DTA measure 1lassu Date: 2025415:1144 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1035.60 s Mass = 923.500 mg data_number = 1288 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3448 -2.2727 260.0734 262.3461 264.4555 2.1640 -2.2706 260.0932 262.3637 264.4657 2.9733 -2.2686 260.1178 262.3864 264.4704 3.7618 -2.2671 260.1404 262.4075 264.4701 4.5813 -2.2650 260.1694 262.4344 264.4642 5.3598 -2.2625 260.1971 262.4596 264.4484 6.2103 -2.2601 260.2240 262.4842 264.4217 6.9780 -2.2575 260.2504 262.5079 264.4008 7.7978 -2.2548 260.2761 262.5309 264.3778 8.5758 -2.2518 260.3026 262.5544 264.3481 9.3958 -2.2481 260.3349 262.5831 264.3087 10.1843 -2.2444 260.3656 262.6100 264.2633 10.9935 -2.2401 260.4017 262.6418 264.2146 11.8130 -2.2358 260.4371 262.6730 264.1646 12.5810 -2.2316 260.4706 262.7022 264.1105 13.4315 -2.2266 260.5015 262.7281 264.0434 14.2098 -2.2228 260.5334 262.7561 263.9808 15.0293 -2.2181 260.5678 262.7859 263.9110 15.8180 -2.2136 260.6054 262.8190 263.8352 16.6273 -2.2086 260.6438 262.8524 263.7546 17.4468 -2.2033 260.6824 262.8857 263.6702 18.2148 -2.1984 260.7174 262.9158 263.5886 19.0650 -2.1924 260.7566 262.9490 263.4950 19.8433 -2.1867 260.7968 262.9835 263.4043 20.6630 -2.1808 260.8342 263.0151 263.3038 21.4513 -2.1751 260.8726 263.0477 263.2042 22.2610 -2.1693 260.9164 263.0857 263.1017 23.0805 -2.1628 260.9570 263.1198 262.9907 23.8488 -2.1560 260.9942 263.1502 262.8874 24.6990 -2.1493 261.0414 263.1908 262.7660 25.4778 -2.1436 261.0778 263.2214 262.6575 26.2970 -2.1366 261.1205 263.2571 262.5393 27.0858 -2.1303 261.1569 263.2872 262.4232 27.8950 -2.1234 261.1951 263.3184 262.3004 28.7145 -2.1162 261.2388 263.3551 262.1701 29.4828 -2.1100 261.2768 263.3868 262.0523 30.3330 -2.1025 261.3173 263.4198 261.9118 31.1118 -2.0957 261.3581 263.4538 261.7869 31.9313 -2.0886 261.3961 263.4848 261.6496 32.7303 -2.0821 261.4336 263.5157 261.5139 33.5188 -2.0748 261.4725 263.5473 261.3772 34.3490 -2.0663 261.5140 263.5804 261.2378 35.1168 -2.0586 261.5494 263.6079 261.1049 35.9363 -2.0502 261.5919 263.6422 260.9545 36.6938 -2.0429 261.6365 263.6794 260.8224 37.5548 -2.0350 261.6789 263.7140 260.6651 38.3120 -2.0281 261.7184 263.7466 260.5238 39.1313 -2.0201 261.7555 263.7756 260.3647 39.8990 -2.0126 261.7976 263.8102 260.2154 40.7190 -2.0035 261.8368 263.8403 260.0589 41.5283 -1.9951 261.8723 263.8674 259.9018 42.3170 -1.9877 261.9110 263.8987 259.7486 43.1363 -1.9792 261.9504 263.9295 259.5881 43.9040 -1.9711 261.9847 263.9558 259.4357 44.7550 -1.9624 262.0280 263.9905 259.2661 45.5123 -1.9553 262.0701 264.0254 259.1139 46.3528 -1.9465 262.1077 264.0542 258.9420 47.1103 -1.9390 262.1439 264.0829 258.7866 47.9400 -1.9305 262.1826 264.1132 258.6157 48.7288 -1.9225 262.2200 264.1425 258.4527 49.5275 -1.9147 262.2551 264.1698 258.2887 50.3570 -1.9063 262.2932 264.1995 258.1165 51.1150 -1.8982 262.3304 264.2286 257.9576 51.9758 -1.8895 262.3699 264.2594 257.7763 52.7330 -1.8818 262.4049 264.2867 257.6195 53.5630 -1.8733 262.4457 264.3190 257.4456 54.3310 -1.8650 