DTA measure 1Fel_2.dat Date: 2024108:1219 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1113.86 s Mass = 951.000 mg data_number = 1384 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2225 -1.6068 230.0259 231.6327 261.6388 2.0745 -1.6031 230.1506 231.7537 261.6085 2.8365 -1.5954 230.2698 231.8652 261.6213 3.6585 -1.5571 230.3994 231.9565 261.6108 4.4805 -1.5508 230.4997 232.0505 261.6043 5.2425 -1.5956 230.6273 232.2230 261.6020 6.0945 -1.5901 230.7703 232.3604 261.5984 6.8563 -1.5975 230.8766 232.4741 261.6106 7.6780 -1.5625 231.0112 232.5736 261.6045 8.5000 -1.5406 231.1450 232.6856 261.6318 9.2615 -1.5365 231.2543 232.7908 261.6508 10.1140 -1.5322 231.3857 232.9179 261.6998 10.8758 -1.5277 231.4982 233.0258 261.7378 11.6978 -1.5744 231.6225 233.1969 261.7719 12.5203 -1.5790 231.7571 233.3361 261.8039 13.2825 -1.5741 231.8669 233.4410 261.8552 14.1350 -1.5486 231.9937 233.5423 261.9151 14.9270 -1.5242 232.1277 233.6519 261.9788 15.7193 -1.5142 232.2547 233.7689 262.0498 16.5720 -1.5112 232.3828 233.8940 262.1132 17.3338 -1.5296 232.5065 234.0361 262.2038 18.1558 -1.5877 232.6086 234.1963 262.2902 18.9780 -1.5693 232.7234 234.2927 262.3787 19.7405 -1.5592 232.8525 234.4117 262.4750 20.5928 -1.5156 232.9953 234.5110 262.5718 21.3495 -1.5089 233.0763 234.5852 262.6834 22.1700 -1.5094 233.2029 234.7123 262.7945 22.9880 -1.5001 233.3234 234.8234 262.9101 23.7460 -1.4896 233.4607 234.9502 263.0197 24.5940 -1.4833 233.5811 235.0644 263.1690 25.3510 -1.4824 233.6923 235.1747 263.2837 26.1700 -1.4852 233.8035 235.2887 263.4103 26.9580 -1.4811 233.9145 235.3957 263.5476 27.7470 -1.4792 234.0391 235.5183 263.6802 28.5955 -1.4815 234.1744 235.6558 263.8239 29.3540 -1.4836 234.2838 235.7674 263.9814 30.1720 -1.4799 234.4076 235.8875 264.1144 30.9603 -1.4820 234.5071 235.9891 264.2324 31.7490 -1.4812 234.6355 236.1167 264.3752 32.5975 -1.4769 234.7614 236.2383 264.5525 33.3563 -1.4774 234.8748 236.3522 264.7091 34.1760 -1.4794 234.9997 236.4791 264.8562 34.9645 -1.4793 235.1464 236.6257 265.0266 35.7550 -1.4828 235.2566 236.7394 265.1875 36.6048 -1.4785 235.3696 236.8481 265.3366 37.3650 -1.4753 235.4910 236.9664 265.4674 38.1858 -1.4787 235.6197 237.0985 265.6553 39.0043 -1.4806 235.7210 237.2016 265.8096 39.7655 -1.4798 235.8444 237.3243 265.9465 40.6175 -1.4817 235.9697 237.4513 266.1086 41.3798 -1.4827 236.0839 237.5667 266.2558 42.2015 -1.4827 236.2062 237.6889 266.4084 42.9935 -1.4839 236.3257 237.8096 266.5500 43.7855 -1.4813 236.4477 237.9290 266.6853 44.6075 -1.4812 236.5851 238.0663 266.8420 45.3995 -1.4808 236.6965 238.1773 266.9714 46.2215 -1.4827 236.8267 238.3094 267.1329 47.0135 -1.4853 236.9338 238.4191 267.2802 47.8055 -1.4854 237.0635 238.5489 267.4053 48.6275 -1.4841 237.1653 238.6495 267.5540 49.3895 -1.4852 237.2750 238.7602 267.6853 50.2415 -1.4831 237.4043 238.8874 