DTA measure 2Fel_1.dat Date: 2024108:1151 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.02 s Mass = 951.000 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3034 -4.2740 410.7243 414.9983 419.8636 3.9115 -4.3171 410.8421 415.1592 419.9074 5.5043 -4.3307 410.9900 415.3207 419.9413 7.1271 -4.3568 411.1369 415.4937 419.9571 8.7245 -4.3376 411.2496 415.5872 419.9763 10.3233 -4.3226 411.3638 415.6864 419.9449 11.9221 -4.3364 411.5032 415.8396 419.8990 13.5348 -4.3151 411.6162 415.9313 419.8378 15.1489 -4.2858 411.7513 416.0371 419.7498 16.7479 -4.2825 411.8738 416.1563 419.6500 18.3633 -4.2468 411.9936 416.2404 419.5289 19.9638 -4.2424 412.1016 416.3440 419.3869 21.5628 -4.2393 412.2263 416.4657 419.2450 23.1769 -4.2327 412.3429 416.5757 419.0578 24.7909 -4.2286 412.4560 416.6846 418.8764 26.3898 -4.2167 412.5538 416.7705 418.6693 28.0036 -4.2122 412.6692 416.8814 418.4612 29.6026 -4.2074 412.7694 416.9768 418.2665 31.2166 -4.1959 412.8805 417.0763 418.0442 32.8306 -4.1892 412.9759 417.1651 417.7991 34.4295 -4.1729 413.0860 417.2589 417.5776 36.0439 -4.1530 413.1814 417.3344 417.3507 37.6435 -4.1421 413.2595 417.4017 417.1049 39.2581 -4.1298 413.3456 417.4754 416.8501 40.8725 -4.1224 413.4426 417.5650 416.6260 42.4865 -4.1131 413.5422 417.6553 416.3839 44.0853 -4.1005 413.6212 417.7217 416.1265 45.6843 -4.0918 413.6811 417.7729 415.9208 47.3129 -4.0825 413.7629 417.8454 415.6643 48.9270 -4.0698 413.8406 417.9103 415.4351 50.5268 -4.0614 413.8887 417.9501 415.2156 52.1261 -4.0557 413.9701 418.0258 414.9835 53.7450 -4.0522 414.0367 418.0889 414.7430 55.3461 -4.0767 414.1049 418.1816 414.5105 56.9521 -4.0270 414.1643 418.1913 414.3182 58.5430 -4.0122 414.2214 418.2335 414.1113 60.1491 -4.0005 414.2703 418.2708 413.8664 61.7400 -3.9899 414.3237 418.3136 413.6674 63.3460 -3.9773 414.3682 418.3455 413.4511 64.9523 -3.9618 414.4150 418.3768 413.2484 66.5590 -3.9483 414.4607 418.4090 413.0501 68.1956 -3.9401 414.5063 418.4463 412.8666 69.8030 -3.9285 414.5404 418.4689 412.6427 71.3981 -3.9205 414.5644 418.4849 412.4741 73.0084 -3.9046 414.6078 418.5124 412.2589 74.6038 -3.8952 414.6159 418.5111 412.0795 76.2165 -3.8842 414.6732 418.5573 411.8856 77.8306 -3.8699 414.6956 418.5655 411.7235 79.4295 -3.8600 414.7235 418.5835 411.5276 81.0289 -3.8487 414.7398 418.5886 411.3560 82.6295 -3.8363 414.7511 418.5874 411.2013 84.2445 -3.8215 414.7791 418.6006 411.0293 85.8585 -3.8211 414.7710 418.5921 410.8651 87.4581 -3.8180 414.7778 418.5957 410.6923 89.0735 -3.8080 414.8003 418.6083 410.5409 90.6725 -3.7993 414.7902 418.5895 410.3446 92.2715 -3.7861 414.8124 418.5984 410.1945 93.9003 -3.7638 414.8130 418.5768 410.0274 95.4991 -3.7134 414.8106 418.5241 409.8606 97.1129 -3.6867 414.8207 418.5073 409.6976 98.7118 -3.6916 414.8147 418.5063 409.5337 100.3108 -3.6856 414.8172 418.5028 409.3676 