DTA measure 1lassu Date: 2024123:1120 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 742.56 s Mass = 958.900 mg data_number = 1848 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.4725 0.5738 223.8948 223.3210 265.7473 0.9590 0.5764 224.0736 223.4973 265.7589 1.3245 0.5756 224.1978 223.6222 265.7728 1.6910 0.5732 224.3001 223.7269 265.7815 2.1170 0.5732 224.4312 223.8580 265.7867 2.5430 0.5760 224.6037 224.0277 265.8130 2.9085 0.5750 224.7110 224.1359 265.8413 3.2745 0.5754 224.8231 224.2477 265.8317 3.7610 0.5782 224.9961 224.4179 265.8384 4.1265 0.5777 225.1334 224.5558 265.8539 4.4925 0.5776 225.2494 224.6718 265.8576 4.9185 0.5797 225.3956 224.8159 265.8718 5.3450 0.5790 225.5411 224.9621 265.8839 5.7105 0.5813 225.6607 225.0793 265.9033 6.1365 0.5802 225.7961 225.2160 265.9236 6.5630 0.5821 225.9427 225.3606 265.9550 6.9285 0.5822 226.0754 225.4932 265.9584 7.2945 0.5830 226.1943 225.6113 265.9817 7.7810 0.5831 226.3378 225.7546 266.0038 8.1465 0.5824 226.4509 225.8684 266.0204 8.5125 0.5864 226.5685 225.9820 266.0429 8.9385 0.5870 226.7074 226.1205 266.0597 9.3650 0.5861 226.8456 226.2595 266.0988 9.7305 0.5840 226.9555 226.3714 266.1214 10.1565 0.5825 227.1112 226.5286 266.1506 10.5835 0.5834 227.2430 226.6596 266.1711 10.9660 0.5854 227.3559 226.7706 266.2195 11.3325 0.5872 227.4772 226.8899 266.2581 11.7585 0.5875 227.6078 227.0203 266.2894 12.1845 0.5864 227.7664 227.1800 266.3266 12.5505 0.5876 227.8716 227.2840 266.3731 12.9165 0.5873 227.9970 227.4097 266.4094 13.4025 0.5870 228.1589 227.5719 266.4728 13.7685 0.5867 228.2729 227.6862 266.5024 14.1345 0.5851 228.3969 227.8118 266.5579 14.6205 0.5868 228.5484 227.9616 266.6289 14.9875 0.5871 228.6553 228.0682 266.6730 15.3535 0.5861 228.7732 228.1870 266.7129 15.7795 0.5877 228.9043 228.3166 266.7676 16.2055 0.5868 229.0579 228.4712 266.8413 16.5715 0.5896 229.1687 228.5791 266.8964 16.9375 0.5887 229.2861 228.6974 266.9483 17.4235 0.5907 229.4329 228.8421 267.0210 17.7895 0.5873 229.5476 228.9603 267.0881 18.1555 0.5862 229.6522 229.0660 267.1539 18.6415 0.5889 229.8307 229.2418 267.2472 19.0075 0.5866 229.9437 229.3571 267.3027 19.3735 0.5879 230.0500 229.4621 267.3717 19.7995 0.5883 230.1696 229.5813 267.4497 20.2255 0.5880 230.3225 229.7345 267.5078 20.5915 0.5867 230.4325 229.8458 267.5687 20.9570 0.5861 230.5460 229.9599 267.6362 21.4435 0.5910 230.6916 230.1006 267.7331 21.8085 0.5882 230.8013 230.2131 267.7973 22.1735 0.5862 230.9361 230.3499 267.8707 22.6575 0.5852 231.0816 230.4964 267.9439 23.0225 0.5851 231.1947 230.6096 268.0214 23.3860 0.5831 231.3170 230.7340 268.1095 23.8110 0.5851 231.4375 230.8524 268.1986 24.2360 0.5838 231.5614 230.9776 268.2888 24.6000 0.5855 231.6645 231.0789 268.3731 24.9630 0.5827 231.7808 231.1981 268.4554 25.4485 0.5848 231.9322 231.3473 268.5491 25.8125 0.5834 232.0416 231.4582 268.6311 26.1770 0.5811 