DTA measure 2gyors Date: 2024108:1538 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.32 s Mass = 967.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3486 -4.3737 441.4537 445.8274 424.7121 3.9470 -4.3905 441.4072 445.7977 424.6587 5.5606 -4.4047 441.4906 445.8953 424.4856 7.1786 -4.4140 441.5507 445.9648 424.4971 8.7926 -4.4293 441.4422 445.8715 424.6107 10.3919 -4.4326 441.4232 445.8557 424.4273 11.9935 -4.4438 441.5441 445.9879 424.2327 13.6075 -4.4489 441.6711 446.1200 424.2729 15.2216 -4.4492 441.5145 445.9637 423.9725 16.8365 -4.4545 441.5230 445.9775 423.7666 18.4359 -4.4581 441.6653 446.1234 423.6751 20.0355 -4.4895 441.6526 446.1421 423.5142 21.6471 -4.4745 441.6431 446.1176 423.1592 23.2545 -4.4876 441.6400 446.1276 422.9113 24.8520 -4.4963 441.6952 446.1915 422.7350 26.4460 -4.4956 441.7640 446.2596 422.4365 28.0524 -4.5025 441.6876 446.1902 422.2286 29.6445 -4.5133 441.5865 446.0998 422.1590 31.2456 -4.5259 441.5691 446.0949 421.8987 32.9055 -4.5194 441.6340 446.1534 421.6119 34.5049 -4.5306 441.6932 446.2238 421.3771 36.1120 -4.5102 441.7197 446.2299 421.1267 37.7713 -4.5151 441.6034 446.1185 420.8909 39.4450 -4.5266 441.5694 446.0960 420.6876 41.0459 -4.5508 441.5040 446.0548 420.4866 42.6455 -4.5485 441.5554 446.1039 420.4030 44.2606 -4.5541 441.5557 446.1099 420.2111 45.8596 -4.5667 441.5461 446.1128 419.9270 47.4889 -4.5518 441.5009 446.0527 419.7245 49.0888 -4.5632 441.3721 445.9353 419.7085 50.7026 -4.5561 441.3914 445.9476 419.4958 52.3025 -4.5655 441.3888 445.9543 419.2078 53.8981 -4.5803 441.4029 445.9832 418.8475 55.5050 -4.5641 441.4618 446.0259 418.6610 57.1110 -4.5662 441.2067 445.7730 418.6735 58.7171 -4.5588 441.1854 445.7442 418.4556 60.3120 -4.5468 441.1215 445.6684 418.1101 61.9089 -4.5650 441.1418 445.7068 418.0467 63.5318 -4.5837 441.2268 445.8105 417.7958 65.1423 -4.5793 441.1198 445.6990 417.5635 66.7413 -4.5748 441.0032 445.5780 417.4092 68.3405 -4.5901 440.9293 445.5194 417.2326 69.9603 -4.5790 440.8737 445.4527 417.0530 71.5638 -4.5801 440.8898 445.4699 416.8480 73.1791 -4.5832 440.7875 445.3708 416.7494 74.7810 -4.5847 440.7655 445.3502 416.4148 76.3815 -4.5815 440.7164 445.2979 416.1928 77.9816 -4.5552 440.5473 445.1024 416.0989 79.5959 -4.5733 440.4539 445.0272 415.7854 81.2104 -4.5322 440.5103 445.0425 415.5727 82.8276 -4.5127 440.3855 444.8982 415.2762 84.4273 -4.5304 440.4805 445.0109 415.0133 86.0226 -4.5690 440.1793 444.7483 414.9120 87.6139 -4.5567 440.1073 444.6639 414.7415 89.2354 -4.5658 440.1443 444.7101 414.5149 90.8416 -4.5826 440.1202 444.7028 414.3453 92.4386 -4.5917 439.9619 444.5535 414.2392 94.0354 -4.5928 439.6977 444.2905 413.9079 95.6428 -4.6024 439.7749 444.3773 413.7513 97.2521 -4.6066 439.7420 444.3486 413.4988 98.8643 -4.6133 439.6077 444.2210 413.3325 