267.8204 51.0335 -1.4894 237.5325 239.0219 267.9522 51.8255 -1.4921 237.6455 239.1376 268.0922 52.6475 -1.4932 237.7868 239.2800 268.2358 53.4095 -1.4952 237.8999 239.3951 268.3482 54.2615 -1.4979 238.0164 239.5143 268.4555 55.0535 -1.4975 238.1342 239.6317 268.5819 55.8455 -1.4973 238.2604 239.7576 268.7064 56.6728 -1.4954 238.3832 239.8786 268.8318 57.4413 -1.4976 238.4959 239.9935 268.9310 58.2930 -1.4980 238.6298 240.1278 269.0473 59.0553 -1.4992 238.7426 240.2419 269.1516 59.8768 -1.4984 238.8869 240.3853 269.2729 60.6990 -1.5001 238.9957 240.4958 269.3748 61.4605 -1.5007 239.1067 240.6074 269.4751 62.3130 -1.4975 239.2302 240.7277 269.5786 63.0748 -1.5036 239.3364 240.8400 269.6694 63.8968 -1.5016 239.4720 240.9736 269.7591 64.7190 -1.5051 239.5874 241.0924 269.8661 65.4805 -1.5079 239.7045 241.2124 269.9525 66.3330 -1.5053 239.8254 241.3307 270.0282 67.0963 -1.5049 239.9703 241.4752 270.1242 67.9198 -1.5045 240.0905 241.5950 270.2203 68.7420 -1.5077 240.1891 241.6968 270.3056 69.5035 -1.5100 240.2908 241.8008 270.4082 70.3560 -1.5034 240.4424 241.9458 270.4748 71.1178 -1.5034 240.5360 242.0394 270.5446 71.9398 -1.5035 240.6656 242.1691 270.6312 72.7618 -1.5052 240.7873 242.2926 270.7367 73.5235 -1.5092 240.9007 242.4099 270.7913 74.3758 -1.5088 241.0319 242.5407 270.8836 75.1675 -1.5092 241.1533 242.6626 270.9801 75.9595 -1.5116 241.2848 242.7964 271.0587 76.7815 -1.5093 241.3958 242.9051 271.1474 77.5485 -1.5049 241.5099 243.0148 271.2245 78.4005 -1.5079 241.6477 243.1556 271.3139 79.1925 -1.5094 241.7567 243.2661 271.4058 79.9855 -1.5146 241.8737 243.3883 271.5061 80.8078 -1.5094 242.0070 243.5164 271.5823 81.5705 -1.5107 242.1028 243.6135 271.6667 82.4225 -1.5170 242.2366 243.7537 271.7559 83.2145 -1.5169 242.3544 243.8713 271.8477 84.0075 -1.5143 242.4810 243.9953 271.9436 84.8293 -1.5124 242.6065 244.1189 272.0047 85.5870 -1.5144 242.7240 244.2384 272.1012 86.4355 -1.5155 242.8466 244.3621 272.2322 87.2233 -1.5147 242.9578 244.4724 272.3046 88.0115 -1.5191 243.0867 244.6059 272.3894 88.8298 -1.5194 243.1924 244.7118 272.4937 89.5875 -1.5172 243.3029 244.8201 272.5699 90.4365 -1.5148 243.4251 244.9399 272.6715 91.2250 -1.5149 243.5557 245.0706 272.7651 92.0125 -1.5163 243.6737 245.1901 272.8731 92.8315 -1.5170 243.8101 245.3271 272.9840 93.5900 -1.5142 243.9045 245.4187 273.0894 94.4385 -1.5086 244.0096 245.5182 273.1932 95.2268 -1.5084 244.1318 245.6402 273.3101 96.0168 -1.5110 244.2405 245.7515 273.4037 96.8353 -1.5137 244.3614 245.8752 273.5097 97.5945 -1.5147 244.4843 245.9991 273.6169 98.4450 -1.5128 244.6075 246.1203 273.7509 99.2340 -1.5156 244.7150 246.2305 273.8653 100.0233 -1.5187 244.8424 246.3611 273.9607 100.8428 -1.5232 244.9660 246.4891 274.0776 101.6038 -1.5252 245.0899 246.6151 274.2024 102.4553 -1.5259 245.2173 246.7431 274.3148 103.2175 -1.5335 245.3274 