DTA measure 1gyors Date: 2025415:1057 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.36 s Mass = 923.500 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2613 0.5173 225.5315 225.0142 270.9597 2.0493 0.5163 225.8117 225.2955 270.8350 2.8475 0.5168 226.0944 225.5776 270.7078 3.6358 0.5161 226.3745 225.8583 270.5728 4.4753 0.5155 226.6737 226.1583 270.4286 5.2323 0.5155 226.9413 226.4258 270.3001 6.0820 0.5157 227.2403 226.7245 270.1528 6.8498 0.5155 227.5061 226.9905 270.0109 7.6688 0.5153 227.7892 227.2740 269.8613 8.4773 0.5151 228.0727 227.5576 269.7131 9.2653 0.5147 228.3457 227.8311 269.5677 10.0845 0.5151 228.6276 228.1125 269.4110 10.8623 0.5156 228.8933 228.3777 269.2584 11.7120 0.5154 229.1772 228.6619 269.0985 12.4793 0.5150 229.4379 228.9228 268.9519 13.2988 0.5150 229.7146 229.1997 268.7935 14.1073 0.5151 229.9805 229.4654 268.6352 14.8953 0.5156 230.2404 229.7247 268.4842 15.6628 0.5154 230.4945 229.9791 268.3422 16.5230 0.5154 230.7806 230.2652 268.1771 17.2905 0.5155 231.0360 230.5205 268.0338 18.1200 0.5161 231.3059 230.7899 267.8902 18.9078 0.5165 231.5673 231.0509 267.7466 19.7063 0.5172 231.8248 231.3076 267.6043 20.5358 0.5177 232.0891 231.5714 267.4570 21.2928 0.5184 232.3311 231.8127 267.3306 22.1530 0.5185 232.6094 232.0909 267.1916 22.9208 0.5185 232.8590 232.3405 267.0703 23.7500 0.5187 233.1229 232.6042 266.9441 24.5380 0.5195 233.3686 232.8492 266.8259 25.3365 0.5205 233.6207 233.1002 266.7107 26.1658 0.5208 233.8761 233.3553 266.6060 26.9330 0.5212 234.1175 233.5963 266.5106 27.7933 0.5216 234.3863 233.8647 266.4080 28.5505 0.5220 234.6167 234.0947 266.3244 29.3900 0.5215 234.8769 234.3554 266.2380 30.1780 0.5220 235.1191 234.5971 266.1698 30.9763 0.5223 235.3653 234.8430 266.1058 31.7955 0.5226 235.6159 235.0933 266.0445 32.5523 0.5228 235.8476 235.3248 266.0017 33.4125 0.5226 236.1088 235.5862 265.9580 34.1800 0.5218 236.3372 235.8154 265.9299 35.0093 0.5207 236.5793 236.0586 265.9073 35.7973 0.5191 236.8101 236.2910 265.8971 36.5850 0.5188 237.0366 236.5178 265.8955 37.4143 0.5181 237.2725 236.7544 265.9038 38.1713 0.5165 237.4870 236.9706 265.9211 39.0110 0.5151 237.7258 237.2107 265.9543 39.7683 0.5132 237.9371 237.4240 265.9895 40.6180 0.5119 238.1777 237.6658 266.0401 41.3958 0.5097 238.3979 237.8881 266.1049 42.2148 0.5075 238.6254 238.1179 266.1794 43.0130 0.5059 238.8514 238.3455 266.2662 43.8113 0.5035 239.0744 238.5709 266.3658 44.6405 0.5006 239.3050 238.8044 266.4834 45.3975 0.4977 239.5105 239.0129 266.6013 46.2580 0.4946 239.7413 239.2467 266.7434 47.0253 0.4918 239.9497 239.4578 266.8818 47.8440 0.4883 240.1723 239.6841 267.0437 48.6428 0.4850 240.3835 239.8985 267.2075 49.4410 0.4818 240.5881 240.1063 267.3841 50.2703 0.4781 240.8148 240.3366 267.5826 51.0278 0.4743 241.0212 240.5469 267.7742 51.8880 0.4700 241.2540 240.7839 268.0031 52.6558 0.4661 241.4488 240.9827 268.2133 53.4850 0.4607 241.6617 241.2011 268.4527 54.2833 0.4559 241.8691 241.4132 268.6987 55.0710 0.4507 242.0747 241.6239 268.9410 55.9008 0.4457 242.2909 