DTA measure 1faziselso Date: 2024924:1054 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 927.98 s Mass = 953.800 mg data_number = 1155 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0465 0.2859 223.2995 223.0136 265.7483 1.8685 0.2904 223.5646 223.2741 265.7547 2.6605 0.2920 223.8279 223.5358 265.7689 3.4525 0.2952 224.1010 223.8058 265.7860 4.3050 0.2995 224.3683 224.0687 265.8052 5.0670 0.3021 224.6324 224.3303 265.8292 5.8895 0.3046 224.9033 224.5987 265.8656 6.6810 0.3058 225.1386 224.8328 265.8784 7.4725 0.3082 225.4083 225.1001 265.9075 8.3248 0.3094 225.6972 225.3878 265.9251 9.0865 0.3138 225.9322 225.6184 265.9689 9.9088 0.3144 226.1954 225.8810 266.0075 10.7008 0.3163 226.4537 226.1374 266.0792 11.4925 0.3181 226.7165 226.3984 266.1360 12.3448 0.3191 226.9841 226.6650 266.2284 13.1065 0.3205 227.2343 226.9138 266.3259 13.9295 0.3232 227.4986 227.1754 266.4178 14.7218 0.3252 227.7372 227.4120 266.4915 15.5135 0.3289 227.9897 227.6607 266.5975 16.3655 0.3289 228.2588 227.9300 266.7441 17.1275 0.3302 228.5188 228.1886 266.8455 17.9495 0.3327 228.7751 228.4424 266.9803 18.7415 0.3321 229.0157 228.6836 267.1117 19.5335 0.3336 229.2700 228.9364 267.2322 20.3860 0.3358 229.5166 229.1808 267.4023 21.1485 0.3359 229.7569 229.4210 267.5391 21.9705 0.3364 230.0301 229.6937 267.7125 22.7625 0.3377 230.2678 229.9300 267.8523 23.5545 0.3382 230.5152 230.1770 268.0120 24.4065 0.3389 230.7519 230.4130 268.1821 25.1685 0.3372 230.9898 230.6526 268.3403 25.9903 0.3385 231.2471 230.9086 268.5179 26.8125 0.3388 231.5089 231.1700 268.6891 27.5745 0.3384 231.7482 231.4098 268.8708 28.4270 0.3356 231.9927 231.6571 269.0539 29.1888 0.3362 232.2173 231.8810 269.2032 30.0108 0.3368 232.4757 232.1388 269.3707 30.8028 0.3351 232.7083 232.3733 269.5242 31.5945 0.3341 232.9503 232.6162 269.6969 32.4468 0.3345 233.2123 232.8777 269.8693 33.2085 0.3351 233.4331 233.0980 270.0231 34.0315 0.3320 233.6773 233.3453 270.1737 34.8238 0.3286 233.9129 233.5843 270.3341 35.6163 0.3264 234.1356 233.8092 270.4943 36.4650 0.3255 234.3861 234.0606 270.6621 37.2230 0.3269 234.6026 234.2757 270.7844 38.0410 0.3269 234.8482 234.5213 270.9237 38.8298 0.3225 235.0856 234.7632 271.0819 39.6265 0.3188 235.3296 235.0108 271.2247 40.4373 0.3211 235.5791 235.2579 271.3683 41.2260 0.3199 235.8239 235.5040 271.5013 42.0445 0.3189 236.0473 235.7285 271.6353 42.8030 0.3181 236.2642 235.9461 271.7561 43.6515 0.3159 236.5048 236.1889 271.8960 44.4100 0.3137 236.7284 236.4147 272.0107 45.2288 0.3138 236.9597 236.6459 272.1659 46.0475 0.3087 237.1872 236.8784 272.2845 46.8070 0.3053 237.4177 237.1125 272.3926 47.6565 0.3037 237.6553 237.3515 272.5422 48.4173 0.3025 237.8805 237.5779 272.6698 49.2378 0.3009 238.1108 237.8099 272.8011 50.0563 0.2976 238.3459 238.0483 272.9226 50.8155 0.2938 238.5576 238.2638 273.0528 51.6665 0.2895 238.8027 238.5132 273.1942 52.4280 0.2888 239.0179 238.7290 273.2945 53.2485 0.2837 239.2402 238.9565 273.4242 54.0405 0.2833 239.4594 239.1761 273.5619 54.8325 0.2835 239.6839 239.4004 273.6820 