262.4786 264.3436 257.2870 55.1503 -1.8570 262.5130 264.3700 257.1179 55.9490 -1.8485 262.5501 264.3986 256.9521 56.7373 -1.8410 262.5871 264.4281 256.7857 57.5778 -1.8325 262.6309 264.4634 256.6120 58.3353 -1.8246 262.6636 264.4881 256.4553 59.1860 -1.8155 262.7035 264.5190 256.2809 59.9640 -1.8075 262.7338 264.5413 256.1272 60.7833 -1.7992 262.7612 264.5604 255.9654 61.5823 -1.7916 262.7920 264.5836 255.8062 62.3710 -1.7836 262.8170 264.6007 255.6559 63.1800 -1.7753 262.8466 264.6219 255.5049 63.9685 -1.7668 262.8761 264.6430 255.3602 64.7880 -1.7581 262.9167 264.6748 255.2070 65.5660 -1.7503 262.9447 264.6951 255.0676 66.4170 -1.7416 262.9742 264.7158 254.9214 67.1848 -1.7345 263.0056 264.7402 254.7868 68.0040 -1.7261 263.0323 264.7585 254.6408 68.8135 -1.7183 263.0606 264.7790 254.5073 69.6020 -1.7109 263.0881 264.7990 254.3844 70.4213 -1.7035 263.1145 264.8181 254.2620 71.1998 -1.6965 263.1437 264.8401 254.1489 72.0503 -1.6882 263.1674 264.8556 254.0306 72.7870 -1.6810 263.1857 264.8667 253.9404 73.6375 -1.6729 263.2127 264.8856 253.8319 74.4158 -1.6657 263.2418 264.9075 253.7428 75.2353 -1.6587 263.2707 264.9294 253.6487 76.0238 -1.6522 263.2932 264.9454 253.5598 76.8330 -1.6459 263.3182 264.9641 253.4772 77.6525 -1.6386 263.3353 264.9739 253.4047 78.4203 -1.6314 263.3555 264.9870 253.3439 79.2710 -1.6246 263.3769 265.0014 253.2812 80.0490 -1.6184 263.3976 265.0160 253.2357 80.8688 -1.6123 263.4133 265.0256 253.1978 81.6573 -1.6062 263.4307 265.0369 253.1651 82.4663 -1.6001 263.4524 265.0525 253.1388 83.2860 -1.5945 263.4698 265.0643 253.1262 84.0538 -1.5893 263.4881 265.0774 253.1223 84.9043 -1.5833 263.5118 265.0951 253.1288 85.6823 -1.5779 263.5315 265.1094 253.1440 86.5018 -1.5717 263.5461 265.1178 253.1647 87.2903 -1.5663 263.5620 265.1284 253.1988 88.0993 -1.5609 263.5749 265.1358 253.2430 88.9190 -1.5563 263.5940 265.1503 253.2928 89.6868 -1.5522 263.6131 265.1653 253.3506 90.5373 -1.5474 263.6293 265.1767 253.4226 91.3158 -1.5435 263.6458 265.1892 253.4962 92.1350 -1.5396 263.6655 265.2051 253.5859 92.9235 -1.5354 263.6818 265.2172 253.6855 93.7330 -1.5317 263.7048 265.2365 253.7956 94.5523 -1.5282 263.7214 265.2496 253.9197 95.3203 -1.5253 263.7336 265.2589 254.0411 96.1503 -1.5218 263.7496 265.2714 254.1822 96.9285 -1.5184 263.7667 265.2852 254.3207 97.7790 -1.5155 263.7849 265.3005 254.4839 98.5468 -1.5130 263.7992 265.3122 254.6474 99.3663 -1.5098 263.8161 265.3260 254.8331 100.1238 -1.5067 263.8335 265.3402 255.0065 100.9538 -1.5043 263.8481 265.3524 255.2061 101.7523 -1.5017 263.8694 265.3711 255.4014 102.5510 -1.4989 263.8875 265.3864 255.6104 103.3708 -1.4967 263.9017 265.3984 255.8305 104.1283 -1.4944 263.9170 265.4115 256.0385 104.9890 -1.4924 263.9341 265.4265 256.2896 105.7463 -1.4910 263.9490 265.4399 256.5165 106.5660 -1.4909 263.9665 265.4573 256.7674 107.3650 -1.4908 263.9810 265.4718 257.0195 108.1640 -1.4902 263.9953 265.4855 257.2801 108.9628 -1.4896 264.0102 265.4998 257.5472 109.7510 -1.4893 264.0303 265.5196 257.8121 110.5705 -1.4893 264.0541 