101.9399 -3.6745 414.7929 418.4674 409.1857 103.5389 -3.6646 414.8040 418.4686 409.0036 105.1530 -3.6547 414.7851 418.4398 408.8177 106.7528 -3.6483 414.7682 418.4165 408.6587 108.3516 -3.6396 414.7608 418.4004 408.4756 109.9806 -3.6266 414.7179 418.3445 408.2911 111.5805 -3.6196 414.6969 418.3165 408.0932 113.1945 -3.6110 414.6883 418.2994 407.9017 114.7935 -3.6014 414.6787 418.2801 407.7034 116.3925 -3.5929 414.6282 418.2211 407.5071 118.0215 -3.5858 414.6045 418.1903 407.3217 119.6351 -3.5735 414.5854 418.1589 407.1249 121.2286 -3.5649 414.5590 418.1239 406.9376 122.8193 -3.5542 414.5219 418.0761 406.7591 124.4260 -3.5507 414.5009 418.0515 406.5614 126.0319 -3.5440 414.4571 418.0011 406.3423 127.6389 -3.5312 414.4124 417.9437 406.1609 129.2306 -3.5243 414.3783 417.9026 405.9688 130.8385 -3.5122 414.3202 417.8324 405.7519 132.4314 -3.5041 414.2810 417.7851 405.5647 134.0559 -3.4977 414.2400 417.7377 405.3608 135.6500 -3.4890 414.1868 417.6758 405.1520 137.2619 -3.4808 414.1281 417.6089 404.9502 138.8579 -3.4745 414.0977 417.5722 404.7386 140.4564 -3.4707 414.0616 417.5323 404.5400 142.0721 -3.4624 414.0056 417.4680 404.3349 143.6861 -3.4462 413.9479 417.3941 404.1410 145.2855 -3.4382 413.8771 417.3152 403.9303 146.8880 -3.4312 413.8054 417.2365 403.7269 148.4868 -3.4208 413.7538 417.1746 403.5188 150.1009 -3.4274 413.6955 417.1229 403.3394 151.7149 -3.4273 413.6428 417.0701 403.1240 153.3138 -3.4167 413.5703 416.9870 402.9422 154.9278 -3.4068 413.4959 416.9027 402.7474 156.5268 -3.3923 413.4352 416.8276 402.5602 158.1256 -3.3746 413.3564 416.7310 402.3681 159.7550 -3.3605 413.2831 416.6436 402.1671 161.3536 -3.3480 413.2236 416.5715 401.9881 162.9526 -3.3426 413.1220 416.4646 401.7769 164.5665 -3.3323 413.0375 416.3697 401.5874 166.1660 -3.3217 412.9872 416.3088 401.3875 167.7965 -3.3145 412.9096 416.2241 401.1775 169.3955 -3.3103 412.8191 416.1294 400.9873 170.9976 -3.2996 412.7476 416.0472 400.7806 172.6005 -3.2900 412.6536 415.9436 400.5837 174.2143 -3.2821 412.5850 415.8671 400.3767 175.8295 -3.2723 412.4761 415.7484 400.1770 177.4389 -3.2630 412.4039 415.6669 399.9959 179.0378 -3.2577 412.3206 415.5783 399.7777 180.6521 -3.2496 412.2200 415.4696 399.5759 182.2518 -3.2433 412.1202 415.3635 399.3984 183.8650 -3.2364 412.0191 415.2554 399.2122 185.4715 -3.2271 411.9348 415.1619 399.0256 187.0631 -3.2177 411.8469 415.0646 398.8275 188.6694 -3.2091 411.7481 414.9571 398.6353 190.2610 -3.1935 411.6368 414.8304 398.4548 191.8686 -3.2122 411.5415 414.7537 398.2677 193.4761 -3.1873 411.4489 414.6362 398.0683 195.0834 -3.1687 411.3370 414.5057 397.8876 196.6755 -3.1655 411.2478 414.4133 397.6887 198.2830 -3.1549 411.1393 414.2942 397.4765 199.9069 -3.1481 411.0339 414.1820 397.2866 201.5023 -3.1444 410.9351 414.0794 397.1060 203.0984 -3.1368 410.8355 413.9724 396.8967 204.7118 -3.1300 