DTA measure 1Fel_1.dat Date: 2024108:1121 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 974.58 s Mass = 951.000 mg data_number = 1199 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2555 -2.3687 201.1687 203.5374 260.5861 2.0175 -2.3631 201.4022 203.7653 260.6143 2.8695 -2.3574 201.6847 204.0421 260.5975 3.6273 -2.3528 201.9353 204.2881 260.5853 4.4450 -2.3477 202.1829 204.5306 260.6117 5.2638 -2.3413 202.4351 204.7764 260.6293 6.0210 -2.3312 202.6909 205.0221 260.6508 6.8693 -2.3265 202.9177 205.2441 260.6502 7.6260 -2.3207 203.1744 205.4951 260.6749 8.4453 -2.3170 203.4529 205.7699 260.7074 9.2640 -2.3124 203.6986 206.0110 260.7772 10.0220 -2.3081 203.9314 206.2395 260.8142 10.8710 -2.2989 204.1867 206.4856 260.8785 11.6583 -2.2908 204.4215 206.7123 260.9244 12.4463 -2.2896 204.6661 206.9556 260.9862 13.2653 -2.2861 204.9234 207.2095 261.0724 14.0543 -2.2801 205.1597 207.4398 261.1668 14.8738 -2.2722 205.4040 207.6763 261.2568 15.6625 -2.2674 205.6537 207.9210 261.3414 16.4520 -2.2652 205.8909 208.1560 261.4672 17.2723 -2.2568 206.1319 208.3887 261.5685 18.0620 -2.2527 206.3751 208.6278 261.6672 18.8813 -2.2505 206.5877 208.8382 261.8035 19.6723 -2.2480 206.8494 209.0974 261.9413 20.4635 -2.2449 207.1114 209.3563 262.0636 21.2903 -2.2400 207.3314 209.5714 262.2049 22.0510 -2.2364 207.5655 209.8018 262.3333 22.9030 -2.2317 207.7973 210.0290 262.4872 23.6950 -2.2289 208.0419 210.2708 262.6278 24.4865 -2.2278 208.2890 210.5167 262.7745 25.3090 -2.2299 208.5388 210.7687 262.9349 26.0705 -2.2281 208.7472 210.9752 263.0994 26.9230 -2.2276 209.0129 211.2405 263.2607 27.7150 -2.2263 209.2733 211.4995 263.4402 28.5065 -2.2222 209.4807 211.7030 263.5737 29.3290 -2.2188 209.7163 211.9351 263.7611 30.0905 -2.2153 209.9282 212.1435 263.9543 30.9430 -2.2150 210.1854 212.4004 264.1315 31.7048 -2.2117 210.4090 212.6207 264.2989 32.5268 -2.2088 210.6429 212.8517 264.4914 33.3488 -2.2063 210.9006 213.1070 264.6603 34.1105 -2.1991 211.1110 213.3101 264.8385 34.9630 -2.1981 211.3613 213.5594 265.0409 35.7248 -2.1928 211.5799 213.7727 265.2242 36.5468 -2.1893 211.8162 214.0055 265.4138 37.3688 -2.1926 212.0635 214.2561 265.6139 38.1305 -2.1941 212.2722 214.4664 265.7806 38.9825 -2.1888 212.5066 214.6954 265.9632 39.7445 -2.1826 212.7303 214.9129 266.1596 40.5665 -2.1845 212.9729 215.1574 266.3517 41.3885 -2.1801 213.1902 215.3703 266.5332 42.1505 -2.1795 213.4274 215.6069 266.7166 43.0025 -2.1766 213.6455 215.8221 266.9071 43.7645 -2.1713 213.8638 216.0351 267.0882 44.5865 -2.1692 214.1115 216.2808 267.2540 45.4085 -2.1731 214.3417 216.5148 267.4568 46.1705 -2.1715 214.5632 216.7347 267.5908 47.0225 -2.1693 214.7899 216.9592 267.7888 47.7845 -2.1665 215.0124 217.1789 267.9605 48.6065 -2.1659 215.2492 217.4151 268.1244 49.4285 -2.1635 215.4895 217.6529 268.2865 50.1905 -2.1617 215.6726 217.8343 