DTA measure 3lassu Date: 2024123:1151 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.43 s Mass = 958.900 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4856 -3.8151 415.5163 419.3314 423.5569 4.0853 -3.8236 415.8600 419.6836 423.5597 5.7005 -3.8376 416.1973 420.0350 423.5292 7.2995 -3.8398 416.5353 420.3751 423.4830 8.9135 -3.8471 416.8887 420.7359 423.4131 10.5309 -3.8529 417.2001 421.0530 423.3029 12.1295 -3.8694 417.5345 421.4039 423.1767 13.7214 -4.0149 417.8512 421.8660 423.0220 15.3304 -4.0527 418.1719 422.2246 422.8404 16.9231 -4.0629 418.4757 422.5386 422.6660 18.5458 -4.0629 418.8113 422.8742 422.4634 20.1378 -4.0298 419.1021 423.1319 422.2706 21.7321 -3.9004 419.4194 423.3197 422.0657 23.3453 -3.8707 419.7168 423.5874 421.8615 24.9444 -3.9031 419.9901 423.8932 421.6504 26.5651 -3.8991 420.2895 424.1886 421.4404 28.1644 -3.8977 420.5730 424.4707 421.2481 29.7783 -3.8886 420.8475 424.7361 421.0396 31.4225 -3.8852 421.1310 425.0162 420.8385 33.0678 -3.8911 421.4069 425.2980 420.5962 34.6670 -3.9002 421.6612 425.5614 420.3944 36.2666 -3.9032 421.9110 425.8142 420.1875 37.8956 -3.9027 422.1704 426.0731 419.9771 39.5099 -3.9018 422.4111 426.3128 419.7624 41.1099 -3.8975 422.6453 426.5429 419.5631 42.7096 -3.8998 422.8888 426.7886 419.3609 44.3228 -3.9028 423.1256 427.0285 419.1576 45.9300 -3.9065 423.3578 427.2642 418.9724 47.5374 -3.9102 423.5768 427.4869 418.7816 49.1300 -3.9163 423.7858 427.7021 418.5937 50.7370 -3.9212 423.9975 427.9187 418.4045 52.3310 -3.9252 424.2108 428.1360 418.2311 53.9443 -3.9330 424.4129 428.3459 418.0568 55.5428 -3.9494 424.6001 428.5495 417.9010 57.1566 -3.9532 424.7860 428.7392 417.7242 58.7555 -3.9601 424.9704 428.9305 417.5356 60.3546 -3.9639 425.1570 429.1209 417.3509 61.9836 -3.9662 425.3354 429.3016 417.1504 63.5825 -3.9736 425.5136 429.4872 416.9756 65.1815 -3.9792 425.6811 429.6603 416.7799 66.7955 -3.9875 425.8492 429.8368 416.6001 68.3945 -3.9975 426.0107 430.0082 416.4131 70.0100 -4.0071 426.1681 430.1753 416.2154 71.6251 -4.0246 426.3047 430.3293 416.0164 73.2248 -4.0299 426.4477 430.4776 415.8344 74.8538 -4.0255 426.6039 430.6294 415.6324 76.4834 -4.0515 426.7274 430.7789 415.4033 78.0803 -4.0530 426.8713 430.9243 415.2277 79.6860 -4.0434 426.9974 431.0408 415.0072 81.2770 -4.0452 427.1140 431.1592 414.8112 82.8691 -4.0590 427.2312 431.2902 414.6186 84.4940 -4.0599 427.3504 431.4103 414.4267 86.0890 -4.0639 427.4556 431.5196 414.2318 87.7018 -4.0714 427.5623 431.6337 414.0611 89.3008 -4.0739 427.6609 431.7348 413.8765 90.8998 -4.0798 427.7484 431.8282 413.6819 92.5031 -4.0889 427.8551 431.9440 413.4894 94.1330 -4.0919 427.9410 432.0329 413.3080 95.7316 -4.0996 428.0215 432.1211 