100.4626 -4.5917 439.5312 444.1228 413.1795 102.0623 -4.6001 439.5909 444.1910 413.0855 103.6766 -4.6052 439.3556 443.9608 412.8204 105.2758 -4.6003 439.2559 443.8562 412.6884 106.9049 -4.5914 439.2752 443.8665 412.4689 108.5035 -4.6162 439.1012 443.7174 412.3285 110.1035 -4.6017 438.9892 443.5909 412.0907 111.7185 -4.6019 438.9223 443.5242 411.7513 113.3198 -4.5999 438.6477 443.2477 411.6358 114.9495 -4.5984 438.7609 443.3593 411.3668 116.5488 -4.6166 438.6889 443.3055 411.1451 118.1519 -4.5992 438.5141 443.1133 411.0418 119.7461 -4.5913 438.4138 443.0052 410.8496 121.3394 -4.5763 438.3532 442.9295 410.4971 122.9610 -4.5966 438.1871 442.7837 410.3335 124.5528 -4.5816 437.9208 442.5025 410.1866 126.1623 -4.5964 437.9329 442.5293 410.0187 127.7549 -4.6065 437.7124 442.3189 409.8874 129.3636 -4.6222 437.6502 442.2724 409.6172 130.9909 -4.6299 437.6770 442.3069 409.2491 132.5885 -4.6144 437.5712 442.1856 409.0153 134.1874 -4.5704 437.3456 441.9160 408.8764 135.7869 -4.5798 437.2860 441.8658 408.6226 137.4008 -4.5957 437.1246 441.7203 408.4144 139.0298 -4.5917 437.0013 441.5930 408.3144 140.6295 -4.6020 436.8869 441.4889 408.1803 142.2296 -4.5960 436.7584 441.3543 407.8248 143.8450 -4.5849 436.7324 441.3173 407.6412 145.4446 -4.6035 436.5698 441.1733 407.5750 147.0586 -4.5791 436.3516 440.9307 407.3302 148.6759 -4.5736 436.2166 440.7903 407.2101 150.2881 -4.5726 436.1782 440.7508 406.9803 151.8813 -4.5684 436.0102 440.5787 406.7052 153.4754 -4.5988 435.9027 440.5015 406.4241 155.0685 -4.5998 435.7659 440.3656 406.2884 156.6909 -4.5939 435.6387 440.2327 405.9550 158.2983 -4.5978 435.4807 440.0785 405.8702 159.9065 -4.5964 435.3448 439.9412 405.6117 161.5021 -4.5940 435.1605 439.7545 405.4335 163.1004 -4.5857 435.1366 439.7223 405.2567 164.7338 -4.5910 434.8924 439.4834 405.0310 166.3320 -4.5725 434.7155 439.2880 404.8228 167.9315 -4.5811 434.6707 439.2518 404.7072 169.5305 -4.5753 434.5035 439.0788 404.4706 171.1445 -4.5728 434.4174 438.9903 404.2811 172.7619 -4.5697 434.2560 438.8257 404.0267 174.3655 -4.5710 434.1068 438.6778 403.7943 175.9795 -4.5819 433.9298 438.5118 403.6381 177.5793 -4.5744 433.7068 438.2812 403.4774 179.1816 -4.5737 433.6407 438.2144 403.1310 180.7975 -4.5444 433.5200 438.0645 403.0229 182.4094 -4.5302 433.2616 437.7918 402.7629 184.0051 -4.5701 432.9992 437.5693 402.5290 185.6051 -4.5655 433.0549 437.6204 402.4239 187.2118 -4.5771 432.8082 437.3853 402.1502 188.8198 -4.5848 432.7525 437.3373 402.0068 190.4280 -4.5751 432.6931 437.2682 401.7032 192.0378 -4.5795 432.4388 437.0183 401.5795 193.6341 -4.5710 432.2396 436.8106 401.4699 195.2323 -4.5629 432.1711 436.7340 401.0945 196.8468 -4.5704 431.9634 436.5338 400.8994 198.4623 -4.5503 431.8642 436.4146 400.6921 200.0778 -4.5523 431.6711 436.2234 400.5238 