DTA measure 1_6fazis_masik Date: 202548:1627 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 141.43 s Mass = 100.000 mg data_number = 704 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.2930 -1.7197 272.8464 274.5660 237.3528 0.4620 -1.7197 272.8243 274.5441 237.3239 0.6720 -1.7196 272.7966 274.5162 237.2946 0.8410 -1.7199 272.7742 274.4941 237.2701 1.0100 -1.7199 272.7509 274.4708 237.2510 1.3440 -1.7196 272.7089 274.4285 237.2051 1.5120 -1.7194 272.6884 274.4078 237.1803 1.6810 -1.7198 272.6691 274.3889 237.1589 1.8910 -1.7201 272.6410 274.3611 237.1277 2.0600 -1.7205 272.6205 274.3410 237.1029 2.2290 -1.7202 272.5984 274.3185 237.0780 2.4390 -1.7199 272.5718 274.2917 237.0465 2.7310 -1.7201 272.5337 274.2539 237.0038 2.9000 -1.7199 272.5099 274.2298 236.9772 3.1100 -1.7205 272.4857 274.2062 236.9456 3.2790 -1.7205 272.4628 274.1833 236.9219 3.4480 -1.7208 272.4409 274.1617 236.8986 3.6580 -1.7210 272.4133 274.1342 236.8672 3.8260 -1.7215 272.3915 274.1130 236.8433 4.1190 -1.7217 272.3576 274.0794 236.7980 4.3290 -1.7216 272.3318 274.0533 236.7676 4.4980 -1.7215 272.3138 274.0353 236.7450 4.6670 -1.7215 272.2916 274.0130 236.7189 4.8770 -1.7216 272.2635 273.9852 236.6895 5.0450 -1.7216 272.2405 273.9621 236.6682 5.2560 -1.7214 272.2136 273.9351 236.6346 5.5480 -1.7216 272.1746 273.8962 236.5915 5.7170 -1.7218 272.1537 273.8755 236.5675 5.9270 -1.7221 272.1271 273.8492 236.5386 6.0960 -1.7216 272.1074 273.8290 236.5152 6.2640 -1.7218 272.0856 273.8073 236.4909 6.4740 -1.7217 272.0569 273.7786 236.4637 6.6430 -1.7219 272.0349 273.7568 236.4380 6.9360 -1.7219 271.9978 273.7197 236.3929 7.1460 -1.7222 271.9690 273.6912 236.3609 7.3150 -1.7224 271.9484 273.6708 236.3348 7.4840 -1.7223 271.9257 273.6480 236.3105 7.6940 -1.7227 271.9005 273.6232 236.2829 7.8620 -1.7225 271.8770 273.5995 236.2580 8.0310 -1.7223 271.8551 273.5774 236.2345 8.3650 -1.7229 271.8152 273.5381 236.1831 8.5340 -1.7230 271.7935 273.5165 236.1632 8.7030 -1.7232 271.7696 273.4928 236.1386 8.9130 -1.7236 271.7440 273.4676 236.1078 9.0810 -1.7235 271.7240 273.4475 236.0827 9.2920 -1.7238 271.6950 273.4187 236.0516 9.4600 -1.7239 271.6736 273.3976 236.0284 9.7530 -1.7237 271.6401 273.3638 235.9857 9.9630 -1.7238 271.6146 273.3385 235.9581 10.1320 -1.7241 271.5927 273.3169 235.9365 10.3010 -1.7246 271.5703 273.2949 235.9142 10.5110 -1.7244 271.5432 273.2676 235.8859 10.6790 -1.7246 271.5175 273.2422 235.8600 10.8480 -1.7248 271.4936 273.2184 235.8357 11.0580 -1.7247 271.4669 273.1916 235.8084 11.3510 -1.7251 271.4262 273.1512 235.7644 11.5200 -1.7247 271.4045 273.1292 235.7465 11.7300 -1.7248 271.3772 273.1020 235.7185 11.8980 -1.7248 271.3551 273.0798 235.6958 12.0670 -1.7249 271.3328 273.0577 235.6708 12.2770 -1.7244 271.3051 273.0294 235.6434 12.4460 -1.7241 271.2850 273.0091 235.6207 12.7390 -1.7243 271.2500 272.9743 235.5794 12.9490 -1.7246 271.2234 272.9480 235.5478 13.1180 -1.7245 271.2004 272.9248 235.5252 13.3280 -1.7249 271.1773 272.9022 235.4946 13.4960 -1.7255 271.1586 272.8842 235.4708 13.6650 -1.7258 