DTA measure 2felfutes1 Date: 2024108:1150 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.10 s Mass = 966.900 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3905 -4.4048 429.8903 434.2951 424.0536 3.9863 -4.4119 430.0432 434.4550 424.0604 5.5793 -4.4226 430.2035 434.6261 424.0624 7.1870 -4.4294 430.3667 434.7961 424.0244 8.7786 -4.4353 430.5177 434.9529 423.9923 10.3921 -4.4468 430.6578 435.1046 423.9100 11.9894 -4.4526 430.7990 435.2516 423.8013 13.5905 -4.4563 430.9366 435.3929 423.6594 15.2038 -4.4529 431.0787 435.5316 423.4952 16.7994 -4.4559 431.2195 435.6753 423.3318 18.4075 -4.4609 431.3454 435.8062 423.1403 20.0215 -4.4643 431.4826 435.9469 422.9398 21.6355 -4.4708 431.6022 436.0730 422.6955 23.2495 -4.4725 431.7523 436.2247 422.4686 24.8485 -4.4803 431.8668 436.3471 422.2346 26.4471 -4.4813 431.9834 436.4647 422.0063 28.0610 -4.4856 432.1124 436.5979 421.7770 29.6749 -4.4905 432.2225 436.7130 421.5567 31.2888 -4.4912 432.3268 436.8180 421.3234 32.8876 -4.4928 432.4369 436.9297 421.0969 34.5016 -4.4959 432.5369 437.0328 420.8739 36.0971 -4.5004 432.6493 437.1498 420.6392 37.6983 -4.4959 432.7278 437.2237 420.4132 39.2908 -4.4979 432.8348 437.3327 420.2074 40.9195 -4.5005 432.9075 437.4080 420.0122 42.5145 -4.5008 432.9914 437.4923 419.8120 44.1086 -4.5022 433.0802 437.5824 419.6428 45.7196 -4.5055 433.1803 437.6858 419.4685 47.3171 -4.5087 433.2468 437.7555 419.2962 48.9306 -4.5121 433.3176 437.8297 419.1172 50.5298 -4.5174 433.3983 437.9156 418.9305 52.1436 -4.5205 433.4672 437.9877 418.7450 53.7426 -4.5200 433.5282 438.0482 418.5796 55.3566 -4.5239 433.5811 438.1049 418.3952 56.9624 -4.5298 433.6351 438.1649 418.2204 58.5816 -4.5359 433.6998 438.2357 418.0539 60.1805 -4.5390 433.7645 438.3035 417.8688 61.7945 -4.5399 433.8135 438.3534 417.6652 63.3935 -4.5462 433.8725 438.4187 417.4747 64.9955 -4.5454 433.8992 438.4446 417.2762 66.6255 -4.5453 433.9351 438.4803 417.0770 68.2203 -4.5463 433.9770 438.5232 416.8916 69.8114 -4.5482 434.0153 438.5635 416.6933 71.4175 -4.5502 434.0545 438.6047 416.5139 73.0088 -4.5544 434.0851 438.6395 416.3237 74.6168 -4.5571 434.0993 438.6564 416.1335 76.2284 -4.5556 434.1352 438.6908 415.9453 77.8148 -4.5570 434.1484 438.7054 415.7457 79.4325 -4.5630 434.1714 438.7343 415.5268 81.0468 -4.5668 434.1925 438.7593 415.3143 82.6465 -4.5690 434.1997 438.7687 415.1278 84.2454 -4.5730 434.2149 438.7878 414.9064 85.8591 -4.5762 434.2213 438.7975 414.7011 87.4730 -4.5777 434.2258 438.8035 414.4871 89.0718 -4.5857 434.2385 438.8243 414.2678 90.6856 -4.5933 434.2212 438.8145 414.0524 92.2846 -4.5981 434.2179 438.8160 413.8488 93.8993 -4.6025 434.2183 438.8208 413.6561 95.5138 -4.6038 434.1937 438.7975 