DTA measure 1gyors Date: 2024108:158 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.26 s Mass = 967.000 mg data_number = 1263 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2973 -0.1572 244.7649 244.9221 266.4115 2.1473 -0.1548 244.9904 245.1451 266.4594 2.8833 -0.1305 245.2704 245.4009 266.4219 3.7570 -0.1397 245.4396 245.5793 266.3975 4.5160 -0.1407 245.5393 245.6800 266.4697 5.3365 -0.1155 245.7531 245.8686 266.4051 6.1250 -0.1177 245.9095 246.0272 266.6094 6.9138 -0.1162 246.1849 246.3010 266.6006 7.7625 -0.1174 246.1629 246.2804 266.5012 8.5208 -0.1003 246.4988 246.5991 266.4998 9.3415 -0.0870 246.6769 246.7640 266.3907 10.1620 -0.1004 246.7101 246.8105 266.6461 10.9228 -0.1126 246.8301 246.9427 266.8789 11.7760 -0.0909 247.0104 247.1013 266.7734 12.5378 -0.1013 247.1524 247.2537 266.8341 13.3618 -0.0927 247.1861 247.2788 266.8000 14.1545 -0.0897 247.2969 247.3866 266.9301 14.9465 -0.0794 247.5305 247.6098 267.1132 15.7990 -0.0640 247.6364 247.7005 267.2677 16.5605 -0.0312 247.8931 247.9243 267.3298 17.3838 -0.0209 248.0847 248.1056 267.4282 18.1758 0.0060 248.2232 248.2172 267.6178 18.9675 0.0000 248.5568 248.5568 267.5287 19.7898 0.0157 248.6495 248.6338 267.6732 20.5815 0.0234 248.6314 248.6080 267.8804 21.4038 0.0158 248.8182 248.8024 267.8700 22.1958 0.0044 249.0714 249.0670 268.0182 22.9875 0.0023 249.1301 249.1278 268.2071 23.8580 -0.0046 249.3258 249.3303 268.4584 24.5955 -0.0259 249.4632 249.4892 268.7077 25.4480 -0.0342 249.5535 249.5877 268.8689 26.2095 -0.0416 249.8517 249.8933 268.9551 27.0315 -0.0227 249.9240 249.9468 269.1649 27.8535 -0.0147 250.2280 250.2427 269.3027 28.6155 -0.0015 250.1186 250.1201 269.6043 29.4698 0.0020 250.4504 250.4484 269.6385 30.2325 -0.0013 250.5893 250.5906 269.7728 31.0538 0.0103 250.6307 250.6204 270.0447 31.8690 0.0156 250.7752 250.7596 270.4889 32.6283 0.0186 250.8091 250.7905 270.6160 33.4760 0.0122 251.0107 250.9985 270.5595 34.2340 0.0257 251.1578 251.1321 270.5793 35.0520 0.0393 251.2732 251.2340 270.6224 35.8703 0.0516 251.5536 251.5020 270.7745 36.6290 0.0410 251.5883 251.5473 270.9375 37.4785 0.0252 251.7422 251.7169 271.1883 38.2370 0.0092 251.8505 251.8413 271.2451 39.0558 0.0135 252.0186 252.0051 271.4661 39.8743 0.0138 252.0963 252.0825 271.7071 40.6348 0.0329 252.2258 252.1929 271.8190 41.4885 0.0316 252.4113 252.3797 272.1067 42.2490 0.0257 252.5415 252.5158 272.2566 43.0695 0.0284 252.6801 252.6518 272.3403 43.8915 0.0207 252.9103 252.8896 272.4681 44.6535 0.0364 252.9575 252.9211 272.6617 45.5055 0.0338 253.2398 253.2059 272.8687 46.2975 0.0408 253.3703 253.3294 272.8350 47.0895 0.0418 253.3965 253.3547 272.9829 47.9118 0.0165 253.6043 253.5878 273.2248 48.6735 0.0435 253.7510 253.7076 273.2483 49.5255 0.0310 253.9083 253.8774 273.3801 50.2875 0.0319 254.0611 254.0291 273.3788 51.1095 0.0298 254.1294 254.0996 273.6078 51.9315 0.0220 254.3808 254.3587 273.6042 52.6930 0.0431 254.4223 254.3792 273.7841 53.5450 0.0433 254.4297 254.3865 273.9915 54.3145 0.0483 254.6817 254.6334 274.0308 55.1478 0.0209 