201.6804 -4.5499 431.5215 436.0714 400.2369 203.2830 -4.5445 431.3282 435.8727 400.1241 204.8826 -4.5404 431.2038 435.7442 399.8690 206.5130 -4.5364 431.0792 435.6157 399.6266 208.1136 -4.5408 430.8823 435.4231 399.4227 209.7275 -4.5353 430.7557 435.2911 399.1500 211.3270 -4.4974 430.6099 435.1073 398.9641 212.9265 -4.5220 430.4219 434.9439 398.8267 214.5446 -4.5599 430.1552 434.7150 398.6159 216.1453 -4.5197 430.0814 434.6011 398.2800 217.7398 -4.5349 430.0251 434.5599 398.1915 219.3411 -4.5318 429.7772 434.3090 398.1118 220.9526 -4.5320 429.5828 434.1149 397.8652 222.5454 -4.5272 429.3528 433.8800 397.6751 224.1535 -4.5173 429.3174 433.8346 397.4570 225.7648 -4.5192 429.2181 433.7373 397.0486 227.3634 -4.5063 428.9932 433.4995 396.9336 228.9785 -4.5136 428.7109 433.2245 396.8793 230.5825 -4.5020 428.5341 433.0362 396.6630 232.1879 -4.5249 428.3827 432.9076 396.4496 233.7931 -4.5077 428.2852 432.7929 396.2828 235.4121 -4.5048 428.1217 432.6265 396.0870 237.0173 -4.5054 427.9047 432.4102 395.9491 238.6206 -4.4970 427.7728 432.2698 395.7256 240.2196 -4.4869 427.4594 431.9463 395.4941 241.8200 -4.4927 427.4210 431.9138 395.1252 243.4346 -4.4772 427.1348 431.6119 394.9967 245.0501 -4.4844 426.9592 431.4436 394.8666 246.6555 -4.4758 426.9243 431.4000 394.5345 248.2508 -4.4686 426.7516 431.2203 394.3200 249.8585 -4.4617 426.4943 430.9560 394.1566 251.4519 -4.4473 426.3893 430.8366 393.8978 253.0611 -4.4296 426.1596 430.5892 393.6480 254.6721 -4.4174 425.9738 430.3912 393.5071 256.2773 -4.4346 425.6907 430.1253 393.3665 257.8726 -4.4391 425.6379 430.0770 393.1338 259.4866 -4.4339 425.4294 429.8633 392.8225 261.0771 -4.4329 425.2566 429.6895 392.7382 262.7078 -4.4389 425.0871 429.5261 392.5587 264.3106 -4.4399 424.9495 429.3893 392.2309 265.9151 -4.4293 424.7392 429.1685 392.0521 267.5175 -4.4195 424.6130 429.0325 391.8526 269.1315 -4.4223 424.4665 428.8889 391.5735 270.7324 -4.4294 424.2671 428.6966 391.3609 272.3513 -4.4072 423.9946 428.4018 391.2495 273.9654 -4.4125 423.8763 428.2888 391.0016 275.5653 -4.4108 423.6505 428.0612 390.9121 277.1725 -4.4031 423.3739 427.7770 390.6304 278.7715 -4.3971 423.3993 427.7964 390.3321 280.3818 -4.3828 423.0369 427.4197 390.1567 281.9905 -4.3936 422.9571 427.3507 390.0040 283.5855 -4.3890 422.6960 427.0850 389.7958 285.1774 -4.3881 422.5174 426.9054 389.5811 286.7889 -4.3753 422.2609 426.6362 389.5133 288.3830 -4.3729 422.1727 426.5457 389.2022 289.9945 -4.3640 422.0298 426.3938 388.9725 291.6114 -4.3616 421.8055 426.1671 388.7899 293.2134 -4.3644 421.6434 426.0078 388.5864 294.8175 -4.3551 421.4994 425.8545 388.4183 296.4221 -4.3395 421.2606 425.6001 388.1321 298.0151 -4.3196 421.0022 425.3218 387.9552 299.6469 -4.3349 420.9534 425.2884 387.7610 301.2478 -4.3280 420.6784 425.0064 387.4649 