DTA measure 1pb_updown4 Date: 2025326:1028 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.92 s Mass = 937.3 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4955 0.9317 206.2061 205.2743 206.9839 4.0945 0.9375 206.1978 205.2603 206.9225 5.6934 0.9322 206.1947 205.2626 206.8696 7.3071 0.9312 206.2043 205.2731 206.7767 8.9058 0.9361 206.2175 205.2814 206.7212 10.5350 0.9331 206.2037 205.2706 206.6760 12.1339 0.9324 206.2139 205.2814 206.6187 13.7338 0.9330 206.2062 205.2732 206.5763 15.3315 0.9338 206.2206 205.2869 206.5648 16.9390 0.9336 206.2265 205.2929 206.5593 18.5451 0.9400 206.2405 205.3005 206.5640 20.1511 0.9402 206.2321 205.2919 206.5690 21.7420 0.9465 206.2350 205.2885 206.6082 23.3341 0.9384 206.2421 205.3037 206.6492 24.9418 0.9446 206.2389 205.2943 206.7313 26.5633 0.9493 206.2459 205.2966 206.8216 28.1559 0.9518 206.2366 205.2848 206.9130 29.7625 0.9513 206.2448 205.2935 207.0203 31.3571 0.9519 206.2471 205.2952 207.1566 32.9548 0.9495 206.2481 205.2986 207.3141 34.5689 0.9479 206.2517 205.3038 207.4681 36.1826 0.9476 206.2776 205.3300 207.6620 37.7816 0.9458 206.2918 205.3461 207.8561 39.3806 0.9428 206.3068 205.3640 208.0580 40.9796 0.9398 206.2982 205.3584 208.2767 42.6085 0.9355 206.2836 205.3481 208.5073 44.2075 0.9258 206.3159 205.3902 208.7443 45.8215 0.9229 206.3377 205.4148 208.9853 47.4205 0.9227 206.3406 205.4179 209.2189 49.0195 0.9178 206.3534 205.4356 209.4714 50.6485 0.9112 206.3594 205.4483 209.7378 52.2625 0.9074 206.3676 205.4602 209.9770 53.8615 0.9071 206.3938 205.4867 210.2582 55.4605 0.9006 206.4078 205.5072 210.4973 57.0743 0.8970 206.4190 205.5220 210.7761 58.6816 0.8945 206.4339 205.5393 211.0637 60.3100 0.8901 206.4578 205.5677 211.3286 61.9098 0.8866 206.4942 205.6076 211.5913 63.5088 0.8815 206.4974 205.6160 211.8529 65.1228 0.8810 206.5270 205.6459 212.1140 66.7369 0.8846 206.5579 205.6733 212.3565 68.3508 0.8846 206.5941 205.7095 212.5936 69.9496 0.8837 206.6023 205.7187 212.8386 71.5636 0.8786 206.6409 205.7623 213.0959 73.1626 0.8757 206.6740 205.7983 213.3169 74.7924 0.8637 206.6973 205.8336 213.5707 76.3915 0.8689 206.7515 205.8826 213.7879 78.0058 0.8603 206.7956 205.9353 213.9906 79.6046 0.8482 206.8112 205.9629 214.1981 81.1969 0.8448 206.8304 205.9857 214.4114 82.8029 0.8412 206.8880 206.0468 214.6159 84.4090 0.8399 206.9116 206.0717 214.7998 86.0004 0.8347 206.9441 206.1094 214.9962 87.6080 0.8281 206.9962 206.1680 215.1835 89.1990 0.8261 207.0321 206.2059 215.3553 90.8064 0.8239 207.0817 206.2577 215.5062 92.4146 0.8181 207.1303 206.3122 215.7101 94.0224 0.8137 207.1593 206.3455 215.8816 95.6174 0.8096 207.2068 206.3972 216.0414 97.2136 0.7849 207.2594 206.4745 216.2162 98.8403 0.7848 207.3194 206.5345 216.4065 100.4385 0.7980 207.3491 206.5512 216.5601 102.0374 0.7957 207.4044 206.6087 216.7506 103.6363 0.7947 207.4545 206.6598 216.9107 105.2500 0.7934 207.5148 206.7214 217.0890 106.8488 0.7920 207.5523 206.7602 217.2618 108.4629 0.7818 207.6336 206.8517 217.4574 110.0769 0.7806 207.6683 206.8877 217.6160 111.6758 0.7729 207.7339 