271.1385 272.8643 235.4469 13.8750 -1.7261 271.1061 272.8322 235.4182 14.1680 -1.7265 271.0676 272.7942 235.3780 14.3370 -1.7267 271.0464 272.7730 235.3550 14.5470 -1.7273 271.0190 272.7463 235.3273 14.7150 -1.7273 270.9999 272.7272 235.3037 14.8840 -1.7275 270.9775 272.7051 235.2789 15.0940 -1.7276 270.9549 272.6825 235.2453 15.2630 -1.7277 270.9325 272.6602 235.2195 15.5560 -1.7279 270.8966 272.6245 235.1803 15.7660 -1.7281 270.8716 272.5997 235.1538 15.9350 -1.7282 270.8534 272.5817 235.1293 16.1450 -1.7289 270.8269 272.5558 235.0971 16.3130 -1.7287 270.8071 272.5359 235.0750 16.4820 -1.7289 270.7846 272.5136 235.0516 16.6920 -1.7288 270.7589 272.4877 235.0229 16.9850 -1.7290 270.7175 272.4465 234.9805 17.1540 -1.7287 270.6955 272.4242 234.9563 17.3640 -1.7286 270.6696 272.3983 234.9241 17.5320 -1.7291 270.6458 272.3749 234.8999 17.7010 -1.7294 270.6233 272.3527 234.8812 17.9110 -1.7299 270.5958 272.3256 234.8524 18.0800 -1.7294 270.5732 272.3026 234.8312 18.3730 -1.7293 270.5320 272.2614 234.7886 18.5830 -1.7296 270.5040 272.2336 234.7596 18.7520 -1.7298 270.4817 272.2115 234.7363 18.9200 -1.7300 270.4604 272.1904 234.7153 19.1300 -1.7300 270.4309 272.1609 234.6864 19.2990 -1.7304 270.4112 272.1417 234.6624 19.5090 -1.7309 270.3841 272.1150 234.6318 19.8020 -1.7313 270.3497 272.0810 234.5882 19.9710 -1.7314 270.3306 272.0620 234.5641 20.1810 -1.7316 270.3016 272.0332 234.5337 20.3490 -1.7314 270.2806 272.0120 234.5087 20.5180 -1.7316 270.2607 271.9923 234.4871 20.7280 -1.7316 270.2361 271.9677 234.4579 20.8970 -1.7320 270.2162 271.9482 234.4344 21.0660 -1.7322 270.1940 271.9262 234.4113 21.4000 -1.7320 270.1483 271.8803 234.3649 21.5680 -1.7319 270.1269 271.8587 234.3442 21.7370 -1.7318 270.1051 271.8369 234.3200 21.9470 -1.7316 270.0769 271.8085 234.2904 22.1160 -1.7319 270.0526 271.7844 234.2661 22.3260 -1.7324 270.0264 271.7588 234.2374 22.4950 -1.7322 270.0036 271.7358 234.2132 22.7880 -1.7324 269.9640 271.6964 234.1728 22.9980 -1.7325 269.9365 271.6690 234.1465 23.1660 -1.7325 269.9141 271.6466 234.1235 23.3350 -1.7324 269.8912 271.6236 234.0997 23.5450 -1.7321 269.8656 271.5977 234.0714 23.7140 -1.7319 269.8427 271.5746 234.0497 23.8830 -1.7321 269.8204 271.5525 234.0284 24.2170 -1.7322 269.7795 271.5117 233.9814 24.3860 -1.7328 269.7580 271.4908 233.9603 24.5540 -1.7329 269.7344 271.4673 233.9353 24.7640 -1.7329 269.7087 271.4417 233.9051 24.9330 -1.7331 269.6863 271.4194 233.8800 25.1020 -1.7329 269.6645 271.3974 233.8578 25.3120 -1.7332 269.6333 271.3665 233.8283 25.6040 -1.7337 269.5937 271.3273 233.7879 25.7730 -1.7335 269.5738 271.3074 233.7640 25.9830 -1.7337 269.5479 271.2815 233.7350 26.1520 -1.7337 269.5302 271.2639 233.7114 26.3620 -1.7341 269.5033 271.2374 233.6845 26.5310 -1.7348 269.4808 271.2156 233.6610 26.6990 -1.7348 269.4607 271.1956 233.6377 27.0340 -1.7347 269.4198 271.1544 233.5924 27.2020 -1.7345 269.3981 271.1326 233.5691 27.3710 -1.7350 269.3746 271.1096 233.5449 27.5810 -1.7355 269.3443 271.0798 233.5121 27.7500 -1.7359 269.3231 271.0590 233.4872 