DTA measure 2meres_updown3 Date: 2025319:940 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.96 s Mass = 925.000 mg data_number = 1027 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4199 -5.5201 440.2518 445.7719 421.3212 4.0426 -5.5285 440.2392 445.7677 421.5201 5.6499 -5.5371 440.2160 445.7531 421.7334 7.2416 -5.5463 440.1951 445.7413 421.9665 8.8488 -5.5556 440.1772 445.7328 422.2221 10.4611 -5.5655 440.1633 445.7288 422.4854 12.0635 -5.5769 440.1521 445.7290 422.7498 13.6759 -5.5883 440.1348 445.7230 423.0157 15.3143 -5.6003 440.1173 445.7176 423.2874 16.9056 -5.6105 440.1008 445.7113 423.5433 18.5129 -5.6210 440.0866 445.7076 423.7939 20.1201 -5.6315 440.0780 445.7095 424.0182 21.7220 -5.6427 440.0622 445.7049 424.2357 23.3345 -5.6532 440.0467 445.7000 424.4399 24.9366 -5.6640 440.0333 445.6972 424.6137 26.5440 -5.6750 440.0244 445.6995 424.7670 28.1668 -5.6865 440.0235 445.7099 424.9003 29.7741 -5.6964 440.0256 445.7220 425.0112 31.3554 -5.7063 440.0214 445.7278 425.0987 32.9524 -5.7158 440.0141 445.7299 425.1559 34.5548 -5.7251 440.0051 445.7302 425.1906 36.1570 -5.7329 440.0029 445.7358 425.2020 37.7644 -5.7410 440.0146 445.7557 425.1812 39.3458 -5.7477 440.0199 445.7676 425.1288 40.9478 -5.7544 440.0192 445.7736 425.0555 42.5706 -5.7615 440.0176 445.7791 424.9585 44.1728 -5.7679 440.0190 445.7869 424.8373 45.7646 -5.7740 440.0221 445.7961 424.6890 47.3666 -5.7793 440.0232 445.8024 424.5063 48.9789 -5.7839 440.0237 445.8076 424.3049 50.5653 -5.7886 440.0257 445.8143 424.0890 52.1778 -5.7928 440.0263 445.8192 423.8469 53.7795 -5.7960 440.0242 445.8202 423.5863 55.3866 -5.7990 440.0207 445.8197 423.3065 56.9783 -5.8007 440.0189 445.8196 422.9990 58.5960 -5.8019 440.0134 445.8153 422.6764 60.2085 -5.8019 440.0086 445.8105 422.3406 61.8106 -5.8022 439.9956 445.7979 421.9946 63.4231 -5.8025 439.9841 445.7866 421.6277 65.0148 -5.8014 439.9678 445.7692 421.2521 66.6166 -5.8000 439.9561 445.7562 420.8658 68.2291 -5.7997 439.9423 445.7420 420.4681 69.8361 -5.7977 439.9192 445.7169 420.0629 71.4433 -5.7942 439.8962 445.6903 419.6517 73.0505 -5.7909 439.8707 445.6616 419.2321 74.6576 -5.7875 439.8457 445.6332 418.8077 76.2650 -5.7832 439.8202 445.6033 418.3752 77.8773 -5.7802 439.7855 445.5657 417.9268 79.4846 -5.7763 439.7407 445.5171 417.4837 81.0914 -5.7724 439.6938 445.4662 417.0441 82.6831 -5.7686 439.6445 445.4131 416.6013 84.2905 -5.7643 439.5899 445.3542 416.1489 85.9078 -5.7604 439.5323 445.2928 415.7070 87.5203 -5.7574 439.4764 445.2338 415.2674 89.1223 -5.7529 439.4127 445.1656 414.8395 90.7348 -5.7477 439.3491 445.0968 414.4087 92.3369 -5.7430 439.2857 445.0287 413.9893 93.9441 -5.7391 439.2114 444.9505 413.5672 95.5411 -5.7354 