246.8610 274.4236 104.0388 -1.5369 245.4289 246.9659 274.5167 104.8313 -1.5387 245.5535 247.0922 274.6209 105.6225 -1.5381 245.6687 247.2068 274.7489 106.4753 -1.5389 245.7980 247.3369 274.8705 107.2368 -1.5439 245.9215 247.4654 274.9648 108.0588 -1.5402 246.0247 247.5649 275.0850 108.8510 -1.5400 246.1402 247.6802 275.2004 109.6425 -1.5417 246.2695 247.8111 275.2989 110.4650 -1.5446 246.3774 247.9220 275.4156 111.2265 -1.5488 246.4928 248.0416 275.5251 112.0790 -1.5510 246.6079 248.1589 275.6599 112.8710 -1.5483 246.7349 248.2832 275.7572 113.6625 -1.5487 246.8454 248.3941 275.8697 114.4850 -1.5471 246.9711 248.5182 276.0107 115.2465 -1.5462 247.0764 248.6226 276.1200 116.0990 -1.5476 247.1897 248.7373 276.2212 116.8608 -1.5471 247.3295 248.8766 276.3432 117.6828 -1.5476 247.4578 249.0054 276.4505 118.5048 -1.5508 247.5617 249.1125 276.5577 119.2665 -1.5533 247.6770 249.2302 276.6692 120.1190 -1.5541 247.7871 249.3411 276.7840 120.8808 -1.5524 247.9064 249.4589 276.8810 121.7028 -1.5565 248.0325 249.5889 277.0001 122.5245 -1.5544 248.1646 249.7190 277.1180 123.2865 -1.5574 248.2784 249.8358 277.2041 124.1388 -1.5577 248.3952 249.9529 277.3260 124.9010 -1.5567 248.5133 250.0699 277.4368 125.7235 -1.5583 248.6032 250.1615 277.5601 126.5455 -1.5603 248.7483 250.3086 277.6836 127.3075 -1.5621 248.8722 250.4343 277.7754 128.1595 -1.5635 248.9891 250.5526 277.9003 128.9215 -1.5630 249.0930 250.6560 277.9964 129.7435 -1.5655 249.2404 250.8058 278.1103 130.5655 -1.5664 249.3542 250.9206 278.2137 131.3275 -1.5678 249.4536 251.0214 278.3282 132.1795 -1.5684 249.5770 251.1454 278.4345 132.9415 -1.5705 249.6814 251.2519 278.5463 133.7635 -1.5703 249.7926 251.3629 278.6591 134.5855 -1.5726 249.9122 251.4848 278.7732 135.3475 -1.5742 250.0355 251.6097 278.8723 136.1993 -1.5779 250.1541 251.7319 278.9975 136.9913 -1.5780 250.2626 251.8405 279.0997 137.7835 -1.5764 250.3794 251.9557 279.2039 138.6053 -1.5779 250.4911 252.0690 279.3065 139.3665 -1.5741 250.6060 252.1801 279.4179 140.2190 -1.5787 250.7364 252.3151 279.5322 141.0110 -1.5858 250.8642 252.4500 279.6708 141.8025 -1.5881 250.9977 252.5858 279.7403 142.6250 -1.5866 251.1095 252.6960 279.8495 143.4168 -1.5902 251.1971 252.7872 279.9702 144.2395 -1.5919 251.3064 252.8983 280.0678 145.0320 -1.5909 251.4234 253.0143 280.1703 145.8245 -1.5908 251.5474 253.1382 280.2635 146.6470 -1.5957 251.6833 253.2790 280.3651 147.4388 -1.5953 251.7995 253.3948 280.4562 148.2608 -1.5946 251.9132 253.5078 280.5558 149.0508 -1.5963 252.0286 253.6249 280.6512 149.8390 -1.5975 252.1418 253.7393 280.7440 150.6570 -1.5968 252.2717 253.8685 280.8483 151.4450 -1.6000 252.3854 253.9854 280.9372 152.2640 -1.6030 252.5047 254.1077 281.0399 153.0520 -1.6027 252.6020 254.2047 281.0956 153.8400 -1.6055 252.7313 254.3368 281.1911 154.6580 -1.6068 252.8479 254.4547 281.3021 