DTA measure 1pbupdown3 Date: 20251015:1030 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.74 s Mass = 1334.3 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2308 0.2951 255.5468 255.2517 276.4578 1.9870 0.2942 255.6641 255.3699 276.5502 2.8253 0.3005 255.7876 255.4871 276.5851 3.5815 0.3037 255.9138 255.6101 276.5998 4.4503 0.3062 256.0827 255.7765 276.6084 5.2058 0.3116 256.2248 255.9131 276.6044 6.0338 0.3164 256.4283 256.1118 276.5695 6.8310 0.3158 256.6254 256.3096 276.5105 7.6283 0.3157 256.7601 256.4443 276.4403 8.4563 0.3154 256.9452 256.6297 276.3507 9.2118 0.3177 257.1311 256.8134 276.2464 10.0805 0.3256 257.2595 256.9339 276.1121 10.8368 0.3305 257.4077 257.0771 276.0115 11.6648 0.3347 257.5520 257.2173 275.8768 12.4620 0.3381 257.6537 257.3156 275.7749 13.2593 0.3436 257.7702 257.4267 275.6630 14.0863 0.3494 257.9003 257.5509 275.5560 14.8425 0.3542 258.0529 257.6988 275.4426 15.7115 0.3610 258.2423 257.8813 275.3302 16.4780 0.3667 258.3999 258.0332 275.2573 17.3060 0.3663 258.5733 258.2070 275.1710 18.0928 0.3695 258.7248 258.3553 275.1200 18.8995 0.3714 258.9018 258.5304 275.1245 19.7173 0.3778 259.0569 258.6791 275.1265 20.4838 0.3810 259.1909 258.8099 275.1672 21.3425 0.3848 259.3729 258.9881 275.2290 22.1090 0.3902 259.5026 259.1124 275.3455 22.9268 0.3932 259.6517 259.2585 275.5455 23.7233 0.3947 259.7677 259.3730 275.7564 24.5100 0.3977 259.9028 259.5051 276.0136 25.3073 0.3996 260.0774 259.6778 276.3292 26.1045 0.4052 260.2200 259.8148 276.6689 26.9223 0.4062 260.3689 259.9626 277.0390 27.6888 0.4082 260.5178 260.1096 277.4038 28.5473 0.4141 260.6867 260.2726 277.7950 29.3028 0.4163 260.8436 260.4273 278.1952 30.1308 0.4183 260.9687 260.5504 278.6601 30.9280 0.4207 261.1334 260.7128 279.0449 31.7150 0.4230 261.2608 260.8378 279.4302 32.5430 0.4307 261.4057 260.9750 279.8828 33.3095 0.4347 261.5570 261.1222 280.2596 34.1678 0.4294 261.7195 261.2901 280.6839 34.9338 0.4310 261.8479 261.4169 281.0418 35.7515 0.4340 261.9815 261.5475 281.3592 36.5590 0.4341 262.1063 261.6722 281.6509 37.3460 0.4371 262.2632 261.8261 281.9289 38.1735 0.4352 262.4254 261.9902 282.1598 38.9395 0.4353 262.5720 262.1367 282.3480 39.7983 0.4364 262.7322 262.2959 282.5038 40.5648 0.4356 262.8729 262.4372 282.6036 41.3825 0.4357 263.0532 262.6176 282.7285 42.1893 0.4390 263.2186 262.7796 282.8040 42.9760 0.4385 263.3906 262.9521 282.8553 43.8040 0.4377 263.5463 263.1085 282.8813 44.6013 0.4375 263.7209 263.2834 282.8705 45.4293 0.4397 263.8284 263.3887 282.8441 46.2265 0.4408 263.9626 263.5218 282.7876 47.0125 0.4388 264.0866 263.6477 282.7270 47.8508 0.4388 264.2425 263.8037 282.6402 48.6070 0.4394 264.3994 263.9601 282.5564 49.4658 0.4432 264.5410 264.0978 