DTA measure 2gyors Date: 2025415:1124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1469.45 s Mass = 923.500 mg data_number = 1828 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2063 -5.5568 440.4985 446.0553 421.1971 1.9840 -5.5606 440.4880 446.0486 421.2809 2.8343 -5.5654 440.4789 446.0443 421.3745 3.5705 -5.5704 440.4695 446.0399 421.4606 4.4313 -5.5757 440.4574 446.0330 421.5708 5.1880 -5.5801 440.4430 446.0231 421.6695 6.0173 -5.5860 440.4275 446.0135 421.7828 6.8158 -5.5908 440.4125 446.0033 421.8914 7.6143 -5.5957 440.4009 445.9966 422.0005 8.4333 -5.6015 440.3891 445.9906 422.1211 9.2005 -5.6064 440.3766 445.9829 422.2385 10.0610 -5.6129 440.3697 445.9825 422.3711 10.8180 -5.6193 440.3575 445.9768 422.4896 11.6473 -5.6251 440.3448 445.9700 422.6182 12.4460 -5.6310 440.3354 445.9664 422.7439 13.2443 -5.6369 440.3283 445.9652 422.8702 14.0323 -5.6433 440.3210 445.9643 422.9975 14.8310 -5.6488 440.3104 445.9592 423.1185 15.6603 -5.6539 440.3072 445.9611 423.2505 16.4170 -5.6597 440.3025 445.9622 423.3672 17.2778 -5.6661 440.2931 445.9593 423.5008 18.0450 -5.6715 440.2868 445.9583 423.6153 18.8748 -5.6768 440.2785 445.9552 423.7389 19.6628 -5.6828 440.2717 445.9545 423.8554 20.4615 -5.6886 440.2596 445.9483 423.9654 21.2908 -5.6951 440.2467 445.9417 424.0740 22.0583 -5.7013 440.2385 445.9398 424.1720 22.9188 -5.7074 440.2323 445.9397 424.2803 23.6450 -5.7118 440.2257 445.9374 424.3687 24.5053 -5.7180 440.2223 445.9403 424.4706 25.2728 -5.7236 440.2188 445.9424 424.5531 26.1020 -5.7285 440.2132 445.9417 424.6370 26.8900 -5.7340 440.2065 445.9404 424.7120 27.6885 -5.7396 440.2005 445.9400 424.7810 28.5180 -5.7445 440.1935 445.9380 424.8495 29.2750 -5.7498 440.1880 445.9378 424.9070 30.1358 -5.7557 440.1858 445.9416 424.9540 30.9033 -5.7609 440.1849 445.9458 424.9924 31.7328 -5.7661 440.1828 445.9489 425.0323 32.4898 -5.7707 440.1793 445.9500 425.0644 33.3293 -5.7751 440.1770 445.9521 425.0867 34.1178 -5.7789 440.1771 445.9559 425.1012 34.9058 -5.7829 440.1751 445.9580 425.1102 35.7353 -5.7869 440.1745 445.9614 425.1147 36.5030 -5.7904 440.1750 445.9654 425.1137 37.3633 -5.7951 440.1729 445.9680 425.1010 38.1203 -5.7987 440.1689 445.9676 425.0879 38.9603 -5.8025 440.1694 445.9720 425.0685 39.7485 -5.8060 440.1664 445.9724 425.0411 40.5470 -5.8094 440.1641 445.9735 425.0034 41.3763 -5.8132 440.1635 445.9767 424.9603 42.1435 -5.8163 440.1671 445.9834 424.9102 42.9730 -5.8199 440.1697 445.9896 424.8566 43.7613 -5.8234 440.1715 445.9950 424.7980 44.5800 -5.8252 440.1729 445.9981 424.7326 45.3580 -5.8275 440.1727 446.0002 424.6602 46.2080 -5.8301 440.1690 445.9991 424.5782 46.9753 -5.8325 440.1678 446.0003 424.4948 47.7948 -5.8345 440.1679 