DTA measure 2felfutes2 Date: 2024108:1218 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1083.95 s Mass = 5000.000 mg data_number = 1345 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1665 -0.6465 245.7424 246.3889 266.2449 1.9885 -0.6411 245.8863 246.5274 266.2638 2.7805 -0.6357 246.0403 246.6761 266.2840 3.5725 -0.6320 246.1889 246.8208 266.2851 4.4245 -0.6250 246.3414 246.9665 266.3067 5.1865 -0.6206 246.4882 247.1088 266.3255 6.0085 -0.6165 246.6580 247.2745 266.3313 6.8005 -0.6102 246.8050 247.4152 266.3553 7.5918 -0.6054 246.9505 247.5559 266.3803 8.4443 -0.5989 247.1156 247.7145 266.4019 9.2060 -0.5952 247.2410 247.8362 266.4516 10.0278 -0.5912 247.3913 247.9825 266.4768 10.8198 -0.5879 247.5288 248.1168 266.5351 11.6115 -0.5842 247.6879 248.2721 266.5901 12.4340 -0.5787 247.8462 248.4249 266.6457 13.2255 -0.5737 247.9831 248.5568 266.7093 14.0478 -0.5718 248.1331 248.7049 266.7879 14.8398 -0.5676 248.2849 248.8525 266.8770 15.6315 -0.5603 248.4367 248.9970 266.9475 16.4538 -0.5563 248.5873 249.1436 267.0520 17.2455 -0.5529 248.7113 249.2641 267.1336 18.1950 -0.5491 248.8841 249.4332 267.2498 19.0893 -0.5458 249.0468 249.5926 267.3830 19.8490 -0.5431 249.1847 249.7278 267.4875 20.6670 -0.5385 249.3340 249.8725 267.5918 21.4550 -0.5336 249.4834 250.0170 267.7319 22.2430 -0.5314 249.6314 250.1628 267.8446 23.0910 -0.5246 249.7872 250.3119 267.9970 23.8490 -0.5239 249.9138 250.4377 268.1152 24.6680 -0.5211 250.0678 250.5889 268.2238 25.4883 -0.5180 250.2054 250.7234 268.3508 26.2470 -0.5153 250.3399 250.8552 268.4842 27.0970 -0.5129 250.4985 251.0114 268.6235 27.8585 -0.5116 250.6273 251.1389 268.7696 28.6790 -0.5077 250.7841 251.2919 268.9061 29.5008 -0.5072 250.9363 251.4435 269.0411 30.2625 -0.5040 251.0648 251.5688 269.1556 31.1148 -0.5009 251.1992 251.7001 269.2988 31.8765 -0.4999 251.3371 251.8370 269.4347 32.6988 -0.4982 251.4740 251.9722 269.5552 33.5208 -0.4967 251.6274 252.1241 269.7050 34.2825 -0.4937 251.7642 252.2579 269.8077 35.1348 -0.4933 251.9130 252.4062 269.9343 35.8965 -0.4895 252.0524 252.5418 270.0671 36.7188 -0.4893 252.1876 252.6768 270.1985 37.5408 -0.4915 252.3577 252.8492 270.3290 38.3035 -0.4876 252.4915 252.9792 270.4423 39.1568 -0.4841 252.6340 253.1181 270.5619 39.9185 -0.4847 252.7590 253.2437 270.6678 40.7405 -0.4821 252.8980 253.3800 270.7632 41.5625 -0.4825 253.0419 253.5244 270.8851 42.3245 -0.4807 253.1776 253.6583 270.9815 43.1770 -0.4807 253.3180 253.7986 271.1061 43.9395 -0.4754 253.4544 253.9298 271.1986 44.7615 -0.4753 253.6051 254.0804 271.3135 45.5838 -0.4761 253.7382 254.2143 271.3839 46.3465 -0.4774 253.8665 254.3439 271.4814 47.1985 -0.4758 254.0204 254.4962 271.5909 47.9605 -0.4752 254.1447 254.6199 271.6715 48.9135 -0.4761 254.3040 254.7801 271.8078 49.8095 -0.4764 254.4806 254.9570 271.9218 50.6018 -0.4750 254.6131 255.0881 