413.1228 97.3456 -4.1067 428.1062 432.2129 412.9176 98.9446 -4.1149 428.1836 432.2985 412.7282 100.5586 -4.1231 428.2615 432.3846 412.5396 102.1664 -4.1280 428.3323 432.4602 412.3313 103.7835 -4.1373 428.3870 432.5244 412.1316 105.3828 -4.1488 428.4433 432.5921 411.9447 106.9825 -4.1532 428.5121 432.6653 411.7608 108.5965 -4.1622 428.5792 432.7414 411.5684 110.2064 -4.1701 428.6305 432.8006 411.3807 111.7980 -4.1786 428.6615 432.8401 411.1851 113.4053 -4.1828 428.7202 432.9030 410.9944 114.9978 -4.1931 428.7575 432.9506 410.7829 116.5915 -4.2017 428.8012 433.0029 410.5827 118.2156 -4.2102 428.8243 433.0344 410.3605 119.8145 -4.2107 428.8664 433.0771 410.1535 121.4135 -4.2214 428.9011 433.1226 409.9512 123.0169 -4.2318 428.9263 433.1582 409.7599 124.6315 -4.2378 428.9346 433.1723 409.5496 126.2305 -4.2423 428.9751 433.2174 409.3289 127.8595 -4.2502 428.9791 433.2293 409.1360 129.4583 -4.2554 428.9830 433.2385 408.9362 131.0569 -4.2610 428.9826 433.2436 408.7433 132.6708 -4.2661 429.0072 433.2733 408.5460 134.2696 -4.2767 429.0005 433.2772 408.3730 135.8988 -4.2800 429.0107 433.2907 408.1752 137.4986 -4.2876 429.0076 433.2952 408.0048 139.0981 -4.2911 428.9925 433.2835 407.8273 140.7126 -4.3016 428.9987 433.3002 407.6395 142.3221 -4.3022 428.9711 433.2733 407.4480 143.9284 -4.3070 428.9578 433.2648 407.2563 145.5206 -4.3143 428.9458 433.2601 407.0490 147.1289 -4.3206 428.9327 433.2533 406.8494 148.7258 -4.3282 428.9150 433.2433 406.6626 150.3386 -4.3316 428.8890 433.2206 406.4673 151.9528 -4.3372 428.8682 433.2055 406.2863 153.5516 -4.3409 428.8338 433.1747 406.0922 155.1656 -4.3490 428.7949 433.1439 405.8900 156.7646 -4.3564 428.7697 433.1261 405.6957 158.3786 -4.3584 428.7315 433.0898 405.4824 159.9926 -4.3650 428.6881 433.0531 405.2821 161.5915 -4.3720 428.6451 433.0172 405.0862 163.2055 -4.3764 428.6001 432.9765 404.8767 164.8045 -4.3816 428.5458 432.9274 404.6677 166.4185 -4.3879 428.5016 432.8895 404.4413 168.0334 -4.3911 428.4613 432.8524 404.2209 169.6331 -4.3920 428.3969 432.7889 404.0245 171.2471 -4.3976 428.3455 432.7430 403.7944 172.8470 -4.4062 428.2883 432.6945 403.5795 174.4561 -4.4058 428.2374 432.6431 403.3648 176.0624 -4.4112 428.1649 432.5761 403.1730 177.6546 -4.4168 428.1118 432.5285 402.9726 179.2621 -4.4209 428.0259 432.4469 402.7648 180.8564 -4.4238 427.9628 432.3866 402.5599 182.4533 -4.4295 427.9068 432.3363 402.3636 184.0824 -4.4295 427.8447 432.2742 402.1635 185.6811 -4.4333 427.7623 432.1956 401.9700 187.2800 -4.4385 427.6850 432.1235 401.7849 188.8788 -4.4451 427.6120 432.0572 401.5846 190.4928 -4.4485 427.5403 431.9888 401.4013 192.1066 -4.4509 427.4490 431.8999 401.2157 193.7208 -4.4533 427.3662 431.8195 401.0158 