DTA measure 1lassu Date: 2024108:166 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.54 s Mass = 967.000 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0655 -0.5203 248.4764 248.9967 266.1336 1.8905 -0.4998 248.8131 249.3129 266.0257 2.6828 -0.4985 248.9880 249.4865 266.0979 3.4745 -0.5059 249.2861 249.7920 266.0688 4.3268 -0.4993 249.3908 249.8901 266.1888 5.0888 -0.5011 249.3972 249.8983 266.3589 5.9108 -0.5159 249.6556 250.1715 266.4308 6.7028 -0.5247 249.8517 250.3764 266.4452 7.4945 -0.5296 249.9423 250.4719 266.5936 8.3243 -0.5063 250.0723 250.5786 266.6424 9.0875 -0.4973 250.2527 250.7500 266.5244 9.9393 -0.5024 250.1626 250.6650 266.6033 10.6985 -0.4952 250.3073 250.8025 266.6249 11.5180 -0.4812 250.4996 250.9808 266.6537 12.3360 -0.4854 250.6458 251.1312 266.6640 13.0940 -0.4606 250.7190 251.1796 266.7438 13.9440 -0.4607 250.8241 251.2848 266.8149 14.7020 -0.4474 251.0184 251.4658 266.8418 15.5200 -0.4489 251.0424 251.4913 266.9363 16.3380 -0.4460 251.4064 251.8524 266.8642 17.0960 -0.4495 251.5249 251.9743 266.9666 17.9465 -0.4158 251.5162 251.9320 267.0846 18.7050 -0.4403 251.7866 252.2269 267.1750 19.5280 -0.4360 251.8985 252.3345 267.2909 20.3040 -0.4494 252.0979 252.5473 267.4320 21.1228 -0.4196 252.0564 252.4760 267.5392 21.9413 -0.4164 252.1767 252.5931 267.7510 22.7000 -0.4255 252.3063 252.7318 267.9422 23.5485 -0.4423 252.3267 252.7689 268.0583 24.3370 -0.4179 252.4628 252.8806 268.1691 25.1260 -0.4194 252.6817 253.1011 268.2710 25.9443 -0.4364 252.8837 253.3201 268.4774 26.7330 -0.4282 252.8967 253.3249 268.6087 27.5523 -0.4126 253.1106 253.5232 268.6492 28.3413 -0.4041 253.0790 253.4831 268.9265 29.1310 -0.3868 253.2344 253.6212 268.9901 29.9805 -0.4020 253.4020 253.8040 269.2307 30.7400 -0.4004 253.4573 253.8577 269.3662 31.5618 -0.4087 253.7209 254.1296 269.4038 32.3508 -0.3948 253.7996 254.1945 269.6013 33.1413 -0.3810 253.8842 254.2652 269.7381 33.9910 -0.3838 254.1489 254.5328 269.7671 34.7508 -0.3721 254.1041 254.4762 269.9140 35.5748 -0.3910 254.1601 254.5511 270.0523 36.3670 -0.4161 254.4038 254.8199 270.2593 37.1585 -0.4036 254.5944 254.9980 270.4890 37.9818 -0.3754 254.6711 255.0465 270.7924 38.7735 -0.3733 254.7676 255.1410 270.6915 39.5958 -0.4024 254.6861 255.0885 270.9251 40.3880 -0.3828 254.9470 255.3299 270.8522 41.1805 -0.3847 255.0250 255.4098 270.7365 42.0028 -0.3808 255.1678 255.5487 270.9178 42.7645 -0.3948 255.2783 255.6732 270.9756 43.6180 -0.4208 255.5166 255.9374 270.8919 44.4098 -0.4080 255.6398 256.0479 270.8820 45.2015 -0.4030 255.6790 256.0820 270.9852 46.0238 -0.3955 255.7287 256.1242 271.1239 46.7855 -0.4160 255.8634 256.2794 271.1958 47.6375 -0.4114 256.0268 256.4383 271.6347 48.4315 -0.4040 256.0822 256.4862 271.6815 49.2235 -0.4046 256.1656 256.5702 271.6686 50.0463 -0.3976 256.4108 256.8084 272.0038 50.8243 -0.3652 