410.7226 413.8526 396.6993 206.3106 -3.1247 410.6111 413.7358 396.5034 207.9339 -3.1181 410.5098 413.6279 396.2859 209.5329 -3.1102 410.3956 413.5059 396.0938 211.1466 -3.1024 410.2796 413.3819 395.8981 212.7456 -3.0973 410.1814 413.2786 395.6896 214.3445 -3.0878 410.0500 413.1378 395.4878 215.9585 -3.0779 409.9311 413.0089 395.2978 217.5725 -3.0709 409.8162 412.8871 395.0912 219.1865 -3.0664 409.7033 412.7697 394.8936 220.7855 -3.0583 409.5798 412.6381 394.6886 222.3845 -3.0490 409.4655 412.5145 394.5090 223.9985 -3.0420 409.3353 412.3774 394.3072 225.6124 -3.0372 409.2227 412.2599 394.1132 227.2125 -3.0302 409.1012 412.1313 393.9178 228.8158 -3.0151 408.9821 411.9971 393.7229 230.4298 -3.0116 408.8569 411.8685 393.5388 232.0288 -3.0034 408.7512 411.7546 393.3413 233.6429 -2.9983 408.6040 411.6023 393.1338 235.2569 -2.9951 408.4754 411.4704 392.9278 236.8558 -2.9861 408.3562 411.3423 392.7182 238.4548 -2.9801 408.2126 411.1926 392.5178 240.0693 -2.9743 408.0950 411.0693 392.3118 241.6844 -2.9698 407.9597 410.9294 392.0951 243.2836 -2.9652 407.8323 410.7975 391.8881 244.8975 -2.9549 407.7089 410.6637 391.6940 246.4969 -2.9510 407.5652 410.5162 391.4866 248.0953 -2.9429 407.4412 410.3841 391.2624 249.7169 -2.9327 407.2877 410.2204 391.0500 251.3080 -2.9253 407.1580 410.0833 390.8570 252.9150 -2.9219 407.0265 409.9484 390.6426 254.5060 -2.9140 406.8984 409.8124 390.4341 256.0970 -2.9067 406.7652 409.6719 390.2431 257.7193 -2.8929 406.6118 409.5047 390.0321 259.3220 -2.8907 406.4770 409.3677 389.8298 260.9304 -2.8869 406.3329 409.2198 389.6229 262.5240 -2.8804 406.2069 409.0873 389.4290 264.1325 -2.8715 406.0722 408.9437 389.2133 265.7445 -2.8674 405.9221 408.7895 389.0140 267.3573 -2.8595 405.7809 408.6403 388.8211 268.9555 -2.8543 405.6292 408.4835 388.6358 270.5545 -2.8492 405.5089 408.3581 388.4230 272.1534 -2.8450 405.3452 408.1902 388.2288 273.7824 -2.8455 405.1957 408.0412 388.0432 275.3810 -2.8402 405.0441 407.8844 387.8487 276.9948 -2.8340 404.9067 407.7407 387.6482 278.5938 -2.8220 404.7657 407.5876 387.4508 280.1929 -2.8181 404.6179 407.4361 387.2641 281.8219 -2.8134 404.4670 407.2804 387.0453 283.4211 -2.8055 404.2953 407.1007 386.8675 285.0368 -2.7983 404.1699 406.9682 386.6389 286.6356 -2.7968 404.0255 406.8223 386.4359 288.2348 -2.7895 403.8670 406.6565 386.2449 289.8636 -2.7824 403.7112 406.4936 386.0446 291.4776 -2.7787 403.5620 406.3407 385.8382 293.0766 -2.7732 403.4007 406.1739 385.6191 294.6773 -2.7671 403.2458 406.0128 385.4172 296.2765 -2.7630 403.0910 405.8540 385.2237 297.9063 -2.7586 402.9187 405.6773 385.0022 299.5055 -2.7496 402.7796 405.5292 384.8035 301.1045 -2.7427 402.6249 405.3676 384.6029 302.7189 -2.7386 402.4685 405.2071 384.3858 304.3185 -2.7342 402.3140 405.0482 384.2111 305.9323 -2.7310 402.1583 404.8892 384.0037 307.5459 -2.7336 401.9786 