55.6845 0.2779 239.9162 239.6384 273.8022 56.4465 0.2766 240.1419 239.8654 273.9217 57.2685 0.2738 240.3677 240.0939 274.0565 58.0605 0.2637 240.5803 240.3167 274.1979 58.8525 0.2602 240.8052 240.5449 274.3253 59.6745 0.2594 241.0137 240.7543 274.4462 60.4665 0.2569 241.2447 240.9877 274.5656 61.2883 0.2534 241.4821 241.2287 274.6845 62.0805 0.2498 241.7004 241.4506 274.8115 62.8723 0.2476 241.9145 241.6669 274.9282 63.6943 0.2447 242.1264 241.8818 275.0617 64.4555 0.2394 242.3312 242.0918 275.1790 65.3080 0.2357 242.5875 242.3518 275.3156 66.0998 0.2334 242.8027 242.5693 275.4424 66.8915 0.2304 243.0103 242.7799 275.5607 67.7138 0.2260 243.2372 243.0113 275.6750 68.4755 0.2217 243.4351 243.2134 275.7961 69.3278 0.2175 243.6778 243.4603 275.9324 70.1198 0.2107 243.8867 243.6760 276.0534 70.9115 0.2090 244.1018 243.8928 276.1604 71.7338 0.2066 244.3147 244.1081 276.2888 72.4955 0.2011 244.5225 244.3214 276.4072 73.3478 0.1985 244.7540 244.5555 276.5413 74.1398 0.1936 244.9634 244.7699 276.6625 74.9315 0.1901 245.1808 244.9907 276.8007 75.7538 0.1873 245.3848 245.1975 276.9309 76.5155 0.1825 245.5927 245.4101 277.0537 77.3683 0.1793 245.8218 245.6425 277.1950 78.1605 0.1728 246.0214 245.8486 277.3294 78.9525 0.1688 246.2302 246.0614 277.4505 79.7748 0.1642 246.4494 246.2852 277.5901 80.5375 0.1610 246.6629 246.5019 277.7382 81.3895 0.1598 246.8845 246.7247 277.8813 82.1815 0.1573 247.1067 246.9494 278.0155 82.9735 0.1508 247.2980 247.1472 278.1575 83.7955 0.1434 247.5063 247.3629 278.3114 84.5573 0.1389 247.7118 247.5729 278.4392 85.4093 0.1353 247.9286 247.7933 278.5927 86.2013 0.1319 248.1269 247.9950 278.7387 86.9925 0.1279 248.3373 248.2095 278.8727 87.8150 0.1230 248.5411 248.4180 279.0265 88.6065 0.1176 248.7548 248.6372 279.1598 89.4295 0.1140 248.9826 248.8686 279.3131 90.2218 0.1115 249.1752 249.0637 279.4440 91.0318 0.1069 249.3619 249.2551 279.5933 91.8135 0.1029 249.5620 249.4591 279.7404 92.6358 0.0988 249.7743 249.6755 279.8817 93.4580 0.0923 249.9856 249.8933 280.0275 94.2205 0.0863 250.1955 250.1092 280.1551 95.0728 0.0811 250.4197 250.3385 280.3191 95.8345 0.0775 250.5951 250.5175 280.4599 96.6568 0.0725 250.8153 250.7428 280.6112 97.4785 0.0697 251.0235 250.9538 280.7266 98.2405 0.0662 251.2115 251.1454 280.8524 99.0933 0.0612 251.4354 251.3742 280.9916 99.8855 0.0524 251.6357 251.5832 281.1247 100.6778 0.0465 251.8122 251.7656 281.2565 101.4970 0.0431 252.0246 251.9815 281.3851 102.2558 0.0389 252.2190 252.1801 281.5159 103.1040 0.0344 252.4396 252.4053 281.6491 103.8623 0.0319 252.6235 252.5916 281.7464 104.6820 0.0240 252.8292 252.8052 281.8728 105.5008 0.0198 253.0414 253.0215 281.9917 106.2600 0.0130 253.2186 253.2056 282.1000 107.1080 0.0091 253.4196 253.4105 282.2296 107.8960 0.0074 253.6191 253.6117 282.3749 108.6840 0.0001 253.8086 253.8085 282.4835 109.5023 -0.0044 253.9996 254.0041 282.6016 110.2610 -0.0093 254.2076 254.2169 282.7093 111.1103 -0.0119 254.4218 254.4337 282.8497 111.8990 -0.0181 254.5974 254.6155 282.9799 112.6885 -0.0269 254.7776 254.8045 