155.4460 -1.6092 252.9721 254.5813 281.3745 156.2648 -1.6085 253.0859 254.6944 281.4524 157.0533 -1.6110 253.1964 254.8075 281.5804 157.8420 -1.6209 253.3373 254.9583 281.6595 158.6608 -1.6267 253.4360 255.0628 281.7615 159.4278 -1.6333 253.5479 255.1812 281.8540 160.2780 -1.6326 253.6622 255.2949 281.9613 161.0660 -1.6345 253.7698 255.4043 282.0681 161.8550 -1.6387 253.9094 255.5481 282.1404 162.6740 -1.6411 254.0233 255.6643 282.2373 163.4330 -1.6498 254.1256 255.7754 282.3425 164.2838 -1.6595 254.2464 255.9060 282.4389 165.0725 -1.6597 254.3323 255.9920 282.5356 165.8620 -1.6634 254.4556 256.1190 282.6263 166.6818 -1.6663 254.5799 256.2462 282.7115 167.4435 -1.6652 254.7058 256.3711 282.8150 168.2938 -1.6647 254.8099 256.4746 282.9243 169.0858 -1.6715 254.9293 256.6007 283.0361 169.8775 -1.6727 255.0452 256.7179 283.1327 170.6995 -1.6706 255.1673 256.8379 283.2328 171.4615 -1.6702 255.2701 256.9404 283.3305 172.3135 -1.6687 255.3842 257.0529 283.4375 173.0758 -1.6708 255.4987 257.1696 283.5374 173.8975 -1.6733 255.6345 257.3078 283.6210 174.6895 -1.6755 255.7415 257.4170 283.7269 175.4815 -1.6760 255.8573 257.5333 283.8127 176.3335 -1.6892 255.9779 257.6672 283.9298 177.0955 -1.7171 256.0754 257.7924 284.0312 177.9775 -1.7330 256.2187 257.9517 284.1415 178.8895 -1.7004 256.3412 258.0417 284.2761 179.6515 -1.6845 256.4713 258.1558 284.3648 180.4735 -1.6875 256.5898 258.2773 284.4698 181.2655 -1.6914 256.6754 258.3668 284.5679 182.0575 -1.6929 256.8039 258.4968 284.6699 182.8795 -1.6956 256.9116 258.6072 284.7582 183.6715 -1.6986 257.0286 258.7273 284.8540 184.4935 -1.6962 257.1467 258.8429 284.9836 185.2855 -1.6935 257.2627 258.9562 285.0673 186.1375 -1.6970 257.4181 259.1151 285.1654 186.9288 -1.6968 257.5251 259.2220 285.2739 187.7513 -1.6897 257.6090 259.2987 285.3974 188.5128 -1.6858 257.7154 259.4012 285.4985 189.3650 -1.6833 257.8512 259.5345 285.6065 190.1268 -1.6796 257.9566 259.6362 285.6934 190.9488 -1.7005 258.0782 259.7787 285.8312 191.7710 -1.7143 258.1967 259.9110 285.9425 192.5325 -1.7399 258.3127 260.0526 286.0486 193.3850 -1.7322 258.4264 260.1587 286.1647 194.1770 -1.7185 258.5537 260.2722 286.2770 194.9685 -1.7158 258.6450 260.3609 286.4170 195.7910 -1.7184 258.7686 260.4870 286.5383 196.5525 -1.7237 258.8714 260.5951 286.6510 197.4050 -1.7294 258.9899 260.7193 286.7670 198.1970 -1.7414 259.1107 260.8521 286.8635 198.9885 -1.7470 259.2260 260.9729 286.9894 199.8123 -1.7674 259.3479 261.1153 287.1128 200.5778 -1.7902 259.4435 261.2337 287.2175 201.4298 -1.7988 259.5719 261.3707 287.3485 202.2218 -1.7953 259.6916 261.4869 287.4643 203.0135 -1.7979 259.7946 261.5925 287.5827 203.8358 -1.7995 259.9169 261.7163 287.7178 204.6275 -1.7990 260.0164 261.8155 287.8225 205.4495 -1.7984 260.1478 261.9463 287.9457 206.2415 -1.7989 260.2519 262.0508 288.0572 207.0345 -1.8013 260.3635 