268.4578 51.0428 -2.1596 215.9164 218.0759 268.6226 51.8053 -2.1582 216.1385 218.2967 268.7745 52.6275 -2.1567 216.3782 218.5349 268.9359 53.4493 -2.1535 216.5789 218.7325 269.1123 54.2105 -2.1575 216.7782 218.9358 269.2552 55.0630 -2.1559 217.0150 219.1709 269.4150 55.8248 -2.1535 217.2569 219.4105 269.5367 56.6468 -2.1491 217.4804 219.6295 269.7012 57.4690 -2.1438 217.7233 219.8671 269.8495 58.2305 -2.1444 217.9171 220.0614 269.9851 59.0830 -2.1453 218.1572 220.3026 270.1228 59.8750 -2.1427 218.3907 220.5335 270.2509 60.7580 -2.1417 218.6246 220.7663 270.3842 61.6100 -2.1377 218.8598 220.9975 270.5290 62.4920 -2.1387 219.0826 221.2213 270.6653 63.2538 -2.1389 219.2864 221.4253 270.7660 64.0758 -2.1368 219.5470 221.6838 270.8742 64.8978 -2.1337 219.7553 221.8890 270.9968 65.6595 -2.1343 219.9427 222.0769 271.1173 66.5118 -2.1343 220.1727 222.3070 271.2525 67.2700 -2.1357 220.3975 222.5332 271.3595 68.0890 -2.1314 220.6339 222.7653 271.4868 68.9040 -2.1289 220.8608 222.9897 271.5898 69.6640 -2.1288 221.0413 223.1701 271.6995 70.5120 -2.1277 221.2666 223.3944 271.8338 71.2688 -2.1290 221.4585 223.5875 271.9225 72.0938 -2.1233 221.6728 223.7961 272.0282 72.8900 -2.1196 221.8865 224.0061 272.1457 73.6780 -2.1167 222.0968 224.2135 272.2338 74.4968 -2.1191 222.3279 224.4470 272.3412 75.2853 -2.1213 222.5343 224.6555 272.4604 76.1040 -2.1172 222.7517 224.8690 272.5838 76.8920 -2.1160 222.9601 225.0761 272.6844 77.6800 -2.1146 223.1680 225.2826 272.7987 78.4983 -2.1120 223.3812 225.4932 272.9130 79.2873 -2.1138 223.5776 225.6914 273.0301 80.1668 -2.1108 223.8346 225.9454 273.1469 81.0460 -2.1095 224.0635 226.1730 273.2793 81.8953 -2.1090 224.2792 226.3882 273.3991 82.6753 -2.1086 224.4676 226.5762 273.5137 83.4953 -2.1069 224.6895 226.7964 273.6460 84.2555 -2.1088 224.8877 226.9965 273.7378 85.1075 -2.1068 225.1181 227.2250 273.8746 85.8695 -2.1038 225.3049 227.4087 273.9846 86.6905 -2.1135 225.5133 227.6268 274.1001 87.5115 -2.1457 225.7520 227.8977 274.2305 88.2735 -2.1505 225.9471 228.0976 274.3573 89.1255 -2.1399 226.1919 228.3318 274.4796 89.8875 -2.1117 226.3630 228.4746 274.5930 90.7095 -2.0956 226.5765 228.6721 274.7251 91.5615 -2.0949 226.7949 228.8897 274.8656 92.3285 -2.0926 226.9941 229.0867 274.9965 93.1685 -2.0867 227.2138 229.3005 275.1251 93.9305 -2.0873 227.4076 229.4949 275.2602 94.7525 -2.0880 227.6101 229.6981 275.3891 95.5445 -2.0899 227.8253 229.9152 275.5285 96.3365 -2.0882 228.0243 230.1125 275.6798 97.1585 -2.0843 228.2270 230.3114 275.7964 97.9505 -2.0829 228.4227 230.5056 275.9327 98.7725 -2.0873 228.6384 230.7257 276.0966 99.5645 -2.0871 228.8282 230.9153 276.2288 100.3563 -2.0857 229.0443 231.1300 276.3893 101.2085 -2.0837 229.2495 231.3332 276.5395 101.9700 -2.0868 229.4186 231.5054 276.6564 102.7923 -2.0847 229.6279 231.7126 276.8027 103.5845 -2.0811 229.8366 