283.1059 113.5078 -0.0288 254.9884 255.0172 283.2186 114.2980 -0.0339 255.1779 255.2117 283.3547 115.1175 -0.0419 255.3928 255.4347 283.4943 115.9085 -0.0487 255.5893 255.6380 283.6176 116.6988 -0.0539 255.7734 255.8274 283.7389 117.5485 -0.0550 255.9746 256.0297 283.8783 118.3095 -0.0610 256.1558 256.2169 284.0021 119.1308 -0.0689 256.3533 256.4222 284.1443 119.9225 -0.0733 256.5405 256.6138 284.2800 120.7140 -0.0772 256.7329 256.8101 284.4261 121.5663 -0.0820 256.9590 257.0410 284.5740 122.3278 -0.0876 257.1236 257.2113 284.6845 123.1500 -0.0917 257.3246 257.4163 284.8098 123.9420 -0.0989 257.5255 257.6244 284.9512 124.7335 -0.1036 257.7229 257.8265 285.1001 125.5558 -0.1050 257.8993 258.0043 285.2377 126.3475 -0.1099 258.0793 258.1891 285.3758 127.1698 -0.1162 258.2771 258.3933 285.5084 127.9618 -0.1192 258.4714 258.5907 285.6328 128.7535 -0.1236 258.6702 258.7938 285.7653 129.5758 -0.1298 258.8453 258.9751 285.9157 130.3675 -0.1347 259.0340 259.1687 286.0458 131.1898 -0.1419 259.2249 259.3669 286.1792 131.9815 -0.1473 259.4274 259.5747 286.3298 132.7735 -0.1494 259.6106 259.7601 286.4752 133.5958 -0.1586 259.7905 259.9491 286.5929 134.3575 -0.1628 259.9677 260.1304 286.7265 135.2098 -0.1675 260.1800 260.3474 286.8862 136.0015 -0.1749 260.3428 260.5177 287.0054 136.7935 -0.1784 260.5432 260.7216 287.1359 137.6155 -0.1807 260.7384 260.9191 287.2847 138.3775 -0.1856 260.9265 261.1121 287.4084 139.2295 -0.1929 261.1148 261.3077 287.5431 140.0215 -0.1985 261.2861 261.4845 287.6713 140.8135 -0.2059 261.4770 261.6829 287.8012 141.6355 -0.2092 261.6698 261.8790 287.9430 142.3973 -0.2115 261.8520 262.0635 288.0774 143.2493 -0.2169 262.0671 262.2840 288.2287 144.0415 -0.2228 262.2442 262.4670 288.3563 144.8330 -0.2295 262.4252 262.6547 288.5060 145.6553 -0.2335 262.5902 262.8238 288.6474 146.4165 -0.2370 262.7769 263.0139 288.7684 147.2690 -0.2426 262.9949 263.2375 288.9114 148.0608 -0.2489 263.1549 263.4038 289.0449 148.8525 -0.2543 263.3188 263.5731 289.1716 149.6748 -0.2591 263.5081 263.7672 289.3106 150.4365 -0.2642 263.6827 263.9469 289.4483 151.2888 -0.2709 263.8692 264.1401 289.5839 152.0808 -0.2761 264.0583 264.3343 289.7131 152.8725 -0.2807 264.2353 264.5160 289.8728 153.6948 -0.2864 264.4359 264.7223 290.0163 154.4565 -0.2917 264.6045 264.8962 290.1257 155.3088 -0.2974 264.8155 265.1128 290.2792 156.1008 -0.3019 264.9855 265.2874 290.4128 156.8925 -0.3053 265.1488 265.4540 290.5567 157.7150 -0.3101 265.3391 265.6492 290.6911 158.4775 -0.3148 265.5092 265.8240 290.8255 159.3300 -0.3218 265.7223 266.0441 290.9693 160.0925 -0.3249 265.8941 266.2190 291.1006 160.9153 -0.3289 266.0683 266.3972 291.2523 161.7375 -0.3371 266.2578 266.5949 291.3748 162.4995 -0.3415 266.4228 266.7643 291.5019 163.3520 -0.3471 266.6183 266.9654 291.6451 164.1145 -0.3540 266.7857 267.1398 291.7470 164.9350 -0.3594 266.9668 267.3262 291.8795 165.7528 -0.3599 267.1519 267.5118 292.0180 166.5108 -0.3660 267.3108 267.6769 292.1457 167.3590 -0.3701 267.5025 267.8726 292.2968 168.1163 -0.3740 267.6606 268.0346 292.4118 