262.1648 288.1860 207.8568 -1.8060 260.4922 262.2982 288.2961 208.6495 -1.8082 260.6024 262.4106 288.3902 209.4715 -1.8110 260.7215 262.5325 288.5035 210.2635 -1.8115 260.8323 262.6439 288.6122 211.0565 -1.8107 260.9311 262.7419 288.7370 211.8785 -1.8085 261.0703 262.8788 288.8284 212.6705 -1.8102 261.1933 263.0036 288.9245 213.4933 -1.8109 261.3066 263.1175 289.0465 214.2838 -1.8141 261.4219 263.2359 289.1653 215.0713 -1.8150 261.5234 263.3384 289.2633 215.8908 -1.8172 261.6501 263.4674 289.3771 216.6788 -1.8183 261.7638 263.5821 289.4922 217.4968 -1.8229 261.8739 263.6968 289.5813 218.2848 -1.8251 261.9724 263.7975 289.6879 219.0730 -1.8297 262.0970 263.9267 289.7809 219.8910 -1.8321 262.2108 264.0428 289.8786 220.6788 -1.8324 262.3327 264.1651 289.9717 221.4978 -1.8337 262.4466 264.2803 290.0718 222.2860 -1.8352 262.5644 264.3996 290.1606 223.0738 -1.8363 262.6849 264.5213 290.2713 223.8920 -1.8372 262.7873 264.6245 290.4029 224.6800 -1.8386 262.8851 264.7237 290.4943 225.4983 -1.8395 262.9978 264.8373 290.5970 226.2875 -1.8432 263.1012 264.9444 290.6806 227.0783 -1.8482 263.2299 265.0781 290.7981 227.8978 -1.8497 263.3552 265.2048 290.8836 228.6870 -1.8505 263.4650 265.3155 290.9838 229.5070 -1.8495 263.5841 265.4335 291.0885 230.2970 -1.8522 263.7052 265.5574 291.1883 231.0870 -1.8574 263.8145 265.6720 291.2757 231.9085 -1.8607 263.9359 265.7965 291.3771 232.6685 -1.8620 264.0388 265.9008 291.4611 233.5200 -1.8616 264.1712 266.0329 291.5805 234.2820 -1.8601 264.2718 266.1319 291.6620 235.1040 -1.8615 264.3871 266.2487 291.7606 235.9263 -1.8650 264.4982 266.3631 291.8539 236.6875 -1.8665 264.6047 266.4712 291.9581 237.5403 -1.8692 264.7307 266.5999 292.0549 238.3018 -1.8719 264.8366 266.7084 292.1586 239.1238 -1.8692 264.9512 266.8203 292.2436 239.9168 -1.8691 265.0589 266.9281 292.3286 240.7095 -1.8709 265.1909 267.0618 292.4135 241.5320 -1.8719 265.3080 267.1799 292.5345 242.3238 -1.8763 265.4091 267.2854 292.6255 243.1458 -1.8823 265.5191 267.4015 292.7254 243.9380 -1.8833 265.6364 267.5197 292.8283 244.7295 -1.8841 265.7439 267.6280 292.9355 245.5520 -1.8831 265.8520 267.7351 293.0288 246.3135 -1.8836 265.9779 267.8616 293.1198 247.1660 -1.8882 266.0822 267.9705 293.2334 247.9580 -1.8909 266.1971 268.0879 293.3475 248.7495 -1.8927 266.3153 268.2080 293.4510 249.5718 -1.8902 266.4390 268.3292 293.5540 250.3335 -1.8910 266.5543 268.4453 293.6585 251.1858 -1.8940 266.6656 268.5596 293.7749 251.9778 -1.8952 266.7735 268.6686 293.8764 252.7695 -1.8992 266.8980 268.7972 293.9776 253.5915 -1.9014 267.0095 268.9110 294.0796 254.3535 -1.9016 267.1186 269.0202 294.1956 255.2055 -1.9061 267.2509 269.1570 294.3150 255.9675 -1.9243 267.3441 269.2684 294.4218 256.7895 -1.9459 267.4561 269.4021 294.5607 257.6115 -1.9533 267.5621 269.5155 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