254.7088 254.6880 274.2903 55.9400 0.0300 254.8476 254.8176 274.3713 56.7325 0.0224 254.9140 254.8917 274.5002 57.5548 0.0114 255.1608 255.1494 274.6896 58.3465 -0.0158 255.2831 255.2989 274.5668 59.1688 -0.0058 255.4633 255.4691 274.7019 59.9620 0.0204 255.6498 255.6294 274.6716 60.7545 0.0233 255.7740 255.7508 274.8444 61.5768 0.0228 255.8626 255.8398 274.9450 62.3385 0.0111 255.9470 255.9360 274.9463 63.1913 0.0188 256.1462 256.1274 275.1228 63.9790 0.0143 256.2091 256.1948 275.3192 64.7670 0.0059 256.2501 256.2442 275.4720 65.5855 0.0174 256.4103 256.3930 275.7108 66.3440 -0.0005 256.5836 256.5841 275.8916 67.1928 -0.0017 256.8786 256.8803 276.1458 67.9813 0.0124 257.1135 257.1010 276.3455 68.7700 0.0140 257.1804 257.1665 276.7094 69.5895 -0.0159 257.3005 257.3164 276.9144 70.3490 -0.0152 257.4320 257.4472 276.9252 71.1975 -0.0071 257.5288 257.5359 277.0180 71.9873 -0.0025 257.5495 257.5520 277.1330 72.7780 -0.0167 257.7416 257.7583 277.3381 73.5980 -0.0211 257.9914 258.0125 277.3881 74.3595 -0.0128 258.1122 258.1250 277.4695 75.2135 -0.0147 258.1811 258.1958 277.6612 76.0058 -0.0259 258.3119 258.3378 277.7021 76.7975 -0.0090 258.3384 258.3474 277.8494 77.6208 0.0025 258.5544 258.5519 278.0437 78.3825 0.0003 258.5449 258.5446 278.1813 79.2348 -0.0248 259.0127 259.0376 278.3160 79.9970 -0.0197 259.0609 259.0806 278.4669 80.8198 0.0019 259.1481 259.1463 278.5253 81.6418 -0.0087 259.5285 259.5372 278.7479 82.4035 -0.0049 259.7027 259.7076 278.7782 83.2555 -0.0198 259.8209 259.8407 278.9361 84.0475 -0.0272 260.0406 260.0677 279.0358 84.8408 -0.0174 260.1775 260.1949 279.0409 85.6655 0.0003 260.4195 260.4192 279.3016 86.4275 -0.0047 260.5269 260.5316 279.3482 87.2810 -0.0207 260.6296 260.6503 279.5142 88.0435 -0.0196 260.6815 260.7011 279.5176 88.8655 -0.0084 260.9512 260.9596 279.6338 89.6875 -0.0425 261.1579 261.2004 279.8271 90.4495 -0.0324 261.1494 261.1817 279.9438 91.3038 -0.0336 261.3729 261.4065 279.9578 92.0665 -0.0331 261.5721 261.6052 280.0291 92.8883 -0.0143 261.7561 261.7704 280.1330 93.7100 -0.0131 262.0280 262.0411 280.1565 94.4715 -0.0405 262.2154 262.2559 280.3964 95.3233 -0.0532 262.4165 262.4697 280.6118 96.0815 -0.0351 262.6502 262.6853 280.6238 96.9008 -0.0822 262.8702 262.9525 280.7592 97.7188 -0.1075 262.8754 262.9829 280.9875 98.4768 -0.1175 262.9736 263.0910 281.1659 99.3273 -0.1419 263.2619 263.4038 281.2331 100.0858 -0.1538 263.3290 263.4828 281.4513 100.9058 -0.1495 263.6552 263.8047 281.6145 101.7238 -0.1483 263.7701 263.9184 281.7860 102.4830 -0.1207 263.8658 263.9865 281.9921 103.3315 -0.0753 264.0504 264.1257 281.9762 104.1210 -0.0861 264.0295 264.1156 282.0775 104.9118 -0.1028 264.2466 264.3494 282.2729 105.7170 -0.1093 264.3391 264.4484 282.4860 106.5155 -0.1121 264.4322 264.5443 282.6590 107.3358 -0.1223 264.6095 264.7318 282.6544 108.1275 -0.1199 264.7045 264.8244 282.7520 108.9490 -0.1245 264.8320 264.9564 282.8278 109.7410 -0.1204 264.8863 265.0067 282.9186 110.5340 -0.1243 264.9453 265.0696 283.1620 111.3560 -0.1037 265.0987 265.2024 283.2775 