168.9348 -0.3828 267.8473 268.2301 292.5574 169.7228 -0.3853 268.0317 268.4169 292.6788 170.5105 -0.3916 268.1992 268.5908 292.8032 171.3598 -0.3992 268.3961 268.7954 292.9546 172.1185 -0.4037 268.5611 268.9647 293.0638 172.9368 -0.4063 268.7482 269.1544 293.2112 173.7248 -0.4142 268.9287 269.3429 293.3457 174.5143 -0.4205 269.0955 269.5160 293.4791 175.3638 -0.4249 269.2824 269.7073 293.6023 176.1233 -0.4299 269.4436 269.8735 293.7225 176.9420 -0.4347 269.6287 270.0634 293.8671 177.7610 -0.4371 269.8158 270.2528 294.0098 178.5210 -0.4437 269.9921 270.4358 294.1213 179.3710 -0.4489 270.1540 270.6029 294.2645 180.1315 -0.4550 270.3259 270.7809 294.3987 180.9538 -0.4595 270.5046 270.9641 294.5304 181.7458 -0.4633 270.6763 271.1396 294.6634 182.5370 -0.4670 270.8444 271.3114 294.7962 183.3878 -0.4757 271.0407 271.5164 294.9436 184.1495 -0.4805 271.2084 271.6889 295.0718 184.9718 -0.4860 271.3913 271.8773 295.1901 185.7638 -0.4911 271.5598 272.0510 295.3213 186.5555 -0.4961 271.7409 272.2371 295.4626 187.3778 -0.4986 271.9037 272.4022 295.6007 188.1695 -0.5033 272.0767 272.5800 295.7320 188.9918 -0.5094 272.2590 272.7684 295.8577 189.7838 -0.5156 272.4230 272.9386 295.9667 190.5755 -0.5175 272.5815 273.0989 296.1016 191.3975 -0.5215 272.7687 273.2901 296.2433 192.1895 -0.5259 272.9383 273.4642 296.3658 193.0118 -0.5284 273.1330 273.6615 296.5016 193.8035 -0.5340 273.2945 273.8285 296.6135 194.5955 -0.5369 273.4658 274.0027 296.7422 195.4175 -0.5427 273.6289 274.1715 296.8722 196.2095 -0.5476 273.7877 274.3352 296.9753 197.0315 -0.5525 273.9694 274.5220 297.1231 197.8235 -0.5572 274.1349 274.6921 297.2538 198.6155 -0.5627 274.3072 274.8699 297.3858 199.4375 -0.5683 274.5019 275.0702 297.5090 200.2295 -0.5727 274.6700 275.2427 297.6196 201.0515 -0.5758 274.8291 275.4049 297.7603 201.8435 -0.5834 274.9871 275.5705 297.8867 202.6355 -0.5857 275.1737 275.7595 297.9948 203.4573 -0.5905 275.3518 275.9423 298.1281 204.2490 -0.6022 275.5207 276.1229 298.2378 205.0708 -0.6111 275.7009 276.3120 298.3810 205.8630 -0.6106 275.8562 276.4668 298.5123 206.6545 -0.6142 276.0258 276.6400 298.6493 207.4770 -0.6125 276.2115 276.8240 298.7779 208.2685 -0.6154 276.3824 276.9977 298.8828 209.0908 -0.6218 276.5383 277.1601 299.0392 209.8828 -0.6271 276.6955 277.3226 299.1571 210.6745 -0.6318 276.8642 277.4960 299.2736 211.5268 -0.6379 277.0551 277.6930 299.4175 212.2885 -0.6426 277.2164 277.8590 299.5360 213.1108 -0.6479 277.3799 278.0278 299.6754 213.9028 -0.6508 277.5527 278.2035 299.8105 214.6945 -0.6522 277.7295 278.3817 299.9042 215.5465 -0.6573 277.9019 278.5593 300.0528 216.3085 -0.6635 278.0618 278.7253 300.1697 217.1310 -0.6664 278.2317 278.8981 300.2913 217.9535 -0.6706 278.4018 279.0724 300.4271 218.7155 -0.6780 278.5657 279.2437 300.5583 219.5675 -0.6824 278.7470 279.4293 300.7024 220.3295 -0.6875 278.8994 279.5868 300.8202 221.1515 -0.6889 279.0541 279.7430 300.9616 221.9735 -0.6921 279.2547 279.9468 301.0911 222.7355 -0.6973 279.4019 280.0992 301.2382 223.5875 -0.7045 279.5591 280.2637 301.3942 