231.9178 276.9669 104.3758 -2.0838 230.0593 232.1431 277.1139 105.1983 -2.0848 230.2476 232.3324 277.2712 105.9900 -2.0843 230.4405 232.5248 277.4106 106.8118 -2.0832 230.6537 232.7368 277.5682 107.6040 -2.0809 230.8450 232.9259 277.7132 108.3955 -2.0844 231.0468 233.1312 277.8549 109.2180 -2.0795 231.2456 233.3251 278.0167 110.0098 -2.0689 231.4492 233.5181 278.1709 110.8318 -2.0644 231.6593 233.7237 278.3319 111.6240 -2.0606 231.8396 233.9002 278.4844 112.4155 -2.0605 232.0386 234.0990 278.6241 113.2380 -2.0596 232.2569 234.3165 278.7505 114.0298 -2.0613 232.4559 234.5172 278.9104 114.8518 -2.0602 232.6367 234.6970 279.0519 115.6440 -2.0602 232.8494 234.9096 279.1894 116.4355 -2.0618 233.0359 235.0978 279.3156 117.2578 -2.0623 233.2250 235.2873 279.4715 118.0195 -2.0586 233.4062 235.4648 279.6067 118.8718 -2.0618 233.6438 235.7056 279.7668 119.6635 -2.0613 233.8371 235.8985 279.9064 120.4555 -2.0624 234.0057 236.0680 280.0278 121.2775 -2.0637 234.2116 236.2753 280.1659 122.0395 -2.0654 234.3790 236.4444 280.3007 122.8915 -2.0621 234.6105 236.6726 280.4292 123.6678 -2.0608 234.7834 236.8442 280.5833 124.4895 -2.0587 234.9795 237.0381 280.7095 125.2815 -2.0640 235.2119 237.2759 280.8503 126.0735 -2.0631 235.3875 237.4506 280.9940 126.9260 -2.0648 235.5778 237.6425 281.1074 127.6885 -2.0659 235.7740 237.8398 281.2438 128.5105 -2.0626 235.9655 238.0280 281.3735 129.3025 -2.0668 236.1512 238.2180 281.5168 130.0945 -2.0651 236.3531 238.4182 281.6457 130.9458 -2.0672 236.5524 238.6197 281.7668 131.7040 -2.0700 236.7239 238.7940 281.9015 132.5228 -2.0685 236.9072 238.9757 282.0068 133.3118 -2.0670 237.1020 239.1689 282.1413 134.1030 -2.0695 237.2784 239.3479 282.2864 134.9228 -2.0732 237.4657 239.5388 282.4134 135.7110 -2.0747 237.6943 239.7690 282.5297 136.5288 -2.0730 237.8762 239.9492 282.6389 137.3170 -2.0709 238.0772 240.1481 282.7767 138.1055 -2.0705 238.2604 240.3308 282.9109 138.9553 -2.0732 238.4395 240.5128 283.0417 139.7140 -2.0721 238.6259 240.6980 283.1591 140.5325 -2.0811 238.8436 240.9247 283.2761 141.3508 -2.0843 239.0418 241.1261 283.3971 142.1088 -2.0863 239.2058 241.2921 283.5230 142.9585 -2.0899 239.3859 241.4758 283.6623 143.7188 -2.0913 239.5933 241.6846 283.7856 144.5385 -2.0900 239.7684 241.8584 283.9035 145.3573 -2.0903 239.9766 242.0669 284.0364 146.1175 -2.0868 240.1424 242.2291 284.1605 146.9675 -2.0875 240.3478 242.4354 284.2524 147.7280 -2.0923 240.5127 242.6050 284.3818 148.5478 -2.0894 240.6884 242.7778 284.5183 149.3685 -2.0904 240.8737 242.9640 284.6379 150.1298 -2.0945 241.0441 243.1387 284.7720 150.9820 -2.0923 241.2720 243.3643 284.8831 151.7440 -2.0901 241.4442 243.5343 284.9921 152.5660 -2.0926 241.6281 243.7207 285.1317 153.3583 -2.0956 241.7937 243.8894 285.2434 154.1495 -2.0974 241.9894 244.0868 285.3645 155.0020 -2.0942 242.1924 244.2866 285.4802 