439.1351 444.8705 413.1600 97.1275 -5.7308 439.0568 444.7876 412.7628 98.7449 -5.7260 438.9679 444.6940 412.3728 100.3521 -5.7209 438.8779 444.5988 412.0080 101.9334 -5.7168 438.7883 444.5051 411.6527 103.5355 -5.7126 438.6961 444.4087 411.3049 105.1428 -5.7100 438.5959 444.3059 410.9713 106.7296 -5.7073 438.5036 444.2109 410.6500 108.3316 -5.7045 438.4024 444.1069 410.3342 109.9389 -5.7021 438.2969 443.9990 410.0349 111.5410 -5.6995 438.1856 443.8850 409.7474 113.1636 -5.6973 438.0688 443.7661 409.4782 114.7555 -5.6943 437.9487 443.6430 409.2248 116.3628 -5.6915 437.8321 443.5236 408.9874 117.9700 -5.6897 437.7098 443.3995 408.7624 119.5563 -5.6883 437.5855 443.2738 408.5578 121.1688 -5.6861 437.4536 443.1397 408.3663 122.7706 -5.6842 437.3293 443.0135 408.1888 124.3833 -5.6820 437.1945 442.8766 408.0306 125.9695 -5.6801 437.0660 442.7461 407.8813 127.5766 -5.6785 436.9293 442.6078 407.7427 129.1993 -5.6777 436.7835 442.4612 407.6127 130.8011 -5.6780 436.6462 442.3242 407.4951 132.4135 -5.6775 436.5049 442.1824 407.3861 134.0000 -5.6781 436.3673 442.0454 407.2949 135.6123 -5.6788 436.2237 441.9025 407.2013 137.2143 -5.6790 436.0797 441.7587 407.1177 138.8214 -5.6795 435.9313 441.6108 407.0447 140.4336 -5.6809 435.7837 441.4646 406.9727 142.0410 -5.6822 435.6434 441.3255 406.9050 143.6430 -5.6830 435.4928 441.1759 406.8418 145.2554 -5.6832 435.3389 441.0222 406.7822 146.8628 -5.6837 435.1861 440.8699 406.7236 148.4699 -5.6847 435.0387 440.7234 406.6624 150.0819 -5.6868 434.8972 440.5840 406.5951 151.6840 -5.6880 434.7448 440.4327 406.5199 153.2810 -5.6892 434.5882 440.2774 406.4502 154.8883 -5.6904 434.4333 440.1236 406.3758 156.5110 -5.6919 434.2820 439.9739 406.2983 158.1130 -5.6935 434.1284 439.8219 406.2155 159.7050 -5.6958 433.9859 439.6817 406.1267 161.2966 -5.6973 433.8516 439.5489 406.0299 162.8939 -5.6972 433.7064 439.4036 405.9300 164.5014 -5.6981 433.5580 439.2561 405.8187 166.1035 -5.6991 433.4147 439.1139 405.7032 167.6901 -5.6994 433.2746 438.9740 405.5759 169.2923 -5.7007 433.1322 438.8329 405.4512 170.9150 -5.7017 432.9825 438.6842 405.3128 172.5170 -5.7021 432.8394 438.5415 405.1712 174.1139 -5.7008 432.6957 438.3966 405.0166 175.7261 -5.7002 432.5558 438.2560 404.8481 177.3233 -5.7007 432.4112 438.1119 404.6776 178.9200 -5.7006 432.2636 437.9643 404.5003 180.5220 -5.7010 432.1135 437.8145 404.3044 182.1345 -5.6992 431.9694 437.6686 404.1094 183.7519 -5.6978 431.8228 437.5206 403.9159 185.3591 -5.6967 431.6750 437.3717 403.7044 186.9663 -5.6949 431.5299 437.2248 403.4752 188.5681 -5.6928 431.3857 437.0785 403.2441 190.1808 -5.6902 431.2363 436.9265 403.0100 191.7828 -5.6887 431.0927 436.7813 402.7776 193.3953 -5.6864 430.9379 