256.5389 256.9041 272.1678 51.6465 -0.3853 256.6911 257.0764 272.3357 52.4385 -0.4083 256.7151 257.1234 272.4878 53.2605 -0.4059 256.9430 257.3489 272.6915 54.0525 -0.4021 257.1281 257.5302 272.9145 54.8445 -0.4039 257.1332 257.5371 272.9600 55.6665 -0.3974 257.3671 257.7645 273.0564 56.4283 -0.4152 257.4898 257.9049 272.9048 57.2810 -0.4047 257.6004 258.0051 273.1285 58.0730 -0.4226 257.6300 258.0526 273.2136 58.8645 -0.4146 257.6696 258.0842 273.3570 59.6880 -0.4282 257.8450 258.2733 273.3568 60.4515 -0.4491 257.8607 258.3098 273.7836 61.3045 -0.4292 258.1000 258.5292 273.8724 62.0968 -0.4165 258.2808 258.6973 274.0469 62.8885 -0.3946 258.4131 258.8077 274.0199 63.7125 -0.3861 258.4938 258.8799 274.2485 64.4745 -0.3810 258.5177 258.8987 274.3354 65.3268 -0.3941 258.7283 259.1224 274.3904 66.1188 -0.3740 258.8615 259.2355 274.5599 66.9105 -0.3786 259.0054 259.3840 274.4277 67.7355 -0.3740 259.1691 259.5431 274.5952 68.4975 -0.3964 259.3241 259.7205 274.7810 69.3495 -0.3971 259.4737 259.8708 274.7882 70.1415 -0.3968 259.5101 259.9069 275.0219 70.9465 -0.3951 259.7543 260.1494 275.0488 71.7230 -0.3969 259.8936 260.2905 275.0486 72.5455 -0.4013 260.1395 260.5407 275.1562 73.3683 -0.4135 260.2469 260.6604 275.2551 74.1235 -0.3982 260.3813 260.7795 275.5046 74.9673 -0.4064 260.6200 261.0264 275.3814 75.7215 -0.3940 260.6029 260.9969 275.4020 76.5318 -0.4128 260.7962 261.2090 275.4079 77.3168 -0.3788 260.8993 261.2781 275.6394 78.1018 -0.3818 260.9756 261.3574 275.7042 78.9175 -0.3924 261.0637 261.4561 275.7889 79.6718 -0.3715 261.2391 261.6106 275.6685 80.5195 -0.3739 261.4371 261.8110 275.8118 81.3045 -0.3815 261.6559 262.0374 275.8495 82.0920 -0.3832 261.8010 262.1842 276.1056 82.9093 -0.3800 261.9532 262.3332 276.2518 83.6673 -0.3910 262.0936 262.4846 276.3204 84.5173 -0.3927 262.3966 262.7894 276.2607 85.2755 -0.3878 262.5313 262.9191 276.6259 86.0935 -0.3818 262.6568 263.0386 276.5493 86.9115 -0.3891 262.7254 263.1145 276.8682 87.6703 -0.4079 262.7947 263.2026 277.0874 88.5208 -0.3986 263.0366 263.4352 277.1643 89.2800 -0.4295 263.1572 263.5867 277.3502 90.0985 -0.4376 263.3076 263.7452 277.5051 90.9168 -0.4335 263.3845 263.8179 277.7392 91.7013 -0.4326 263.3880 263.8206 277.8558 92.5215 -0.4494 263.5016 263.9510 277.9988 93.2828 -0.4247 263.6799 264.1046 277.9911 94.1330 -0.4183 263.8489 264.2672 278.0657 94.9240 -0.4117 263.9333 264.3450 278.0735 95.7155 -0.4314 264.1075 264.5389 278.2317 96.5378 -0.4277 264.2911 264.7188 278.1352 97.2995 -0.3975 264.2944 264.6919 278.2086 98.1525 -0.4105 264.4439 264.8544 278.3238 98.9145 -0.3963 264.6413 265.0377 278.3149 99.7368 -0.4282 264.8381 265.2663 278.4340 100.5293 -0.4036 264.9428 265.3464 278.5305 101.3215 -0.3973 265.1152 265.5125 278.7931 102.1738 -0.4123 265.2290 265.6413 278.8388 102.9363 -0.3887 265.2939 265.6826 278.9847 