272.0183 51.3935 -0.4739 254.7435 255.2174 272.1092 52.2160 -0.4709 254.8915 255.3624 272.1945 52.9750 -0.4717 255.0268 255.4985 272.2818 53.8233 -0.4726 255.1712 255.6438 272.4011 54.6113 -0.4747 255.3012 255.7759 272.4771 55.4000 -0.4724 255.4272 255.8996 272.5741 56.2190 -0.4706 255.5748 256.0454 272.6563 56.9775 -0.4707 255.6942 256.1649 272.7411 57.8263 -0.4699 255.8497 256.3196 272.8620 58.6203 -0.4693 255.9908 256.4601 272.9673 59.4208 -0.4721 256.1257 256.5977 273.0605 60.2110 -0.4721 256.2659 256.7380 273.1513 61.0025 -0.4728 256.4129 256.8857 273.2507 61.8243 -0.4717 256.5453 257.0170 273.3623 62.5865 -0.4725 256.6608 257.1333 273.4681 63.4383 -0.4699 256.8075 257.2774 273.5725 64.2003 -0.4729 256.9361 257.4089 273.6847 65.0218 -0.4742 257.0840 257.5582 273.8003 65.8443 -0.4733 257.2170 257.6903 273.9146 66.6055 -0.4731 257.3460 257.8192 274.0203 67.4580 -0.4737 257.4907 257.9645 274.1485 68.2195 -0.4734 257.6327 258.1061 274.2533 69.1368 -0.4733 257.7822 258.2556 274.3788 70.0538 -0.4750 257.9280 258.4030 274.5260 70.8155 -0.4768 258.0464 258.5232 274.6252 71.6678 -0.4750 258.1988 258.6738 274.7412 72.4598 -0.4761 258.3559 258.8320 274.8519 73.2515 -0.4728 258.4865 258.9593 274.9756 74.0738 -0.4739 258.6081 259.0821 275.0914 74.8355 -0.4769 258.7485 259.2254 275.2186 75.6878 -0.4798 258.8995 259.3793 275.3489 76.4798 -0.4803 259.0283 259.5086 275.4523 77.2715 -0.4815 259.1775 259.6590 275.5608 78.0940 -0.4839 259.2929 259.7768 275.6710 78.8565 -0.4834 259.4141 259.8975 275.8011 79.7085 -0.4845 259.5393 260.0237 275.9444 80.5005 -0.4854 259.6857 260.1711 276.0587 81.2925 -0.4859 259.8148 260.3007 276.1566 82.1145 -0.4877 259.9359 260.4236 276.2736 82.9065 -0.4875 260.0821 260.5696 276.3663 83.7285 -0.4887 260.2135 260.7022 276.4712 84.5200 -0.4907 260.3398 260.8305 276.5737 85.3090 -0.4894 260.4599 260.9494 276.6774 86.1273 -0.4872 260.6244 261.1116 276.7710 86.9160 -0.4898 260.7454 261.2351 276.8645 87.7340 -0.4946 260.8942 261.3888 276.9588 88.5220 -0.4957 261.0340 261.5297 277.0494 89.3110 -0.4966 261.1521 261.6487 277.1396 90.1293 -0.4985 261.2840 261.7826 277.2280 90.9195 -0.4999 261.4098 261.9096 277.3188 91.7400 -0.5027 261.5451 262.0478 277.4153 92.5305 -0.5010 261.6719 262.1729 277.5023 93.3213 -0.5043 261.8094 262.3137 277.5854 94.1725 -0.5044 261.9401 262.4445 277.6789 94.9345 -0.5067 262.0805 262.5873 277.7782 95.7565 -0.5075 262.2114 262.7189 277.8618 96.5485 -0.5066 262.3508 262.8573 277.9569 97.3405 -0.5119 262.4857 262.9977 278.0614 98.1625 -0.5132 262.6090 263.1222 278.1747 98.9545 -0.5155 262.7273 263.2428 278.2703 99.8020 -0.5152 262.8791 263.3943 278.3828 100.5605 -0.5168 263.0038 263.5206 278.4713 101.3825 -0.5171 263.1305 263.6476 278.5870 102.1745 -0.5207 263.2515 263.7722 278.6926 102.9965 -0.5216 263.3906 263.9121 278.8100 103.7885 -0.5225 263.5377 