265.5434 258.0944 111.3488 -1.4897 264.0784 265.5681 258.3664 112.1993 -1.4897 264.0945 265.5842 258.6673 112.9670 -1.4906 264.1111 265.6017 258.9418 113.7865 -1.4916 264.1326 265.6241 259.2337 114.5753 -1.4921 264.1505 265.6426 259.5290 115.3843 -1.4929 264.1694 265.6623 259.8339 116.2040 -1.4945 264.1968 265.6913 260.1445 116.9718 -1.4958 264.2237 265.7195 260.4334 117.8220 -1.4973 264.2429 265.7401 260.7564 118.6003 -1.4989 264.2677 265.7666 261.0569 119.4198 -1.5008 264.2903 265.7911 261.3664 120.2083 -1.5025 264.3115 265.8139 261.6655 121.0173 -1.5043 264.3327 265.8370 261.9713 121.8060 -1.5061 264.3568 265.8630 262.2679 122.6048 -1.5080 264.3799 265.8880 262.5762 123.4240 -1.5109 264.4031 265.9140 262.8852 124.2023 -1.5133 264.4272 265.9405 263.1732 125.0530 -1.5160 264.4594 265.9754 263.4925 125.8103 -1.5185 264.4926 266.0111 263.7692 126.6508 -1.5210 264.5267 266.0477 264.0757 127.4390 -1.5230 264.5587 266.0817 264.3598 128.2378 -1.5251 264.5894 266.1145 264.6435 129.0573 -1.5277 264.6210 266.1487 264.9306 129.8358 -1.5302 264.6480 266.1782 265.2020 130.6550 -1.5331 264.6898 266.2229 265.4806 131.4230 -1.5352 264.7243 266.2595 265.7333 132.2840 -1.5379 264.7620 266.3000 266.0146 133.0413 -1.5402 264.7972 266.3374 266.2569 133.8713 -1.5424 264.8361 266.3785 266.5226 134.6703 -1.5451 264.8699 266.4150 266.7691 135.4690 -1.5485 264.9080 266.4565 267.0043 136.2888 -1.5518 264.9472 266.4990 267.2445 137.0565 -1.5546 264.9826 266.5372 267.4657 137.9173 -1.5582 265.0246 266.5828 267.7104 138.6750 -1.5608 265.0636 266.6244 267.9166 139.5048 -1.5640 265.1050 266.6690 268.1354 140.2728 -1.5670 265.1408 266.7079 268.3317 141.1023 -1.5703 265.1853 266.7555 268.5389 141.9013 -1.5740 265.2300 266.8040 268.7293 142.7003 -1.5772 265.2735 266.8507 268.9142 143.5200 -1.5801 265.3160 266.8961 269.1023 144.2875 -1.5830 265.3585 266.9415 269.2682 145.1488 -1.5859 265.4075 266.9934 269.4521 145.9063 -1.5885 265.4535 267.0420 269.6013 146.7360 -1.5917 265.5046 267.0963 269.7613 147.5353 -1.5943 265.5518 267.1461 269.9100 148.3340 -1.5976 265.5936 267.1911 270.0468 149.1533 -1.5999 265.6367 267.2366 270.1825 149.9215 -1.6020 265.6845 267.2865 270.2995 150.7820 -1.6036 265.7388 267.3424 270.4232 151.5085 -1.6055 265.7867 267.3922 270.5293 152.3698 -1.6073 265.8410 267.4483 270.6444 153.1378 -1.6091 265.8899 267.4990 270.7437 153.9675 -1.6113 265.9440 267.5554 270.8459 154.7560 -1.6141 266.0002 267.6143 270.9362 155.5550 -1.6160 266.0574 267.6734 271.0206 156.3850 -1.6186 266.1119 267.7305 271.1048 157.1423 -1.6202 266.1600 267.7802 271.1763 158.0035 -1.6213 266.2237 267.8450 271.2527 158.7713 -1.6222 266.2758 267.8980 271.3139 159.6013 -1.6236 266.3353 267.9589 271.3790 160.3900 -1.6254 266.3950 268.0203 271.4347 161.1885 -1.6268 266.4538 268.0807 271.4810 162.0190 -1.6280 266.5110 268.1390 271.5263 162.7763 -1.6290 266.5644 268.1934 271.5688 163.6370 -1.6305 266.6294 268.2599 271.6055 164.3948 -1.6319 266.6852 268.3171 271.6310 165.2140 -1.6327 266.7461 268.3789 271.6586 166.0128 -1.6337 266.8052 