112.1488 -0.1102 265.2907 265.4010 283.2550 112.9708 -0.1308 265.5402 265.6710 283.4439 113.7635 -0.1396 265.6659 265.8055 283.5474 114.5565 -0.1361 265.8001 265.9362 283.7236 115.3788 -0.1264 265.9096 266.0360 283.9709 116.1705 -0.1043 266.0196 266.1239 284.0771 116.9928 -0.0862 266.1936 266.2799 284.1365 117.7848 -0.0409 266.3629 266.4038 284.3234 118.5765 -0.0495 266.4594 266.5089 284.4899 119.4288 -0.0623 266.5990 266.6612 284.5703 120.1905 -0.0530 266.7082 266.7612 284.5658 121.0135 -0.0611 266.8411 266.9022 284.8625 121.8060 -0.0711 266.9679 267.0390 284.8832 122.5995 -0.0662 267.1326 267.1987 285.1321 123.4515 -0.0809 267.2714 267.3523 285.3357 124.2135 -0.0802 267.3945 267.4747 285.3417 125.0375 -0.0965 267.6080 267.7045 285.4233 125.8360 -0.0719 267.7650 267.8370 285.6725 126.6455 -0.0926 267.8121 267.9047 285.7312 127.4375 -0.0852 267.9513 268.0365 286.0098 128.2280 -0.0837 267.8762 267.9600 286.0688 129.0760 -0.0761 268.0759 268.1520 286.2687 129.8340 -0.0851 268.2419 268.3270 286.4695 130.6520 -0.1032 268.5747 268.6778 286.7619 131.4400 -0.1064 268.7723 268.8787 286.9093 132.2310 -0.1054 268.5531 268.6585 287.0450 133.0503 -0.1095 268.8355 268.9450 287.1879 133.8390 -0.1150 268.9400 269.0550 287.3773 134.6578 -0.1333 269.1627 269.2960 287.5778 135.4468 -0.1440 269.3397 269.4837 287.6788 136.2370 -0.1476 269.6328 269.7804 287.8002 137.0553 -0.1436 269.5920 269.7355 287.8817 137.8455 -0.1579 269.7713 269.9292 288.0266 138.6665 -0.1502 269.8722 270.0223 288.2265 139.4575 -0.1404 270.0440 270.1844 288.3138 140.2495 -0.1412 270.1360 270.2772 288.4146 141.0715 -0.1504 270.3539 270.5043 288.5157 141.8635 -0.1398 270.4014 270.5412 288.5381 142.6855 -0.1328 270.5006 270.6334 288.7299 143.4785 -0.1306 270.6506 270.7812 288.8745 144.2715 -0.1434 270.6283 270.7717 288.8930 145.0935 -0.1407 270.9338 271.0746 289.0259 145.8555 -0.1270 271.0434 271.1704 289.1088 146.7245 -0.1224 271.1292 271.2516 289.2372 147.4625 -0.1261 271.2982 271.4244 289.2587 148.3145 -0.1323 271.5075 271.6399 289.3770 149.1065 -0.1419 271.4833 271.6252 289.5724 149.8985 -0.1479 271.6780 271.8259 289.6385 150.7203 -0.1529 271.9071 272.0600 289.7907 151.4815 -0.1296 272.0677 272.1972 289.8553 152.3340 -0.1358 272.1607 272.2964 289.9937 153.1258 -0.1424 272.4348 272.5772 290.1768 153.9175 -0.1523 272.5173 272.6696 290.3875 154.7398 -0.1651 272.6683 272.8334 290.3728 155.5015 -0.1601 272.8487 273.0088 290.5032 156.3538 -0.1590 272.8873 273.0463 290.6665 157.1458 -0.1682 272.9065 273.0747 290.8136 157.9375 -0.1642 272.9884 273.1526 290.8295 158.7603 -0.1711 273.2488 273.4198 290.9720 159.5225 -0.1568 273.5886 273.7454 291.1535 160.3730 -0.1616 273.8231 273.9847 291.3768 161.1348 -0.1625 273.8889 274.0514 291.6245 161.9540 -0.1875 273.8810 274.0685 291.7413 162.7433 -0.1812 274.1453 274.3265 291.8912 163.5320 -0.1671 274.2068 274.3738 292.0347 164.3800 -0.1642 274.4097 274.5739 292.0822 165.1380 -0.2012 274.5920 274.7932 292.2949 165.9588 -0.2296 274.6219 274.8514 292.5308 166.7533 -0.2159 274.9299 275.1457 292.6039 