27.9190 -1.7355 269.2991 271.0346 233.4654 28.1290 -1.7353 269.2711 271.0064 233.4360 28.4210 -1.7358 269.2314 270.9672 233.3976 28.5900 -1.7356 269.2093 270.9450 233.3752 28.8000 -1.7359 269.1825 270.9183 233.3444 28.9690 -1.7358 269.1613 270.8971 233.3206 29.1790 -1.7360 269.1317 270.8677 233.2900 29.3480 -1.7362 269.1084 270.8446 233.2672 29.5160 -1.7360 269.0871 270.8231 233.2453 29.8500 -1.7361 269.0443 270.7804 233.1959 30.0190 -1.7360 269.0241 270.7601 233.1739 30.1880 -1.7361 269.0043 270.7403 233.1497 30.3980 -1.7361 268.9739 270.7100 233.1222 30.5670 -1.7365 268.9487 270.6852 233.0969 30.7350 -1.7369 268.9250 270.6620 233.0724 30.9450 -1.7370 268.8985 270.6355 233.0410 31.2380 -1.7370 268.8570 270.5940 233.0002 31.4070 -1.7370 268.8334 270.5704 232.9760 31.6170 -1.7368 268.8074 270.5442 232.9449 31.7860 -1.7368 268.7858 270.5226 232.9237 31.9960 -1.7369 268.7551 270.4920 232.8980 32.1650 -1.7371 268.7322 270.4693 232.8745 32.3330 -1.7366 268.7092 270.4458 232.8481 32.6670 -1.7369 268.6643 270.4012 232.8017 32.8360 -1.7370 268.6416 270.3786 232.7793 33.0050 -1.7369 268.6183 270.3552 232.7553 33.2150 -1.7373 268.5891 270.3264 232.7276 33.3840 -1.7374 268.5657 270.3031 232.7044 33.5520 -1.7374 268.5420 270.2794 232.6815 33.7630 -1.7375 268.5131 270.2506 232.6524 33.9310 -1.7375 268.4917 270.2291 232.6274 34.2240 -1.7376 268.4514 270.1890 232.5876 34.4340 -1.7378 268.4234 270.1612 232.5534 34.6030 -1.7379 268.3986 270.1365 232.5291 34.8130 -1.7384 268.3691 270.1075 232.5026 34.9820 -1.7385 268.3466 270.0851 232.4812 35.1510 -1.7388 268.3270 270.0658 232.4566 35.3600 -1.7389 268.3026 270.0415 232.4295 35.6530 -1.7392 268.2639 270.0031 232.3900 35.8220 -1.7393 268.2429 269.9822 232.3664 36.0320 -1.7401 268.2190 269.9591 232.3357 36.2010 -1.7400 268.1949 269.9348 232.3134 36.3690 -1.7400 268.1741 269.9141 232.2905 36.5800 -1.7401 268.1472 269.8872 232.2646 36.7480 -1.7399 268.1252 269.8650 232.2424 37.0410 -1.7398 268.0863 269.8261 232.2039 37.2510 -1.7394 268.0557 269.7951 232.1741 37.4200 -1.7391 268.0307 269.7698 232.1532 37.6300 -1.7392 268.0016 269.7408 232.1226 37.7990 -1.7393 267.9808 269.7202 232.1000 37.9670 -1.7393 267.9608 269.7001 232.0763 38.1770 -1.7394 267.9299 269.6693 232.0473 38.4700 -1.7397 267.8911 269.6308 232.0058 38.6390 -1.7399 267.8680 269.6078 231.9833 38.8490 -1.7399 267.8406 269.5805 231.9520 39.0180 -1.7396 267.8197 269.5593 231.9328 39.1860 -1.7397 267.7962 269.5360 231.9082 39.3960 -1.7396 267.7676 269.5072 231.8777 39.5650 -1.7396 267.7475 269.4870 231.8544 39.8580 -1.7397 267.7058 269.4455 231.8136 40.0680 -1.7394 267.6812 269.4207 231.7848 40.2370 -1.7393 267.6586 269.3979 231.7611 40.4470 -1.7395 267.6269 269.3664 231.7359 40.6150 -1.7396 267.6089 269.3485 231.7123 40.7840 -1.7398 267.5872 269.3270 231.6871 40.9940 -1.7403 267.5603 269.3006 231.6579 41.2870 -1.7401 267.5191 269.2592 231.6178 41.4560 -1.7397 267.4949 269.2346 231.5988 41.6660 -1.7394 267.4648 269.2042 231.5691 41.8340 -1.7394 267.4458 269.1852 231.5477 42.0030 -1.7395 267.4235 269.1630 