232.1443 231.5632 268.7079 26.6610 0.5819 232.3006 231.7188 268.8154 27.0250 0.5804 232.4193 231.8389 268.8865 27.3890 0.5807 232.5204 231.9397 268.9664 27.8130 0.5819 232.6507 232.0687 269.0563 28.2385 0.5813 232.7817 232.2004 269.1489 28.6045 0.5786 232.9009 232.3223 269.2314 29.0290 0.5797 233.0384 232.4587 269.3124 29.4535 0.5822 233.1621 232.5800 269.3990 29.8195 0.5788 233.2735 232.6947 269.4856 30.1850 0.5770 233.3864 232.8095 269.5585 30.6705 0.5767 233.5299 232.9532 269.6570 31.0365 0.5772 233.6479 233.0706 269.7291 31.4060 0.5767 233.7554 233.1787 269.8030 31.8315 0.5741 233.8744 233.3003 269.8920 32.2575 0.5719 233.9938 233.4219 269.9832 32.6235 0.5700 234.1080 233.5380 270.0509 32.9895 0.5695 234.2186 233.6491 270.0958 33.4755 0.5671 234.3445 233.7774 270.2153 33.8415 0.5670 234.4560 233.8890 270.2927 34.2075 0.5636 234.5880 234.0244 270.3444 34.6935 0.5653 234.7373 234.1719 270.4344 35.0595 0.5647 234.8319 234.2673 270.4967 35.4255 0.5637 234.9347 234.3710 270.5732 35.8515 0.5614 235.0684 234.5071 270.6630 36.2775 0.5599 235.2014 234.6415 270.7477 36.6430 0.5576 235.3017 234.7440 270.8027 37.0095 0.5547 235.4082 234.8534 270.8750 37.4955 0.5519 235.5672 235.0153 270.9651 37.8615 0.5493 235.6682 235.1189 271.0356 38.2270 0.5502 235.7808 235.2306 271.1159 38.7135 0.5507 235.9122 235.3615 271.1873 39.0795 0.5491 236.0073 235.4581 271.2583 39.4445 0.5481 236.1073 235.5592 271.3180 39.8710 0.5470 236.2413 235.6943 271.3989 40.2970 0.5458 236.3793 235.8335 271.4694 40.6625 0.5450 236.4987 235.9537 271.5499 41.0890 0.5419 236.6232 236.0814 271.6286 41.5150 0.5400 236.7632 236.2232 271.6946 41.8805 0.5399 236.8614 236.3215 271.7628 42.2465 0.5352 236.9685 236.4333 271.8259 42.7335 0.5342 237.0958 236.5616 271.8990 43.0985 0.5323 237.2032 236.6709 271.9702 43.4645 0.5289 237.3154 236.7865 272.0258 43.8930 0.5295 237.4480 236.9185 272.0875 44.3200 0.5338 237.5627 237.0289 272.1431 44.6855 0.5386 237.6659 237.1272 272.2024 45.1115 0.5410 237.7858 237.2447 272.2815 45.5380 0.5412 237.9129 237.3717 272.3450 45.9035 0.5402 238.0230 237.4827 272.4141 46.2695 0.5382 238.1376 237.5994 272.4629 46.7560 0.5381 238.2755 237.7374 272.5248 47.1215 0.5354 238.3767 237.8413 272.5859 47.4875 0.5321 238.4890 237.9569 272.6386 47.9135 0.5245 238.6099 238.0854 272.7039 48.3400 0.5196 238.7219 238.2023 272.7641 48.7055 0.5207 238.8174 238.2967 272.8135 49.1315 0.5159 238.9621 238.4463 272.8887 49.5580 0.5106 239.0855 238.5749 272.9447 49.9235 0.5104 239.1996 238.6892 272.9863 50.2895 0.5083 239.2932 238.7849 273.0254 50.7755 0.5054 239.4240 238.9185 273.1050 51.1415 0.5045 239.5183 239.0138 273.1482 51.5075 0.5006 239.6350 239.1344 273.2061 51.9940 0.4997 239.7699 239.2701 273.2831 52.3595 0.4970 239.8705 239.3735 273.3400 52.7255 0.4948 239.9781 239.4833 273.3945 53.1515 0.4927 240.0989 239.6062 273.4553 53.5775 0.4885 240.2256 