413.4509 97.1128 -4.6067 434.1941 438.8009 413.2552 98.7145 -4.6096 434.1777 438.7872 413.0503 100.3331 -4.6140 434.1586 438.7726 412.8662 101.9260 -4.6187 434.1537 438.7724 412.6720 103.5320 -4.6207 434.1060 438.7268 412.4780 105.1384 -4.6230 434.0899 438.7129 412.2977 106.7455 -4.6209 434.0645 438.6854 412.1029 108.3411 -4.6174 434.0291 438.6465 411.9377 109.9516 -4.6190 434.0007 438.6197 411.7464 111.5496 -4.6243 433.9654 438.5896 411.5542 113.1788 -4.6253 433.9381 438.5634 411.3398 114.7775 -4.6267 433.8854 438.5122 411.1566 116.3765 -4.6288 433.8666 438.4954 410.9562 117.9949 -4.6353 433.8180 438.4533 410.7561 119.5935 -4.6352 433.7722 438.4074 410.5604 121.1925 -4.6403 433.7338 438.3741 410.3669 122.8215 -4.6419 433.6818 438.3238 410.1640 124.4205 -4.6431 433.6320 438.2750 409.9807 126.0345 -4.6484 433.5765 438.2249 409.7795 127.6331 -4.6508 433.5222 438.1730 409.5774 129.2318 -4.6536 433.4650 438.1186 409.3782 130.8608 -4.6579 433.4032 438.0612 409.1747 132.4744 -4.6606 433.3453 438.0060 408.9600 134.0661 -4.6635 433.2705 437.9340 408.7373 135.6571 -4.6654 433.1919 437.8574 408.5202 137.2640 -4.6687 433.1365 437.8052 408.2941 138.8668 -4.6691 433.0673 437.7365 408.0983 140.4609 -4.6702 432.9997 437.6699 407.8783 142.0893 -4.6739 432.9280 437.6019 407.6629 143.6880 -4.6749 432.8602 437.5350 407.4591 145.2869 -4.6770 432.7837 437.4607 407.2465 146.8856 -4.6784 432.7051 437.3835 407.0288 148.4996 -4.6814 432.6157 437.2971 406.8271 150.1154 -4.6815 432.5440 437.2255 406.6176 151.7148 -4.6848 432.4590 437.1438 406.3916 153.3286 -4.6855 432.3591 437.0447 406.1919 154.9276 -4.6862 432.2734 436.9596 405.9900 156.5266 -4.6877 432.1921 436.8798 405.7834 158.1556 -4.6912 432.0885 436.7797 405.5905 159.7545 -4.6917 431.9989 436.6906 405.3938 161.3694 -4.6949 431.9129 436.6078 405.1889 162.9838 -4.6965 431.8355 436.5320 404.9898 164.5821 -4.6950 431.7320 436.4270 404.8029 166.1746 -4.6955 431.6357 436.3312 404.6146 167.7810 -4.6986 431.5284 436.2270 404.4277 169.3871 -4.6978 431.4146 436.1124 404.2346 170.9950 -4.6998 431.3174 436.0172 404.0305 172.5920 -4.7026 431.2213 435.9239 403.8692 174.1905 -4.7003 431.1141 435.8145 403.6650 175.8045 -4.7037 431.0053 435.7090 403.4733 177.4185 -4.7055 430.8884 435.5939 403.2783 179.0175 -4.7061 430.7892 435.4953 403.0735 180.6215 -4.7039 430.6852 435.3891 402.8694 182.2275 -4.7070 430.5546 435.2616 402.6561 183.8415 -4.7077 430.4442 435.1519 402.4461 185.4403 -4.7060 430.3299 435.0359 402.2328 187.0539 -4.7098 430.2084 434.9182 402.0356 188.6679 -4.7085 430.0892 434.7977 401.8446 190.2678 -4.7065 429.9790 434.6854 401.6195 191.8666 -4.7075 429.8551 434.5626 401.4290 193.4813 -4.7093 429.7279 434.4372 401.2147 