DTA measure 2pb_updown_3 Date: 202691:1514 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.33 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2613 -4.7345 184.9208 189.6553 246.7013 2.0475 -4.7254 185.1420 189.8674 246.5930 2.8448 -4.7048 185.4602 190.1651 246.5676 3.6728 -4.6915 185.7459 190.4374 246.4337 4.4383 -4.6916 185.9846 190.6763 246.4286 5.2970 -4.6855 186.2527 190.9381 246.4989 6.0533 -4.6781 186.4961 191.1742 246.5214 6.8905 -4.6718 186.8043 191.4761 246.5172 7.6775 -4.6452 187.0030 191.6482 246.4601 8.4845 -4.6296 187.2618 191.8914 246.4076 9.3018 -4.6200 187.5799 192.1999 246.3374 10.0785 -4.6081 187.8056 192.4137 246.2786 10.9265 -4.6041 188.1184 192.7225 246.2136 11.6925 -4.5852 188.4212 193.0064 246.1988 12.5205 -4.5803 188.6956 193.2759 246.1548 13.3168 -4.5837 189.0006 193.5843 246.1268 14.1140 -4.5657 189.2908 193.8565 246.1267 14.9318 -4.5618 189.5988 194.1606 246.1056 15.7075 -4.5499 189.7940 194.3439 246.0595 16.5560 -4.5424 190.0723 194.6147 246.0385 17.3120 -4.5249 190.3689 194.8938 246.0355 18.1495 -4.5059 190.4490 194.9548 246.0212 18.9058 -4.4887 190.6407 195.1294 246.0614 19.7233 -4.4855 190.8775 195.3630 246.0674 20.5300 -4.4718 191.1824 195.6542 246.0521 21.3170 -4.4449 191.4145 195.8594 246.1337 22.1445 -4.4245 191.6857 196.1102 246.1991 22.9105 -4.4276 191.8257 196.2532 246.1527 23.7590 -4.4276 192.1116 196.5393 246.0844 24.5248 -4.4163 192.3637 196.7799 246.0647 25.3525 -4.4037 192.4730 196.8767 246.1305 26.1293 -4.3934 192.6845 197.0779 246.1643 26.9460 -4.3789 192.8759 197.2548 246.2371 27.7433 -4.3641 193.2157 197.5798 246.2183 28.5400 -4.3558 193.5063 197.8620 246.1254 29.3675 -4.3520 193.7281 198.0801 246.1399 30.1340 -4.3436 193.9647 198.3083 246.2324 30.9820 -4.3280 194.0641 198.3921 246.4109 31.7583 -4.3189 194.3304 198.6493 246.4285 32.5760 -4.3053 194.5809 198.8861 246.3713 33.3415 -4.2829 194.7268 199.0097 246.3513 34.1695 -4.2666 194.9858 199.2524 246.5523 34.9668 -4.2450 195.2296 199.4746 246.6428 35.7630 -4.2438 195.5022 199.7460 246.7018 36.5808 -4.2266 195.7343 199.9609 246.8530 37.3570 -4.2121 195.8994 200.1115 246.9094 38.2050 -4.1942 196.1725 200.3667 246.9558 38.9715 -4.1880 196.4513 200.6393 247.0251 39.7993 -4.1926 196.6782 200.8708 247.1222 40.6060 -4.1774 196.8695 201.0469 247.1653 41.3930 -4.1637 197.1707 201.3344 247.2689 42.2003 -4.1527 197.4275 201.5802 247.4120 42.9865 -4.1403 197.6816 201.8219 247.5849 43.8248 -4.1357 197.8916 202.0273 247.7762 44.5803 -4.1197 198.0331 202.1528 247.8756 45.4490 -4.1032 198.3090 202.4122 248.0781 46.2053 -4.1035 198.4676 202.5711 248.1855 47.0428 -4.1048 198.7675 202.8724 248.3139 47.8295 -4.1010 199.0712 203.1722 248.4223 48.6165 -4.0812 199.3655 203.4468 248.5409 49.4435 -4.0556 199.6424 203.6980 248.7373 50.2100 -4.0492 199.8775 203.9268 248.9400 51.0585 -4.0451 200.1387 204.1838 249.0638 51.8343 -4.0472 200.2577 204.3049 249.1736 52.6520 -4.0372 200.3825 204.4196 249.2367 53.4080 -4.0065 200.5883 204.5948 249.4190 54.2455 -3.9873 200.7888 204.7761 249.6781 55.0325 -3.9785 200.9551 204.9336 249.9358 55.8293 -3.9522 201.1740 205.1262 250.1688 56.6568 -3.9517 201.3058 205.2575 250.4259 57.4233 -3.9478 201.4500 205.3978 250.5700 58.2815 -3.9415 201.5627 205.5043 250.6780 59.0373 -3.9351 201.6730 205.6082 250.8690 59.8755 -3.9182 201.9316 205.8498 251.0682 60.6618 -3.9106 202.2522 206.1627 251.2604 61.4588 -3.9008 202.5275 206.4283 251.4636 62.2663 -3.8878 202.7674 206.6552 251.6441 63.0628 -3.8681 203.0031 206.8712 251.8069 63.8905 -3.8692 203.3022 207.1714 251.9911 64.6570 -3.8525 203.4550 207.3075 252.1732 65.5045 -3.8485 203.5943 207.4428 252.4859 66.2813 -3.8444 203.7952 207.6396 252.5716 67.0990 -3.8447 204.0385 207.8832 252.7445 67.8953 -3.8390 204.3181 208.1571 252.9623 68.6925 -3.8182 204.4914 208.3095 253.1697 69.5200 -3.8108 204.8066 208.6174 253.3704 70.2860 -3.8123 204.8941 208.7064 253.5357 71.1345 -3.8156 204.9920 208.8075 253.7491 71.9105 -3.7915 205.2335 209.0250 253.9313 72.7280 -3.7796 205.5031 209.2827 254.1318 73.5253 -3.7786 205.6898 209.4684 254.2572 74.3218 -3.7767 205.9172 209.6939 254.3857 75.1495 -3.7751 206.1441 209.9192 254.6109 75.9160 -3.7642 206.4169 210.1811 254.7835 76.7638 -3.7583 206.7080 210.4662 255.0052 77.5403 -3.7408 206.8024 210.5432 255.2138 78.3580 -3.7300 206.9664 210.6963 255.3859 79.1545 -3.7264 207.2630 210.9894 255.6097 79.9515 -3.7172 207.5835 211.3007 255.7368 80.7795 -3.7012 207.6816 211.3828 255.8100 81.5350 -3.7023 207.8724 211.5747 255.9337 82.3935 -3.7089 207.9500 211.6589 256.1269 83.1600 -3.7043 208.0408 211.7450 256.2276 83.9768 -3.7026 208.1861 211.8887 256.4505 84.7740 -3.6955 208.4302 212.1257 256.6303 85.5708 -3.6959 208.6805 212.3763 256.7952 86.3983 -3.6957 208.8595 212.5552 257.0147 87.1545 -3.6877 209.0193 212.7070 257.1655 88.0228 -3.6781 209.3155 212.9937 257.3120 88.7788 -3.6674 209.5584 213.2259 257.4276 89.5965 -3.6508 209.8857 213.5365 257.5630 90.4033 -3.6459 210.1442 213.7901 257.7579 91.1900 -3.6355 210.3702 214.0056 257.8910 92.0180 -3.6253 210.4636 214.0889 257.8814 92.7840 -3.6339 210.6898 214.3238 258.0696 93.6423 -3.6353 210.9089 214.5442 258.2896 94.4088 -3.6254 211.0459 214.6713 258.4502 95.2260 -3.6087 211.0982 214.7069 258.6055 96.0330 -3.5940 211.3189 214.9130 258.6675 96.8200 -3.5776 211.5763 215.1539 258.7587 97.6470 -3.5661 211.7405 215.3065 258.9174 98.4135 -3.5562 211.9560 215.5121 259.0095 99.2723 -3.5533 212.1720 215.7253 259.2945 100.0378 -3.5514 212.3045 215.8559 259.2923 100.8555 -3.5577 212.4320 215.9896 259.4059 101.6630 -3.5723 212.7233 216.2956 259.5967 102.4490 -3.5670 212.9553 216.5224 259.7019 103.2770 -3.5555 213.2284 216.7839 259.8600 104.0433 -3.5506 213.3569 216.9074 260.0471 104.9013 -3.5480 213.5635 217.1116 260.1459 105.6678 -3.5377 213.8046 217.3423 260.2679 106.4855 -3.5360 214.0248 217.5608 260.3034 107.2920 -3.5244 214.2048 217.7292 260.4221 108.0893 -3.5228 214.4262 217.9490 260.5861 108.9173 -3.5264 214.4825 218.0089 260.7214 109.6725 -3.5311 214.5459 218.0770 260.8768 110.5415 -3.5089 214.7467 218.2556 260.9463 111.2978 -3.5005 214.9887 218.4892 261.0522 112.1248 -3.4939 215.2476 218.7415 261.2080 112.9220 -3.4962 215.3670 218.8632 261.3926 113.7085 -3.4943 215.5979 219.0922 261.5144 114.5053 -3.4907 215.7545 219.2452 261.6180 115.3025 -3.4915 215.9969 219.4884 261.7447 116.1300 -3.4831 216.2752 219.7583 261.8986 116.8960 -3.4782 216.4518 219.9300 261.9455 117.7445 -3.4747 216.6190 220.0937 262.1344 118.5203 -3.4755 216.8193 220.2948 262.0887 119.3380 -3.4609 216.9409 220.4018 262.2541 120.1250 -3.4657 217.1460 220.6116 262.4059 120.9315 -3.4504 217.3993 220.8497 262.5051 121.7185 -3.4485 217.6753 221.1238 262.5612 122.5153 -3.4462 217.8689 221.3150 262.7161 123.3428 -3.4375 217.9586 221.3961 262.9078 124.1093 -3.4473 218.1843 221.6316 262.8974 124.9673 -3.4299 218.4674 221.8973 262.9456 125.7335 -3.4209 218.5662 221.9871 263.0858 126.5615 -3.4232 218.7621 222.1853 263.2404 127.3578 -3.4213 218.9215 222.3427 263.4501 128.1550 -3.4071 219.1146 222.5217 263.5942 128.9725 -3.3905 219.3390 222.7296 263.7241 129.7485 -3.3842 219.4488 222.8331 263.8759 130.5970 -3.3749 219.6755 223.0503 263.9543 131.3423 -3.3677 219.8202 223.1879 264.0026 132.1905 -3.3499 219.9817 223.3316 264.0746 132.9673 -3.3433 220.1325 223.4758 264.1548 133.7840 -3.3353 220.4024 223.7377 264.3222 134.5813 -3.3333 220.5463 223.8795 264.3920 135.3785 -3.3270 220.7452 224.0721 264.4732 136.2055 -3.3268 220.9368 224.2636 264.6456 136.9720 -3.3244 221.0888 224.4131 264.7803 137.8308 -3.3212 221.2641 224.5853 264.9087 138.5963 -3.3364 221.4802 224.8165 265.0779 139.4243 -3.3418 221.6947 225.0366 265.1981 140.1903 -3.3352 221.8130 225.1482 265.3288 141.0178 -3.3254 222.0107 225.3360 265.5833 141.8150 -3.3223 222.1688 225.4912 265.7453 142.6115 -3.3166 222.2696 225.5861 265.9035 143.4393 -3.3141 222.5203 225.8344 265.9404 144.1955 -3.3053 222.6285 225.9338 265.9985 145.0535 -3.3037 222.9390 226.2427 266.1812 145.8095 -3.2894 223.0850 226.3745 266.2661 146.6375 -3.2928 223.1875 226.4803 266.3189 147.4338 -3.2929 223.4299 226.7228 266.4571 148.2310 -3.2772 223.6382 226.9154 266.5566 149.0485 -3.2630 223.7764 227.0395 266.7007 149.8143 -3.2476 223.9789 227.2265 266.7189 150.6423 -3.2494 224.2753 227.5248 266.8043 151.3978 -3.2531 224.4926 227.7457 266.9365 152.2665 -3.2595 224.6295 227.8891 267.1073 153.0225 -3.2596 224.8509 228.1105 267.3247 153.8600 -3.2584 225.0743 228.3327 267.3747 154.6163 -3.2547 225.2289 228.4836 267.4921 155.4540 -3.2336 225.3544 228.5881 267.6660 156.2405 -3.2284 225.4972 228.7255 267.8249 157.0378 -3.2319 225.7445 228.9764 267.9901 157.8655 -3.2237 225.9044 229.1281 268.1807 158.6313 -3.2208 226.0172 229.2380 268.4123 159.4900 -3.2206 226.2041 229.4247 268.5300 160.2463 -3.2259 226.3128 229.5387 268.7324 161.0835 -3.2460 226.3805 229.6265 268.8574 161.8705 -3.2336 226.5832 229.8168 268.9689 162.6778 -3.2164 226.7136 229.9300 268.9905 163.4948 -3.2089 226.8983 230.1073 269.1217 164.2715 -3.1994 227.0967 230.2961 269.2238 165.1095 -3.1886 227.3855 230.5741 269.4314 165.8753 -3.1795 227.6202 230.7997 269.6151 