155.7638 -2.0955 242.3688 244.4643 285.6235 156.5858 -2.0952 242.5783 244.6735 285.7539 157.3783 -2.0923 242.7351 244.8274 285.8674 158.1695 -2.0943 242.9281 245.0224 285.9673 158.9920 -2.0935 243.1257 245.2192 286.1093 159.7838 -2.0945 243.2989 245.3933 286.2338 160.6058 -2.0917 243.4753 245.5670 286.3640 161.3980 -2.0952 243.6413 245.7364 286.4849 162.1895 -2.0964 243.8234 245.9198 286.6284 163.0120 -2.0962 244.0212 246.1174 286.7446 163.8038 -2.0963 244.2052 246.3015 286.8687 164.6258 -2.0962 244.3949 246.4910 287.0086 165.4178 -2.0891 244.5727 246.6618 287.1461 166.2095 -2.0824 244.7574 246.8398 287.2705 167.0320 -2.0786 244.9521 247.0307 287.4103 167.7935 -2.0796 245.1293 247.2089 287.5413 168.6460 -2.0781 245.3154 247.3935 287.6934 169.4378 -2.0810 245.4832 247.5642 287.8404 170.2295 -2.0846 245.6598 247.7444 287.9513 171.0518 -2.0857 245.8410 247.9266 288.0785 171.8135 -2.0805 246.0295 248.1099 288.2332 172.6655 -2.0777 246.2013 248.2790 288.3841 173.4575 -2.0801 246.3746 248.4546 288.5153 174.2533 -2.0855 246.5648 248.6503 288.6697 175.0575 -2.0850 246.7424 248.8274 288.8086 175.8495 -2.0872 246.9165 249.0037 288.9403 176.6715 -2.0898 247.1082 249.1980 289.0830 177.4635 -2.0910 247.2989 249.3899 289.2253 178.2855 -2.0892 247.4684 249.5577 289.3644 179.0775 -2.0901 247.6354 249.7255 289.5025 179.8695 -2.0929 247.8189 249.9119 289.6611 180.6915 -2.0931 247.9962 250.0893 289.7927 181.4835 -2.0944 248.1829 250.2773 289.9438 182.3060 -2.0946 248.3638 250.4584 290.0961 183.0983 -2.0946 248.5377 250.6323 290.2391 183.8900 -2.0955 248.7063 250.8018 290.3746 184.7123 -2.0948 248.8772 250.9720 290.5118 185.5038 -2.0964 249.0621 251.1586 290.6622 186.3258 -2.1004 249.2533 251.3538 290.8069 187.1180 -2.1009 249.4147 251.5156 290.9763 187.9105 -2.0989 249.5759 251.6748 291.1009 188.7630 -2.1044 249.7929 251.8973 291.2613 189.5248 -2.1033 249.9625 252.0658 291.3847 190.3475 -2.1009 250.1150 252.2158 291.5348 191.1403 -2.1094 250.2931 252.4025 291.6910 191.9315 -2.1122 250.4960 252.6082 291.8157 192.7838 -2.1063 250.6948 252.8012 291.9673 193.5458 -2.1102 250.8479 252.9581 292.0927 194.3678 -2.1139 251.0143 253.1283 292.2382 195.1600 -2.1116 251.1844 253.2961 292.3665 195.9508 -2.1117 251.3624 253.4741 292.5021 196.7990 -2.1140 251.5396 253.6535 292.6275 197.5570 -2.1153 251.7074 253.8227 292.7433 198.3750 -2.1147 251.8867 254.0014 292.8833 199.1930 -2.1135 252.0641 254.1776 293.0379 199.9510 -2.1155 252.2339 254.3494 293.1592 200.8000 -2.1187 252.4318 254.5505 293.2799 201.5583 -2.1183 252.5576 254.6759 293.3874 202.3760 -2.1222 252.7270 254.8493 293.5161 203.1940 -2.1177 252.9268 255.0445 293.6505 203.9520 -2.1243 253.0906 255.2149 293.7686 204.8005 -2.1207 253.2844 255.4051 293.8939 205.5520 -2.1235 253.4262 255.5498 294.0366 206.4020 -2.1258 253.6046 255.7305 294.1679 207.1905 -2.1235 253.7764 