.0776 91.2955 0.0663 253.3970 253.3307 258.2930 92.1540 0.0515 253.3675 253.3160 258.4603 92.9198 0.0385 253.3237 253.2852 258.5315 93.7375 0.0242 253.3659 253.3417 258.6381 94.5445 0.0132 253.4186 253.4054 258.7961 95.3310 0.0078 253.4420 253.4342 258.9200 96.1283 0.0116 253.4172 253.4055 259.0146 96.9248 0.0036 253.3689 253.3653 259.1444 97.7525 -0.0031 253.5264 253.5295 259.2365 98.5190 -0.0056 253.4983 253.5039 259.2629 99.3665 -0.0072 253.4106 253.4178 259.4267 100.1433 -0.0010 253.4268 253.4277 259.5105 100.9608 -0.0053 253.5336 253.5389 259.6381 101.7573 -0.0145 253.5528 253.5673 259.7212 102.5545 -0.0209 253.6855 253.7064 259.8495 103.3820 -0.0523 253.6705 253.7228 259.9500 104.1480 -0.0741 253.6668 253.7409 260.0695 104.9965 -0.0834 253.6519 253.7353 260.1466 105.7728 -0.0799 253.6003 253.6802 260.2119 106.5900 -0.0876 253.5984 253.6860 260.3441 107.3565 -0.0977 253.6281 253.7258 260.4774 108.1838 -0.1112 253.6412 253.7524 260.5064 108.9808 -0.1118 253.7357 253.8475 260.5933 109.7780 -0.1087 253.7735 253.8821 260.6980 110.5948 -0.1322 253.6907 253.8229 260.7946 111.3715 -0.1434 253.6138 253.7572 260.9107 112.2198 -0.1199 253.6935 253.8134 261.1480 112.9855 -0.1173 253.6731 253.7904 261.2675 113.8135 -0.1354 253.6709 253.8063 261.3974 114.6103 -0.1400 253.7285 253.8684 261.4830 115.4070 -0.1480 253.8699 254.0179 261.6514 116.2248 -0.1631 253.9413 254.1044 261.6866 117.0010 -0.1706 253.9541 254.1247 261.6429 117.8490 -0.1612 253.9293 254.0905 261.8070 118.6258 -0.1602 253.9077 254.0679 261.9392 119.4430 -0.1700 254.1061 254.2761 262.0678 120.2500 -0.1862 254.0593 254.2454 262.1405 121.0473 -0.1999 254.0220 254.2218 262.1764 121.8540 -0.2078 254.1008 254.3086 262.3058 122.6510 -0.2112 254.2053 254.4165 262.4443 123.4688 -0.2333 254.2937 254.5271 262.5140 124.2445 -0.2454 254.3176 254.5630 262.6308 125.0930 -0.2466 254.2068 254.4534 262.6491 125.8595 -0.2500 254.2017 254.4517 262.8069 126.6868 -0.2477 254.2069 254.4546 262.7997 127.4838 -0.2418 254.2137 254.4555 262.9205 128.2810 -0.2473 254.2169 254.4642 262.9514 129.0773 -0.2736 254.2847 254.5583 263.0003 129.8745 -0.2837 254.3604 254.6441 263.1402 130.7123 -0.2660 254.3786 254.6446 263.3635 131.4783 -0.2566 254.4227 254.6793 263.3794 132.3165 -0.2466 254.3489 254.5956 263.4386 133.0823 -0.2479 254.3918 254.6397 263.5563 133.9305 -0.2488 254.4340 254.6828 263.5596 134.7073 -0.2546 254.4541 254.7087 263.6702 135.5240 -0.2889 254.4182 254.7071 263.6863 136.3213 -0.3067 254.4329 254.7396 263.8899 137.1183 -0.3139 254.4482 254.7621 264.0357 137.9455 -0.3384 254.5502 254.8886 264.0868 138.7120 -0.3536 254.4702 254.8238 263.9946 139.5600 -0.3526 254.4651 254.8177 264.0851 140.3363 -0.3636 254.4899 254.8535 264.1345 141.1643 -0.3651 254.5203 254.8854 264.1991 141.9403 -0.3728 254.5150 254.8878 264.2693 142.7885 -0.3691 254.4728 254.8419 264.4456 143.5653 -0.3749 254.6293 255.0042 264.5186 144.3823 -0.3854 254.7434 255.1288 264.7554 145.1793 -0.3935 254.7660 255.1595 264.8433 145.9763 -0.3958 254.7586 255.1544 264.9894 146.8035 -0.4012 254.7397 255.1409 265.0160 147.5700 -0.4209 254.8293 255.2502 264.9836 148.4285 -0.4499 254.9572 255.4071 265.0686 149.1635 -0.4649 255.0073 255.4722 265.2380 150.0223 -0.4671 255.0366 255.5037 265.3438 150.7883 -0.4750 255.0312 255.5062 265.4196 151.6055 -0.4760 254.9625 255.4385 265.4162 152.4130 -0.4832 254.8731 255.3563 265.5471 153.1993 -0.4987 254.8177 255.3164 265.6225 154.0578 -0.5094 