446.0024 424.4057 48.5723 -5.8361 440.1682 446.0043 424.3173 49.3918 -5.8380 440.1678 446.0059 424.2151 50.2003 -5.8395 440.1682 446.0077 424.1022 50.9883 -5.8400 440.1649 446.0050 423.9937 51.8078 -5.8409 440.1581 445.9990 423.8738 52.5855 -5.8422 440.1539 445.9962 423.7506 53.4355 -5.8434 440.1596 446.0030 423.6151 54.2030 -5.8442 440.1635 446.0077 423.4902 55.0223 -5.8449 440.1570 446.0019 423.3491 55.8310 -5.8448 440.1551 445.9999 423.2053 56.6188 -5.8456 440.1539 445.9994 423.0651 57.4588 -5.8456 440.1514 445.9970 422.9074 58.2158 -5.8453 440.1495 445.9949 422.7637 59.0660 -5.8458 440.1426 445.9884 422.5976 59.8438 -5.8454 440.1361 445.9815 422.4435 60.6628 -5.8451 440.1306 445.9756 422.2739 61.4613 -5.8446 440.1212 445.9658 422.1029 62.2598 -5.8445 440.1141 445.9585 421.9313 63.0893 -5.8450 440.1067 445.9516 421.7445 63.8463 -5.8451 440.1005 445.9456 421.5747 64.7070 -5.8451 440.0905 445.9356 421.3765 65.4745 -5.8450 440.0800 445.9250 421.1986 66.2938 -5.8451 440.0637 445.9088 421.0074 67.1023 -5.8441 440.0542 445.8983 420.8123 67.8908 -5.8430 440.0403 445.8833 420.6193 68.6890 -5.8422 440.0273 445.8695 420.4201 69.4875 -5.8415 440.0172 445.8587 420.2177 70.3170 -5.8410 440.0028 445.8438 420.0061 71.0740 -5.8400 439.9925 445.8325 419.8097 71.9345 -5.8387 439.9775 445.8162 419.5875 72.7330 -5.8364 439.9661 445.8024 419.3778 73.5210 -5.8347 439.9504 445.7851 419.1692 74.3503 -5.8331 439.9368 445.7698 418.9489 75.1180 -5.8311 439.9206 445.7517 418.7460 75.9783 -5.8301 439.9018 445.7319 418.5177 76.7148 -5.8287 439.8867 445.7154 418.3262 77.5750 -5.8271 439.8676 445.6946 418.0911 78.3323 -5.8253 439.8441 445.6694 417.8841 79.1615 -5.8239 439.8189 445.6428 417.6534 79.9603 -5.8219 439.7991 445.6210 417.4359 80.7585 -5.8206 439.7734 445.5940 417.2141 81.5880 -5.8184 439.7509 445.5692 416.9872 82.3450 -5.8166 439.7263 445.5429 416.7763 83.2053 -5.8145 439.6965 445.5110 416.5349 83.9730 -5.8132 439.6685 445.4816 416.3264 84.8023 -5.8113 439.6387 445.4501 416.0995 85.6008 -5.8096 439.6077 445.4173 415.8765 86.3993 -5.8074 439.5783 445.3857 415.6523 87.2183 -5.8053 439.5492 445.3545 415.4257 87.9753 -5.8029 439.5199 445.3228 415.2231 88.8360 -5.8001 439.4840 445.2841 414.9918 89.5620 -5.7978 439.4495 445.2473 414.7952 90.4225 -5.7959 439.4052 445.2011 414.5703 91.1898 -5.7944 439.3725 445.1669 414.3648 92.0088 -5.7922 439.3357 445.1279 414.1487 92.8073 -5.7904 439.2972 445.0876 413.9411 93.5953 -5.7883 439.2621 445.0504 413.7381 94.4143 -5.7865 439.2194 445.0059 413.5299 95.1923 -5.7849 439.1837 444.9686 413.3347 96.0110 -5.7826 439.1426 444.9253 413.1278 96.7785 -5.7808 439.1017 444.8825 412.9379 97.6288 -5.7790 439.0574 444.8364 412.7263 98.3858 -5.7766 439.0218 444.7984 412.5428 99.2253 -5.7742 438.9748 444.7490 412.3442 100.0138 -5.7728 438.9303 444.7031 412.1580 100.8120 -5.7719 438.8871 444.6590 411.9742 101.6003 -5.7706 438.8434 444.6140 411.7926 102.4090 -5.7685 438.7958 444.5643 411.6076 103.2280 -5.7675 438.7488 444.5162 411.4294 103.9955 -5.7652 438.7031 444.4683 411.2618 104.8558 -5.7635 438.6471 444.4106 411.0716 105.6130 -5.7626 438.5960 444.3586 410.9169 106.4423 -5.7609 438.5476 444.3085 410.7509 107.2303 -5.7593 438.4918 444.2511 410.5968 108.0290 -5.7580 438.4316 444.1896 410.4366 108.8585 -5.7565 438.3700 444.1265 410.2805 109.6155 -5.7555 438.3131 444.0686 410.1436 110.4450 -5.7543 438.2516 444.0059 409.9920 111.2125 -5.7533 438.1925 443.9457 409.8509 112.0730 -5.7519 438.1302 443.8821 409.7053 112.8300 -5.7513 438.0761 443.8275 409.5798 113.6595 -5.7512 438.0113 443.7625 409.4473 114.4578 -5.7507 437.9491 443.6998 409.3230 115.2458 -5.7502 437.8885 443.6386 409.2034 116.0753 -5.7496 437.8247 443.5743 409.0799 116.8428 -5.7487 437.7649 443.5136 408.9686 117.7033 -5.7475 437.6931 443.4406 408.8466 118.4293 -5.7470 437.6373 443.3843 408.7472 119.3000 -5.7468 437.5642 443.3111 408.6354 120.0570 -5.7465 437.4998 443.2463 408.5432 120.8865 -5.7465 437.4391 443.1856 408.4442 121.6848 -5.7467 437.3764 443.1231 408.3477 122.4730 -5.7469 437.3118 443.0586 408.2588 123.3023 -5.7473 437.2430 442.9903 408.1690 124.0698 -5.7477 437.1784 442.9261 408.0891 124.9303 -5.7474 437.1065 442.8539 408.0011 125.6873 -5.7471 437.0425 442.7897 407.9247 126.5170 -5.7467 436.9731 442.7198 407.8499 127.3153 -5.7473 436.9028 442.6501 407.7806 128.1030 -5.7480 436.8362 442.5842 407.7153 128.9328 -5.7481 436.7683 442.5164 407.6429 129.7000 -5.7490 436.7052 442.4542 407.5797 130.5603 -5.7498 436.6224 442.3722 407.5133 131.3278 -5.7505 436.5519 442.3024 407.4655 132.1573 -5.7514 436.4750 442.2264 407.4167 132.9143 -5.7525 436.4046 442.1571 407.3708 133.7435 -5.7540 436.3332 442.0872 407.3132 134.5423 -5.7552 436.2665 442.0217 407.2682 135.3303 -5.7569 436.1996 441.9565 407.2276 136.1600 -5.7585 436.1256 441.8840 407.1848 136.9273 -5.7591 436.0538 441.8129 407.1500 137.7878 -5.7600 435.9702 441.7302 407.1056 138.5550 -5.7606 435.9003 441.6609 407.0712 139.3843 -5.7614 435.8234 441.5848 407.0301 140.1725 -5.7624 435.7512 441.5137 407.0008 140.9710 -5.7631 435.6786 441.4417 406.9729 141.8003 -5.7641 435.6049 441.3691 406.9433 142.5678 -5.7649 435.5336 441.2985 406.9096 143.4283 -5.7651 435.4551 441.2202 406.8739 144.1855 -5.7657 435.3909 441.1566 406.8421 145.0253 -5.7658 435.3100 441.0758 406.8080 145.8130 -5.7655 435.2333 440.9988 406.7804 146.6118 -5.7660 435.1597 440.9256 406.7507 147.4308 -5.7670 