239.7371 273.5244 53.9430 0.4861 240.3260 239.8399 273.5645 54.3070 0.4858 240.4158 239.9300 273.6098 54.7910 0.4841 240.5409 240.0568 273.6816 55.1550 0.4802 240.6495 240.1692 273.7219 55.5190 0.4769 240.7555 240.2786 273.7770 56.0030 0.4764 240.9013 240.4249 273.8745 56.3670 0.4785 240.9993 240.5208 273.9467 56.7310 0.4747 241.1089 240.6342 273.9855 57.1550 0.4728 241.2327 240.7599 274.0493 57.5795 0.4706 241.3521 240.8815 274.1023 57.9440 0.4685 241.4475 240.9791 274.1656 58.3080 0.4687 241.5410 241.0724 274.2228 58.7935 0.4696 241.6752 241.2056 274.2893 59.1580 0.4680 241.7721 241.3041 274.3493 59.5220 0.4677 241.8855 241.4178 274.4098 60.0065 0.4662 242.0033 241.5371 274.5012 60.3710 0.4652 242.0841 241.6189 274.5560 60.7350 0.4658 242.1859 241.7201 274.6208 61.1595 0.4612 242.3106 241.8495 274.6884 61.5855 0.4588 242.4578 241.9990 274.7347 61.9510 0.4534 242.5610 242.1076 274.8019 62.3185 0.4534 242.6561 242.2027 274.8656 62.8105 0.4536 242.7978 242.3441 274.9512 63.1765 0.4548 242.8787 242.4239 274.9973 63.5425 0.4531 242.9779 242.5247 275.0676 63.9685 0.4513 243.0975 242.6462 275.1288 64.3950 0.4501 243.2266 242.7765 275.1986 64.7605 0.4478 243.3363 242.8885 275.2531 65.1265 0.4446 243.4244 242.9798 275.3086 65.6130 0.4457 243.5518 243.1062 275.3880 65.9785 0.4432 243.6533 243.2101 275.4502 66.3445 0.4413 243.7552 243.3139 275.5107 66.7705 0.4397 243.8694 243.4298 275.5883 67.1970 0.4368 243.9911 243.5544 275.6643 67.5625 0.4340 244.0921 243.6582 275.7208 67.9885 0.4289 244.2220 243.7931 275.7962 68.4145 0.4268 244.3369 243.9101 275.8660 68.7805 0.4269 244.4311 244.0042 275.9228 69.1465 0.4226 244.5222 244.0996 275.9959 69.6335 0.4210 244.6407 244.2196 276.0854 70.0005 0.4165 244.7371 244.3206 276.1449 70.3665 0.4119 244.8505 244.4386 276.2075 70.7925 0.4099 244.9690 244.5590 276.2788 71.2785 0.4100 245.0984 244.6885 276.3490 71.7045 0.4097 245.2227 244.8131 276.4153 72.1305 0.4058 245.3269 244.9211 276.4894 72.6165 0.4016 245.4548 245.0532 276.5759 73.0425 0.3971 245.5513 245.1542 276.6380 73.4085 0.3926 245.6535 245.2610 276.7112 73.7745 0.3911 245.7652 245.3741 276.7546 74.2605 0.3885 245.9110 245.5225 276.8475 74.6265 0.3855 245.9876 245.6021 276.8953 74.9925 0.3784 246.0759 245.6975 276.9693 75.4185 0.3799 246.1921 245.8122 277.0346 75.8445 0.3808 246.3183 245.9375 277.0974 76.2105 0.3794 246.4249 246.0455 277.1596 76.6365 0.3782 246.5260 246.1478 277.2156 77.0625 0.3745 246.6397 246.2652 277.2981 77.4285 0.3721 246.7377 246.3656 277.3691 77.7945 0.3678 246.8378 246.4700 277.4356 78.2805 0.3682 246.9618 246.5936 277.5184 78.6460 0.3659 247.0592 246.6933 277.5887 79.0125 0.3623 247.1558 246.7935 277.6421 79.4385 0.3592 247.2743 246.9150 277.7202 79.8640 0.3602 247.3925 247.0323 277.7772 80.2300 0.3594 247.4611 247.1017 277.8443 80.6560 0.3566 247.5776 247.2210 277.9099 81.0820 0.3540 247.6958 247.3418 277.9802 