241.8452 269.2139 56.6680 0.4407 242.4903 242.0496 269.4783 57.5283 0.4347 242.7129 242.2782 269.7802 58.2853 0.4296 242.9072 242.4776 270.0491 59.1150 0.4228 243.1144 242.6915 270.3545 59.9133 0.4159 243.3181 242.9023 270.6533 60.7010 0.4093 243.5216 243.1123 270.9559 61.5308 0.4026 243.7334 243.3308 271.2873 62.2980 0.3963 243.9297 243.5334 271.5981 63.1585 0.3887 244.1468 243.7582 271.9474 63.9158 0.3811 244.3377 243.9567 272.2641 64.7348 0.3734 244.5451 244.1717 272.6103 65.5330 0.3654 244.7436 244.3782 272.9498 66.3208 0.3572 244.9389 244.5817 273.2910 67.1605 0.3485 245.1473 244.7988 273.6645 67.9178 0.3404 245.3381 244.9976 274.0019 68.7678 0.3319 245.5523 245.2204 274.3803 69.5350 0.3240 245.7444 245.4203 274.7235 70.3540 0.3148 245.9503 245.6356 275.0913 71.1625 0.3054 246.1544 245.8489 275.4560 71.9508 0.2966 246.3545 246.0579 275.8122 72.7698 0.2874 246.5643 246.2768 276.1835 73.5473 0.2775 246.7584 246.4809 276.5287 74.3973 0.2672 246.9696 246.7024 276.9070 75.1645 0.2575 247.1591 246.9016 277.2471 75.9838 0.2473 247.3664 247.1192 277.6169 76.7613 0.2369 247.5564 247.3195 277.9628 77.5803 0.2264 247.7626 247.5362 278.3201 78.3893 0.2169 247.9606 247.7437 278.6715 79.1773 0.2078 248.1539 247.9461 279.0168 79.9960 0.1967 248.3620 248.1653 279.3670 80.7740 0.1865 248.5546 248.3681 279.6891 81.6240 0.1754 248.7666 248.5912 280.0404 82.3913 0.1644 248.9554 248.7910 280.3503 83.2108 0.1534 249.1665 249.0131 280.6782 84.0193 0.1436 249.3678 249.2242 280.9995 84.8073 0.1329 249.5648 249.4318 281.3062 85.6470 0.1212 249.7818 249.6606 281.6219 86.4038 0.1108 249.9790 249.8683 281.8954 87.2645 0.0988 250.2015 250.1028 282.2028 88.0318 0.0888 250.3974 250.3086 282.4735 88.8508 0.0779 250.6047 250.5269 282.7568 89.6283 0.0677 250.7991 250.7314 283.0203 90.4475 0.0565 251.0022 250.9457 283.2904 91.2460 0.0453 251.2004 251.1551 283.5491 92.0338 0.0346 251.3961 251.3615 283.7925 92.8733 0.0232 251.6070 251.5838 284.0468 93.6303 0.0129 251.7981 251.7852 284.2671 94.4803 0.0016 252.0226 252.0210 284.5024 95.2583 -0.0086 252.2184 252.2270 284.7135 96.0670 -0.0188 252.4219 252.4407 284.9215 96.8653 -0.0283 252.6205 252.6489 285.1221 97.6533 -0.0386 252.8183 252.8570 285.3155 98.4728 -0.0499 253.0263 253.0761 285.5048 99.2503 -0.0600 253.2278 253.2878 285.6744 100.1003 -0.0708 253.4422 253.5130 285.8551 100.8570 -0.0804 253.6364 253.7169 286.0020 101.6868 -0.0911 253.8545 253.9456 286.1549 102.4540 -0.1007 254.0512 254.1519 286.2931 103.2833 -0.1107 254.2640 254.3748 286.4311 104.0715 -0.1208 254.4657 254.5864 286.5572 104.8700 -0.1303 254.6703 254.8007 286.6812 105.6993 -0.1402 254.8796 255.0199 286.8068 106.4563 -0.1484 255.0711 255.2195 286.9078 107.2860 -0.1581 255.2789 255.4370 287.0117 108.0530 -0.1669 255.4753 255.6423 287.1058 108.9133 -0.1775 255.6940 255.8715 287.2017 109.6705 -0.1861 255.8883 256.0744 287.2781 110.4998 -0.1960 256.1002 256.2962 287.3534 111.2983 -0.2047 256.2999 256.5047 287.4255 112.0860 -0.2134 256.4977 256.7111 287.4850 112.9153 -0.2224 256.7066 256.9290 