268.4389 271.6823 166.8013 -1.6342 266.8661 268.5003 271.6998 167.6005 -1.6357 266.9264 268.5621 271.7113 168.4098 -1.6369 266.9904 268.6273 271.7204 169.2398 -1.6376 267.0488 268.6865 271.7232 169.9970 -1.6385 267.1063 268.7448 271.7263 170.8478 -1.6384 267.1732 268.8116 271.7296 171.6158 -1.6384 267.2339 268.8723 271.7241 172.4350 -1.6376 267.2974 268.9350 271.7171 173.2240 -1.6376 267.3560 268.9936 271.7130 174.0330 -1.6367 267.4199 269.0566 271.7022 174.8523 -1.6355 267.4780 269.1135 271.6855 175.6203 -1.6345 267.5320 269.1666 271.6707 176.4710 -1.6332 267.5997 269.2329 271.6525 177.2285 -1.6324 267.6594 269.2919 271.6332 178.0585 -1.6312 267.7290 269.3602 271.6103 178.8573 -1.6301 267.7842 269.4143 271.5860 179.6563 -1.6284 267.8465 269.4749 271.5576 180.4758 -1.6266 267.9146 269.5412 271.5271 181.2333 -1.6241 267.9699 269.5940 271.4974 182.0940 -1.6220 268.0338 269.6558 271.4630 182.8620 -1.6209 268.0974 269.7183 271.4314 183.6918 -1.6191 268.1706 269.7898 271.3980 184.4490 -1.6175 268.2301 269.8476 271.3668 185.2795 -1.6160 268.2899 269.9059 271.3358 186.0780 -1.6149 268.3527 269.9677 271.3073 186.8663 -1.6130 268.4160 270.0290 271.2813 187.6963 -1.6114 268.4800 270.0914 271.2502 188.4538 -1.6090 268.5401 270.1491 271.2113 189.3145 -1.6067 268.6127 270.2194 271.1698 190.0828 -1.6045 268.6744 270.2788 271.1446 190.9020 -1.6021 268.7353 270.3373 271.1189 191.7010 -1.6000 268.7963 270.3963 271.0896 192.4998 -1.5924 268.8611 270.4535 271.0672 193.3298 -1.5867 268.9272 270.5139 271.0499 194.0873 -1.5842 268.9836 270.5678 271.0362 194.9278 -1.5743 269.0508 270.6251 271.0215 195.6850 -1.5648 269.1120 270.6768 271.0032 196.5455 -1.5590 269.1714 270.7304 270.9912 197.3138 -1.5554 269.2277 270.7831 270.9801 198.1333 -1.5519 269.2945 270.8464 270.9695 198.9323 -1.5501 269.3551 270.9051 270.9599 199.7313 -1.5468 269.4109 270.9578 270.9563 200.5610 -1.5441 269.4765 271.0206 270.9647 201.3188 -1.5425 269.5366 271.0791 270.9694 202.1795 -1.5400 269.6092 271.1492 270.9762 202.9163 -1.5374 269.6647 271.2022 270.9854 203.7670 -1.5351 269.7302 271.2652 271.0012 204.5450 -1.5323 269.7878 271.3201 271.0181 205.3648 -1.5298 269.8472 271.3770 271.0453 206.1633 -1.5286 269.9090 271.4376 271.0777 206.9623 -1.5275 269.9668 271.4943 271.1117 207.7920 -1.5261 270.0292 271.5553 271.1489 208.5705 -1.5249 270.0977 271.6226 271.1869 209.4000 -1.5236 270.1599 271.6835 271.2318 210.1578 -1.5226 270.2166 271.7392 271.2776 211.0185 -1.5207 270.2830 271.8037 271.3352 211.7553 -1.5196 270.3361 271.8557 271.3921 212.6163 -1.5182 270.4047 271.9229 271.4654 213.3740 -1.5161 270.4664 271.9825 271.5342 214.2035 -1.5149 270.5330 272.0479 271.6129 215.0025 -1.5135 270.5916 272.1051 271.6922 215.7910 -1.5124 270.6474 272.1597 271.7795 216.6208 -1.5118 270.7094 272.2212 271.8722 217.3888 -1.5111 270.7669 272.2781 271.9646 218.2498 -1.5096 270.8315 272.3411 272.0734 219.0070 -1.5088 270.8862 272.3950 272.1702 219.8370 -1.5077 270.9465 272.4542 272.2843 220.6360 -1.5068 271.0135 272.5204 272.4036 221.4243 -1.5054 271.0741 