81.4475 0.3531 247.7936 247.4404 278.0411 81.8135 0.3513 247.9010 247.5497 278.1153 82.3005 0.3483 248.0308 247.6825 278.1992 82.6810 0.3490 248.1291 247.7800 278.2626 83.0455 0.3464 248.2263 247.8799 278.3354 83.4715 0.3421 248.3286 247.9865 278.4007 83.8980 0.3390 248.4440 248.1050 278.4692 84.2635 0.3364 248.5424 248.2059 278.5145 84.6295 0.3351 248.6449 248.3098 278.5727 85.1160 0.3318 248.7712 248.4394 278.6571 85.4825 0.3268 248.8535 248.5267 278.7364 85.8485 0.3236 248.9501 248.6265 278.7877 86.2745 0.3214 249.0475 248.7261 278.8604 86.7010 0.3191 249.1680 248.8490 278.9321 87.0660 0.3176 249.2619 248.9443 278.9900 87.4300 0.3144 249.3570 249.0425 279.0466 87.9145 0.3139 249.4631 249.1492 279.1335 88.2780 0.3132 249.5640 249.2507 279.1971 88.6420 0.3102 249.6790 249.3688 279.2595 89.1260 0.3059 249.8043 249.4983 279.3383 89.4905 0.2990 249.8932 249.5943 279.3986 89.8540 0.2981 249.9773 249.6792 279.4471 90.2780 0.2952 250.0876 249.7924 279.5302 90.7020 0.2924 250.1959 249.9035 279.6087 91.0660 0.2929 250.2904 249.9975 279.6555 91.4300 0.2915 250.3994 250.1078 279.7125 91.9145 0.2853 250.5090 250.2238 279.7778 92.2780 0.2837 250.6054 250.3217 279.8413 92.6420 0.2790 250.6994 250.4204 279.9015 93.0765 0.2778 250.7999 250.5220 279.9871 93.5040 0.2743 250.9021 250.6277 280.0519 93.8680 0.2716 251.0184 250.7468 280.1208 94.2925 0.2693 251.1193 250.8500 280.1920 94.7180 0.2665 251.2165 250.9500 280.2601 95.0835 0.2622 251.3118 251.0496 280.3193 95.4490 0.2588 251.4038 251.1450 280.3836 95.9350 0.2569 251.5285 251.2716 280.4607 96.3005 0.2554 251.6205 251.3651 280.5376 96.6665 0.2513 251.7190 251.4676 280.5955 97.0925 0.2485 251.8323 251.5838 280.6556 97.5190 0.2455 251.9465 251.7010 280.7295 97.8845 0.2453 252.0353 251.7899 280.7905 98.2505 0.2443 252.1229 251.8786 280.8521 98.7375 0.2427 252.2487 252.0060 280.9344 99.1025 0.2393 252.3405 252.1012 280.9983 99.4685 0.2351 252.4371 252.2020 281.0487 99.9550 0.2320 252.5613 252.3293 281.1285 100.3205 0.2276 252.6471 252.4195 281.2089 100.6865 0.2259 252.7419 252.5160 281.2467 101.1125 0.2225 252.8547 252.6323 281.3349 101.5390 0.2232 252.9536 252.7304 281.4173 101.9045 0.2207 253.0427 252.8220 281.4783 102.2705 0.2172 253.1411 252.9239 281.5252 102.7570 0.2136 253.2569 253.0433 281.5963 103.1225 0.2129 253.3502 253.1373 281.6589 103.4885 0.2101 253.4386 253.2285 281.7157 103.9750 0.2049 253.5456 253.3406 281.7923 104.3405 0.2002 253.6476 253.4474 281.8544 104.7065 0.1977 253.7549 253.5573 281.9139 105.1325 0.1949 253.8610 253.6661 281.9954 105.5595 0.1941 253.9627 253.7686 282.0776 105.9255 0.1918 254.0407 253.8488 282.1177 106.2915 0.1886 254.1296 253.9410 282.1830 106.7780 0.1867 254.2539 254.0672 282.2510 107.1445 0.1847 254.3491 254.1644 282.3216 107.5105 0.1820 254.4357 254.2537 282.3781 107.9365 0.1804 254.5394 254.3591 282.4652 108.3630 0.1759 254.6498 254.4739 