167.5610 -0.2167 274.9823 275.1991 292.6694 168.3493 -0.2065 275.0860 275.2925 292.7478 169.1435 -0.1953 275.1662 275.3615 292.8800 169.9648 -0.2038 275.3624 275.5662 293.0173 170.7540 -0.2052 275.5723 275.7775 293.0894 171.5730 -0.2207 275.7454 275.9661 293.1972 172.3633 -0.2241 275.8203 276.0444 293.3980 173.1535 -0.2357 275.9015 276.1371 293.5926 174.0048 -0.2483 276.0618 276.3101 293.7153 174.7665 -0.2449 276.1885 276.4334 293.8499 175.5888 -0.2351 276.4788 276.7139 293.9178 176.3810 -0.2275 276.5741 276.8016 294.0734 177.1738 -0.2346 276.6061 276.8407 294.1702 178.0310 -0.2587 276.8126 277.0713 294.3402 178.8225 -0.2686 276.8890 277.1577 294.5016 179.6145 -0.2795 277.0117 277.2912 294.6250 180.4665 -0.2656 277.1461 277.4117 294.7762 181.2308 -0.2850 277.3106 277.5956 294.8873 182.0545 -0.2740 277.5040 277.7781 295.0020 182.8493 -0.2820 277.5449 277.8270 295.1093 183.6415 -0.2701 277.7048 277.9749 295.1778 184.4650 -0.2867 277.9006 278.1873 295.3583 185.2275 -0.2798 277.8519 278.1316 295.5509 186.0810 -0.2922 278.1194 278.4117 295.7567 186.8468 -0.2931 278.1602 278.4533 295.9514 187.6870 -0.3177 278.4335 278.7512 296.2683 188.4545 -0.3047 278.4704 278.7751 296.3720 189.2765 -0.3053 278.6161 278.9214 296.5067 190.0690 -0.3106 278.9188 279.2295 296.7611 190.8610 -0.3368 279.0455 279.3823 297.0427 191.7130 -0.3482 279.1818 279.5300 297.2394 192.5278 -0.3211 279.3509 279.6720 297.2906 193.3170 -0.3273 279.4540 279.7813 297.4593 194.1340 -0.3389 279.6683 280.0072 297.5195 194.9223 -0.3530 279.7791 280.1321 297.7222 195.7103 -0.3684 279.8912 280.2596 297.7922 196.5288 -0.3495 280.1707 280.5202 297.9460 197.3170 -0.3536 280.1856 280.5392 297.9721 198.1358 -0.3572 280.4039 280.7611 298.0307 198.9250 -0.3586 280.5719 280.9305 298.2820 199.7150 -0.3749 280.6513 281.0262 298.3293 200.5333 -0.3642 280.7761 281.1403 298.4079 201.3220 -0.3494 280.9162 281.2656 298.4500 202.1408 -0.3480 280.9984 281.3463 298.5256 202.9290 -0.3533 281.1187 281.4720 298.7332 203.7188 -0.3451 281.3094 281.6546 298.6837 204.5693 -0.3340 281.4940 281.8280 298.7189 205.3295 -0.3529 281.6310 281.9839 298.8775 206.1545 -0.3527 281.8654 282.2181 298.9538 206.9465 -0.3463 281.8306 282.1769 299.0351 207.7380 -0.3375 281.9979 282.3354 299.1488 208.5613 -0.3520 282.0508 282.4029 299.2379 209.3528 -0.3437 282.2133 282.5570 299.3054 210.1748 -0.3414 282.2571 282.5985 299.3964 210.9673 -0.3432 282.3367 282.6799 299.6040 211.7603 -0.3663 282.4816 282.8479 299.7914 212.5850 -0.3254 282.6760 283.0014 299.6776 213.3485 -0.3185 282.8139 283.1324 299.7744 214.2008 -0.3351 283.0436 283.3787 299.8912 215.0528 -0.3147 283.0307 283.3454 299.8927 215.9070 -0.3171 283.1509 283.4679 299.9744 216.6685 -0.3501 283.3965 283.7466 300.1349 217.4908 -0.3417 283.5384 283.8801 300.4030 218.3128 -0.3205 283.6288 283.9493 300.4882 219.0745 -0.2990 283.7625 284.0615 300.6105 219.9273 -0.2801 283.9292 284.2094 300.7898 220.6895 -0.2864 284.1950 284.4814 301.0600 221.5118 -0.3025 284.2038 284.5063 301.2744 222.3093 -0.3216 284.4141 284.7357 