282.4457 50.2323 0.4440 264.6657 264.2217 282.3443 51.0603 0.4457 264.8601 264.4144 282.2196 51.8575 0.4497 265.0182 264.5685 282.1293 52.6445 0.4542 265.1968 264.7426 282.0215 53.4820 0.4530 265.3785 264.9255 281.9345 54.2483 0.4544 265.5131 265.0587 281.8452 55.0968 0.4576 265.6469 265.1892 281.7755 55.8633 0.4555 265.7862 265.3306 281.7082 56.6810 0.4561 265.9223 265.4662 281.6727 57.4470 0.4564 266.0392 265.5828 281.6590 58.2745 0.4558 266.1959 265.7401 281.6515 59.0615 0.4570 266.3281 265.8711 281.7118 59.8485 0.4587 266.4542 265.9955 281.7829 60.6868 0.4591 266.6176 266.1585 281.9017 61.4428 0.4611 266.7687 266.3076 282.0478 62.2905 0.4655 266.9047 266.4392 282.2543 63.0673 0.4688 267.0215 266.5528 282.4823 63.8850 0.4738 267.1889 266.7151 282.7055 64.6823 0.4742 267.3323 266.8581 282.9616 65.4795 0.4715 267.4808 267.0092 283.2611 66.2760 0.4731 267.6310 267.1579 283.5839 67.0730 0.4736 267.7612 267.2875 283.9216 67.8908 0.4714 267.8869 267.4155 284.3257 68.6675 0.4703 268.0353 267.5650 284.7000 69.5160 0.4695 268.2012 267.7317 285.1163 70.2825 0.4703 268.3418 267.8715 285.5220 71.1100 0.4660 268.4285 267.9625 285.9439 71.9068 0.4623 268.5582 268.0960 286.3245 72.7040 0.4638 268.6945 268.2308 286.7360 73.5218 0.4646 268.8756 268.4110 287.0795 74.2985 0.4642 269.0348 268.5706 287.4222 75.1465 0.4643 269.1712 268.7070 287.7761 75.8920 0.4626 269.3274 268.8648 287.9852 76.7405 0.4605 269.5071 269.0466 288.2265 77.5173 0.4567 269.6411 269.1844 288.4326 78.3350 0.4560 269.7750 269.3190 288.6718 79.1320 0.4512 269.9450 269.4938 288.7893 79.9285 0.4499 270.1023 269.6525 288.9098 80.7565 0.4468 270.2423 269.7956 289.0374 81.5230 0.4459 270.3706 269.9248 289.0997 82.3715 0.4451 270.5005 270.0554 289.1471 83.1483 0.4463 270.6242 270.1778 289.1716 83.9660 0.4465 270.7617 270.3151 289.1820 84.7623 0.4432 270.8999 270.4567 289.1658 85.5595 0.4391 271.0484 270.6092 289.1099 86.3875 0.4387 271.2029 270.7643 289.0433 87.1540 0.4389 271.3523 270.9134 288.9868 88.0025 0.4374 271.5165 271.0791 288.8852 88.7380 0.4368 271.6529 271.2161 288.8087 89.5858 0.4356 271.8147 271.3790 288.7102 90.3523 0.4354 271.9428 271.5074 288.5826 91.1803 0.4357 272.0591 271.6235 288.5132 91.9673 0.4379 272.1885 271.7507 288.4379 92.7645 0.4341 272.3461 271.9120 288.3596 93.5923 0.4305 272.4746 272.0441 288.3023 94.3580 0.4295 272.5930 272.1634 288.2493 95.2065 0.4321 272.7410 272.3089 288.2354 95.9833 0.4354 272.8993 272.4639 288.2204 96.8010 0.4329 273.0636 272.6307 288.2336 97.5983 0.4316 273.2083 272.7767 288.2516 98.3950 0.4333 273.3480 272.9147 288.3071 99.2225 0.4371 273.5005 273.0634 288.4151 99.9890 0.4373 273.6513 273.2140 288.5139 100.8068 0.4353 273.8036 273.3684 288.6785 101.5835 