254.8017 255.3111 265.7475 154.7935 -0.5141 254.8753 255.3894 265.8343 155.6415 -0.5058 255.0629 255.5688 266.0041 156.4075 -0.5114 255.2256 255.7370 265.9858 157.2355 -0.5291 255.2330 255.7620 266.0598 158.0220 -0.5226 255.3741 255.8967 266.0958 158.8085 -0.5090 255.5691 256.0781 266.0827 159.6468 -0.5074 255.6395 256.1468 266.1958 160.4025 -0.5105 255.6232 256.1338 266.2863 161.2505 -0.5196 255.6985 256.2181 266.4495 161.9965 -0.5188 255.6788 256.1976 266.4812 162.8443 -0.5283 255.7639 256.2922 266.6679 163.6105 -0.5384 255.8681 256.4065 266.7559 164.4383 -0.5339 255.9590 256.4929 266.9065 165.2245 -0.5384 255.9165 256.4549 266.9497 166.0218 -0.5435 255.8525 256.3960 267.0384 166.8493 -0.5636 255.8804 256.4440 267.0852 167.6050 -0.5658 255.9635 256.5293 267.0520 168.4638 -0.5773 256.0019 256.5792 267.2569 169.2298 -0.5792 255.9823 256.5616 267.5487 170.0573 -0.5833 256.0600 256.6433 267.6718 170.8238 -0.5886 256.1232 256.7118 267.7822 171.6408 -0.5936 256.1427 256.7363 267.7516 172.4480 -0.6065 256.1304 256.7369 267.7588 173.2348 -0.6113 256.0765 256.6879 267.8887 174.0620 -0.6175 255.9955 256.6130 267.9311 174.8285 -0.6239 256.1384 256.7623 267.9459 175.6768 -0.6055 256.1961 256.8016 268.0604 176.4425 -0.6315 256.0768 256.7083 268.1910 177.2705 -0.6314 256.2057 256.8371 268.3353 178.0673 -0.6310 256.2037 256.8346 268.4523 178.8640 -0.6400 256.1864 256.8264 268.6088 179.6818 -0.6599 256.3530 257.0128 268.7760 180.4578 -0.6777 256.4390 257.1166 268.9729 181.2855 -0.6686 256.5321 257.2007 269.0570 182.0415 -0.6828 256.5966 257.2793 269.2806 182.8995 -0.6882 256.6460 257.3342 269.3390 183.6660 -0.6965 256.6787 257.3752 269.3076 184.4938 -0.7008 256.7528 257.4536 269.3668 185.2800 -0.6959 256.7657 257.4616 269.5412 186.0875 -0.6939 256.7841 257.4781 269.5130 186.9050 -0.6994 256.8529 257.5523 269.4952 187.6810 -0.7067 256.9276 257.6343 269.6522 188.5295 -0.7177 256.9243 257.6420 269.7032 189.3055 -0.7165 257.0832 257.7997 269.7809 190.1230 -0.7334 257.1365 257.8699 269.9830 190.9203 -0.7400 257.1209 257.8610 270.1380 191.7168 -0.7471 257.1359 257.8830 270.2424 192.5240 -0.7505 257.1603 257.9108 270.4122 193.3110 -0.7468 257.2694 258.0162 270.6237 194.1380 -0.7533 257.2083 257.9617 270.7921 194.9045 -0.7555 257.2652 258.0207 270.8835 195.7633 -0.7575 257.3189 258.0764 270.8919 196.5288 -0.7551 257.3941 258.1492 270.9801 197.3465 -0.7712 257.5531 258.3244 271.0266 198.1540 -0.7714 257.5769 258.3483 271.0908 198.9400 -0.7611 257.5251 258.2862 271.2290 199.7680 -0.7744 257.6989 258.4733 271.3514 200.5345 -0.7751 257.7949 258.5700 271.4082 201.3923 -0.7794 257.8676 258.6470 271.4257 202.1588 -0.7881 257.9833 258.7714 271.5232 202.9763 -0.7826 258.1026 258.8852 271.6522 203.7830 -0.7707 258.1142 258.8849 271.8543 204.5700 -0.7749 258.1348 258.9098 271.9425 205.3980 -0.7884 258.1231 258.9115 272.0461 206.1635 -0.8013 258.1484 258.9497 272.1497 207.0223 -0.8155 258.2309 259.0464 272.3109 207.7885 -0.8275 258.1762 259.0037 272.4367 208.6055 -0.8267 258.1463 258.9730 272.5239 209.4130 -0.8529 258.1889 259.0418 272.4647 210.2098 -0.8518 258.2510 259.1028 272.6598 211.0373 -0.8453 258.2431 259.0883 272.7277 211.7935 -0.8505 258.2944 259.1450 272.7016 212.6620 -0.8577 258.3748 259.2325 272.7035 213.4178 -0.8568 258.4310 259.2878 272.7504 214.2560 -0.8598 258.5766 259.4364 272.9755 215.0425 -0.8724 258.6622 259.5346 273.1656 215.8495 -0.8630 258.6378 259.5008 273.4267 216.6673 -0.8728 258.6528 