195.3196 -4.4556 427.2867 431.7423 400.8325 196.9186 -4.4605 427.1880 431.6485 400.6375 198.5326 -4.4644 427.1124 431.5768 400.4288 200.1616 -4.4602 427.0244 431.4846 400.2287 201.7606 -4.4614 426.9348 431.3963 400.0297 203.3605 -4.4646 426.8415 431.3062 399.8084 204.9750 -4.4652 426.7472 431.2124 399.6097 206.5875 -4.4656 426.6562 431.1218 399.3945 208.1949 -4.4679 426.5523 431.0201 399.1959 209.7870 -4.4684 426.4496 430.9180 398.9972 211.3930 -4.4712 426.3629 430.8341 398.8081 212.9858 -4.4737 426.2642 430.7379 398.5830 214.6133 -4.4796 426.1401 430.6198 398.3751 216.2116 -4.4811 426.0387 430.5198 398.1740 217.8105 -4.4808 425.9352 430.4161 397.9862 219.4245 -4.4823 425.8174 430.2997 397.7605 221.0235 -4.4824 425.7093 430.1918 397.5735 222.6225 -4.4846 425.6090 430.0935 397.3721 224.2526 -4.4861 425.4849 429.9710 397.1928 225.8545 -4.4844 425.3809 429.8653 397.0052 227.4531 -4.4874 425.2512 429.7385 396.8179 229.0668 -4.4863 425.1409 429.6272 396.6052 230.6656 -4.4868 425.0234 429.5102 396.3959 232.2948 -4.4877 424.9081 429.3958 396.1818 233.8938 -4.4857 424.7940 429.2798 395.9736 235.4936 -4.4850 424.6744 429.1594 395.7622 237.1076 -4.4895 424.5561 429.0456 395.5405 238.7046 -4.4932 424.4399 428.9330 395.3380 240.3260 -4.4950 424.3058 428.8009 395.1222 241.9175 -4.4927 424.1756 428.6682 394.9192 243.5103 -4.4922 424.0488 428.5410 394.7090 245.1184 -4.4936 423.9239 428.4175 394.5032 246.7146 -4.4958 423.7944 428.2901 394.2931 248.3439 -4.4953 423.6634 428.1588 394.0828 249.9426 -4.4960 423.5241 428.0202 393.8795 251.5416 -4.4955 423.3929 427.8883 393.6807 253.1556 -4.4970 423.2730 427.7700 393.4825 254.7546 -4.4954 423.1248 427.6203 393.2697 256.3696 -4.4923 422.9989 427.4913 393.0564 257.9836 -4.4916 422.8571 427.3487 392.8808 259.5975 -4.4918 422.7226 427.2144 392.6695 261.1969 -4.4888 422.5841 427.0729 392.4736 262.7965 -4.4860 422.4381 426.9240 392.2793 264.4255 -4.4867 422.2960 426.7827 392.0923 266.0276 -4.4888 422.1608 426.6496 391.9014 267.6430 -4.4863 422.0040 426.4903 391.6996 269.2421 -4.4842 421.8711 426.3553 391.4906 270.8399 -4.4804 421.7289 426.2093 391.2895 272.4618 -4.4773 421.5808 426.0581 391.0913 274.0528 -4.4769 421.4361 425.9131 390.8644 275.6600 -4.4738 421.2896 425.7634 390.6483 277.2528 -4.4743 421.1458 425.6202 390.4464 278.8631 -4.4731 421.0042 425.4773 390.2152 280.4774 -4.4718 420.8435 425.3153 389.9971 282.0764 -4.4704 420.6929 425.1633 389.7801 283.6750 -4.4645 420.5494 425.0139 389.5719 285.2886 -4.4650 420.3926 424.8576 389.3499 286.8878 -4.4633 420.2482 424.7115 389.1481 288.4866 -4.4608 420.0934 424.5541 388.9381 290.1158 -4.4555 419.9341 424.3896 388.7119 291.7156 -4.4553 419.7801 424.2354 388.5093 