0.4367 273.9520 273.5153 288.8877 102.4320 0.4361 274.1116 273.6755 289.1841 103.1978 0.4367 274.2511 273.8144 289.4334 104.0255 0.4356 274.3960 273.9604 289.7100 104.8228 0.4315 274.5681 274.1366 290.0237 105.6200 0.4293 274.6994 274.2701 290.3596 106.4378 0.4284 274.8068 274.3784 290.7361 107.2140 0.4261 274.9248 274.4986 291.1040 108.0723 0.4242 275.0952 274.6710 291.4937 108.8080 0.4178 275.2553 274.8375 291.8288 109.6668 0.4171 275.3827 274.9656 292.2316 110.4333 0.4154 275.5302 275.1147 292.5986 111.2715 0.4116 275.6935 275.2819 292.9808 112.0583 0.4140 275.8404 275.4264 293.2921 112.8548 0.4107 275.9841 275.5734 293.5987 113.6828 0.4121 276.0902 275.6781 293.8980 114.4493 0.4122 276.2167 275.8045 294.1402 115.3080 0.4118 276.3696 275.9578 294.4064 116.0643 0.4087 276.5128 276.1041 294.5924 116.9018 0.4048 276.6243 276.2195 294.7872 117.6988 0.3994 276.7450 276.3457 294.9623 118.4960 0.3990 276.8930 276.4940 295.1103 119.3138 0.3977 277.0321 276.6344 295.2294 120.0803 0.3971 277.1915 276.7943 295.3415 120.9383 0.3990 277.3463 276.9473 295.3769 121.6943 0.3959 277.5119 277.1160 295.4076 122.5223 0.3949 277.6596 277.2647 295.4044 123.2888 0.3899 277.8275 277.4377 295.3797 124.1065 0.3849 277.9764 277.5914 295.3518 124.9035 0.3826 278.1293 277.7467 295.3026 125.7000 0.3812 278.3048 277.9236 295.2625 126.5178 0.3736 278.4934 278.1199 295.1993 127.2945 0.3729 278.6429 278.2700 295.1347 128.1430 0.3716 278.7943 278.4228 295.0761 128.9095 0.3681 278.9262 278.5581 294.9910 129.7373 0.3619 279.0585 278.6966 294.8910 130.5338 0.3602 279.2152 278.8550 294.8066 131.3310 0.3619 279.3537 278.9918 294.7275 132.1488 0.3592 279.4740 279.1148 294.6835 132.9255 0.3592 279.5704 279.2112 294.6886 133.7740 0.3581 279.7016 279.3435 294.6895 134.5405 0.3589 279.8518 279.4929 294.6944 135.3683 0.3612 280.0128 279.6516 294.7230 136.1648 0.3602 280.1552 279.7950 294.7549 136.9620 0.3588 280.3010 279.9422 294.8581 137.7798 0.3583 280.4579 280.0996 294.9636 138.5565 0.3573 280.6046 280.2473 295.0694 139.4050 0.3544 280.7838 280.4293 295.2421 140.1715 0.3562 280.9335 280.5773 295.4543 140.9988 0.3575 281.0860 280.7285 295.6609 141.7958 0.3598 281.2094 280.8495 295.8972 142.5930 0.3629 281.3506 280.9877 296.1748 143.4108 0.3596 281.4908 281.1312 296.5155 144.1875 0.3601 281.6129 281.2528 296.8476 145.0360 0.3614 281.7569 281.3954 297.1744 145.8018 0.3579 281.9255 281.5676 297.5268 146.6295 0.3543 282.0902 281.7359 297.8975 147.4370 0.3520 282.2495 281.8976 298.2682 148.2240 0.3515 282.3879 282.0364 298.6111 149.0520 0.3495 282.5519 282.2024 298.9832 149.8185 0.3439 282.6741 282.3303 299.3068 150.6768 0.3416 282.7851 282.4436 299.6677 151.4325 0.3400 282.8855 282.5455 299.9535 