259.5255 273.4512 217.4330 -0.8807 258.7372 259.6179 273.5998 218.2915 -0.8884 258.8853 259.7737 273.6853 219.0580 -0.8957 258.9102 259.8060 273.6896 219.8648 -0.9019 258.9987 259.9006 273.7589 220.6413 -0.9049 258.9604 259.8653 273.8260 221.4590 -0.9108 258.9443 259.8551 273.9662 222.2450 -0.9153 259.0924 260.0077 274.0322 223.0423 -0.9097 259.1295 260.0392 274.1419 223.8700 -0.9042 259.1263 260.0305 274.2026 224.6255 -0.9059 259.1091 260.0150 274.2357 225.4843 -0.9221 259.2807 260.2028 274.3036 226.2400 -0.9272 259.4977 260.4249 274.4329 227.0675 -0.9484 259.5362 260.4845 274.7028 227.8648 -0.9716 259.6275 260.5990 274.8258 228.6615 -0.9773 259.6050 260.5823 274.9776 229.4480 -0.9949 259.6423 260.6372 275.0878 230.2453 -1.0051 259.7099 260.7150 275.0232 231.0728 -1.0234 259.8083 260.8317 275.0937 231.8285 -1.0388 259.9101 260.9489 275.1902 232.6975 -1.0384 259.8520 260.8905 275.4292 233.4530 -1.0420 259.9934 261.0354 275.5488 234.2910 -1.0501 260.0093 261.0594 275.5676 235.0780 -1.0448 260.0919 261.1367 275.6058 235.8743 -1.0485 260.1664 261.2148 275.6092 236.6715 -1.0542 260.1920 261.2462 275.7304 237.4585 -1.0572 260.2907 261.3479 275.7956 238.2958 -1.0584 260.3824 261.4408 275.9264 239.0520 -1.0689 260.5155 261.5844 275.9488 239.9105 -1.0645 260.5499 261.6143 276.0410 240.6763 -1.0779 260.4502 261.5281 276.2367 241.5043 -1.0663 260.4940 261.5604 276.3256 242.3013 -1.0543 260.5616 261.6160 276.5767 243.0875 -1.0317 260.6585 261.6902 276.7362 243.9258 -1.0291 260.6635 261.6926 276.8589 244.6818 -1.0294 260.8511 261.8806 277.0575 245.5398 -1.0455 260.9710 262.0165 277.1607 246.2755 -1.0654 261.0208 262.0862 277.2188 247.1440 -1.0577 260.9721 262.0298 277.3525 247.8998 -1.0631 261.0969 262.1600 277.5428 248.7278 -1.0661 261.2558 262.3220 277.6215 249.5245 -1.0715 261.3052 262.3767 277.7473 250.3213 -1.0866 261.4518 262.5383 277.8054 251.1493 -1.0985 261.4537 262.5522 277.9071 251.9048 -1.1132 261.4218 262.5351 278.0056 252.7735 -1.1237 261.4134 262.5371 278.0975 253.5298 -1.1259 261.5208 262.6468 278.1592 254.3570 -1.1327 261.6442 262.7769 278.3627 255.1540 -1.1378 261.6829 262.8206 278.5144 255.9513 -1.1380 261.7530 262.8910 278.5563 256.7785 -1.1417 261.8616 263.0032 278.5807 257.5345 -1.1378 261.8476 262.9855 278.7288 258.4035 -1.1278 261.8366 262.9644 278.8390 259.1588 -1.1304 261.8522 262.9826 279.0247 259.9868 -1.1239 261.8823 263.0062 279.0693 260.7840 -1.1228 261.8842 263.0069 279.0388 261.5803 -1.1422 261.9829 263.1251 279.2985 262.4083 -1.1343 262.0075 263.1418 279.4276 263.1645 -1.1442 262.0402 263.1844 279.5086 264.0328 -1.1694 262.1717 263.3411 279.6033 264.7888 -1.1733 262.3392 263.5125 279.7307 265.6168 -1.1875 262.4123 263.5998 279.8776 266.4133 -1.2037 262.4865 263.6903 280.0301 267.2103 -1.1978 262.5926 263.7903 280.1040 268.0383 -1.2036 262.6636 263.8671 280.1575 268.7938 -1.2009 262.7435 263.9443 280.3410 269.6625 -1.2155 262.7739 263.9894 280.4924 270.3880 -1.2101 262.8673 264.0774 280.4402 271.2563 -1.2124 263.0106 264.2230 280.5683 272.0123 -1.2302 263.1194 264.3496 280.5344 272.8503 -1.2343 263.2384 264.4728 280.6474 273.6365 -1.2291 263.3293 264.5584 280.8329 274.4440 -1.2197 263.2941 264.5138 281.0155 275.2513 -1.2306 263.4004 264.6310 281.0565 276.0375 -1.2426 263.5075 264.7501 281.1179 276.8758 -1.2601 263.5762 264.8363 281.2725 277.6313 -1.2705 263.5636 264.8341 281.2154 278.5000 -1.2560 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