231.5248 42.2130 -1.7398 267.3945 269.1343 231.4962 42.3820 -1.7398 267.3745 269.1142 231.4757 42.6750 -1.7395 267.3324 269.0719 231.4376 42.8850 -1.7390 267.3048 269.0438 231.4077 43.0540 -1.7387 267.2839 269.0226 231.3837 43.2640 -1.7389 267.2579 268.9969 231.3560 43.4320 -1.7391 267.2353 268.9744 231.3311 43.6010 -1.7391 267.2140 268.9530 231.3082 43.8110 -1.7391 267.1894 268.9285 231.2791 44.1040 -1.7393 267.1489 268.8882 231.2368 44.2730 -1.7390 267.1275 268.8664 231.2144 44.4830 -1.7381 267.1018 268.8399 231.1883 44.6510 -1.7380 267.0782 268.8163 231.1665 44.8200 -1.7384 267.0598 268.7982 231.1439 45.0300 -1.7382 267.0346 268.7727 231.1158 45.1990 -1.7377 267.0110 268.7487 231.0933 45.4920 -1.7375 266.9757 268.7132 231.0519 45.7020 -1.7374 266.9470 268.6844 231.0227 45.8700 -1.7376 266.9263 268.6639 231.0002 46.0800 -1.7378 266.8991 268.6369 230.9749 46.2490 -1.7380 266.8790 268.6170 230.9540 46.4180 -1.7380 266.8571 268.5951 230.9296 46.6280 -1.7375 266.8342 268.5717 230.9033 46.9210 -1.7374 266.7924 268.5298 230.8657 47.0890 -1.7374 266.7743 268.5117 230.8423 47.2990 -1.7371 266.7495 268.4866 230.8148 47.4680 -1.7362 266.7270 268.4632 230.7955 47.6370 -1.7365 266.7044 268.4409 230.7710 47.8470 -1.7361 266.6754 268.4115 230.7449 48.0160 -1.7361 266.6531 268.3892 230.7242 48.3500 -1.7359 266.6078 268.3437 230.6791 48.5180 -1.7361 266.5848 268.3210 230.6571 48.6870 -1.7364 266.5616 268.2980 230.6352 48.8970 -1.7365 266.5347 268.2712 230.6101 49.0660 -1.7364 266.5108 268.2472 230.5864 49.2340 -1.7367 266.4893 268.2260 230.5673 49.4450 -1.7369 266.4591 268.1960 230.5413 49.7370 -1.7369 266.4218 268.1587 230.5054 49.9060 -1.7374 266.3975 268.1348 230.4802 50.1160 -1.7373 266.3699 268.1072 230.4545 50.2850 -1.7372 266.3426 268.0798 230.4317 50.4950 -1.7371 266.3131 268.0502 230.4035 50.6640 -1.7372 266.2941 268.0313 230.3815 50.8320 -1.7371 266.2711 268.0081 230.3569 51.0430 -1.7373 266.2439 267.9812 230.3290 51.3350 -1.7371 266.2038 267.9409 230.2896 51.5040 -1.7371 266.1834 267.9205 230.2665 51.7140 -1.7373 266.1522 267.8895 230.2374 51.8830 -1.7375 266.1277 267.8652 230.2134 52.0520 -1.7377 266.1038 267.8416 230.1944 52.2620 -1.7376 266.0752 267.8128 230.1640 52.4300 -1.7376 266.0510 267.7886 230.1397 52.7230 -1.7371 266.0159 267.7531 230.1022 52.9330 -1.7370 265.9916 267.7286 230.0694 53.1020 -1.7366 265.9697 267.7063 230.0484 53.3120 -1.7363 265.9437 267.6800 230.0183 53.4810 -1.7365 265.9199 267.6564 229.9945 53.6490 -1.7367 265.8977 267.6344 229.9727 53.8590 -1.7369 265.8680 267.6049 229.9466 54.1520 -1.7371 265.8348 267.5719 229.9097 54.3210 -1.7372 265.8145 267.5517 229.8850 54.5310 -1.7372 265.7854 267.5226 229.8575 54.7000 -1.7372 265.7613 267.4985 229.8370 54.8680 -1.7368 265.7382 267.4750 229.8138 55.0790 -1.7370 265.7125 267.4495 229.7836 55.2470 -1.7369 265.6884 267.4253 229.7611 55.5400 -1.7374 265.6511 267.3885 229.7211 55.7500 -1.7371 265.6195 267.3567 229.6943 55.9190 -1.7372 265.5955 267.3327 229.6716 56.0870 -1.7373 265.5721 267.3094 229.6517 56.2980 -1.7372 265.5433 