287.5459 113.6828 -0.2310 256.9020 257.1330 287.5987 114.5430 -0.2402 257.1213 257.3615 287.6485 115.3108 -0.2484 257.3132 257.5615 287.6870 116.1400 -0.2559 257.5222 257.7781 287.7235 116.8968 -0.2627 257.7123 257.9750 287.7509 117.7260 -0.2713 257.9193 258.1906 287.7756 118.5243 -0.2794 258.1207 258.4001 287.7969 119.3123 -0.2870 258.3210 258.6080 287.8147 120.1420 -0.2947 258.5303 258.8250 287.8236 120.9095 -0.3017 258.7231 259.0248 287.8263 121.7700 -0.3095 258.9432 259.2526 287.8218 122.5370 -0.3158 259.1381 259.4539 287.8229 123.3665 -0.3229 259.3500 259.6729 287.8208 124.1548 -0.3297 259.5526 259.8823 287.8145 124.9530 -0.3363 259.7519 260.0883 287.8058 125.7825 -0.3428 259.9544 260.2972 287.7886 126.5398 -0.3491 260.1387 260.4877 287.7726 127.4000 -0.3559 260.3472 260.7031 287.7576 128.1570 -0.3616 260.5320 260.8936 287.7390 128.9865 -0.3675 260.7344 261.1019 287.7142 129.7743 -0.3736 260.9244 261.2980 287.6899 130.5728 -0.3790 261.1209 261.4999 287.6639 131.4020 -0.3850 261.3229 261.7080 287.6332 132.1588 -0.3910 261.5035 261.8944 287.6052 132.9780 -0.3968 261.7088 262.1056 287.5744 133.7558 -0.4022 261.9005 262.3027 287.5444 134.6058 -0.4074 262.0991 262.5065 287.5088 135.3730 -0.4119 262.2822 262.6942 287.4776 136.1918 -0.4162 262.4803 262.8964 287.4509 137.0008 -0.4212 262.6767 263.0979 287.4147 137.7888 -0.4267 262.8645 263.2912 287.3804 138.6283 -0.4321 263.0643 263.4965 287.3430 139.3853 -0.4372 263.2442 263.6814 287.3139 140.2048 -0.4420 263.4352 263.8772 287.2843 140.9823 -0.4466 263.6181 264.0648 287.2575 141.8320 -0.4517 263.8193 264.2710 287.2366 142.5995 -0.4557 264.0019 264.4577 287.2133 143.4188 -0.4599 264.1911 264.6510 287.2006 144.2273 -0.4641 264.3808 264.8450 287.1861 145.0153 -0.4687 264.5660 265.0347 287.1715 145.8343 -0.4723 264.7537 265.2260 287.1608 146.6123 -0.4770 264.9298 265.4068 287.1590 147.4620 -0.4819 265.1249 265.6067 287.1555 148.2293 -0.4860 265.3012 265.7872 287.1573 149.0488 -0.4907 265.4876 265.9783 287.1642 149.8573 -0.4950 265.6683 266.1633 287.1739 150.6453 -0.4985 265.8452 266.3437 287.1854 151.4645 -0.5028 266.0266 266.5294 287.2089 152.2423 -0.5071 266.1983 266.7054 287.2371 153.0920 -0.5122 266.3870 266.8992 287.2706 153.8598 -0.5163 266.5602 267.0765 287.3040 154.6890 -0.5211 266.7442 267.2653 287.3454 155.4873 -0.5258 266.9204 267.4462 287.3917 156.2753 -0.5298 267.0890 267.6188 287.4444 157.1153 -0.5340 267.2737 267.8077 287.5040 157.8723 -0.5378 267.4369 267.9747 287.5674 158.7325 -0.5426 267.6259 268.1686 287.6472 159.4998 -0.5470 267.7916 268.3386 287.7274 160.3190 -0.5508 267.9676 268.5184 287.8201 161.0860 -0.5548 268.1263 268.6811 287.9082 161.9053 -0.5600 268.3001 268.8601 288.0120 162.6930 -0.5651 268.4668 269.0319 288.1169 163.4915 -0.5698 268.6387 269.2085 288.2272 164.3103 -0.5740 268.8146 269.3886 288.3501 165.0880 -0.5784 268.9828 269.5612 288.4709 165.9383 -0.5836 269.1645 269.7481 288.6091 166.6950 -0.5882 269.3228 269.9110 288.7429 167.5243 -0.5930 269.4938 270.0869 288.8900 168.3228 -0.5974 269.6596 