282.5473 108.7285 0.1701 254.7439 254.5738 282.6061 109.0945 0.1625 254.8325 254.6700 282.6738 109.5810 0.1575 254.9594 254.8019 282.7407 109.9465 0.1546 255.0398 254.8852 282.8036 110.3125 0.1520 255.1353 254.9833 282.8646 110.7990 0.1501 255.2533 255.1032 282.9493 111.1655 0.1543 255.3463 255.1919 283.0023 111.5315 0.1561 255.4310 255.2749 283.0503 111.9575 0.1541 255.5291 255.3750 283.1249 112.3835 0.1492 255.6447 255.4955 283.2076 112.7495 0.1472 255.7412 255.5939 283.2599 113.1155 0.1436 255.8205 255.6769 283.3253 113.6015 0.1411 255.9319 255.7908 283.4021 113.9675 0.1375 256.0148 255.8772 283.4713 114.3335 0.1333 256.1035 255.9702 283.5229 114.8195 0.1329 256.2476 256.1146 283.6013 115.1855 0.1321 256.3266 256.1945 283.6578 115.5515 0.1296 256.4095 256.2799 283.7214 115.9775 0.1258 256.5116 256.3857 283.8048 116.4040 0.1209 256.6264 256.5055 283.8764 116.7705 0.1184 256.7032 256.5848 283.9326 117.1365 0.1165 256.7936 256.6770 283.9818 117.6225 0.1127 256.9291 256.8163 284.0573 117.9885 0.1104 257.0254 256.9150 284.1244 118.3545 0.1081 257.1021 256.9940 284.1861 118.8405 0.1049 257.2210 257.1161 284.2756 119.2060 0.1012 257.3104 257.2092 284.3199 119.5695 0.0985 257.3758 257.2773 284.3803 119.9930 0.0980 257.4677 257.3697 284.4801 120.4175 0.0930 257.5843 257.4913 284.5366 120.7815 0.0843 257.6789 257.5946 284.5829 121.1460 0.0785 257.7725 257.6940 284.6423 121.6300 0.0760 257.8866 257.8106 284.7411 121.9940 0.0732 257.9754 257.9022 284.7878 122.3580 0.0708 258.0641 257.9933 284.8536 122.8420 0.0660 258.1725 258.1065 284.9244 123.2070 0.0584 258.2632 258.2048 284.9594 123.5710 0.0530 258.3679 258.3149 285.0093 123.9950 0.0512 258.4678 258.4167 285.0909 124.4195 0.0443 258.5544 258.5101 285.1642 124.7850 0.0406 258.6312 258.5906 285.2176 125.1495 0.0373 258.7150 258.6777 285.2900 125.6355 0.0373 258.8297 258.7924 285.3855 126.0015 0.0344 258.9121 258.8777 285.4409 126.3675 0.0348 259.0091 258.9743 285.5028 126.7925 0.0334 259.1174 259.0839 285.5612 127.2185 0.0303 259.2289 259.1986 285.6223 127.5840 0.0250 259.3172 259.2922 285.6949 128.0085 0.0221 259.4172 259.3951 285.7655 128.4345 0.0181 259.5140 259.4959 285.8371 128.8005 0.0165 259.6058 259.5893 285.9044 129.1665 0.0141 259.6908 259.6766 285.9592 129.6525 0.0177 259.8098 259.7921 286.0318 130.0185 0.0116 259.8925 259.8810 286.0977 130.3845 0.0070 259.9824 259.9754 286.1497 130.8105 0.0063 260.0738 260.0674 286.2213 131.2365 0.0066 260.1665 260.1599 286.2944 131.6025 0.0014 260.2564 260.2551 286.3515 131.9685 -0.0028 260.3387 260.3415 286.4145 132.4545 -0.0049 260.4666 260.4715 286.5014 132.8205 -0.0074 260.5592 260.5666 286.5635 133.1865 -0.0110 260.6401 260.6511 286.6463 133.6725 -0.0159 260.7663 260.7821 286.7201 134.0385 -0.0169 260.8457 260.8625 286.7598 134.4045 -0.0184 260.9249 260.9433 286.8223 134.8305 -0.0234 261.0242 261.0476 286.8881 135.2565 -0.0264 261.1259 261.1523 286.9659 135.6225 -0.0291 261.2041 261.2332 287.0397 135.9885 -0.0349 261.2951 261.3300 287.1073 136.4745 -0.0348 261.4068 261.4415 287.1749 136.8395 -0.0396 261.5072 261.5467 287.2374 137.2055 -0.0408 261.5915 261.6323 287.3006 137.6925 -0.0440 261.6863 261.7303 287.3662 138.0580 -0.0461 261.7786 261.8246 287.4412 138.4240 -0.0494 261.8749 261.9243 287.5202 138.8505 -0.0532 261.9605 262.0137 287.5763 139.2765 -0.0556 262.0608 262.1163 287.6631 139.6425 -0.0574 262.1513 262.2087 287.7085 140.0085 -0.0599 262.2369 262.2968 287.7593 140.4955 -0.0607 262.3536 262.4143 287.8283 140.8605 -0.0660 262.4420 262.5079 287.8968 141.2265 -0.0669 262.5250 262.5919 287.9587 141.7150 -0.0711 262.6295 262.7006 288.0389 142.0805 -0.0739 262.7110 262.7849 288.1009 142.4465 -0.0783 262.7991 262.8774 288.1623 142.8725 -0.0806 262.9023 262.9829 288.2190 143.2990 -0.0836 263.0100 263.0936 288.2852 143.6645 -0.0871 263.0881 263.1752 288.3516 144.0305 -0.0884 263.1651 263.2535 288.4109 144.5180 -0.0856 263.2988 263.3845 288.5021 144.8845 -0.0906 263.3731 263.4637 288.5486 145.2505 -0.0955 263.4577 263.5532 288.6196 145.7370 -0.0987 263.5887 263.6874 288.7103 146.1025 -0.1018 263.6725 263.7743 288.7458 146.4685 -0.1019 263.7405 263.8424 288.8186 146.8945 -0.1072 263.8499 263.9571 288.8778 147.3210 -0.1106 263.9592 264.0698 288.9467 147.6865 -0.1148 264.0249 264.1397 289.0046 148.0525 -0.1161 264.0916 264.2077 289.0700 148.5390 -0.1167 264.1962 264.3129 289.1432 148.9055 -0.1180 264.2832 264.4011 289.2072 149.2715 -0.1197 264.3796 264.4992 289.2592 149.7580 -0.1234 264.5018 264.6252 289.3514 150.1245 -0.1288 264.5952 264.7240 289.4083 150.4905 -0.1349 264.6581 264.7930 289.4547 150.9165 -0.1343 264.7511 264.8855 289.5242 151.3410 -0.1333 264.8546 264.9878 289.5916 151.7050 -0.1370 264.9424 265.0794 289.6340 152.0690 -0.1391 265.0245 265.1635 289.7003 152.5540 -0.1414 265.1313 265.2727 289.7755 152.9180 -0.1466 265.2356 265.3821 289.8445 153.2820 -0.1502 265.3166 265.4668 289.9015 153.7660 -0.1537 265.4160 265.5698 289.9805 154.1300 -0.1565 265.4972 265.6537 290.0460 154.4940 -0.1567 265.5697 265.7264 290.0934 154.9180 -0.1569 265.6668 265.8236 290.1656 155.3430 -0.1577 265.7640 265.9217 290.2330 155.7070 -0.1598 265.8625 266.0223 290.3102 156.1310 -0.1618 265.9580 266.1197 290.3694 156.5555 -0.1626 266.0432 266.2058 290.4391 156.9200 -0.1673 266.1114 266.2788 290.5156 157.2850 -0.1698 266.1864 266.3563 290.5879 157.7695 -0.1746 266.3182 266.4928 290.6533 158.1345 -0.1719 266.3932 266.5651 290.7211 158.4990 -0.1735 266.4755 266.6490 290.7931 158.9250 -0.1751 266.5779 266.7530 290.8824 159.3510 -0.1809 266.6916 266.8725 290.9522 159.7160 -0.1848 266.7774 266.9621 291.0071 160.0815 -0.1894 266.8486 267.0379 291.0706 160.5680 -0.1938 266.9584 267.1522 291.1535 160.9335 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