302.8470 -4.3221 420.5725 424.8945 387.2484 304.4616 -4.3126 420.2800 424.5927 387.0058 306.0618 -4.3044 420.1814 424.4858 386.8677 307.6718 -4.2989 419.9640 424.2629 386.7164 309.2884 -4.2919 419.6260 423.9178 386.5028 310.9023 -4.2886 419.6474 423.9360 386.2462 312.4963 -4.2846 419.4477 423.7323 386.0110 314.0880 -4.2849 419.2066 423.4915 385.7831 315.6940 -4.2665 419.0739 423.3404 385.7293 317.3160 -4.2647 418.8280 423.0928 385.3910 318.9160 -4.2497 418.7804 423.0301 385.1453 320.5085 -4.2399 418.5325 422.7723 384.9207 322.1168 -4.2525 418.3415 422.5941 384.7542 323.7131 -4.2425 418.0996 422.3422 384.5344 325.3259 -4.2291 417.9422 422.1713 384.3386 326.9455 -4.2141 417.5859 421.7999 384.1785 328.5456 -4.2153 417.4301 421.6454 383.9319 330.1475 -4.2020 417.2813 421.4834 383.7418 331.7519 -4.2076 417.1252 421.3329 383.6369 333.3581 -4.1958 416.9950 421.1908 383.3209 334.9678 -4.2002 416.6948 420.8950 383.0685 336.5850 -4.2008 416.5620 420.7629 383.0235 338.1943 -4.1940 416.2854 420.4794 382.8044 339.7978 -4.1727 416.2469 420.4196 382.6255 341.4006 -4.1752 416.0246 420.1998 382.3801 343.0173 -4.1828 415.7584 419.9411 382.2079 344.6115 -4.1749 415.4807 419.6556 382.0170 346.2228 -4.1515 415.4505 419.6020 381.7093 347.8155 -4.1325 415.3331 419.4656 381.5488 349.4234 -4.1414 414.9863 419.1278 381.2911 351.0165 -4.1320 414.9199 419.0520 381.0918 352.6111 -4.1205 414.5325 418.6530 380.9323 354.2378 -4.1216 414.2550 418.3767 380.6322 355.8479 -4.1182 414.1799 418.2981 380.3455 357.4474 -4.1168 413.9059 418.0227 380.2326 359.0545 -4.1057 413.7989 417.9046 380.0090 360.6574 -4.1114 413.5894 417.7008 379.7939 362.2598 -4.1123 413.3570 417.4693 379.5692 363.8640 -4.0849 413.3452 417.4302 379.4349 365.4823 -4.0775 413.0985 417.1760 379.1501 367.0965 -4.0595 412.9000 416.9595 379.0499 368.6968 -4.0561 412.7137 416.7698 378.6931 370.2980 -4.0600 412.3677 416.4277 378.6390 371.8975 -4.0355 412.1905 416.2260 378.3989 373.5268 -4.0423 412.0268 416.0691 378.1212 375.1315 -4.0225 411.8238 415.8464 377.9483 376.7340 -4.0321 411.7816 415.8137 377.6974 378.3305 -4.0308 411.5150 415.5458 377.5198 379.9285 -4.0135 411.3255 415.3390 377.2829 381.5229 -4.0165 411.0840 415.1004 377.0978 383.1299 -4.0115 410.9143 414.9258 376.9214 384.7411 -4.0117 410.5967 414.6084 376.6640 386.3370 -3.9966 410.4522 414.4488 376.3134 387.9494 -3.9911 410.3652 414.3563 376.2020 389.5545 -3.9783 410.1762 414.1546 376.0353 391.1561 -3.9759 409.9221 413.8981 375.6829 392.7731 -3.9750 409.5481 413.5231 375.4851 394.3878 -3.9697 409.5747 413.5445 375.3930 395.9879 -3.9715 409.2917 413.2631 375.2333 397.5891 -3.9567 409.0846 413.0414 375.0575 399.1959 -3.9683 408.8667 412.8350 374.8513 400.8014 -3.9787 408.8241 412.8028 374.6802 402.4259 -3.9818 408.6242 412.6060 374.3507 404.0285 -3.9683 408.3578 412.3260 374.2281 405.6275 -3.9460 408.1182 412.0641 373.9612 407.2415 -3.9318 407.8470 411.7788 373.7142 408.8390 -3.9328 407.7791 411.7119 373.6569 410.4376 -3.9322 407.5511 411.4834 373.5096 412.0468 -3.9183 407.2749 411.1931 373.3247 413.6550 -3.9195 407.0734 410.9929 373.1149 415.2483 -3.9306 406.8232 410.7538 372.9420 416.8419 -3.9420 406.6965 410.6385 372.8216 418.4519 -3.9432 406.4976 410.4408 372.6946 420.0616 -3.9319 406.3549 410.2868 372.5026 421.6801 -3.9238 406.1424 410.0663 372.3102 423.2813 -3.9189 405.9218 409.8407 372.0482 424.8819 -3.9007 405.8053 409.7060 371.7590 426.4815 -3.9067 405.5632 409.4699 371.6488 428.0955 -3.9110 405.3356 409.2467 371.5370 429.7136 -3.9027 405.1483 409.0510 371.2740 431.3194 -3.9032 405.0196 408.9228 371.0011 432.9198 -3.8981 404.8238 408.7219 370.7506 434.5336 -3.8983 404.5333 408.4316 370.6083 436.1334 -3.8814 404.2119 408.0933 370.1352 437.7326 -3.8585 404.1513 408.0097 369.9813 439.3653 -3.8692 403.9329 407.8021 369.8114 440.9634 -3.8644 403.7659 407.6304 369.6586 442.5555 -3.8590 403.6009 407.4599 369.4280 444.1490 -3.8449 403.3866 407.2315 369.1753 445.7576 -3.8570 403.1664 407.0233 368.9233 447.3648 -3.8461 402.8132 406.6593 368.8722 448.9730 -3.8434 402.8320 406.6754 368.5395 450.5766 -3.8378 402.7281 406.5659 368.3829 452.1774 -3.8212 402.4111 406.2323 368.1919 453.7756 -3.8064 402.0575 405.8639 367.8490 455.3748 -3.7996 401.9670 405.7666 367.6325 457.0049 -3.7997 401.7670 405.5667 367.5176 458.6080 -3.8256 401.6261 405.4517 367.3869 460.2130 -3.8108 401.4510 405.2617 367.1513 461.8205 -3.8232 401.1536 404.9768 367.0401 463.4200 -3.8143 401.0073 404.8215 366.7328 465.0241 -3.8006 400.7519 404.5526 366.5577 466.6395 -3.8035 400.6241 404.4276 366.3948 468.2560 -3.7756 400.4166 404.1923 366.2233 469.8565 -3.7779 400.1634 403.9413 365.9722 471.4649 -3.7836 399.8660 403.6496 365.5848 473.0621 -3.7826 399.6032 403.3858 365.3578 474.6549 -3.7732 399.3718 403.1450 365.0281 476.2778 -3.7694 399.2701 403.0396 364.7859 477.8841 -3.7447 399.1439 402.8886 364.3366 479.4776 -3.7362 398.9234 402.6596 364.0216 481.0834 -3.7464 398.6895 402.4359 363.8223 482.6843 -3.7362 398.5210 402.2573 363.6448 484.2818 -3.7146 398.1724 401.8870 363.3920 485.8993 -3.7227 398.0404 401.7631 363.3529 487.5134 -3.7364 397.9458 401.6823 363.2563 489.1125 -3.7043 397.6584 401.3627 363.1521 490.7131 -3.6981 397.4310 401.1291 362.9187 492.3231 -3.6871 397.3419 401.0290 362.7009 493.9249 -3.6975 397.0272 400.7247 362.5692 495.5548 -3.6905 396.9468 400.6373 362.2820 497.1561 -3.6990 396.5904 400.2893 362.2107 498.7584 -3.6944 396.4452 400.1396 362.0237 500.3586 -3.6918 396.1989 399.8907 361.7544 501.9851 -3.6933 396.0769 399.7702 361.5956 503.5855 -3.6727 395.7610 399.4337 361.3300 505.2000 -3.6795 395.5465 399.2259 361.1873 506.7954 -3.6829 395.5598 399.2427 361.0699 508.3870 -3.6654 395.2268 398.8922 360.7723 509.9930 -3.6681 394.9340 398.6021 360.6314 511.5996 -3.6700 394.7604 398.4304 360.3835 513.2078 -3.6576 394.5525 398.2100 360.2451 514.8008 -3.6541 394.4074 398.0615 359.8945 516.4134 -3.6617 394.2402 397.9019 359.7749 518.0121 -3.6527 393.9278 397.5805 359.5704 519.6260 -3.6413 393.8124 397.4537 359.2651 521.2388 -3.6448 393.5739 397.2187 359.1821 522.8486 -3.6480 393.4061 397.0541 359.0022 524.4475 -3.6254 393.1779 396.8034 358.7538 526.0470 -3.6383 393.0315 396.6698 358.5414 527.6615 -3.6200 392.7439 396.3639 358.3395 529.2606 -3.6042 392.6029 396.2071 358.1666 530.8899 -3.6002 392.4581 396.0584 357.8946 532.4884 -3.6010 392.1176 395.7186 357.6498 534.0956 -3.6098 391.9639 395.5737 357.4541 535.7096 -3.6023 391.7624 395.3647 357.2548 537.3090 -3.5960 391.6368 395.2328 357.0131 538.9001 -3.5877 391.3080 394.8957 356.8499 540.5221 -3.5965 391.1238 394.7203 356.6964 542.1233 -3.5789 391.0869 394.6659 356.3421 543.7178 -3.6007 390.7299 394.3306 356.1789 545.3114 -3.5862 390.5762 394.1623 355.9178 546.9200 -3.5723 390.5011 394.0734 355.6960 548.5291 -3.5576 390.2032 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-0.9868 256.8020 257.7888 222.7682 1596.9459 -0.9694 256.5445 257.5140 222.5812 1598.5800 -0.9132 256.3049 257.2181 222.4168 1600.1731 -0.9121 256.1927 257.1048 222.2222 1601.7700 -0.9021 256.0288 256.9309 221.9521 1603.3616 -0.9091 255.8641 256.7732 221.8462 1604.9680 -0.8784 255.5889 256.4673 221.8265 1606.5740 -0.8984 255.3704 256.2688 221.7405 1608.1843 -0.8650 255.1603 256.0253 221.8240 1609.7773 -0.8503 255.1698 256.0201 221.4772 1611.3704 -0.8711 254.9191 255.7902 221.4639 1612.9786 -0.8407 254.7222 255.5629 221.1918 1614.5863 -0.8856 254.5612 255.4468 220.9826 1616.1959 -0.9315 254.4724 255.4039 220.8129 1617.7898 -0.9204 254.2337 255.1540 220.6884 1619.4001 -0.9245 254.0080 254.9324 220.4257 1620.9944 -0.9357 253.7515 254.6872 220.1871 1622.6215 -0.9913 253.6297 254.6210 219.9882 1624.2199 -1.0202 253.3676 254.3878 219.8621 1625.8188 -1.0228 253.2683 254.2911 219.6113 1627.4333 -0.9957 253.0114 254.0071 219.3695 1629.0365 -0.9882 252.8452 253.8334 219.2167 1630.6508 -0.9960 252.6894 253.6854 218.9696 1632.2498 -0.9654 252.4723 253.4377 218.7764 1633.8636 -0.9554 252.4631 253.4185 218.2596 1635.4625 -0.9318 252.1198 253.0516 218.0120 1637.0648 -0.9283 251.9398 252.8682 217.8839 1638.6785 -0.9305 251.8849 252.8154 217.8615 1640.2926 -0.9327 251.5787 252.5114 217.8180 1641.8925 -0.9261 251.4049 252.3310 217.6480 1643.4915 -0.9371 251.2368 252.1739 217.7285 1645.1051 -0.9325 250.9390 251.8715 217.7985 1646.7038 -0.9026 250.8190 251.7216 217.6061 1648.3150 -0.8841 250.7361 251.6202 217.3603