436.6244 402.5342 194.9818 -5.6828 430.7891 436.4719 402.2871 196.6045 -5.6791 430.6373 436.3164 402.0286 198.2119 -5.6751 430.4864 436.1615 401.7711 199.8140 -5.6718 430.3292 436.0010 401.5029 201.4264 -5.6683 430.1737 435.8421 401.2298 203.0286 -5.6650 430.0207 435.6857 400.9605 204.6410 -5.6620 429.8692 435.5312 400.6949 206.2430 -5.6586 429.7244 435.3830 400.4137 207.8659 -5.6547 429.5701 435.2248 400.1207 209.4733 -5.6503 429.4223 435.0726 399.8331 211.0754 -5.6469 429.2588 434.9058 399.5478 212.6879 -5.6428 429.0953 434.7381 399.2580 214.2900 -5.6387 428.9422 434.5809 398.9760 215.9023 -5.6352 428.7717 434.4069 398.6896 217.5148 -5.6314 428.6038 434.2352 398.3981 219.1373 -5.6261 428.4377 434.0637 398.1075 220.7289 -5.6204 428.2691 433.8895 397.8207 222.3360 -5.6153 428.1058 433.7211 397.5334 223.9333 -5.6093 427.9417 433.5510 397.2549 225.5353 -5.6048 427.7725 433.3773 396.9742 227.1271 -5.6009 427.6043 433.2052 396.7076 228.7293 -5.5965 427.4305 433.0270 396.4379 230.3260 -5.5908 427.2524 432.8431 396.1667 231.9384 -5.5845 427.0885 432.6731 395.8929 233.5351 -5.5801 426.9157 432.4958 395.6313 235.1321 -5.5749 426.7448 432.3198 395.3730 236.7394 -5.5691 426.5712 432.1404 395.1088 238.3465 -5.5644 426.3952 431.9595 394.8495 239.9434 -5.5598 426.2170 431.7768 394.5955 241.5559 -5.5546 426.0322 431.5868 394.3436 243.1426 -5.5487 425.8520 431.4007 394.0997 244.7496 -5.5433 425.6782 431.2215 393.8574 246.3620 -5.5365 425.4914 431.0278 393.6223 247.9589 -5.5305 425.3065 430.8370 393.4015 249.5609 -5.5253 425.1203 430.6456 393.1883 251.1679 -5.5198 424.9424 430.4623 392.9684 252.7751 -5.5148 424.7596 430.2745 392.7531 254.3719 -5.5102 424.5806 430.0908 392.5456 255.9945 -5.5059 424.3955 429.9014 392.3322 257.6016 -5.5011 424.2078 429.7089 392.1354 259.1881 -5.4961 424.0193 429.5155 391.9428 260.8005 -5.4908 423.8281 429.3190 391.7562 262.4076 -5.4861 423.6400 429.1262 391.5718 264.0148 -5.4817 423.4512 428.9328 391.3825 265.6219 -5.4776 423.2624 428.7400 391.1971 267.2294 -5.4742 423.0794 428.5536 391.0234 268.8368 -5.4706 422.8873 428.3579 390.8554 270.4439 -5.4667 422.6918 428.1584 390.6808 272.0460 -5.4629 422.4996 427.9625 390.5100 273.6531 -5.4580 422.3050 427.7630 390.3468 275.2656 -5.4538 422.1132 427.5670 390.1872 276.8780 -5.4491 421.9164 427.3655 390.0244 278.4748 -5.4453 421.7229 427.1682 389.8676 280.0768 -5.4410 421.5295 426.9705 389.7091 281.6888 -5.4377 421.3351 426.7727 389.5513 283.3013 -5.4351 421.1381 426.5733 389.3952 284.9035 -5.4321 420.9485 426.3806 389.2332 286.5264 -5.4280 420.7524 426.1805 389.0754 288.1075 -5.4233 420.5664 425.9897 388.9145 289.7095 -5.4197 420.3803 425.8000 388.7524 291.3115 -5.4154 420.1855 425.6009 