224.3795 -0.7067 279.7299 280.4366 301.5254 225.1708 -0.7076 279.8923 280.5998 301.6549 225.9933 -0.7119 280.0607 280.7726 301.8160 226.7848 -0.7168 280.2324 280.9492 301.9638 227.6068 -0.7222 280.3855 281.1077 302.1027 228.3988 -0.7267 280.5550 281.2818 302.2473 229.1885 -0.7319 280.7215 281.4534 302.4051 230.0063 -0.7373 280.9108 281.6481 302.5656 230.7940 -0.7425 281.0608 281.8034 302.7112 231.6120 -0.7473 281.2186 281.9659 302.8601 232.4003 -0.7526 281.3821 282.1347 302.9869 233.1880 -0.7566 281.5504 282.3070 303.1411 234.0073 -0.7610 281.7286 282.4897 303.2924 234.7970 -0.7642 281.8861 282.6502 303.4078 235.6153 -0.7663 282.0480 282.8143 303.5605 236.4030 -0.7712 282.2152 282.9864 303.6992 237.1910 -0.7783 282.3742 283.1525 303.8105 238.0400 -0.7821 282.5488 283.3309 303.9477 238.7990 -0.7878 282.7014 283.4891 304.0579 239.6188 -0.7910 282.8798 283.6708 304.1985 240.4085 -0.7953 283.0399 283.8352 304.3155 241.1980 -0.7994 283.2024 284.0018 304.4380 242.0470 -0.8036 283.3765 284.1801 304.5664 242.8065 -0.8074 283.5196 284.3270 304.6773 243.6278 -0.8146 283.6855 284.5002 304.8024 244.4190 -0.8183 283.8410 284.6593 304.9368 245.2105 -0.8230 284.0001 284.8232 305.0618 246.0625 -0.8260 284.1904 285.0164 305.1973 246.8233 -0.8295 284.3533 285.1828 305.3088 247.6448 -0.8344 284.5018 285.3362 305.4258 248.4368 -0.8380 284.6710 285.5090 305.5505 249.2285 -0.8418 284.8296 285.6714 305.6664 250.0505 -0.8470 284.9760 285.8229 305.7874 250.8125 -0.8538 285.1244 285.9782 305.9126 251.6645 -0.8563 285.2940 286.1503 306.0153 252.4565 -0.8606 285.4817 286.3423 306.1395 253.2485 -0.8619 285.6348 286.4967 306.2757 254.0705 -0.8695 285.7980 286.6674 306.4179 254.8480 -0.8764 285.9776 286.8541 306.5290 255.6565 -0.8799 286.1388 287.0188 306.6654 256.4485 -0.8849 286.2983 287.1832 306.8175 257.3005 -0.8835 286.4521 287.3357 306.9545 258.0625 -0.8864 286.5933 287.4797 307.0720 258.8845 -0.8928 286.7623 287.6550 307.2059 259.6765 -0.8961 286.9351 287.8312 307.3564 260.4680 -0.8997 287.0866 287.9863 307.5040 261.2908 -0.9031 287.2548 288.1579 307.6507 262.0828 -0.9078 287.3986 288.3064 307.7928 262.9050 -0.9121 287.5872 288.4993 307.9292 263.6970 -0.9172 287.7456 288.6628 308.0710 264.4885 -0.9227 287.8895 288.8122 308.2252 265.3108 -0.9270 288.0445 288.9715 308.3705 266.0725 -0.9326 288.2065 289.1390 308.5033 266.9253 -0.9325 288.3983 289.3308 308.6628 267.7178 -0.9358 288.5545 289.4902 308.8058 268.5095 -0.9393 288.7117 289.6510 308.9508 269.3318 -0.9446 288.8740 289.8186 309.1040 270.0935 -0.9500 289.0173 289.9672 309.2424 270.9458 -0.9509 289.1923 290.1432 309.4023 271.7075 -0.9592 289.3298 290.2890 309.5361 272.5298 -0.9629 289.4983 290.4612 309.6667 273.3518 -0.9680 289.6737 290.6416 309.8180 274.1135 -0.9704 289.8272 290.7977 309.9366 274.9663 -0.9740 289.9883 290.9624 310.0845 275.7285 -0.9784 290.1391 291.1176 310.1958 276.5505 -0.9815 290.2906 291.2721 310.3235 277.3468 -0.9898 290.4530 291.4427 310.4413 278.1405 -0.9965 290.6176 291.6141 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