152.2605 0.3379 283.0328 282.6949 300.2618 153.0578 0.3373 283.1703 282.8330 300.5445 153.8448 0.3377 283.2962 282.9585 300.7636 154.6728 0.3360 283.4422 283.1062 300.9709 155.4393 0.3310 283.5863 283.2553 301.1698 156.2873 0.3287 283.7079 283.3792 301.3168 157.0225 0.3289 283.8350 283.5061 301.4068 157.8813 0.3268 284.0079 283.6811 301.5163 158.6478 0.3231 284.1544 283.8313 301.5682 159.4655 0.3210 284.3117 283.9907 301.6102 160.2730 0.3155 284.4703 284.1548 301.6106 161.0593 0.3085 284.6005 284.2920 301.6396 161.8870 0.3022 284.7496 284.4474 301.6575 162.6535 0.3020 284.8723 284.5703 301.6444 163.5020 0.3036 284.9981 284.6945 301.5868 164.2685 0.3025 285.1320 284.8294 301.5260 165.0963 0.2967 285.3000 285.0032 301.4339 165.8928 0.2956 285.4644 285.1689 301.3711 166.6900 0.2877 285.6191 285.3314 301.2994 167.5078 0.2887 285.7989 285.5102 301.2166 168.2843 0.2878 285.9506 285.6628 301.1570 169.1320 0.2892 286.1164 285.8271 301.0881 169.8985 0.2854 286.2863 286.0009 301.0579 170.7265 0.2837 286.4502 286.1665 301.0017 171.5238 0.2843 286.5876 286.3033 300.9889 172.3208 0.2844 286.7090 286.4246 300.9879 173.1173 0.2856 286.8267 286.5411 300.9885 173.9145 0.2886 286.9285 286.6399 301.0252 174.7425 0.2891 287.0730 286.7839 301.1100 175.5090 0.2863 287.1969 286.9106 301.2027 176.3675 0.2798 287.3490 287.0692 301.3216 177.1333 0.2769 287.4685 287.1915 301.4637 177.9613 0.2766 287.6230 287.3464 301.6332 178.7585 0.2780 287.7534 287.4754 301.8296 179.5558 0.2749 287.8957 287.6208 302.0552 180.3835 0.2733 288.0624 287.7891 302.3313 181.1493 0.2717 288.2187 287.9469 302.6572 182.0080 0.2671 288.3484 288.0813 302.9802 182.7643 0.2605 288.4806 288.2201 303.2965 183.6025 0.2578 288.6212 288.3635 303.6606 184.3680 0.2578 288.7674 288.5096 304.0026 185.1858 0.2558 288.8775 288.6217 304.3638 185.9830 0.2525 289.0090 288.7566 304.7109 186.7700 0.2490 289.1605 288.9115 305.1011 187.5975 0.2464 289.3431 289.0967 305.4758 188.3635 0.2439 289.4616 289.2177 305.7902 189.2120 0.2391 289.6094 289.3703 306.1131 189.9683 0.2360 289.7696 289.5337 306.3983 190.7963 0.2321 289.9084 289.6763 306.6920 191.5625 0.2291 290.0284 289.7993 306.9226 192.4205 0.2286 290.1627 289.9341 307.1837 193.1870 0.2222 290.3096 290.0874 307.3998 194.0150 0.2148 290.5069 290.2920 307.5886 194.7713 0.2124 290.6530 290.4406 307.6649 195.6095 0.2109 290.7977 290.5868 307.7506 196.3963 0.2084 290.9481 290.7397 307.8505 197.1928 0.2077 291.1169 290.9093 307.9364 198.0208 0.2045 291.2671 291.0626 307.9778 198.7873 0.1986 291.3976 291.1991 307.9977 199.6460 0.1935 291.5596 291.3661 307.9892 200.3918 0.1913 291.6900 291.4987 308.0053 201.2293 0.1892 291.8537 291.6644 307.9881 201.9855 0.1902 292.0073 291.8170 307.9398 