388.5939 292.9084 -5.4129 419.9958 425.4086 388.4378 294.5156 -5.4097 419.8025 425.2122 388.2778 296.1178 -5.4056 419.6095 425.0151 388.1176 297.7094 -5.4014 419.4263 424.8277 387.9491 299.3114 -5.3977 419.2484 424.6461 387.7810 300.9136 -5.3943 419.0587 424.4530 387.6195 302.5365 -5.3908 418.8632 424.2540 387.4479 304.1333 -5.3864 418.6721 424.0585 387.2767 305.7299 -5.3823 418.4865 423.8688 387.1002 307.3370 -5.3793 418.2965 423.6758 386.9234 308.9393 -5.3754 418.1056 423.4810 386.7401 310.5516 -5.3717 417.9133 423.2850 386.5603 312.1536 -5.3687 417.7245 423.0932 386.3763 313.7660 -5.3654 417.5405 422.9059 386.1843 315.3679 -5.3614 417.3529 422.7142 385.9941 316.9905 -5.3559 417.1634 422.5193 385.7961 318.5823 -5.3512 416.9763 422.3275 385.5971 320.1843 -5.3481 416.7822 422.1303 385.3889 321.7966 -5.3443 416.5890 421.9332 385.1744 323.3986 -5.3398 416.4024 421.7422 384.9745 325.0109 -5.3347 416.2088 421.5435 384.7607 326.6129 -5.3298 416.0176 421.3474 384.5413 328.2203 -5.3241 415.8292 421.1532 384.3252 329.8430 -5.3192 415.6398 420.9590 384.1103 331.4450 -5.3143 415.4538 420.7681 383.8944 333.0575 -5.3087 415.2648 420.5734 383.6698 334.6595 -5.3030 415.0829 420.3859 383.4420 336.2565 -5.2979 414.8986 420.1965 383.2163 337.8586 -5.2936 414.7054 419.9990 382.9989 339.4659 -5.2880 414.5131 419.8010 382.7730 341.0731 -5.2820 414.3199 419.6019 382.5424 342.6906 -5.2763 414.1257 419.4020 382.3100 344.3030 -5.2702 413.9334 419.2037 382.0782 345.9000 -5.2650 413.7434 419.0084 381.8414 347.5020 -5.2599 413.5411 418.8010 381.6051 349.1146 -5.2545 413.3472 418.6017 381.3663 350.7168 -5.2485 413.1575 418.4061 381.1261 352.3086 -5.2438 412.9659 418.2096 380.8870 353.9106 -5.2378 412.7717 418.0095 380.6513 355.5128 -5.2314 412.5742 417.8056 380.4125 357.1148 -5.2257 412.3734 417.5991 380.1645 358.7168 -5.2195 412.1812 417.4007 379.9218 360.3188 -5.2126 411.9911 417.2036 379.6830 361.9258 -5.2055 411.7932 416.9987 379.4452 363.5124 -5.1992 411.5966 416.7958 379.2104 365.1144 -5.1931 411.4031 416.5962 378.9718 366.7218 -5.1866 411.2052 416.3918 378.7433 368.3238 -5.1806 411.0155 416.1962 378.5221 369.9311 -5.1737 410.8255 415.9992 378.2894 371.5379 -5.1658 410.6278 415.7936 378.0549 373.1451 -5.1600 410.4291 415.5891 377.8250 374.7523 -5.1541 410.2299 415.3840 377.5875 376.3543 -5.1485 410.0356 415.1841 377.3572 377.9511 -5.1427 409.8463 414.9891 377.1290 379.5531 -5.1381 409.6490 414.7872 376.9014 381.1654 -5.1324 409.4574 414.5898 376.6770 382.7678 -5.1271 409.2712 414.3983 376.4557 384.3904 -5.1219 409.0783 414.2002 376.2289 385.9821 -5.1169 408.8860 414.0029 376.0014 387.5840 -5.1121 408.6874 413.7995 375.7803 389.1965 -5.1062 408.4824 413.5887 375.5662 