166.7340 -3.1767 227.8006 230.9773 269.7372 167.4898 -3.1680 227.8873 231.0553 269.9211 168.3275 -3.1719 228.0913 231.2632 270.1523 169.1145 -3.1789 228.3180 231.4969 270.3813 169.9113 -3.1757 228.5323 231.7080 270.5914 170.7388 -3.1619 228.7019 231.8638 270.7803 171.5053 -3.1648 228.8634 232.0282 270.8686 172.3635 -3.1696 228.9693 232.1389 271.0241 173.1193 -3.1607 229.1649 232.3256 271.1179 173.9575 -3.1609 229.5178 232.6786 271.1937 174.7133 -3.1510 229.6819 232.8329 271.2620 175.5715 -3.1424 229.7869 232.9294 271.3159 176.3380 -3.1370 229.8714 233.0084 271.4139 177.1550 -3.1401 230.1829 233.3230 271.4523 177.9520 -3.1459 230.2765 233.4223 271.6217 178.7390 -3.1476 230.4897 233.6374 271.6965 179.5663 -3.1479 230.5690 233.7169 271.7660 180.3325 -3.1425 230.7004 233.8429 271.8844 181.1913 -3.1346 230.8262 233.9608 272.0639 181.9263 -3.1291 230.9858 234.1149 272.1185 182.7745 -3.1156 231.1527 234.2683 272.2816 183.5408 -3.1074 231.3256 234.4330 272.4343 184.3680 -3.1158 231.5427 234.6584 272.5718 185.1653 -3.1198 231.6704 234.7902 272.6756 185.9620 -3.1163 231.7902 234.9065 272.6771 186.7793 -3.1070 232.0044 235.1114 272.8123 187.5458 -3.1046 232.1981 235.3027 273.0090 188.4043 -3.1195 232.4954 235.6148 273.1448 189.1598 -3.1226 232.6293 235.7519 273.2226 189.9878 -3.1227 232.8551 235.9778 273.2945 190.7845 -3.1092 233.0501 236.1594 273.3741 191.5813 -3.1127 233.2742 236.3869 273.4905 192.4093 -3.1209 233.4851 236.6060 273.7282 193.1645 -3.1149 233.5695 236.6844 273.9212 194.0335 -3.1199 233.6852 236.8051 274.1339 194.7898 -3.0963 233.8974 236.9937 274.3201 195.6168 -3.0771 234.0911 237.1683 274.3498 196.4140 -3.0772 234.2422 237.3194 274.5129 197.2108 -3.0790 234.3292 237.4082 274.6529 198.0690 -3.0727 234.5409 237.6136 274.7670 198.8253 -3.0635 234.7506 237.8142 274.9156 199.6630 -3.0499 235.0092 238.0591 275.0920 200.4598 -3.0517 235.1760 238.2277 275.2443 201.2570 -3.0382 235.2500 238.2882 275.4087 202.0743 -3.0497 235.3455 238.3953 275.6098 202.8505 -3.0606 235.5871 238.6478 275.7130 203.6990 -3.0646 235.8967 238.9613 275.8703 204.4440 -3.0603 236.0600 239.1203 276.0594 205.2925 -3.0422 236.1287 239.1710 276.2133 206.0693 -3.0326 236.1932 239.2258 276.4169 206.8860 -3.0382 236.4184 239.4566 276.7009 207.6833 -3.0304 236.5607 239.5911 276.8876 208.4800 -3.0377 236.7243 239.7620 276.9669 209.3075 -3.0611 236.9349 239.9960 277.1207 210.0638 -3.0561 237.1606 240.2167 277.2985 210.9218 -3.0458 237.3252 240.3710 277.5249 211.6778 -3.0337 237.4462 240.4799 277.4925 212.5058 -3.0305 237.6167 240.6472 277.5834 213.3020 -3.0345 237.7400 240.7746 277.7060 214.0993 -3.0382 237.9045 240.9427 277.7869 214.9168 -3.0326 238.1440 241.1766 277.9144 215.6825 -3.0300 238.3194 241.3494 277.9981 216.5413 -3.0236 238.5449 241.5686 278.1067 217.3073 -3.0211 238.7919 241.8130 278.2582 218.1245 -3.0175 239.0481 242.0656 278.4282 218.9320 -3.0103 239.1788 242.1890 278.5557 219.7183 -2.9976 239.2780 242.2756 278.6619 220.5460 -2.9946 239.4104 242.4050 278.8036 221.3123 -2.9896 239.6557 242.6453 