103.7588 -0.4208 265.4099 265.8306 279.1349 104.5508 -0.4223 265.5515 265.9738 279.2191 105.3425 -0.4236 265.6186 266.0423 279.2148 106.1658 -0.4785 265.7815 266.2601 279.3927 106.9575 -0.4828 265.8244 266.3072 279.5788 107.7795 -0.4437 265.9334 266.3772 279.6052 108.5720 -0.4801 266.0341 266.5142 279.8025 109.3668 -0.4637 266.2244 266.6881 279.9987 110.1925 -0.4892 266.3085 266.7977 280.0984 110.9555 -0.4920 266.5299 267.0219 280.1125 111.8195 -0.5124 266.4222 266.9346 280.3780 112.5625 -0.5330 266.5533 267.0863 280.4478 113.4145 -0.5001 266.7902 267.2903 280.3758 114.1765 -0.5080 266.7014 267.2094 280.6514 114.9980 -0.4963 266.8351 267.3314 280.6221 115.8200 -0.4998 266.9759 267.4757 280.8750 116.5815 -0.4742 267.0309 267.5051 280.6975 117.4355 -0.4756 267.2385 267.7141 280.8760 118.1988 -0.4683 267.5306 267.9988 280.8186 119.0218 -0.4868 267.6323 268.1191 280.9170 119.8145 -0.4845 267.6503 268.1348 281.0369 120.6065 -0.4470 267.7853 268.2323 281.2803 121.4588 -0.4578 267.9630 268.4209 281.2822 122.2205 -0.4346 267.9086 268.3431 281.5415 123.0428 -0.4548 267.9482 268.4030 281.6754 123.8358 -0.4618 268.1636 268.6254 281.6751 124.6285 -0.4969 268.2977 268.7945 281.7711 125.4808 -0.4920 268.4540 268.9460 281.8950 126.2425 -0.5071 268.6185 269.1256 281.9161 127.0645 -0.5161 268.5958 269.1119 281.9180 127.8565 -0.5373 268.7132 269.2505 282.1635 128.6485 -0.5516 268.8450 269.3966 282.2294 129.5005 -0.5424 269.0120 269.5544 282.1022 130.2625 -0.5469 269.0290 269.5759 282.1227 131.0845 -0.5831 269.2488 269.8319 282.4228 131.8765 -0.5960 269.2709 269.8669 282.6514 132.6970 -0.5897 269.4534 270.0431 282.6213 133.4885 -0.5910 269.5834 270.1744 282.7170 134.2805 -0.5743 269.8587 270.4330 282.9118 135.1323 -0.5524 269.7341 270.2865 282.9394 135.8943 -0.5794 269.8452 270.4245 283.0345 136.7178 -0.5612 269.9769 270.5382 283.1802 137.5100 -0.5960 270.1445 270.7404 283.3010 138.3015 -0.5774 270.2055 270.7829 283.3439 139.1538 -0.5994 270.3685 270.9679 283.6190 139.9155 -0.5918 270.4820 271.0738 283.6437 140.7395 -0.5567 270.7180 271.2748 283.8247 141.5340 -0.5415 270.7500 271.2915 284.0226 142.3265 -0.5255 270.6550 271.1805 284.1409 143.1498 -0.5241 270.8429 271.3670 284.2039 143.9415 -0.5052 270.9910 271.4961 284.3417 144.7638 -0.5119 271.0854 271.5972 284.3931 145.5558 -0.5169 271.2770 271.7939 284.5124 146.3475 -0.5166 271.2984 271.8149 284.4413 147.1710 -0.4893 271.5494 272.0387 284.4956 147.9635 -0.4882 271.4851 271.9733 284.7865 148.7855 -0.5038 271.7546 272.2584 284.7854 149.5775 -0.4854 271.8898 272.3751 284.8332 150.3695 -0.5300 271.9334 272.4634 284.9889 151.2215 -0.5369 272.0831 272.6200 285.2827 151.9858 -0.5365 272.2872 272.8236 285.2945 152.8098 -0.5248 272.4378 272.9626 285.3394 153.6035 -0.5365 272.6752 273.2117 285.4013 154.3965 -0.5334 272.7514 273.2848 285.6444 155.2183 -0.5321 