202.8545 0.1884 292.1796 291.9912 307.8354 203.6108 0.1879 292.3280 292.1401 307.7552 204.4388 0.1853 292.4868 292.3015 307.6954 205.2353 0.1836 292.5847 292.4011 307.6233 206.0425 0.1838 292.7444 292.5606 307.5525 206.8603 0.1829 292.8698 292.6870 307.4778 207.6268 0.1794 293.0163 292.8368 307.4428 208.4855 0.1763 293.1659 292.9896 307.3698 209.2203 0.1766 293.3145 293.1379 307.3309 210.0790 0.1757 293.4658 293.2901 307.2814 210.8660 0.1773 293.6034 293.4261 307.2765 211.6735 0.1759 293.7007 293.5248 307.2980 212.4605 0.1767 293.8460 293.6694 307.3156 213.2573 0.1739 294.0148 293.8409 307.3783 214.0848 0.1733 294.1995 294.0262 307.4843 214.8615 0.1723 294.3240 294.1517 307.6435 215.7100 0.1683 294.4931 294.3249 307.8645 216.4663 0.1660 294.6277 294.4617 308.0752 217.3038 0.1674 294.8019 294.6345 308.3256 218.0905 0.1677 294.9412 294.7734 308.5790 218.8775 0.1685 295.0765 294.9080 308.8298 219.7055 0.1656 295.2162 295.0506 309.1306 220.4720 0.1581 295.3642 295.2061 309.4351 221.3205 0.1556 295.5127 295.3571 309.8277 222.0965 0.1537 295.6710 295.5173 310.1984 222.9140 0.1509 295.8397 295.6888 310.5615 223.7113 0.1499 295.9779 295.8280 310.9384 224.5085 0.1505 296.1081 295.9576 311.2866 225.3055 0.1515 296.2543 296.1028 311.6596 226.1020 0.1477 296.4000 296.2524 311.9629 226.9198 0.1480 296.5339 296.3859 312.2702 227.6965 0.1475 296.6440 296.4965 312.5406 228.5450 0.1478 296.7765 296.6286 312.8186 229.3108 0.1441 296.9204 296.7762 313.0866 230.1385 0.1409 297.0460 296.9051 313.3464 230.9358 0.1376 297.1760 297.0384 313.5579 231.7330 0.1323 297.3233 297.1910 313.7190 232.5508 0.1277 297.4976 297.3700 313.8874 233.3265 0.1230 297.6572 297.5342 314.0171 234.1750 0.1156 297.8132 297.6976 314.1100 234.9415 0.1155 297.9624 297.8469 314.1775 235.7695 0.1113 298.1116 298.0003 314.2281 236.5668 0.1078 298.2719 298.1641 314.2348 237.3640 0.0999 298.4297 298.3298 314.2399 238.1808 0.1023 298.5521 298.4498 314.2085 238.9575 0.1026 298.6764 298.5738 314.1701 239.8060 0.0969 298.7869 298.6900 314.1028 240.5828 0.0945 298.9274 298.8328 314.0500 241.3998 0.0912 299.0948 299.0037 313.9710 242.2070 0.0885 299.2242 299.1356 313.8951 242.9940 0.0833 299.4061 299.3227 313.8256 243.8220 0.0835 299.5711 299.4876 313.7445 244.5883 0.0840 299.7307 299.6468 313.6872 245.4465 0.0828 299.8928 299.8100 313.6332 246.2128 0.0778 300.0273 299.9495 313.5757 247.0305 0.0765 300.1585 300.0820 313.5137 247.8380 0.0762 300.3174 300.2413 313.5254 248.6250 0.0778 300.4907 300.4129 313.5403 249.4420 0.0786 300.6289 300.5503 313.6084 250.2185 0.0801 300.7798 300.6997 313.6703 251.0670 0.0778 300.9399 300.8621 313.7637 251.8233 0.0722 301.0703 300.9981 313.8658 252.6615 0.0708 301.2273 301.1565 313.9686 