264.0602 278.9090 104.5805 -0.5270 263.6591 264.1861 278.9998 105.4025 -0.5267 263.7926 264.3193 279.1179 106.1945 -0.5286 263.9123 264.4410 279.2260 107.0163 -0.5297 264.0646 264.5943 279.3456 107.8085 -0.5315 264.1824 264.7139 279.4639 108.5995 -0.5318 264.3117 264.8434 279.5718 109.4220 -0.5350 264.4584 264.9934 279.6910 110.2445 -0.5366 264.5804 265.1170 279.7959 110.9975 -0.5382 264.7011 265.2394 279.8935 111.8498 -0.5416 264.8309 265.3725 279.9931 112.6115 -0.5448 264.9499 265.4947 280.1004 113.4345 -0.5452 265.0880 265.6333 280.2167 114.2268 -0.5480 265.2209 265.7689 280.3387 115.0185 -0.5499 265.3462 265.8961 280.4438 115.8713 -0.5491 265.5201 266.0692 280.5641 116.6323 -0.5503 265.6259 266.1762 280.6703 117.4500 -0.5511 265.7348 266.2859 280.7803 118.2380 -0.5534 265.8846 266.4380 280.8929 119.0260 -0.5562 266.0068 266.5630 281.0036 119.8448 -0.5595 266.1333 266.6927 281.0977 120.8305 -0.5599 266.2876 266.8476 281.2291 121.6510 -0.5639 266.4212 266.9851 281.3478 122.4393 -0.5654 266.5479 267.1133 281.4733 123.2280 -0.5677 266.6739 267.2416 281.5611 124.0780 -0.5707 266.8096 267.3803 281.6754 124.8395 -0.5734 266.9296 267.5030 281.7932 125.6618 -0.5739 267.0656 267.6396 281.9093 126.4540 -0.5744 267.1920 267.7664 282.0107 127.2455 -0.5753 267.3312 267.9065 282.1301 128.0978 -0.5766 267.4575 268.0342 282.2401 128.8595 -0.5821 267.5668 268.1489 282.3311 129.6818 -0.5856 267.7135 268.2991 282.4578 130.4738 -0.5857 267.8251 268.4108 282.5444 131.2655 -0.5893 267.9508 268.5401 282.6477 132.0878 -0.5909 268.0882 268.6791 282.7624 132.8795 -0.5935 268.2094 268.8029 282.8644 133.7018 -0.5936 268.3355 268.9290 282.9740 134.4938 -0.5966 268.4603 269.0570 283.0910 135.2855 -0.5976 268.5876 269.1853 283.1948 136.1075 -0.6008 268.7166 269.3174 283.3090 136.8995 -0.6033 268.8410 269.4443 283.4156 137.7218 -0.6050 268.9877 269.5927 283.5214 138.5135 -0.6048 269.1045 269.7093 283.6240 139.3055 -0.6050 269.2361 269.8411 283.7153 140.1580 -0.6097 269.3787 269.9884 283.8254 140.9205 -0.6127 269.4946 270.1072 283.9241 141.7433 -0.6149 269.6229 270.2379 284.0325 142.5355 -0.6196 269.7544 270.3741 284.1410 143.3275 -0.6206 269.8649 270.4855 284.2413 144.1800 -0.6215 269.9901 270.6116 284.3518 144.9425 -0.6234 270.1199 270.7433 284.4610 145.7645 -0.6276 270.2483 270.8759 284.5711 146.5565 -0.6293 270.3727 271.0020 284.6675 147.3478 -0.6318 270.5107 271.1425 284.7746 148.2005 -0.6334 270.6390 271.2724 284.8673 148.9590 -0.6336 270.7621 271.3957 284.9696 149.7773 -0.6364 270.8909 271.5273 285.0840 150.5960 -0.6364 271.0215 271.6579 285.1995 151.4068 -0.6393 271.1501 271.7893 285.2994 152.1658 -0.6434 271.2511 271.8945 285.3821 152.9840 -0.6477 271.3936 272.0413 285.4939 153.7720 -0.6496 271.5132 272.1628 285.5907 154.5623 -0.6524 271.6298 272.2821 285.6938 155.4115 -0.6528 271.7619 272.4147 285.8121 