272.9750 273.5071 285.7449 155.9795 -0.5065 273.0156 273.5221 285.9417 156.8340 -0.4857 272.9872 273.4729 286.2359 157.6258 -0.5022 273.0351 273.5373 286.2133 158.4175 -0.5275 273.1897 273.7173 286.3333 159.2410 -0.5082 273.4252 273.9335 286.5459 160.0070 -0.5439 273.4335 273.9774 286.8184 160.8608 -0.5368 273.6011 274.1379 286.9532 161.6230 -0.5522 273.7103 274.2625 287.0048 162.4468 -0.5591 273.8932 274.4523 287.1746 163.2468 -0.5522 274.0132 274.5654 287.2830 164.0415 -0.5383 274.0385 274.5768 287.3168 164.8645 -0.5466 274.2990 274.8456 287.3820 165.6565 -0.5779 274.5039 275.0817 287.5476 166.4788 -0.5627 274.5580 275.1207 287.7399 167.2705 -0.5592 274.5297 275.0890 287.8498 168.0625 -0.5573 274.6935 275.2508 288.0250 168.8848 -0.5638 274.8371 275.4009 288.0459 169.6785 -0.5543 275.0591 275.6134 288.0866 170.5015 -0.5502 275.1144 275.6647 288.1722 171.2923 -0.5384 275.3221 275.8605 288.2628 172.0810 -0.5106 275.3432 275.8538 288.4261 172.8990 -0.5450 275.4300 275.9749 288.4395 173.6568 -0.5379 275.3693 275.9072 288.5148 174.5070 -0.5594 275.6775 276.2369 288.6111 175.2948 -0.5553 275.8880 276.4432 288.7545 176.0830 -0.5508 275.8500 276.4008 288.7732 176.9020 -0.5652 275.9675 276.5327 288.7309 177.6610 -0.5828 276.2427 276.8255 288.8557 178.5093 -0.5522 276.4863 277.0385 288.8902 179.2685 -0.5652 276.3958 276.9611 288.9796 180.0898 -0.5778 276.6011 277.1789 289.0534 180.9083 -0.5955 276.7263 277.3218 289.1564 181.6678 -0.5936 276.8028 277.3964 289.2659 182.5203 -0.5954 276.8793 277.4747 289.3458 183.2828 -0.5957 276.9810 277.5767 289.5361 184.1130 -0.6110 277.1539 277.7649 289.6568 184.9013 -0.6003 277.2535 277.8539 289.6427 185.6908 -0.5887 277.3431 277.9317 289.7170 186.5100 -0.5959 277.6097 278.2056 289.8800 187.3000 -0.6003 277.6198 278.2202 290.0030 188.1215 -0.6082 277.7025 278.3107 290.1120 188.9095 -0.6146 277.8272 278.4418 290.2104 189.6993 -0.6014 277.9546 278.5560 290.3054 190.5480 -0.6224 278.1726 278.7950 290.4218 191.3068 -0.6289 278.2852 278.9141 290.4126 192.1265 -0.6226 278.3536 278.9761 290.5732 192.9460 -0.6354 278.3695 279.0049 290.7512 193.7060 -0.6327 278.4229 279.0556 290.8480 194.5573 -0.6268 278.4946 279.1214 290.9854 195.3180 -0.6342 278.7097 279.3439 291.0003 196.1398 -0.6285 279.0364 279.6649 291.1366 196.9618 -0.6200 279.0334 279.6535 291.3800 197.7235 -0.6402 279.2688 279.9090 291.4434 198.5765 -0.6385 279.4311 280.0696 291.6006 199.3385 -0.6531 279.3641 280.0172 291.6432 200.1605 -0.6640 279.2835 279.9476 291.7967 200.9530 -0.6285 279.4903 280.1187 291.8680 201.7445 -0.6304 279.6593 280.2896 291.9800 202.5965 -0.6283 279.5881 280.2164 292.1345 203.3610 -0.6521 279.6692 280.3213 292.1825 204.1855 -0.6527 279.8795 280.5322 292.3179 204.9775 -0.6415 280.1599 280.8014 292.4488 205.7695 -0.6567 280.4157 281.0724 292.5456 206.6215 -0.6393 280.3210 