195.0956 -4.7073 429.6085 434.3157 401.0185 196.7079 -4.7074 429.4884 434.1958 400.8238 198.2990 -4.7074 429.3582 434.0656 400.6319 199.8900 -4.7053 429.2370 433.9423 400.4372 201.5070 -4.7065 429.1097 433.8163 400.2516 203.1006 -4.7057 428.9911 433.6968 400.0513 204.7120 -4.7085 428.8570 433.5656 399.8579 206.3258 -4.7074 428.7351 433.4425 399.6493 207.9248 -4.7068 428.6007 433.3075 399.4443 209.5236 -4.7057 428.4684 433.1741 399.2264 211.1376 -4.7028 428.3299 433.0327 399.0249 212.7366 -4.7013 428.1965 432.8978 398.8165 214.3658 -4.7004 428.0576 432.7580 398.5971 215.9646 -4.6975 427.9219 432.6194 398.3757 217.5641 -4.6971 427.7830 432.4801 398.1546 219.1785 -4.6948 427.6423 432.3371 397.9446 220.7888 -4.6926 427.4988 432.1913 397.7323 222.3915 -4.6921 427.3623 432.0543 397.5269 224.0205 -4.6937 427.2328 431.9264 397.3004 225.6195 -4.6886 427.0902 431.7788 397.0948 227.2189 -4.6858 426.9476 431.6334 396.8793 228.8326 -4.6841 426.7916 431.4757 396.6829 230.4260 -4.6859 426.6570 431.3430 396.4685 232.0480 -4.6815 426.4991 431.1806 396.2625 233.6400 -4.6778 426.3582 431.0360 396.0716 235.2323 -4.6762 426.2284 430.9045 395.8567 236.8410 -4.6745 426.0751 430.7496 395.6536 238.4391 -4.6704 425.9158 430.5862 395.4524 240.0525 -4.6664 425.7670 430.4334 395.2481 241.6381 -4.6654 425.6206 430.2861 395.0540 243.2683 -4.6623 425.4517 430.1139 394.8463 244.8668 -4.6601 425.3058 429.9660 394.6607 246.4656 -4.6574 425.1600 429.8174 394.4651 248.0648 -4.6565 425.0155 429.6720 394.2680 249.6786 -4.6526 424.8567 429.5093 394.0901 251.2870 -4.6492 424.7059 429.3551 393.8950 252.8946 -4.6474 424.5473 429.1947 393.6944 254.4936 -4.6446 424.3739 429.0184 393.4825 256.1226 -4.6432 424.2208 428.8641 393.2911 257.7216 -4.6361 424.0635 428.6997 393.0726 259.3205 -4.6354 423.9043 428.5397 392.8694 260.9348 -4.6341 423.7505 428.3846 392.6503 262.5309 -4.6293 423.5879 428.2172 392.4427 264.1430 -4.6264 423.4281 428.0545 392.2195 265.7340 -4.6256 423.2637 427.8893 392.0093 267.3405 -4.6245 423.1066 427.7311 391.8058 268.9351 -4.6181 422.9472 427.5653 391.5913 270.5645 -4.6168 422.7788 427.3957 391.3608 272.1449 -4.6133 422.6198 427.2331 391.1562 273.7575 -4.6082 422.4640 427.0722 390.9346 275.3865 -4.6077 422.2919 426.8996 390.7166 276.9855 -4.6032 422.1277 426.7308 390.5154 278.5845 -4.5989 421.9600 426.5588 390.3013 280.1985 -4.5955 421.7899 426.3853 390.0989 281.8125 -4.5910 421.6205 426.2115 389.8936 283.4264 -4.5878 421.4558 426.0436 389.6924 285.0254 -4.5850 421.2966 425.8816 389.4892 286.6396 -4.5831 421.1223 425.7053 389.2855 288.2388 -4.5788 420.9473 425.5261 389.0783 289.8526 -4.5740 420.7795 425.3535 388.8705 291.4668 -4.5718 420.5991 425.1708 388.6689 