253.4478 0.0715 301.3455 301.2740 314.1432 254.2345 0.0706 301.4750 301.4044 314.3350 255.0728 0.0693 301.6143 301.5450 314.5922 255.8290 0.0676 301.7794 301.7118 314.8577 256.6878 0.0707 301.9505 301.8798 315.1855 257.4543 0.0696 302.0684 301.9989 315.4757 258.2710 0.0691 302.1927 302.1236 315.8052 259.0683 0.0682 302.3363 302.2681 316.0919 259.8655 0.0644 302.4653 302.4009 316.4207 260.6935 0.0578 302.6081 302.5503 316.7766 261.4600 0.0524 302.7506 302.6981 317.0890 262.2983 0.0495 302.9087 302.8592 317.4692 263.0638 0.0525 303.0696 303.0171 317.7948 263.9225 0.0515 303.2149 303.1634 318.1264 264.6890 0.0475 303.3694 303.3219 318.4211 265.5170 0.0446 303.5332 303.4887 318.7678 266.3040 0.0437 303.6511 303.6074 319.0293 267.1108 0.0379 303.7862 303.7484 319.2916 267.9283 0.0348 303.9349 303.9002 319.5202 268.6948 0.0348 304.0754 304.0407 319.6634 269.5535 0.0278 304.2441 304.2163 319.8422 270.3200 0.0239 304.4038 304.3799 319.9656 271.1480 0.0178 304.5382 304.5204 320.1111 271.9345 0.0173 304.6785 304.6613 320.1811 272.7415 0.0129 304.7925 304.7795 320.2178 273.5695 0.0168 304.9445 304.9277 320.2604 274.3360 0.0139 305.0868 305.0728 320.2737 275.1845 0.0092 305.2368 305.2276 320.2706 275.9613 0.0060 305.3846 305.3787 320.2814 276.7785 0.0041 305.5651 305.5610 320.2566 277.5753 0.0036 305.7517 305.7480 320.2350 278.3725 -0.0007 305.9195 305.9202 320.1946 279.1698 -0.0081 306.0688 306.0769 320.1197 279.9670 -0.0150 306.1912 306.2062 320.0158 280.7848 -0.0167 306.3156 306.3323 319.9476 281.5508 -0.0144 306.4756 306.4899 319.9261 282.4090 -0.0155 306.6496 306.6651 319.9127 283.1653 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424.7258 428.1083 427.0308 936.9208 -3.3484 424.8956 428.2440 427.1018 937.7383 -3.3206 425.0822 428.4028 427.1995 938.5048 -3.2965 425.2545 428.5510 427.3268 939.3635 -3.2691 425.4557 428.7248 427.5122 940.1300 -3.2469 425.6065 428.8534 427.7043 940.9580 -3.2238 425.7692 428.9930 427.9475 941.7440 -3.1983 425.9493 429.1476 428.2548 942.5515 -3.1701 426.1708 429.3409 428.5676 943.3693 -3.1474 426.3454 429.4929 428.9038 944.1358 -3.1268 426.5034 429.6302 429.2551 944.9945 -3.1049 426.7237 429.8286 429.6519 945.7610 -3.0853 426.9087 429.9940 430.0377 946.5890 -3.0655 427.0415 430.1070 430.4602 947.3860 -3.0438 427.1826 430.2264 430.8102 948.1825 -3.0254 427.3629 430.3883 431.1726 949.0105 -3.0102 427.5787 430.5889 431.5687 949.7770 -2.9921 427.7537 430.7457 431.9299 950.6255 -2.9712 427.9527 430.9239 432.2786 951.3715 -2.9572 428.1265 431.0838 432.5874 952.2190 -2.9450 428.3233 431.2682 432.8980 953.0163 -2.9312 428.5270 431.4582 433.1418 953.8135 -2.9181 428.7092 431.6273 433.3411 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