293.3146 -4.4497 419.6240 424.0737 388.3007 294.9291 -4.4478 419.4597 423.9075 388.0822 296.5395 -4.4467 419.3202 423.7669 387.8788 298.1455 -4.4433 419.1506 423.5939 387.6804 299.7595 -4.4417 418.9873 423.4290 387.4777 301.3586 -4.4378 418.8355 423.2733 387.2844 302.9703 -4.4323 418.6708 423.1031 387.0799 304.5608 -4.4282 418.5190 422.9472 386.8843 306.1820 -4.4256 418.3638 422.7894 386.6727 307.7741 -4.4210 418.1857 422.6067 386.4835 309.3824 -4.4084 418.0256 422.4339 386.2742 310.9773 -4.4051 417.8709 422.2760 386.0685 312.5905 -4.4047 417.6978 422.1025 385.8731 314.2045 -4.4115 417.5357 421.9472 385.6857 315.8035 -4.4118 417.3754 421.7872 385.4924 317.4175 -4.4076 417.1978 421.6054 385.2894 319.0165 -4.4050 417.0348 421.4398 385.0844 320.6305 -4.4034 416.8910 421.2944 384.9003 322.2595 -4.3975 416.7102 421.1077 384.6978 323.8585 -4.3902 416.5529 420.9431 384.4979 325.4724 -4.3926 416.3716 420.7642 384.2954 327.0735 -4.3897 416.2004 420.5901 384.0785 328.6746 -4.3886 416.0318 420.4204 383.8615 330.3038 -4.3829 415.8651 420.2480 383.6567 331.9036 -4.3791 415.7079 420.0870 383.4515 333.5029 -4.3697 415.5300 419.8997 383.2391 335.1178 -4.3679 415.3473 419.7152 383.0053 336.7125 -4.3639 415.1788 419.5427 382.8008 338.3174 -4.3574 415.0232 419.3806 382.5868 339.9248 -4.3528 414.8465 419.1993 382.3756 341.5338 -4.3457 414.6595 419.0052 382.1566 343.1291 -4.3505 414.5076 418.8581 381.9678 344.7269 -4.3513 414.3261 418.6774 381.7702 346.3408 -4.3509 414.1482 418.4991 381.5546 347.9396 -4.3457 413.9655 418.3111 381.3519 349.5536 -4.3418 413.7906 418.1324 381.1434 351.1678 -4.3378 413.6222 417.9601 380.9363 352.7666 -4.3335 413.4638 417.7973 380.7320 354.3656 -4.3301 413.2790 417.6090 380.5213 355.9795 -4.3249 413.0946 417.4195 380.3327 357.5938 -4.3189 412.9186 417.2375 380.1258 359.1958 -4.3147 412.7324 417.0471 379.9295 360.8138 -4.3110 412.5534 416.8644 379.7313 362.4139 -4.3099 412.3688 416.6787 379.5304 364.0134 -4.3067 412.1819 416.4886 379.3265 365.6421 -4.3052 412.0139 416.3191 379.1290 367.2411 -4.3012 411.8342 416.1355 378.9242 368.8484 -4.2947 411.6675 415.9622 378.7270 370.4403 -4.2913 411.4775 415.7688 378.5285 372.0329 -4.2883 411.2873 415.5755 378.3378 373.6564 -4.2814 411.1327 415.4140 378.1399 375.2644 -4.2793 410.9476 415.2269 377.9242 376.8608 -4.2713 410.7478 415.0191 377.6964 378.4595 -4.2705 410.5671 414.8376 377.4969 380.0735 -4.2702 410.3810 414.6513 377.2777 381.6874 -4.2650 410.2022 414.4672 377.0658 383.3010 -4.2601 410.0222 414.2823 376.8430 384.9000 -4.2547 409.8324 414.0871 376.6246 386.4988 -4.2505 409.6525 413.9031 376.4142 388.1204 -4.2396 409.4608 413.7004 376.1819 389.7126 -4.2434 409.2798 413.5232 375.9602 391.3416 -4.2415 409.1071 413.3486 375.7508 392.9411 -4.2357 408.9270 413.1627 375.5324 394.5556 -4.2272 408.7237 412.9510 375.3234 396.1550 -4.2221 408.5490 412.7711 375.1081 397.7550 -4.2196 408.3693 412.5889 374.8898 399.3683 -4.2152 408.1789 412.3941 374.6860 400.9750 -4.2084 407.9800 412.1883 374.4748 402.5666 -4.2039 407.8015 412.0054 374.2683 404.1745 -4.1980 407.6296 411.8276 374.0621 405.7691 -4.1937 407.4431 411.6368 373.8508 407.3793 -4.1902 407.2415 411.4317 373.6585 408.9906 -4.1844 407.0588 411.2432 373.4340 410.5896 -4.1818 406.8668 411.0486 373.2408 412.2036 -4.1761 406.6777 410.8538 373.0233 413.8025 -4.1705 406.4957 410.6662 372.8228 415.4316 -4.1673 406.3111 410.4784 372.6106 417.0305 -4.1631 406.1254 410.2885 372.4211 418.6445 -4.1565 405.9169 410.0735 372.2303 420.2435 -4.1508 405.7427 409.8935 372.0153 421.8575 -4.1482 405.5556 409.7038 371.8282 423.4721 -4.1417 405.3588 409.5005 371.6220 425.0859 -4.1278 405.1676 409.2954 371.4213 426.6848 -4.1236 404.9729 409.0965 371.2261 428.2993 -4.1170 404.7872 408.9042 371.0200 429.8986 -4.1160 404.5970 408.7130 370.8295 431.5271 -4.1099 404.3849 408.4948 370.6422 433.1193 -4.1050 404.1834 408.2884 370.4356 434.7113 -4.0990 404.0064 408.1055 370.2361 436.3201 -4.0944 403.8381 407.9325 370.0358 437.9141 -4.0924 403.6278 407.7202 369.8244 439.5420 -4.0991 403.4459 407.5450 369.5995 441.1404 -4.1125 403.2461 407.3586 369.4010 442.7388 -4.0907 403.0534 407.1440 369.1882 444.3401 -4.0798 402.8650 406.9449 368.9667 445.9556 -4.0880 402.6654 406.7534 368.7398 447.5696 -4.0908 402.4801 406.5708 368.5306 449.1838 -4.0848 402.2820 406.3668 368.3099 450.7826 -4.0775 402.0950 406.1725 368.0897 452.3966 -4.0653 401.8867 405.9520 367.8733 453.9956 -4.0619 401.6999 405.7619 367.6813 455.6246 -4.0614 401.4970 405.5584 367.4452 457.2235 -4.0607 401.3058 405.3665 367.2472 458.8379 -4.0561 401.1095 405.1656 367.0264 460.4375 -4.0514 400.9220 404.9733 366.8173 462.0520 -4.0532 400.7162 404.7694 366.6173 463.6673 -4.0532 400.5355 404.5887 366.3932 465.2629 -4.0475 400.3558 404.4033 366.1939 466.8560 -4.0393 400.1485 404.1878 365.9908 468.4638 -4.0352 399.9447 403.9798 365.7911 470.0715 -4.0270 399.7668 403.7938 365.5894 471.6796 -4.0235 399.5631 403.5866 365.3768 473.2748 -4.0226 399.3552 403.3778 365.1586 474.8875 -4.0160 399.1601 403.1761 364.9733 476.4865 -4.0083 398.9914 402.9997 364.7828 478.0851 -4.0030 398.7721 402.7752 364.5890 479.7141 -3.9987 398.5718 402.5705 364.3915 481.3130 -3.9934 398.3847 402.3781 364.1865 482.9119 -3.9903 398.1717 402.1619 363.9801 484.5256 -3.9784 397.9701 401.9485 363.8074 486.1396 -3.9715 397.7868 401.7583 363.5950 487.7549 -3.9609 397.5859 401.5468 363.3830 489.3546 -3.9481 