390.7986 -5.1003 408.2821 413.3824 375.3531 392.4110 -5.0945 408.0754 413.1699 375.1411 394.0131 -5.0882 407.8730 412.9612 374.9282 395.6203 -5.0829 407.6722 412.7550 374.7128 397.2430 -5.0770 407.4697 412.5466 374.5005 398.8449 -5.0728 407.2751 412.3479 374.2928 400.4418 -5.0686 407.0764 412.1450 374.0889 402.0436 -5.0632 406.8754 411.9386 373.8837 403.6561 -5.0575 406.6690 411.7265 373.6833 405.2683 -5.0521 406.4670 411.5191 373.4878 406.8703 -5.0467 406.2692 411.3159 373.2880 408.4825 -5.0405 406.0668 411.1073 373.0925 410.1054 -5.0341 405.8572 410.8914 372.8904 411.6970 -5.0293 405.6512 410.6805 372.6967 413.3095 -5.0244 405.4443 410.4687 372.5028 414.9115 -5.0193 405.2383 410.2576 372.3139 416.5133 -5.0144 405.0401 410.0544 372.1261 418.1101 -5.0099 404.8464 409.8564 371.9400 419.7124 -5.0044 404.6427 409.6470 371.7481 421.3040 -4.9990 404.4370 409.4360 371.5590 422.9060 -4.9927 404.2319 409.2247 371.3821 424.5080 -4.9879 404.0264 409.0142 371.1999 426.1154 -4.9820 403.8218 408.8038 371.0149 427.7225 -4.9765 403.6260 408.6026 370.8272 429.3245 -4.9712 403.4248 408.3960 370.6346 430.9110 -4.9652 403.2177 408.1829 370.4462 432.5234 -4.9591 403.0149 407.9739 370.2606 434.1204 -4.9553 402.8082 407.7634 370.0720 435.7328 -4.9511 402.6091 407.5602 369.8731 437.3346 -4.9471 402.4113 407.3584 369.6864 438.9263 -4.9431 402.2187 407.1618 369.5052 440.5490 -4.9382 402.0070 406.9452 369.3146 442.1561 -4.9329 401.8025 406.7354 369.1266 443.7631 -4.9284 401.5948 406.5231 368.9347 445.3496 -4.9232 401.3899 406.3132 368.7414 446.9621 -4.9168 401.1913 406.1081 368.5491 448.5641 -4.9114 400.9931 405.9045 368.3548 450.1715 -4.9055 400.7824 405.6879 368.1666 451.7786 -4.9000 400.5737 405.4737 367.9765 453.3860 -4.8974 400.3661 405.2635 367.7735 454.9931 -4.8920 400.1649 405.0568 367.5713 456.5950 -4.8870 399.9707 404.8577 367.3807 458.2024 -4.8812 399.7683 404.6494 367.1816 459.8044 -4.8762 399.5631 404.4393 366.9841 461.4170 -4.8713 399.3587 404.2300 366.7811 463.0243 -4.8665 399.1634 404.0299 366.5749 464.6316 -4.8611 398.9680 403.8291 366.3735 466.2234 -4.8559 398.7707 403.6266 366.1715 467.8359 -4.8513 398.5665 403.4178 365.9669 469.4431 -4.8453 398.3720 403.2173 365.7565 471.0604 -4.8395 398.1690 403.0084 365.5443 472.6574 -4.8343 397.9680 402.8023 365.3339 474.2698 -4.8290 397.7625 402.5914 365.1202 475.8718 -4.8245 397.5641 402.3885 364.9068 477.4840 -4.8191 397.3659 402.1851 364.6929 479.0860 -4.8142 397.1697 401.9840 364.4836 480.6931 -4.8068 396.9578 401.7646 364.2644 482.2746 -4.8018 396.7568 401.5585 364.0560 483.8766 -4.7965 396.5529 401.3494 363.8449 485.4886 -4.7916 396.3572 401.1487 363.6238 487.0856 -4.7864 396.1644 400.9508 363.4091 488.6928 -4.7810 395.9625 400.7435 363.1918 490.2999 -4.7770 395.7626 400.5396 362.9666 491.8914 -4.7725 395.5637 400.3362 362.7537 493.4934 -4.7685 395.3731 400.1416 362.5321 495.0954 -4.7632 395.1769 399.9401 362.3137 496.7026 -4.7581 394.9798 399.7379 362.0954 498.2941 -4.7529 394.7733 399.5262 361.8812 499.9170 -4.7466 394.5707 399.3173 361.6582 501.5243 -4.7413 394.3645 399.1057 361.4297 503.1265 -4.7361 394.1565 398.8926 361.2077 504.7234 -4.7306 393.9542 398.6848 360.9845 506.3254 -4.7243 393.7514 398.4756 360.7710 507.9326 -4.7176 393.5628 398.2804 360.5484 509.5400 -4.7104 393.3658 398.0762 360.3320 511.1473 -4.7056 393.1617 397.8673 360.1171 512.7440 -4.7013 392.9595 397.6607 359.8988 514.3616 -4.6961 392.7637 397.4598 359.6737 515.9689 -4.6905 392.5650 397.2556 359.4568 517.5811 -4.6839 392.3599 397.0438 359.2381 519.1728 -4.6769 392.1532 396.8302 359.0199 520.7748 -4.6721 391.9583 396.6304 358.8035 522.3873 -4.6677 391.7513 396.4190 358.5894 523.9945 -4.6623 391.5377 396.2000 358.3770 525.6016 -4.6559 391.3294 395.9853 358.1627 527.2244 -4.6509 391.1190 395.7698 357.9442 528.8261 -4.6457 390.9078 395.5535 357.7223 530.4385 -4.6400 390.7015 395.3416 357.5010 532.0303 -4.6333 390.4960 395.1293 357.2911 533.6326 -4.6275 390.2911 394.9186 357.0774 535.2450 -4.6214 390.0924 394.7138 356.8623 536.8520 -4.6147 389.8857 394.5005 356.6492 538.4594 -4.6082 389.6779 394.2861 356.4381 540.0823 -4.6013 389.4688 394.0701 356.2251 541.6844 -4.5953 389.2604 393.8557 356.0135 543.2968 -4.5889 389.0549 393.6438 355.7942 544.8783 -4.5839 388.8553 393.4393 355.5842 546.4803 -4.5780 388.6507 393.2287 355.3766 548.0825 -4.5725 388.4469 393.0195 355.1644 549.6744 -4.5688 388.2510 392.8198 354.9629 551.2709 -4.5626 388.0474 392.6100 354.7497 552.8728 -4.5567 387.8404 392.3971 354.5400 554.4956 -4.5516 387.6289 392.1805 354.3240 556.0821 -4.5465 387.4270 391.9735 354.1114 557.6896 -4.5408 387.2227 391.7635 353.9058 559.2915 -4.5351 387.0190 391.5541 353.7067 560.8938 -4.5303 386.8168 391.3470 353.4991 562.5060 -4.5257 386.6073 391.1330 353.2938 564.1080 -4.5212 386.4028 390.9240 353.0887 565.6996 -4.5139 386.2024 390.7163 352.8893 567.3016 -4.5079 385.9947 390.5027 352.6852 568.9243 -4.5026 385.7847 390.2873 352.4839 570.5316 -4.4968 385.5773 390.0741 352.2764 572.1389 -4.4914 385.3642 389.8556 352.0719 573.7461 -4.4860 385.1631 389.6490 351.8659 575.3533 -4.4808 384.9609 389.4417 351.6602 576.9449 -4.4767 384.7507 389.2275 351.4525 578.5574 -4.4718 384.5432 389.0150 351.2475 580.1646 -4.4674 384.3372 388.8046 351.0456 581.7821 -4.4628 384.1320 388.5948 350.8420 583.3945 -4.4576 383.9208 388.3784 350.6494 584.9861 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