156.1718 -0.6544 271.8878 272.5422 285.9169 156.9925 -0.6559 272.0185 272.6743 286.0168 157.7845 -0.6592 272.1423 272.8015 286.1105 158.5765 -0.6603 272.2568 272.9171 286.2062 159.3985 -0.6617 272.3806 273.0424 286.3112 160.1905 -0.6668 272.5041 273.1710 286.4163 161.0300 -0.6680 272.6334 273.3014 286.5282 161.8135 -0.6699 272.7694 273.4394 286.6169 162.6355 -0.6712 272.8980 273.5691 286.7140 163.4270 -0.6736 273.0235 273.6971 286.8161 164.2490 -0.6761 273.1448 273.8209 286.9344 165.0410 -0.6805 273.2652 273.9457 287.0406 165.8333 -0.6831 273.4020 274.0851 287.1265 166.6553 -0.6845 273.5159 274.2004 287.2392 167.4470 -0.6880 273.6467 274.3347 287.3390 168.2688 -0.6864 273.7738 274.4602 287.4430 169.0610 -0.6912 273.8879 274.5791 287.5284 169.8525 -0.6922 274.0226 274.7148 287.6313 170.6748 -0.6943 274.1518 274.8461 287.7383 171.4785 -0.6961 274.2697 274.9658 287.8484 172.2515 -0.6987 274.3886 275.0874 287.9334 173.1038 -0.6995 274.5203 275.2198 288.0562 173.8655 -0.7034 274.6396 275.3430 288.1425 174.6878 -0.7070 274.7743 275.4813 288.2379 175.4798 -0.7085 274.8871 275.5957 288.3293 176.2715 -0.7118 275.0142 275.7260 288.4278 177.1238 -0.7140 275.1443 275.8583 288.5621 177.8855 -0.7152 275.2721 275.9873 288.6475 178.7075 -0.7155 275.3920 276.1075 288.7395 179.4995 -0.7194 275.5087 276.2281 288.8428 180.2915 -0.7250 275.6331 276.3580 288.9436 181.1440 -0.7229 275.7568 276.4797 289.0594 181.9323 -0.7265 275.8784 276.6049 289.1546 182.7110 -0.7298 275.9959 276.7257 289.2530 183.5290 -0.7319 276.1130 276.8448 289.3689 184.3170 -0.7338 276.2367 276.9705 289.4706 185.1053 -0.7359 276.3574 277.0933 289.5698 185.9240 -0.7395 276.4889 277.2284 289.6843 186.7130 -0.7411 276.6111 277.3522 289.7940 187.5318 -0.7439 276.7487 277.4926 289.9148 188.3213 -0.7485 276.8686 277.6172 290.0345 189.1120 -0.7515 276.9940 277.7454 290.1434 189.9628 -0.7548 277.1280 277.8829 290.2491 190.7245 -0.7577 277.2429 278.0006 290.3768 191.5465 -0.7592 277.3693 278.1284 290.5129 192.3495 -0.7625 277.4772 278.2397 290.6263 193.1415 -0.7664 277.6092 278.3756 290.7328 193.9335 -0.7689 277.7334 278.5023 290.8556 194.7555 -0.7691 277.8525 278.6216 290.9764 195.5475 -0.7730 277.9755 278.7486 291.1083 196.3695 -0.7785 278.0911 278.8697 291.2157 197.1615 -0.7782 278.2074 278.9856 291.3366 197.9535 -0.7814 278.3285 279.1099 291.4196 198.7755 -0.7839 278.4649 279.2489 291.5410 199.5675 -0.7843 278.6058 279.3901 291.6491 200.3895 -0.7858 278.7254 279.5113 291.7629 201.1815 -0.7876 278.8306 279.6183 291.8537 201.9970 -0.7912 278.9535 279.7447 291.9541 202.7815 -0.7948 279.0671 279.8619 292.0600 203.6033 -0.7958 279.1985 279.9943 292.1499 204.3955 -0.8012 279.3224 280.1235 292.2497 205.2173 -0.8030 279.4503 280.2533 292.3469 206.0095 -0.8068 279.5726 280.3794 292.4471 206.8008 -0.8095 279.6983 280.5078 292.5481 207.6235 -0.8117 279.8165 