280.9603 292.6816 207.3860 -0.6591 280.6403 281.2994 292.6800 208.2095 -0.6711 280.8202 281.4912 292.8394 209.0048 -0.6579 280.8884 281.5463 293.0528 209.7975 -0.6521 280.9499 281.6020 293.2040 210.6253 -0.6799 281.0511 281.7310 293.2472 211.3888 -0.6705 281.1635 281.8341 293.3833 212.2425 -0.6526 281.2954 281.9481 293.4089 213.0070 -0.6559 281.5140 282.1700 293.5178 213.8308 -0.6645 281.5249 282.1893 293.6593 214.6235 -0.6799 281.6185 282.2984 293.7310 215.4145 -0.6865 281.5659 282.2524 293.8975 216.2670 -0.6840 281.8134 282.4974 293.9456 217.0288 -0.6599 281.9617 282.6216 293.9538 217.8518 -0.6587 282.1319 282.7906 293.9987 218.6438 -0.6679 282.2245 282.8924 294.1102 219.4355 -0.6728 282.1990 282.8718 294.3018 220.2593 -0.6784 282.3220 283.0004 294.3536 221.0515 -0.6708 282.5341 283.2049 294.4593 221.8738 -0.6919 282.5276 283.2195 294.5234 222.6660 -0.6942 282.6137 283.3079 294.5338 223.4595 -0.7198 282.8067 283.5265 294.6597 224.2825 -0.7237 282.9312 283.6549 294.8924 225.0745 -0.7408 282.9963 283.7371 294.9839 225.8985 -0.7443 283.0934 283.8377 295.0428 226.6905 -0.7469 283.2108 283.9577 295.1356 227.4825 -0.7387 283.2971 284.0357 295.2096 228.3345 -0.7400 283.3001 284.0402 295.3675 229.0968 -0.7400 283.5055 284.2455 295.4106 229.9195 -0.7477 283.5541 284.3018 295.6558 230.7115 -0.7318 283.6185 284.3503 295.7782 231.5035 -0.7417 283.9644 284.7061 295.9582 232.3260 -0.7389 284.0083 284.7473 296.0799 233.1185 -0.7430 284.1431 284.8860 296.3027 233.9398 -0.7494 284.3285 285.0779 296.5245 234.7325 -0.7568 284.4514 285.2082 296.8331 235.5233 -0.7344 284.5335 285.2679 297.0586 236.3415 -0.7019 284.5207 285.2226 297.2014 237.1000 -0.7119 284.6705 285.3824 297.3457 237.9483 -0.6893 284.7561 285.4454 297.2663 238.7360 -0.7053 284.8414 285.5467 297.5746 239.5245 -0.7141 284.8402 285.5543 297.7420 240.3430 -0.7129 285.0276 285.7405 297.6882 241.1028 -0.6972 285.1181 285.8153 297.8101 241.9530 -0.7092 285.2107 285.9199 297.8571 242.7115 -0.6973 285.4468 286.1440 297.8666 243.5310 -0.7084 285.5811 286.2895 297.8965 244.3490 -0.6882 285.6676 286.3558 297.7447 245.1070 -0.6780 285.8295 286.5076 297.9853 245.9550 -0.6934 285.9820 286.6755 298.1627 246.7433 -0.6901 285.9828 286.6729 298.0877 247.5320 -0.6977 286.0904 286.7881 298.2634 248.3500 -0.7118 286.3481 287.0600 298.2735 249.1380 -0.6946 286.4071 287.1017 298.2130 249.9568 -0.6970 286.4182 287.1152 298.2435 250.7453 -0.7245 286.5719 287.2963 298.3696 251.5350 -0.7423 286.8400 287.5823 298.3780 252.3555 -0.7419 287.0195 287.7613 298.4798 253.1455 -0.7563 287.2507 288.0070 298.7829 253.9660 -0.7759 287.4713 288.2472 299.0056 254.7543 -0.7809 287.5029 288.2839 299.0854 255.5430 -0.7899 287.6136 288.4035 299.2904 256.3925 -0.7742 287.8069 288.5811 299.2306 257.1820 -0.7530 287.7993 288.5523 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