404.7122 383.7849 309.1448 -2.7256 401.8218 404.5475 383.5746 310.7588 -2.7130 401.6879 404.4009 383.3867 312.3551 -2.7084 401.5171 404.2256 383.1838 313.9780 -2.6988 401.3705 404.0693 382.9855 315.5693 -2.6937 401.2027 403.8963 382.7786 317.1761 -2.6877 401.0475 403.7351 382.5763 318.7670 -2.6829 400.8791 403.5620 382.3824 320.3581 -2.6769 400.7270 403.4039 382.1771 321.9793 -2.6705 400.5708 403.2414 381.9798 323.5854 -2.6641 400.3904 403.0545 381.7834 325.1791 -2.6626 400.2285 402.8911 381.5845 326.7731 -2.6550 400.0789 402.7339 381.3813 328.3818 -2.6486 399.9013 402.5500 381.1796 329.9938 -2.6417 399.7451 402.3868 380.9601 331.6073 -2.6374 399.5889 402.2263 380.7522 333.2056 -2.6305 399.4141 402.0446 380.5361 334.8055 -2.6209 399.2445 401.8653 380.3155 336.4046 -2.6220 399.0765 401.6985 380.1077 338.0186 -2.6133 398.9212 401.5345 379.9015 339.6329 -2.6011 398.7699 401.3710 379.6825 341.2316 -2.5948 398.5976 401.1924 379.4543 342.8305 -2.5903 398.4108 401.0011 379.2446 344.4445 -2.5852 398.2468 400.8320 379.0506 346.0436 -2.5767 398.0679 400.6446 378.8130 347.6725 -2.5716 397.9025 400.4740 378.5900 349.2715 -2.5652 397.7357 400.3009 378.3806 350.8705 -2.5593 397.5799 400.1392 378.1784 352.4695 -2.5551 397.4013 399.9564 377.9676 354.0835 -2.5497 397.2288 399.7785 377.7533 355.6971 -2.5424 397.0605 399.6030 377.5425 357.3113 -2.5385 396.8882 399.4267 377.3448 358.9098 -2.5344 396.7072 399.2416 377.1324 360.5238 -2.5294 396.5167 399.0462 376.9395 362.1228 -2.5342 396.3739 398.9081 376.7362 363.7520 -2.5222 396.1948 398.7170 376.5216 365.3508 -2.5021 396.0152 398.5173 376.3202 366.9648 -2.4947 395.8402 398.3349 376.1340 368.5641 -2.4910 395.6692 398.1602 375.9113 370.1793 -2.4875 395.4941 397.9816 375.7186 371.7938 -2.4809 395.3230 397.8039 375.5220 373.3935 -2.4755 395.1530 397.6286 375.3156 375.0079 -2.4704 394.9753 397.4457 375.1248 376.6071 -2.4690 394.7890 397.2580 374.9343 378.2150 -2.4586 394.6145 397.0731 374.7362 379.8210 -2.4531 394.4470 396.9001 374.5322 381.4120 -2.4497 394.2763 396.7260 374.3348 383.0180 -2.4446 394.0989 396.5435 374.1327 384.6095 -2.4335 393.9191 396.3526 373.9546 386.2160 -2.4295 393.7410 396.1705 373.7610 387.8238 -2.4264 393.5580 395.9844 373.5585 389.4323 -2.4182 393.3772 395.7954 373.3651 391.0249 -2.4167 393.2114 395.6281 373.1991 392.6181 -2.4122 393.0354 395.4476 373.0044 394.2443 -2.4086 392.8507 395.2594 372.7847 395.8420 -2.4014 392.6665 395.0679 372.5793 397.4410 -2.3985 392.4978 394.8964 372.4004 399.0410 -2.3921 392.3326 394.7247 372.2051 400.6545 -2.3839 392.1428 394.5267 371.9873 402.2535 -2.3813 391.9490 394.3303 371.8182 403.8675 -2.3807 391.7713 394.1520 371.5852 405.4813 -2.3748 391.6132 393.9880 371.3922 407.0800 -2.3681 391.4305 393.7986 371.1963 408.6789 -2.3616 391.2158 393.5774 370.9774 410.2929 -2.3558 391.0468 393.4026 370.7845 