435.0808 440.8478 406.7177 148.2083 -5.7684 435.0076 440.7760 406.6879 149.0275 -5.7695 434.9284 440.6979 406.6590 149.7950 -5.7705 434.8573 440.6278 406.6322 150.6558 -5.7718 434.7848 440.5566 406.6031 151.4128 -5.7722 434.7171 440.4893 406.5776 152.2423 -5.7724 434.6427 440.4151 406.5469 153.0303 -5.7736 434.5666 440.3402 406.5126 153.8188 -5.7753 434.4924 440.2678 406.4755 154.6480 -5.7769 434.4225 440.1994 406.4342 155.4050 -5.7785 434.3550 440.1336 406.3969 156.2655 -5.7793 434.2752 440.0545 406.3551 157.0328 -5.7804 434.2040 439.9844 406.3191 157.8520 -5.7814 434.1268 439.9082 406.2770 158.6193 -5.7821 434.0555 439.8376 406.2389 159.4385 -5.7832 433.9759 439.7591 406.1955 160.2370 -5.7848 433.9015 439.6863 406.1572 161.0353 -5.7860 433.8315 439.6175 406.1120 161.8545 -5.7859 433.7615 439.5474 406.0629 162.6220 -5.7862 433.6932 439.4794 406.0161 163.4718 -5.7869 433.6217 439.4086 405.9598 164.2288 -5.7870 433.5529 439.3400 405.9076 165.0688 -5.7870 433.4753 439.2623 405.8528 165.8568 -5.7865 433.4000 439.1865 405.8044 166.6553 -5.7870 433.3244 439.1114 405.7517 167.4743 -5.7877 433.2502 439.0378 405.6908 168.2415 -5.7872 433.1764 438.9636 405.6294 169.1018 -5.7872 433.0970 438.8842 405.5630 169.8590 -5.7874 433.0249 438.8124 405.5005 170.6883 -5.7883 432.9520 438.7403 405.4281 171.4868 -5.7884 432.8803 438.6688 405.3539 172.2853 -5.7880 432.8044 438.5923 405.2833 173.1043 -5.7879 432.7262 438.5142 405.2032 173.8715 -5.7877 432.6568 438.4445 405.1229 174.7320 -5.7875 432.5813 438.3688 405.0369 175.4788 -5.7865 432.5150 438.3015 404.9652 176.2980 -5.7856 432.4400 438.2256 404.8821 177.0968 -5.7858 432.3673 438.1531 404.7970 177.9260 -5.7861 432.2938 438.0799 404.7056 178.6933 -5.7859 432.2253 438.0113 404.6208 179.5540 -5.7856 432.1434 437.9289 404.5224 180.3110 -5.7849 432.0713 437.8562 404.4411 181.1405 -5.7844 431.9981 437.7825 404.3490 181.9393 -5.7836 431.9249 437.7085 404.2597 182.7270 -5.7830 431.8530 437.6360 404.1671 183.5565 -5.7815 431.7756 437.5571 404.0613 184.3240 -5.7805 431.7058 437.4863 403.9620 185.1843 -5.7796 431.6244 437.4040 403.8475 185.9418 -5.7790 431.5527 437.3317 403.7512 186.7710 -5.7787 431.4732 437.2519 403.6424 187.5693 -5.7777 431.3989 437.1767 403.5353 188.3888 -5.7764 431.3242 437.1007 403.4253 189.1975 -5.7755 431.2460 437.0214 403.3101 189.9858 -5.7745 431.1715 436.9461 403.1918 190.7840 -5.7736 431.0999 436.8736 403.0754 191.5823 -5.7722 431.0253 436.7975 402.9550 192.4018 -5.7699 430.9526 436.7225 402.8297 193.1793 -5.7683 430.8781 436.6464 402.7123 194.0295 -5.7671 430.7987 436.5658 402.5824 194.7970 -5.7659 430.7300 436.4959 402.4655 195.6160 -5.7640 430.6475 436.4115 402.3363 196.3833 -5.7626 430.5730 436.3356 