293.0648 -4.5694 420.4373 425.0067 388.4603 294.6841 -4.5649 420.2616 424.8265 388.2557 296.2750 -4.5615 420.0906 424.6522 388.0543 297.8661 -4.5593 419.9253 424.4847 387.8676 299.4731 -4.5528 419.7458 424.2986 387.6685 301.0833 -4.5525 419.5694 424.1218 387.4803 302.6949 -4.5488 419.4149 423.9637 387.2767 304.2928 -4.5448 419.2463 423.7910 387.0819 305.8916 -4.5387 419.0683 423.6070 386.8754 307.4906 -4.5368 418.8961 423.4329 386.6705 309.1068 -4.5336 418.7080 423.2417 386.4647 310.7218 -4.5329 418.5288 423.0617 386.2351 312.3206 -4.5296 418.3481 422.8777 386.0365 313.9308 -4.5228 418.1704 422.6932 385.8326 315.5315 -4.5196 418.0024 422.5220 385.5977 317.1455 -4.5164 417.8203 422.3367 385.3993 318.7445 -4.5112 417.6396 422.1508 385.1795 320.3735 -4.5076 417.4535 421.9611 384.9443 321.9736 -4.5026 417.2883 421.7909 384.7407 323.5539 -4.4994 417.1159 421.6153 384.5202 325.1931 -4.4945 416.9289 421.4234 384.3130 326.7854 -4.4925 416.7446 421.2371 384.1116 328.3933 -4.4884 416.5708 421.0592 383.8823 329.9855 -4.4833 416.3851 420.8684 383.6717 331.5781 -4.4794 416.2032 420.6825 383.4763 333.1969 -4.4766 416.0272 420.5038 383.2654 334.8005 -4.4730 415.8570 420.3300 383.0408 336.3995 -4.4695 415.6541 420.1236 382.8469 338.0135 -4.4617 415.4723 419.9340 382.6391 339.6275 -4.4562 415.2965 419.7528 382.4184 341.2265 -4.4518 415.1120 419.5638 382.2166 342.8294 -4.4506 414.9433 419.3940 382.0145 344.4404 -4.4468 414.7456 419.1924 381.8208 346.0500 -4.4387 414.5618 419.0005 381.6109 347.6488 -4.4363 414.3798 418.8161 381.4020 349.2626 -4.4325 414.1980 418.6306 381.2069 350.8616 -4.4276 414.0090 418.4366 381.0094 352.4908 -4.4235 413.8196 418.2432 380.8000 354.0760 -4.4202 413.6289 418.0491 380.6051 355.6816 -4.4131 413.4366 417.8498 380.4017 357.3114 -4.4094 413.2593 417.6687 380.2056 358.9228 -4.4050 413.0681 417.4730 379.9988 360.5140 -4.3997 412.8879 417.2876 379.8155 362.1050 -4.3939 412.7018 417.0958 379.6056 363.7116 -4.3909 412.5228 416.9138 379.4065 365.3104 -4.3872 412.3303 416.7175 379.2178 366.9210 -4.3814 412.1416 416.5231 379.0254 368.5341 -4.3795 411.9526 416.3322 378.8093 370.1326 -4.3727 411.7594 416.1321 378.6086 371.7316 -4.3707 411.5765 415.9472 378.3960 373.3456 -4.3658 411.3948 415.7606 378.1706 374.9483 -4.3586 411.1987 415.5573 377.9516 376.5636 -4.3549 411.0098 415.3647 377.7446 378.1775 -4.3517 410.8152 415.1669 377.5201 379.7765 -4.3448 410.6262 414.9709 377.2900 381.3905 -4.3413 410.4289 414.7702 377.0851 382.9901 -4.3384 410.2427 414.5811 376.8615 384.6071 -4.3336 410.0605 414.3942 376.6559 386.2154 -4.3284 409.8607 414.1891 376.4397 387.8148 -4.3186 409.6780 413.9967 376.2199 389.4439 -4.3146 409.4877 413.8022 375.9956 391.0395 -4.3108 409.2932 413.6040 375.7851 392.6310 -4.3035 409.1057 413.4092 375.5790 394.2373 -4.2980 408.9074 413.2054 375.3747 395.8374 -4.2941 408.7187 413.0128 375.1684 397.4404 -4.2884 408.5244 412.8128 374.9462 399.0500 -4.2850 408.3412 412.6262 374.7363 400.6483 -4.2810 408.1420 412.4230 374.5311 402.2629 -4.2724 407.9518 412.2242 374.3265 403.8770 -4.2702 407.7498 412.0200 374.1143 405.4528 -4.2672 407.5634 411.8305 373.8993 407.0886 -4.2586 407.3703 411.6289 373.6890 408.7029 -4.2543 407.1705 411.4248 373.4716 410.3026 -4.2470 406.9875 411.2345 373.2748 411.9016 -4.2433 406.7863 411.0296 373.0675 413.5156 -4.2387 406.5806 410.8193 372.8695 415.1254 -4.2334 406.3921 410.6255 372.6574 416.7336 -4.2270 406.1993 410.4263 372.4484 418.3475 -4.2224 405.9999 410.2223 372.2645 419.9615 -4.2183 405.8147 410.0330 372.0559 421.5756 -4.2128 405.6249 409.8376 371.8584 423.1718 -4.2084 405.4126 409.6210 371.6554 424.7633 -4.2024 405.2235 409.4260 371.4660 426.3710 -4.1998 405.0146 409.2143 371.2684 427.9944 -4.1936 404.8264 409.0200 371.0556 429.5881 -4.1868 404.6513 408.8380 370.8942 431.1839 -4.1811 404.4378 408.6189 370.6815 432.7825 -4.1793 404.2448 408.4242 370.4898 434.3965 -4.1752 404.0571 408.2324 370.2862 436.0064 -4.1685 403.8560 408.0244 370.0602 437.6225 -4.1640 403.6407 407.8047 369.8542 439.2365 -4.1613 403.4398 407.6011 369.6489 440.8355 -4.1566 403.2794 407.4360 369.4484 442.4345 -4.1508 403.0678 407.2186 369.2470 444.0480 -4.1466 402.8620 407.0086 369.0324 445.6773 -4.1421 402.6787 406.8209 368.8063 447.2756 -4.1382 402.4841 406.6223 368.5964 448.8746 -4.1336 402.2834 406.4170 368.3788 450.4891 -4.1268 402.0789 406.2058 368.1647 452.1036 -4.1221 401.8776 405.9997 367.9697 453.7186 -4.1160 401.6809 405.7969 367.7576 455.3131 -4.1088 401.4847 405.5935 367.5383 456.8985 -4.1032 401.2937 405.3969 367.3400 458.5193 -4.0992 401.1036 405.2028 367.1328 460.1133 -4.0957 400.8877 404.9834 366.9312 461.7225 -4.0896 400.6868 404.7764 366.7336 463.3320 -4.0852 400.4923 404.5776 366.5149 464.9440 -4.0784 400.2919 404.3703 366.2971 466.5426 -4.0731 400.0902 404.1633 366.1013 468.1420 -4.0694 399.8953 403.9646 365.8873 469.7566 -4.0608 399.6996 403.7604 365.6796 471.3706 -4.0566 399.5122 403.5688 365.4705 472.9848 -4.0504 399.3023 403.3527 365.2816 474.5839 -4.0452 399.1099 403.1551 365.0752 476.1835 -4.0424 398.9096 402.9520 364.8759 477.8084 -4.0355 398.7070 402.7426 364.6808 479.4080 -4.0325 398.5112 402.5437 364.4676 481.0225 -4.0283 398.3090 402.3373 364.2756 482.6374 -4.0238 398.0975 402.1213 364.0609 484.2364 -4.0195 397.9154 401.9349 363.8769 485.8349 -4.0124 397.7132 401.7255 363.6857 487.4478 -4.0078 397.5189 401.5267 363.4684 489.0544 -4.0024 397.3243 401.3268 363.2587 490.6609 -3.9939 397.1150 401.1090 363.0509 492.2541 -3.9902 396.9192 400.9094 362.8352 493.8623 -3.9838 396.7123 400.6961 362.6290 495.4568 -3.9815 396.5177 400.4992 362.4169 497.0576 -3.9783 396.3081 400.2864 362.1994 498.6651 -3.9768 396.1165 400.0934 361.9631 500.2976 -3.9700 395.9121 399.8821 361.7402 501.8961 -3.9649 395.7105 399.6754 361.5362 503.4948 -3.9615 395.4941 399.4555 361.3189 505.0963 -3.9550 395.3252 399.2802 361.0934 506.7116 -3.9474 395.1297 399.0771 360.8907 508.3256 -3.9438 394.9164 398.8602 360.6676 509.9398 -3.9380 394.7116 398.6496 360.4558 511.5386 -3.9305 394.5193 398.4498 360.2530 513.1526 -3.9251 394.3261 398.2512 360.0261 514.7516 -3.9184 394.1134 398.0319 359.8088 516.3806 -3.9123 393.9097 397.8219 359.5986 517.9770 -3.9059 393.7048 397.6107 359.3943 519.5941 -3.9037 393.5245 397.4282 359.1763 521.1865 -3.8983 393.3021 397.2004 358.9780 522.7796 -3.8934 393.1009 396.9943 358.7819 524.3866 -3.8872 392.9003 396.7874 358.5749 526.0099 -3.8782 392.6902 396.5685 358.3553 527.6061 -3.8733 392.4963 396.3697 358.1443 529.2049 -3.8658 392.3182 396.1840 357.9422 530.8045 -3.8618 392.1107 395.9725 357.7306 532.4185 -3.8515 391.8978 395.7493 357.5265 534.0325 -3.8490 391.6767 395.5257 357.3216 535.6315 -3.8446 391.5025 395.3471 357.1172 537.2455 -3.8411 391.3005 395.1416 356.9201 538.8435 -3.8363 391.1087 394.9449 356.7199 540.4515 -3.8272 390.9030 394.7302 356.5174 542.0655 -3.8194 390.6848 394.5042 356.3178 543.6801 -3.8118 390.4756 394.2874 356.1169 545.2948 -3.8013 390.2718 394.0731 355.9201 546.8936 -3.7935 390.0768 393.8702 355.7274 548.5076 -3.7883 389.8760 393.6643 355.5261 550.1066 -3.7811 389.6756 393.4567 355.3446 551.7339 -3.7749 389.4734 393.2483 355.1368 553.3255 -3.7679 389.2651 393.0330 354.9383 554.9174 -3.7631 389.0627 392.8258 354.7188 556.5253 -3.7604 388.8538 392.6142 354.5207 558.1340 -3.7537 388.6589 392.4125 354.3111 559.7441 -3.7490 388.4550 392.2039 354.1065 561.3416 -3.7484 388.2632 392.0117 353.8744 562.9556 -3.7421 388.0725 391.8146 353.6697 564.5546 -3.7377 387.8559 391.5936 353.4362 566.1536 -3.7322 387.6502 391.3824 353.2279 567.7828 -3.7285 387.4362 391.1647 353.0123 569.3819 -3.7197 387.2390 390.9587 352.8008 570.9816 -3.7140 387.0522 390.7662 352.5686 572.5959 -3.7087 386.8489 390.5576 352.3608 574.2105 -3.7025 386.6340 390.3366 352.1502 575.8245 -3.6970 386.4256 390.1227 351.9249 577.4235 -3.6932 386.2296 389.9228 351.6964 579.0375 -3.6889 386.0262 389.7151 351.4705 580.6370 -3.6842 385.8154 389.4996 351.2577 582.2515 -3.6792 385.6048 389.2840 351.0626 583.8789 -3.6704 385.3923 389.0626 350.8430 585.4710 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