411.9091 -2.3530 390.8545 393.2075 370.5745 413.5269 -2.3488 390.6850 393.0338 370.3849 415.1258 -2.3468 390.5163 392.8630 370.1601 416.7248 -2.3457 390.3363 392.6820 369.9877 418.3388 -2.3383 390.1445 392.4829 369.7778 419.9526 -2.3327 389.9573 392.2899 369.5819 421.5669 -2.3247 389.7889 392.1136 369.3854 423.1669 -2.3192 389.6132 391.9323 369.1857 424.7665 -2.3146 389.4181 391.7327 368.9820 426.3814 -2.3138 389.2311 391.5449 368.7884 427.9965 -2.3108 389.0468 391.3576 368.5935 429.6106 -2.3088 388.8807 391.1895 368.3938 431.2108 -2.3082 388.6981 391.0063 368.1941 432.8105 -2.3006 388.5153 390.8159 368.0089 434.4244 -2.2957 388.3287 390.6244 367.7893 436.0393 -2.2935 388.1339 390.4275 367.5908 437.6530 -2.2833 387.9690 390.2524 367.3959 439.2535 -2.2742 387.7855 390.0597 367.1846 440.8516 -2.2713 387.5877 389.8590 366.9706 442.4600 -2.2669 387.4272 389.6941 366.7742 444.0664 -2.2573 387.2571 389.5143 366.5654 445.6721 -2.2519 387.0323 389.2842 366.3550 447.2639 -2.2469 386.8656 389.1125 366.1293 448.8708 -2.2435 386.6811 388.9246 365.9229 450.4629 -2.2386 386.4951 388.7338 365.7101 452.0860 -2.2329 386.3059 388.5388 365.4990 453.6795 -2.2273 386.1170 388.3443 365.2954 455.2888 -2.2229 385.9433 388.1662 365.0960 456.8838 -2.2179 385.7506 387.9685 364.8891 458.4818 -2.2135 385.5623 387.7758 364.6869 460.1110 -2.2126 385.3935 387.6061 364.4638 461.7098 -2.2022 385.2104 387.4126 364.2537 463.3088 -2.1933 385.0185 387.2118 364.0372 464.9229 -2.1947 384.8155 387.0102 363.8417 466.5218 -2.1847 384.6441 386.8288 363.6435 468.1510 -2.1799 384.4499 386.6298 363.4122 469.7496 -2.1783 384.2750 386.4532 363.2010 471.3488 -2.1764 384.0920 386.2684 362.9922 472.9625 -2.1684 383.8905 386.0589 362.7947 474.5616 -2.1663 383.6939 385.8602 362.5984 476.1905 -2.1636 383.5171 385.6807 362.3721 477.7895 -2.1547 383.3489 385.5036 362.1825 479.4035 -2.1424 383.1528 385.2952 361.9646 481.0025 -2.1381 382.9487 385.0868 361.7641 482.6165 -2.1343 382.7592 384.8935 361.5673 484.2305 -2.1284 382.5793 384.7078 361.3658 485.8294 -2.1229 382.3724 384.4953 361.1695 487.4438 -2.1197 382.2039 384.3237 360.9562 489.0430 -2.1145 382.0105 384.1249 360.7474 490.6584 -2.1109 381.8204 383.9313 360.5602 492.2738 -2.1061 381.6369 383.7431 360.3654 493.8735 -2.1016 381.4246 383.5262 360.1602 495.4898 -2.0993 381.2504 383.3497 359.9704 497.0888 -2.0976 381.0634 383.1609 359.7701 498.7028 -2.0897 380.8751 382.9648 359.5706 500.3168 -2.0847 380.6840 382.7686 359.3818 501.9306 -2.0794 380.4882 382.5676 359.1536 503.5300 -2.0747 380.3078 382.3826 358.9540 505.1283 -2.0671 380.1181 382.1852 358.7568 506.7500 -2.0602 379.9239 381.9841 358.5629 508.3410 -2.0595 379.7590 381.8184 358.3556 509.9330 -2.0617 379.5664 381.6281 358.1473 511.5394 -2.0638 379.3643 381.4281 357.9327 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