402.2074 197.2440 -5.7610 430.4926 436.2536 402.0633 198.0008 -5.7593 430.4222 436.1815 401.9350 198.8303 -5.7576 430.3468 436.1044 401.7970 199.6288 -5.7559 430.2693 436.0252 401.6644 200.4168 -5.7532 430.1970 435.9503 401.5361 201.2463 -5.7511 430.1213 435.8724 401.3953 202.0138 -5.7491 430.0556 435.8047 401.2657 202.8743 -5.7467 429.9749 435.7215 401.1188 203.6313 -5.7442 429.9023 435.6465 400.9869 204.4710 -5.7423 429.8280 435.5702 400.8435 205.2590 -5.7406 429.7529 435.4936 400.7070 206.0575 -5.7387 429.6766 435.4153 400.5673 206.8870 -5.7370 429.5986 435.3355 400.4195 207.6440 -5.7351 429.5253 435.2604 400.2881 208.5048 -5.7325 429.4430 435.1754 400.1405 209.2720 -5.7297 429.3694 435.0991 400.0061 210.1015 -5.7286 429.2871 435.0157 399.8591 210.8898 -5.7271 429.2131 434.9402 399.7174 211.6885 -5.7252 429.1356 434.8608 399.5748 212.5178 -5.7226 429.0495 434.7721 399.4193 213.2853 -5.7206 428.9720 434.6926 399.2784 214.1148 -5.7186 428.8886 434.6072 399.1297 214.8720 -5.7168 428.8140 434.5308 398.9985 215.7323 -5.7148 428.7270 434.4419 398.8392 216.4893 -5.7128 428.6491 434.3619 398.7055 217.3085 -5.7107 428.5627 434.2734 398.5595 218.1070 -5.7079 428.4837 434.1916 398.4175 218.8953 -5.7053 428.4073 434.1126 398.2721 219.7248 -5.7029 428.3218 434.0247 398.1264 220.4923 -5.7008 428.2432 433.9440 397.9876 221.3320 -5.6982 428.1632 433.8614 397.8354 222.0788 -5.6962 428.0914 433.7876 397.6996 222.9288 -5.6935 428.0075 433.7010 397.5461 223.6860 -5.6915 427.9295 433.6210 397.4093 224.5153 -5.6895 427.8471 433.5365 397.2587 225.3038 -5.6874 427.7654 433.4528 397.1179 226.1020 -5.6847 427.6834 433.3681 396.9796 226.9318 -5.6822 427.6002 433.2824 396.8325 227.6888 -5.6801 427.5197 433.1998 396.6997 228.5493 -5.6777 427.4274 433.1050 396.5463 229.3068 -5.6754 427.3439 433.0193 396.4143 230.1360 -5.6730 427.2551 432.9281 396.2714 230.9343 -5.6704 427.1677 432.8381 396.1349 231.7220 -5.6687 427.0833 432.7520 396.0023 232.5203 -5.6667 426.9961 432.6628 395.8660 233.3088 -5.6643 426.9073 432.5716 395.7345 234.1483 -5.6620 426.8101 432.4721 395.5932 234.9053 -5.6590 426.7251 432.3841 395.4692 235.7658 -5.6552 426.6307 432.2859 395.3307 236.5333 -5.6524 426.5420 432.1944 395.2045 237.3520 -5.6500 426.4530 432.1030 395.0717 238.1508 -5.6478 426.3618 432.0096 394.9442 238.9490 -5.6449 426.2711 431.9160 394.8175 239.7783 -5.6425 426.1766 431.8190 394.6930 240.5355 -5.6408 426.0961 431.7368 394.5808 241.3960 -5.6385 426.0015 431.6400 394.4497 242.1323 -5.6366 425.9209 431.5576 394.3363 242.9930 -5.6336 425.8245 431.4581 394.2092 243.7603 -5.6318 425.7366 431.3684 394.0976 244.5793 -5.6288 425.6482 431.2770 393.9738 245.3780 -5.6269 425.5570 431.1839 393.8571 