272.5795 272.5255 222.2540 -1.5040 271.1383 272.6423 272.6603 223.0220 -1.5031 271.1921 272.6952 272.7891 223.8828 -1.5021 271.2592 272.7613 272.9362 224.6403 -1.5021 271.3172 272.8193 273.0663 225.4705 -1.5011 271.3799 272.8810 273.2237 226.2380 -1.5009 271.4371 272.9380 273.3706 227.0578 -1.5007 271.4990 272.9996 273.5321 227.8568 -1.5005 271.5585 273.0589 273.6945 228.6450 -1.5007 271.6228 273.1235 273.8598 229.4853 -1.5013 271.6867 273.1880 274.0357 230.2430 -1.5017 271.7397 273.2415 274.1998 231.0623 -1.5016 271.8009 273.3025 274.3816 231.8300 -1.5023 271.8619 273.3641 274.5552 232.6808 -1.5025 271.9247 273.4272 274.7486 233.4380 -1.5027 271.9809 273.4835 274.9228 234.2780 -1.5037 272.0480 273.5517 275.1255 235.0668 -1.5045 272.1102 273.6147 275.3143 235.8655 -1.5051 272.1677 273.6728 275.5052 236.6850 -1.5057 272.2306 273.7363 275.7033 237.4423 -1.5057 272.2900 273.7957 275.8923 238.3033 -1.5063 272.3592 273.8655 276.1080 239.0713 -1.5072 272.4216 273.9289 276.3016 239.9010 -1.5079 272.4942 274.0022 276.5159 240.6898 -1.5082 272.5610 274.0692 276.7275 241.4783 -1.5084 272.6260 274.1344 276.9335 242.3080 -1.5087 272.6857 274.1944 277.1504 243.0758 -1.5092 272.7467 274.2559 277.3497 243.9368 -1.5109 272.8127 274.3236 277.5761 244.6940 -1.5123 272.8736 274.3859 277.7768 245.5138 -1.5138 272.9391 274.4529 277.9923 246.3128 -1.5155 273.0069 274.5225 278.2056 247.1113 -1.5176 273.0763 274.5939 278.4152 247.9413 -1.5193 273.1485 274.6679 278.6363 248.6990 -1.5205 273.2130 274.7335 278.8370 249.5595 -1.5216 273.2895 274.8110 279.0581 250.3273 -1.5233 273.3550 274.8783 279.2578 251.1468 -1.5254 273.4315 274.9569 279.4742 251.9458 -1.5274 273.5011 275.0285 279.6846 252.7443 -1.5279 273.5705 275.0984 279.8831 253.5740 -1.5292 273.6468 275.1760 280.0949 254.3318 -1.5304 273.7172 275.2476 280.2836 255.1718 -1.5318 273.7938 275.3256 280.4899 255.9293 -1.5340 273.8597 275.3937 280.6782 256.7800 -1.5364 273.9404 275.4768 280.8863 257.5478 -1.5381 274.0127 275.5508 281.0680 258.3670 -1.5400 274.0882 275.6283 281.2619 259.1763 -1.5422 274.1618 275.7040 281.4493 259.9650 -1.5436 274.2324 275.7760 281.6265 260.8050 -1.5462 274.3098 275.8560 281.8139 261.5628 -1.5488 274.3803 275.9291 281.9735 262.4133 -1.5510 274.4592 276.0102 282.1486 263.1913 -1.5530 274.5383 276.0913 282.3095 264.0110 -1.5548 274.6228 276.1776 282.4762 264.8098 -1.5565 274.7031 276.2596 282.6371 265.5980 -1.5590 274.7806 276.3397 282.7966 266.4385 -1.5607 274.8637 276.4244 282.9625 267.1960 -1.5622 274.9441 276.5062 283.1078 268.0468 -1.5636 275.0273 276.5909 283.2628 268.8248 -1.5651 275.1033 276.6684 283.4008 269.6545 -1.5659 275.1844 276.7503 283.5480 270.4328 -1.5674 275.2609 276.8283 283.6821 271.2628 -1.5698 275.3460 276.9158 283.8153 272.0200 -1.5712 275.4199 276.9912 283.9348 272.8603 -1.5728 275.5051 277.0779 284.0691 273.6490 -1.5743 275.5849 277.1593 284.1952 274.4475 -1.5762 275.6628 277.2390 284.3161 275.2773 -1.5778 275.7416 277.3194 284.4344 276.0348 -1.5794 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