397.4053 401.3535 363.1953 490.9690 -3.9437 397.2020 401.1457 362.9998 492.5686 -3.9394 397.0002 400.9396 362.7951 494.1826 -3.9417 396.7981 400.7398 362.5979 495.7974 -3.9437 396.6118 400.5555 362.3810 497.4070 -3.9458 396.3922 400.3380 362.1687 498.9986 -3.9433 396.2075 400.1508 361.9688 500.5900 -3.9346 396.0237 399.9584 361.7582 502.2131 -3.9291 395.8013 399.7304 361.5328 503.8224 -3.9263 395.6089 399.5352 361.3228 505.4183 -3.9142 395.4307 399.3449 361.1228 507.0166 -3.8973 395.2178 399.1151 360.9171 508.6306 -3.8865 395.0196 398.9062 360.6939 510.2596 -3.8809 394.8197 398.7006 360.4909 511.8585 -3.8757 394.6229 398.4986 360.2870 513.4575 -3.8703 394.4302 398.3005 360.0686 515.0569 -3.8648 394.2349 398.0996 359.8588 516.6721 -3.8611 394.0294 397.8905 359.6461 518.2873 -3.8553 393.8186 397.6739 359.4475 519.9014 -3.8475 393.6254 397.4728 359.2253 521.5003 -3.8436 393.4179 397.2614 359.0202 523.1139 -3.8374 393.2358 397.0733 358.8148 524.7133 -3.8306 393.0443 396.8749 358.6159 526.3435 -3.8255 392.8451 396.6706 358.4115 527.9425 -3.8229 392.6438 396.4667 358.2069 529.5514 -3.8185 392.4420 396.2605 358.0022 531.1433 -3.8117 392.2443 396.0560 357.8040 532.7501 -3.8060 392.0500 395.8560 357.6049 534.3590 -3.8004 391.8465 395.6468 357.3994 535.9551 -3.7946 391.6368 395.4313 357.2053 537.5651 -3.7936 391.4352 395.2288 356.9956 539.1608 -3.7924 391.2564 395.0488 356.7968 540.7896 -3.7873 391.0586 394.8459 356.5823 542.3888 -3.7812 390.8555 394.6368 356.3692 543.9876 -3.7781 390.6542 394.4323 356.1575 545.6016 -3.7714 390.4599 394.2313 355.9279 547.2006 -3.7612 390.2623 394.0235 355.7225 548.8146 -3.7519 390.0554 393.8073 355.5174 550.4295 -3.7430 389.8569 393.5999 355.2884 552.0435 -3.7373 389.6569 393.3941 355.0612 553.6425 -3.7332 389.4662 393.1994 354.8502 555.2415 -3.7267 389.2595 392.9862 354.6386 556.8713 -3.7252 389.0480 392.7731 354.4089 558.4714 -3.7306 388.8486 392.5792 354.2026 560.0854 -3.7272 388.6500 392.3772 353.9772 561.6793 -3.7232 388.4255 392.1487 353.7616 563.2710 -3.7114 388.2338 391.9452 353.5527 564.8920 -3.6953 388.0436 391.7388 353.3253 566.4990 -3.6890 387.8369 391.5260 353.1160 568.0955 -3.6917 387.6350 391.3266 352.8956 569.6930 -3.6821 387.4364 391.1185 352.6970 571.2915 -3.6768 387.2404 390.9171 352.4794 572.9205 -3.6710 387.0503 390.7213 352.2687 574.5193 -3.6670 386.8344 390.5014 352.0631 576.1335 -3.6606 386.6276 390.2882 351.8528 577.7329 -3.6541 386.4244 390.0785 351.6460 579.3338 -3.6483 386.2350 389.8833 351.4404 580.9631 -3.6499 386.0211 389.6710 351.2209 582.5618 -3.6497 385.8125 389.4622 351.0128 584.1766 -3.6412 385.6065 389.2476 350.8059 585.7760 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