246.1763 -5.6252 425.4671 431.0923 393.7375 247.0060 -5.6231 425.3793 431.0024 393.6170 247.7630 -5.6209 425.2929 430.9138 393.5113 248.6235 -5.6180 425.1996 430.8177 393.3892 249.3908 -5.6159 425.1120 430.7279 393.2848 250.2100 -5.6136 425.0158 430.6294 393.1674 251.0083 -5.6119 424.9206 430.5325 393.0584 251.8070 -5.6097 424.8278 430.4374 392.9528 252.6363 -5.6072 424.7322 430.3394 392.8368 253.3935 -5.6053 424.6402 430.2456 392.7360 254.2643 -5.6030 424.5327 430.1356 392.6185 255.0213 -5.6005 424.4477 430.0482 392.5200 255.8508 -5.5992 424.3486 429.9477 392.4127 256.6180 -5.5972 424.2581 429.8553 392.3133 257.4370 -5.5950 424.1601 429.7551 392.2043 258.2458 -5.5924 424.0645 429.6570 392.1058 259.0340 -5.5899 423.9716 429.5615 392.0106 259.8633 -5.5872 423.8733 429.4606 391.9065 260.6308 -5.5854 423.7903 429.3757 391.8141 261.4913 -5.5838 423.6890 429.2728 391.7159 262.2483 -5.5823 423.5960 429.1784 391.6277 263.0883 -5.5804 423.4913 429.0717 391.5333 263.8763 -5.5784 423.3975 428.9759 391.4381 264.6750 -5.5762 423.3044 428.8806 391.3436 265.5043 -5.5741 423.2049 428.7790 391.2449 266.2613 -5.5725 423.1153 428.6878 391.1566 267.1220 -5.5705 423.0112 428.5817 391.0543 267.8788 -5.5691 422.9209 428.4900 390.9680 268.7083 -5.5678 422.8192 428.3870 390.8767 269.4863 -5.5662 422.7262 428.2924 390.7904 270.3363 -5.5643 422.6251 428.1894 390.7020 271.1143 -5.5627 422.5280 428.0907 390.6176 271.9330 -5.5608 422.4298 427.9905 390.5310 272.7313 -5.5579 422.3380 427.8959 390.4454 273.5198 -5.5553 422.2477 427.8030 390.3666 274.3595 -5.5528 422.1459 427.6987 390.2748 275.1168 -5.5496 422.0574 427.6070 390.1976 275.9770 -5.5469 421.9570 427.5039 390.1121 276.7445 -5.5449 421.8725 427.4174 390.0305 277.5638 -5.5432 421.7762 427.3193 389.9438 278.3620 -5.5420 421.6827 427.2247 389.8631 279.1608 -5.5405 421.5895 427.1300 389.7781 279.9900 -5.5383 421.4876 427.0258 389.6877 280.7470 -5.5372 421.3919 426.9291 389.6097 281.5970 -5.5351 421.2891 426.8242 389.5293 282.3643 -5.5337 421.1944 426.7280 389.4495 283.1838 -5.5321 421.0933 426.6254 389.3636 283.9718 -5.5303 421.0002 426.5305 389.2816 284.7700 -5.5280 420.9052 426.4332 389.2013 285.5893 -5.5265 420.8091 426.3356 389.1233 286.3670 -5.5253 420.7154 426.2407 389.0476 287.1858 -5.5232 420.6171 426.1403 388.9666 287.9430 -5.5205 420.5281 426.0487 388.8908 288.8033 -5.5182 420.4233 425.9415 388.8052 289.5603 -5.5163 420.3362 425.8525 388.7295 290.3900 -5.5146 420.2391 425.7536 388.6471 291.1783 -5.5131 420.1428 425.6560 388.5675 291.9768 -5.5110 420.0453 425.5563 388.4882 292.8060 -5.5096 419.9451 425.4547 388.4016 293.5630 -5.5088 419.8541 425.3629 388.3279 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