301.6723 223.1015 -0.3504 284.5385 284.8889 302.0049 223.9533 -0.3520 284.6368 284.9888 302.0668 224.7123 -0.3565 284.7989 285.1554 302.1560 225.5300 -0.3589 284.8688 285.2277 302.3181 226.3180 -0.3555 285.0331 285.3886 302.2188 227.1075 -0.3381 285.0843 285.4224 302.1812 227.9275 -0.3581 285.3137 285.6717 302.3436 228.7103 -0.3597 285.4065 285.7662 302.7379 229.5888 -0.3672 285.5077 285.8749 302.8994 230.4070 -0.3627 285.6542 286.0169 303.0795 231.2555 -0.3949 285.8269 286.2217 303.2304 232.0140 -0.3974 286.0335 286.4309 303.2513 232.8930 -0.3715 286.3412 286.7127 303.5816 233.6828 -0.3748 286.3920 286.7669 303.4610 234.5013 -0.3707 286.5188 286.8894 303.6074 235.2910 -0.3874 286.6614 287.0488 303.7823 236.1110 -0.3909 286.9788 287.3697 303.6848 236.9023 -0.4230 287.0697 287.4927 303.8518 237.6955 -0.4064 287.2145 287.6210 303.9703 238.5250 -0.3956 287.3344 287.7300 304.0304 239.3088 -0.4170 287.4834 287.9004 304.2683 240.1305 -0.3998 287.7438 288.1437 304.3656 240.8925 -0.3981 287.8205 288.2186 304.3719 241.7445 -0.4167 288.0604 288.4771 304.4443 242.5065 -0.4102 288.1861 288.5962 304.6226 243.3285 -0.3924 288.3364 288.7288 304.8436 244.1505 -0.4349 288.4959 288.9307 304.9085 244.9138 -0.4372 288.5727 289.0098 305.0478 245.7685 -0.4188 288.8186 289.2374 305.3888 246.5305 -0.4424 288.9687 289.4111 305.5961 247.3525 -0.4356 289.0191 289.4547 305.6479 248.1445 -0.4310 289.1162 289.5472 305.8660 248.9443 -0.4357 289.2265 289.6622 306.1693 249.7740 -0.4378 289.4232 289.8610 306.2709 250.5355 -0.4286 289.5568 289.9855 306.2747 251.3880 -0.4513 289.6006 290.0519 306.5462 252.1495 -0.4566 289.7942 290.2508 306.7068 252.9718 -0.4502 289.9981 290.4483 306.7040 253.7938 -0.4357 290.1342 290.5699 306.6804 254.5555 -0.4439 290.2594 290.7034 306.9098 255.4120 -0.4538 290.5072 290.9611 307.1521 256.1735 -0.4611 290.6554 291.1164 307.2241 256.9955 -0.4633 290.7495 291.2129 307.3035 257.8140 -0.4703 290.9165 291.3869 307.3927 258.5720 -0.4866 290.9964 291.4831 307.5644 259.5380 -0.4928 291.1471 291.6399 307.8384 260.4178 -0.4841 291.3900 291.8741 307.9192 261.1753 -0.4890 291.4772 291.9662 308.1013 262.0233 -0.4842 291.6554 292.1395 308.1236 262.8410 -0.4866 291.7969 292.2835 308.3177 263.6603 -0.4864 291.9570 292.4434 308.4863 264.4490 -0.4925 292.1148 292.6073 308.6186 265.2680 -0.4928 292.1615 292.6542 308.6985 266.0568 -0.5217 292.2915 292.8131 308.8878 266.8470 -0.5260 292.4688 292.9948 308.8806 267.6665 -0.5206 292.6108 293.1314 309.0436 268.4860 -0.5009 292.7520 293.2529 309.2125 269.2910 -0.5234 292.9527 293.4761 309.3721 270.0998 -0.5261 293.0330 293.5590 309.4065 270.8915 -0.5397 293.2317 293.7714 309.6211 271.7143 -0.5398 293.3148 293.8546 309.6764 272.4765 -0.5327 293.4525 293.9851 309.7027 273.3288 -0.5429 293.6767 294.2196 309.9653 274.1808 -0.5512 293.8095 294.3607 310.0045 274.9438 -0.5442 294.0092 294.5533 310.2047 275.7685 -0.5467 294.1839 294.7306 310.2817 276.5608 -0.5653 294.1788 294.7441 310.4278 277.3838 -0.5773 294.3238 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