280.6281 292.6277 208.4158 -0.8118 279.9402 280.7519 292.7372 209.2378 -0.8162 280.0517 280.8679 292.8311 210.0298 -0.8182 280.1614 280.9796 292.9314 210.8215 -0.8192 280.2916 281.1109 293.0285 211.6470 -0.8221 280.4346 281.2567 293.1300 212.4520 -0.8243 280.5507 281.3751 293.2134 213.2245 -0.8276 280.6598 281.4874 293.3046 214.0730 -0.8311 280.7936 281.6247 293.3924 214.8310 -0.8328 280.9153 281.7481 293.4879 215.6490 -0.8359 281.0325 281.8684 293.5872 216.4375 -0.8367 281.1550 281.9917 293.6964 217.2260 -0.8413 281.2637 282.1050 293.8052 218.0760 -0.8417 281.3873 282.2289 293.9217 218.8343 -0.8438 281.4953 282.3392 294.0179 219.6540 -0.8466 281.6334 282.4800 294.1213 220.4428 -0.8489 281.7496 282.5985 294.2435 221.2340 -0.8512 281.8755 282.7267 294.3457 222.0550 -0.8547 281.9897 282.8444 294.4702 222.8680 -0.8573 282.1194 282.9767 294.5658 223.6465 -0.8609 282.2489 283.1099 294.6967 224.4688 -0.8651 282.3640 283.2291 294.8003 225.2610 -0.8672 282.4892 283.3564 294.9038 226.0525 -0.8661 282.6028 283.4689 295.0110 226.8750 -0.8701 282.7319 283.6020 295.1417 227.6665 -0.8726 282.8412 283.7138 295.2641 228.4888 -0.8725 282.9469 283.8193 295.3730 229.2808 -0.8742 283.0747 283.9489 295.4808 230.0725 -0.8797 283.1910 284.0707 295.5757 230.8948 -0.8842 283.3255 284.2097 295.6933 231.6565 -0.8871 283.4383 284.3253 295.8255 232.5088 -0.8855 283.5735 284.4590 295.9442 233.3178 -0.8875 283.6785 284.5660 296.0740 234.0805 -0.8916 283.8105 284.7021 296.1786 234.9025 -0.8932 283.9261 284.8193 296.2872 235.7248 -0.8935 284.0519 284.9454 296.3922 236.4865 -0.8954 284.1660 285.0613 296.4972 237.3385 -0.8982 284.2984 285.1967 296.6244 238.1005 -0.8999 284.4041 285.3040 296.7366 238.9225 -0.9037 284.5273 285.4311 296.8417 239.7448 -0.9060 284.6607 285.5667 296.9727 240.5075 -0.9091 284.7759 285.6850 297.0819 241.3595 -0.9105 284.8955 285.8060 297.2031 242.1515 -0.9147 285.0103 285.9250 297.3103 242.9635 -0.9171 285.1430 286.0601 297.4307 243.7535 -0.9176 285.2520 286.1696 297.5370 244.5755 -0.9216 285.3724 286.2940 297.6245 245.3370 -0.9252 285.4832 286.4084 297.7089 246.1860 -0.9261 285.6105 286.5366 297.8231 246.9445 -0.9308 285.7293 286.6601 297.9279 247.7638 -0.9345 285.8545 286.7890 298.0283 248.5820 -0.9348 285.9773 286.9121 298.1189 249.3400 -0.9384 286.0863 287.0247 298.2183 250.1880 -0.9375 286.2127 287.1503 298.3243 250.9760 -0.9422 286.3402 287.2824 298.4117 251.7658 -0.9434 286.4546 287.3980 298.5020 252.5848 -0.9460 286.6001 287.5461 298.6012 253.3578 -0.9485 286.6966 287.6451 298.6905 254.1908 -0.9489 286.8248 287.7737 298.7882 254.9518 -0.9551 286.9303 287.8854 298.8700 255.8035 -0.9556 287.0634 288.0190 298.9655 256.5955 -0.9591 287.1747 288.1338 299.0442 257.3875 -0.9639 287.2789 288.2428 299.1326 258.2095 -0.9626 287.4159 288.3785 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