270.2570 289.0447 169.1210 -0.6023 269.8237 270.4261 289.2044 169.9403 -0.6079 269.9896 270.5975 289.3742 170.7075 -0.6124 270.1464 270.7588 289.5378 171.5678 -0.6184 270.3264 270.9448 289.7309 172.3248 -0.6234 270.4813 271.1047 289.9049 173.1540 -0.6284 270.6523 271.2807 290.1039 173.9525 -0.6344 270.8142 271.4487 290.2980 174.7505 -0.6407 270.9776 271.6183 290.4971 175.5698 -0.6472 271.1474 271.7946 290.7084 176.3370 -0.6529 271.3071 271.9600 290.9176 177.1973 -0.6598 271.4788 272.1385 291.1529 177.9540 -0.6649 271.6324 272.2973 291.3644 178.7938 -0.6709 271.7987 272.4696 291.6036 179.5820 -0.6769 271.9597 272.6365 291.8366 180.3803 -0.6834 272.1245 272.8079 292.0761 181.1993 -0.6905 272.2914 272.9819 292.3253 181.9770 -0.6965 272.4482 273.1447 292.5629 182.8273 -0.7039 272.6230 273.3269 292.8294 183.5945 -0.7103 272.7796 273.4899 293.0739 184.4238 -0.7172 272.9496 273.6669 293.3415 185.2118 -0.7237 273.1083 273.8320 293.5948 186.0203 -0.7314 273.2708 274.0021 293.8561 186.8395 -0.7394 273.4348 274.1742 294.1245 187.6070 -0.7473 273.5930 274.3402 294.3796 188.4568 -0.7548 273.7616 274.5164 294.6659 189.2343 -0.7617 273.9209 274.6826 294.9253 190.0533 -0.7692 274.0859 274.8551 295.1990 190.8418 -0.7764 274.2465 275.0229 295.4650 191.6500 -0.7839 274.4135 275.1974 295.7332 192.4380 -0.7912 274.5691 275.3603 295.9926 193.2363 -0.7985 274.7279 275.5264 296.2601 194.0555 -0.8060 274.8971 275.7031 296.5388 194.8125 -0.8136 275.0502 275.8638 296.7949 195.6730 -0.8223 275.2237 276.0460 297.0790 196.4298 -0.8297 275.3802 276.2099 297.3285 197.2590 -0.8374 275.5490 276.3864 297.6022 198.0573 -0.8449 275.7084 276.5533 297.8637 198.8450 -0.8531 275.8638 276.7169 298.1151 199.6743 -0.8611 276.0318 276.8929 298.3844 200.4418 -0.8682 276.1877 277.0559 298.6336 201.2710 -0.8764 276.3609 277.2373 298.8928 202.0280 -0.8841 276.5140 277.3981 299.1192 202.8780 -0.8927 276.6862 277.5789 299.3795 203.6558 -0.9003 276.8440 277.7443 299.6155 204.4750 -0.9080 277.0176 277.9256 299.8546 205.2733 -0.9156 277.1804 278.0960 300.0884 206.0613 -0.9231 277.3420 278.2651 300.3147 206.9010 -0.9309 277.5117 278.4426 300.5456 207.6583 -0.9378 277.6699 278.6077 300.7503 208.5080 -0.9464 277.8440 278.7904 300.9777 209.2858 -0.9540 278.0029 278.9569 301.1792 210.1048 -0.9623 278.1730 279.1354 301.3944 210.9033 -0.9700 278.3411 279.3111 301.6027 211.6913 -0.9781 278.5048 279.4830 301.7985 212.5310 -0.9866 278.6820 279.6685 302.0024 213.2878 -0.9941 278.8403 279.8343 302.1775 214.1273 -1.0018 279.0136 280.0154 302.3714 214.8845 -1.0092 279.1727 280.1819 302.5394 215.7348 -1.0171 279.3528 280.3699 302.7210 216.5123 -1.0247 279.5141 280.5388 302.8829 217.3310 -1.0318 279.6880 280.7198 303.0503 218.1293 -1.0399 279.8532 280.8931 303.2090 218.9278 -1.0476 280.0213 281.0689 303.3660 219.7573 -1.0552 280.1948 281.2501 303.5191 220.5143 -1.0610 280.3547 281.4157 303.6531 221.3850 -1.0678 280.5418 281.6096 303.8033 222.1418 -1.0734 280.7021 281.7755 303.9327 222.9713 -1.0803 280.8764 281.9566 304.0594 223.7698 -1.0872 281.0447 