255.9000 294.2693 207.9790 -2.1265 253.9493 256.0758 294.3556 208.7983 -2.1341 254.1233 256.2574 294.4981 209.5873 -2.1346 254.3161 256.4507 294.5998 210.4063 -2.1309 254.4889 256.6198 294.7157 211.1963 -2.1338 254.6397 256.7735 294.8246 211.9868 -2.1361 254.8167 256.9528 294.9886 212.8075 -2.1365 254.9771 257.1136 295.1167 213.5988 -2.1382 255.1467 257.2849 295.2435 214.4180 -2.1369 255.3263 257.4632 295.3661 215.2095 -2.1401 255.4974 257.6375 295.4590 216.0015 -2.1381 255.6901 257.8282 295.5947 216.8238 -2.1389 255.8784 258.0173 295.7203 217.5855 -2.1396 256.0258 258.1654 295.8291 218.4378 -2.1402 256.1902 258.3304 295.9836 219.1995 -2.1414 256.3362 258.4776 296.0950 220.0215 -2.1440 256.5153 258.6594 296.2201 220.8435 -2.1438 256.6887 258.8325 296.3450 221.6055 -2.1474 256.8404 258.9878 296.4542 222.4575 -2.1451 257.0145 259.1596 296.6072 223.2195 -2.1439 257.1847 259.3286 296.7292 224.0415 -2.1438 257.3606 259.5044 296.9036 224.8335 -2.1459 257.5304 259.6764 297.0128 225.6278 -2.1490 257.7156 259.8646 297.1270 226.4515 -2.1498 257.8662 260.0160 297.2633 227.2435 -2.1525 258.0277 260.1802 297.3929 228.0655 -2.1518 258.2211 260.3729 297.5364 228.8575 -2.1540 258.3688 260.5229 297.6634 229.6495 -2.1587 258.5375 260.6963 297.7954 230.4715 -2.1615 258.7132 260.8747 297.9521 231.2635 -2.1639 258.8753 261.0391 298.0915 232.0855 -2.1637 259.0464 261.2102 298.2323 232.8773 -2.1685 259.2192 261.3877 298.3598 233.6690 -2.1676 259.3763 261.5438 298.4917 234.4913 -2.1637 259.5732 261.7369 298.6086 235.2835 -2.1649 259.7410 261.9058 298.7514 236.1050 -2.1658 259.9065 262.0723 298.8805 236.8975 -2.1654 260.0652 262.2306 299.0184 237.6885 -2.1729 260.2352 262.4081 299.1666 238.5110 -2.1740 260.4061 262.5801 299.3085 239.3028 -2.1766 260.5542 262.7308 299.4500 240.1248 -2.1760 260.7146 262.8906 299.5893 240.9170 -2.1764 260.8616 263.0381 299.7222 241.7085 -2.1783 261.0352 263.2135 299.8647 242.5310 -2.1791 261.2021 263.3812 299.9930 243.3228 -2.1766 261.3775 263.5542 300.1212 244.1448 -2.1772 261.5567 263.7339 300.2704 244.9370 -2.1804 261.7203 263.9007 300.4044 245.7295 -2.1800 261.8854 264.0654 300.5486 246.5523 -2.1786 262.0438 264.2224 300.6817 247.3445 -2.1842 262.1989 264.3831 300.8120 248.1668 -2.1845 262.3933 264.5778 300.9483 248.9588 -2.1886 262.5563 264.7450 301.0855 249.7515 -2.1896 262.7066 264.8962 301.2451 250.5738 -2.1891 262.8700 265.0591 301.3546 251.3655 -2.1920 263.0485 265.2405 301.4939 252.1875 -2.1939 263.1967 265.3906 301.6427 252.9795 -2.1936 263.3708 265.5645 301.7838 253.7715 -2.1965 263.5390 265.7355 301.9363 254.6235 -2.1993 263.7194 265.9188 302.0930 255.3855 -2.1990 263.8729 266.0719 302.2080 256.2075 -2.2021 264.0323 266.2344 302.3612 256.9995 -2.2018 264.1730 266.3748 302.4777 257.7915 -2.2055 264.3209 266.5265 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