278.8997 222.1703 -2.9996 239.6622 242.6618 279.0147 222.9368 -2.9953 239.8013 242.7965 279.1645 223.7540 -2.9780 240.0299 243.0078 279.2754 224.5610 -2.9611 240.1663 243.1274 279.4350 225.3480 -2.9612 240.3200 243.2811 279.5115 226.1550 -2.9743 240.4556 243.4299 279.7037 226.9825 -2.9656 240.5905 243.5561 279.9830 227.7798 -2.9609 240.6780 243.6389 280.1991 228.5763 -2.9633 240.8711 243.8343 280.2304 229.3938 -2.9549 241.1146 244.0695 280.3278 230.1705 -2.9540 241.2063 244.1603 280.4678 231.0180 -2.9530 241.4568 244.4098 280.6531 231.7845 -2.9589 241.6226 244.5815 280.7973 232.6123 -2.9605 241.7768 244.7373 280.8324 233.4088 -2.9647 241.8868 244.8516 280.8699 234.2060 -2.9672 241.9918 244.9590 280.9233 235.0338 -2.9617 242.2249 245.1866 281.0673 235.8098 -2.9552 242.3521 245.3074 281.2853 236.6275 -2.9483 242.5151 245.4635 281.4814 237.4243 -2.9569 242.6640 245.6209 281.5169 238.2518 -2.9627 242.8042 245.7669 281.5918 239.0183 -2.9527 242.9364 245.8891 281.7057 239.8765 -2.9354 243.2087 246.1441 281.8374 240.6323 -2.9395 243.3377 246.2772 281.9931 241.4603 -2.9399 243.4726 246.4125 282.0706 242.2463 -2.9422 243.6239 246.5661 282.2064 243.0435 -2.9378 243.7754 246.7132 282.3556 243.8408 -2.9250 243.9499 246.8748 282.4056 244.6373 -2.9232 244.1459 247.0691 282.5208 245.4548 -2.9199 244.2939 247.2138 282.6828 246.2315 -2.9092 244.6005 247.5097 282.7359 247.0790 -2.9006 244.8869 247.7875 282.8276 247.8455 -2.9073 245.1144 248.0217 282.9739 248.6730 -2.9078 245.3104 248.2183 283.1116 249.4698 -2.9123 245.4761 248.3884 283.2622 250.2670 -2.9238 245.6106 248.5344 283.3385 251.0845 -2.9230 245.7197 248.6426 283.3023 251.8605 -2.9135 245.9538 248.8673 283.3112 252.7090 -2.9026 246.0943 248.9968 283.4683 253.4748 -2.9004 246.2445 249.1449 283.6777 254.3025 -2.9032 246.4684 249.3716 283.9046 255.0998 -2.9048 246.5980 249.5028 284.1221 255.8963 -2.9057 246.7033 249.6090 284.3396 256.7138 -2.9016 246.7868 249.6884 284.4528 257.4905 -2.8902 246.9724 249.8627 284.5440 258.3380 -2.8870 247.0742 249.9612 284.5400 259.1045 -2.8863 247.2329 250.1191 284.7062 259.9323 -2.8844 247.3287 250.2131 284.8722 260.7288 -2.8749 247.6016 250.4765 285.0198 261.5260 -2.8490 247.7833 250.6323 285.0532 262.3433 -2.8469 248.0294 250.8762 285.3470 263.1195 -2.8540 248.1125 250.9665 285.4554 263.9475 -2.8594 248.2348 251.0942 285.6676 264.7135 -2.8584 248.2688 251.1272 285.7624 265.5615 -2.8652 248.4317 251.2968 285.8785 266.3383 -2.8667 248.5703 251.4370 286.0897 267.1555 -2.8684 248.7978 251.6661 286.3161 267.9523 -2.8649 248.8996 251.7645 286.5188 268.7495 -2.8637 248.9426 251.8063 286.6118 269.5870 -2.8541 249.0903 251.9444 286.8110 270.3430 -2.8587 249.2302 252.0889 286.9100 271.2018 -2.8532 249.3925 252.2457 286.9458 271.9673 -2.8499 249.5572 252.4071 286.9827 272.7953 -2.8457 249.7246 252.5703 287.0489 273.5820 -2.8298 249.8556 252.6854 287.1249 274.3785 -2.8316 249.9330 252.7646 287.1496 275.2065 -2.8258 250.1651 252.9909 287.2625 275.9623 -2.8262 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