267.2805 229.6249 56.4660 -1.7372 265.5210 267.2582 229.6031 56.6350 -1.7375 265.4989 267.2364 229.5811 56.9690 -1.7383 265.4547 267.1930 229.5383 57.1380 -1.7383 265.4318 267.1701 229.5160 57.3060 -1.7380 265.4082 267.1462 229.4941 57.5170 -1.7379 265.3806 267.1186 229.4661 57.6850 -1.7380 265.3572 267.0952 229.4445 57.8540 -1.7381 265.3356 267.0736 229.4214 58.0640 -1.7381 265.3087 267.0468 229.3892 58.3570 -1.7383 265.2688 267.0071 229.3514 58.5250 -1.7383 265.2434 266.9817 229.3299 58.7350 -1.7377 265.2159 266.9536 229.3057 58.9040 -1.7377 265.1928 266.9305 229.2835 59.0730 -1.7377 265.1730 266.9107 229.2595 59.2830 -1.7371 265.1444 266.8815 229.2329 59.4520 -1.7372 265.1198 266.8570 229.2126 59.7440 -1.7369 265.0773 266.8143 229.1747 59.9540 -1.7369 265.0508 266.7877 229.1474 60.1230 -1.7370 265.0291 266.7661 229.1249 60.2920 -1.7368 265.0090 266.7458 229.1038 60.5020 -1.7366 264.9826 266.7193 229.0772 60.6710 -1.7367 264.9605 266.6972 229.0556 60.8810 -1.7370 264.9340 266.6710 229.0308 61.1740 -1.7369 264.8938 266.6307 228.9919 61.3420 -1.7369 264.8744 266.6113 228.9684 61.5110 -1.7369 264.8521 266.5890 228.9459 61.7210 -1.7371 264.8244 266.5616 228.9197 61.8900 -1.7370 264.8017 266.5387 228.8977 62.0580 -1.7371 264.7771 266.5142 228.8764 62.2690 -1.7372 264.7493 266.4866 228.8472 62.5610 -1.7377 264.7126 266.4503 228.8082 62.7300 -1.7377 264.6890 266.4267 228.7876 62.9400 -1.7379 264.6612 266.3991 228.7616 63.1090 -1.7381 264.6380 266.3761 228.7387 63.2770 -1.7375 264.6136 266.3511 228.7162 63.4870 -1.7377 264.5866 266.3243 228.6883 63.6560 -1.7374 264.5653 266.3027 228.6628 63.9490 -1.7372 264.5268 266.2640 228.6274 64.1590 -1.7371 264.4977 266.2348 228.6064 64.3280 -1.7371 264.4749 266.2120 228.5841 64.4960 -1.7369 264.4522 266.1891 228.5612 64.7070 -1.7369 264.4270 266.1639 228.5342 64.8750 -1.7372 264.4031 266.1403 228.5114 65.0850 -1.7371 264.3720 266.1091 228.4842 65.3780 -1.7370 264.3323 266.0693 228.4466 65.5470 -1.7370 264.3100 266.0470 228.4232 65.7570 -1.7369 264.2831 266.0200 228.3947 65.9260 -1.7370 264.2601 265.9971 228.3735 66.0940 -1.7371 264.2396 265.9767 228.3542 66.3040 -1.7370 264.2148 265.9518 228.3256 66.4730 -1.7370 264.1930 265.9301 228.3038 66.7660 -1.7370 264.1516 265.8886 228.2654 66.9760 -1.7372 264.1219 265.8591 228.2382 67.1450 -1.7373 264.0986 265.8360 228.2173 67.3130 -1.7376 264.0764 265.8140 228.1937 67.5230 -1.7376 264.0478 265.7854 228.1653 67.6920 -1.7369 264.0242 265.7611 228.1419 67.8610 -1.7364 264.0023 265.7387 228.1187 68.0710 -1.7359 263.9732 265.7090 228.0865 68.3640 -1.7356 263.9353 265.6709 228.0496 68.5320 -1.7357 263.9173 265.6530 228.0278 68.7430 -1.7358 263.8907 265.6265 227.9998 68.9110 -1.7357 263.8693 265.6050 227.9758 69.0800 -1.7359 263.8466 265.5825 227.9535 69.2900 -1.7360 263.8175 265.5535 227.9244 69.4590 -1.7357 263.7954 265.5312 227.9018 69.7520 -1.7356 263.7601 265.4957 227.8645 69.9620 -1.7354 263.7295 265.4649 227.8379 70.1300 -1.7352 263.7043 265.4395 227.8156 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