282.1319 304.1822 224.5578 -1.0933 281.2095 282.3028 304.3003 225.3560 -1.0994 281.3813 282.4807 304.4131 226.1443 -1.1052 281.5463 282.6515 304.5181 226.9630 -1.1109 281.7167 282.8276 304.6339 227.7303 -1.1154 281.8763 282.9917 304.7314 228.5803 -1.1197 282.0579 283.1776 304.8287 229.3580 -1.1251 282.2206 283.3458 304.9178 230.1770 -1.1302 282.3936 283.5238 305.0107 230.9753 -1.1358 282.5590 283.6948 305.0941 231.7735 -1.1417 282.7249 283.8665 305.1750 232.5618 -1.1473 282.8927 284.0401 305.2487 233.3600 -1.1531 283.0611 284.2141 305.3207 234.1890 -1.1589 283.2359 284.3948 305.3909 234.9563 -1.1646 283.3968 284.5615 305.4528 235.8068 -1.1710 283.5762 284.7472 305.5177 236.5638 -1.1763 283.7352 284.9114 305.5749 237.4035 -1.1818 283.9091 285.0910 305.6305 238.1915 -1.1870 284.0744 285.2614 305.6770 238.9898 -1.1930 284.2362 285.4292 305.7212 239.8088 -1.1979 284.4042 285.6021 305.7631 240.5863 -1.2022 284.5686 285.7708 305.8022 241.4363 -1.2075 284.7491 285.9565 305.8467 242.2040 -1.2123 284.9061 286.1184 305.8851 243.0330 -1.2172 285.0798 286.2971 305.9208 243.7898 -1.2217 285.2336 286.4553 305.9527 244.6298 -1.2262 285.4098 286.6360 305.9875 245.4178 -1.2309 285.5787 286.8096 306.0188 246.2160 -1.2358 285.7497 286.9854 306.0432 247.0453 -1.2408 285.9198 287.1605 306.0723 247.8128 -1.2443 286.0802 287.3245 306.0964 248.6628 -1.2484 286.2470 287.4954 306.1275 249.4403 -1.2522 286.4044 287.6566 306.1516 250.2593 -1.2561 286.5807 287.8368 306.1792 251.0370 -1.2597 286.7469 288.0066 306.2013 251.8663 -1.2638 286.9229 288.1868 306.2245 252.6230 -1.2672 287.0829 288.3501 306.2471 253.4838 -1.2707 287.2594 288.5301 306.2764 254.2510 -1.2747 287.4087 288.6834 306.3047 255.0803 -1.2783 287.5790 288.8573 306.3335 255.8788 -1.2819 287.7367 289.0186 306.3617 256.6770 -1.2856 287.9012 289.1868 306.3896 257.4958 -1.2899 288.0635 289.3534 306.4229 258.2530 -1.2936 288.2156 289.5092 306.4532 259.1133 -1.2973 288.3897 289.6870 306.4884 259.8703 -1.3005 288.5404 289.8409 306.5245 260.6995 -1.3036 288.7071 290.0107 306.5657 261.4770 -1.3066 288.8643 290.1709 306.6142 262.3065 -1.3099 289.0302 290.3400 306.6637 263.0948 -1.3126 289.1830 290.4956 306.7123 263.8930 -1.3159 289.3443 290.6602 306.7606 264.6913 -1.3196 289.4999 290.8195 306.8109 265.4790 -1.3226 289.6551 290.9777 306.8717 266.3085 -1.3254 289.8227 291.1481 306.9346 267.0760 -1.3288 289.9790 291.3078 306.9932 267.9363 -1.3331 290.1458 291.4789 307.0625 268.6933 -1.3367 290.2963 291.6330 307.1249 269.5225 -1.3399 290.4600 291.7999 307.1988 270.3208 -1.3436 290.6148 291.9585 307.2796 271.1090 -1.3468 290.7686 292.1154 307.3629 271.9383 -1.3497 290.9290 292.2787 307.4476 272.7058 -1.3531 291.0751 292.4281 307.5289 273.5660 -1.3573 291.2340 292.5913 307.6260 274.3228 -1.3606 291.3794 292.7400 307.7158 275.1520 -1.3646 291.5377 292.9023 307.8217 275.9503 -1.3677 291.6945 293.0622 307.9274 276.7385 -1.3714 291.8458 293.2172 308.0346 277.5678 -1.3755 291.9965 293.3720 308.1529 278.3350 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