206.9610 217.8038 113.2748 0.7700 207.8046 207.0345 217.9981 114.8738 0.7699 207.8451 207.0752 218.1749 116.5028 0.7657 207.8996 207.1339 218.3655 118.1019 0.7599 207.9574 207.1975 218.5664 119.7156 0.7618 208.0155 207.2537 218.7666 121.3146 0.7358 208.0595 207.3237 218.9602 122.9135 0.7489 208.1455 207.3966 219.1629 124.5425 0.7479 208.2159 207.4680 219.3595 126.1415 0.7517 208.2888 207.5371 219.5711 127.7405 0.7507 208.3587 207.6081 219.7815 129.3545 0.7494 208.4186 207.6692 219.9903 130.9535 0.7525 208.4874 207.7350 220.1788 132.5675 0.7520 208.5473 207.7952 220.3836 134.1815 0.7499 208.6258 207.8759 220.5775 135.7953 0.7509 208.7001 207.9492 220.7772 137.3941 0.7451 208.7667 208.0216 220.9833 138.9938 0.7427 208.8506 208.1079 221.1846 140.6250 0.7429 208.9230 208.1801 221.3857 142.2269 0.7379 208.9944 208.2565 221.5921 143.8268 0.7353 209.0630 208.3277 221.8105 145.4360 0.7335 209.1621 208.4285 222.0404 147.0270 0.7308 209.2279 208.4971 222.2429 148.6331 0.7256 209.3242 208.5986 222.4622 150.2391 0.7215 209.3989 208.6774 222.6766 151.8464 0.7217 209.4680 208.7463 222.8950 153.4384 0.7225 209.5703 208.8478 223.1086 155.0308 0.7170 209.6343 208.9173 223.3348 156.6681 0.7135 209.7247 209.0111 223.5523 158.2618 0.7022 209.8039 209.1017 223.7717 159.8558 0.6971 209.8886 209.1915 224.0051 161.4639 0.6908 209.9695 209.2787 224.2177 163.0615 0.6847 210.0760 209.3913 224.4225 164.6895 0.6817 210.1647 209.4830 224.6433 166.2876 0.6777 210.2411 209.5634 224.8750 167.8865 0.6750 210.3382 209.6632 225.0676 169.4855 0.6743 210.4369 209.7626 225.2762 171.0995 0.6723 210.5178 209.8455 225.4847 172.7135 0.6712 210.6294 209.9583 225.6967 174.3275 0.6695 210.7215 210.0520 225.9015 175.9265 0.6630 210.8302 210.1673 226.1031 177.5255 0.6628 210.8959 210.2331 226.3138 179.1395 0.6616 211.0091 210.3475 226.5164 180.7535 0.6601 211.1195 210.4594 226.7204 182.3675 0.6626 211.2105 210.5479 226.9261 183.9664 0.6564 211.3252 210.6688 227.1202 185.5650 0.6519 211.4179 210.7660 227.3356 187.1790 0.6535 211.5301 210.8765 227.5393 188.7929 0.6524 211.6460 210.9936 227.7166 190.3919 0.6486 211.7480 211.0993 227.9351 192.0058 0.6489 211.8422 211.1934 228.1465 193.6048 0.6453 211.9520 211.3067 228.3258 195.2038 0.6431 212.0825 211.4393 228.5137 196.8335 0.6407 212.1704 211.5298 228.7128 198.4328 0.6397 212.2774 211.6377 228.8854 200.0326 0.6383 212.4038 211.7655 229.0753 201.6468 0.6373 212.5189 211.8815 229.2755 203.2455 0.6355 212.6240 211.9885 229.4699 204.8745 0.6355 212.7378 212.1023 229.6662 206.4735 0.6350 212.8627 212.2277 229.8377 208.0724 0.6360 212.9752 212.3391 230.0534 209.6809 0.6362 213.0936 212.4574 230.2258 211.2718 0.6345 213.2053 212.5708 230.4181 212.8655 0.6326 213.3261 212.6935 230.6137 214.4888 0.6335 213.4481 212.8146 230.8229 216.0811 0.6331 213.5695 212.9364 231.0205 217.6734 0.6288 213.6918 213.0630 231.2222 219.2805 0.6256 213.8068 213.1812 231.4479 220.8744 0.6245 213.9397 213.3152 231.6425 222.4976 0.6243 214.0527 213.4284 231.8699 224.0913 0.6261 214.1863 213.5602 232.1000 225.7015 0.6230 214.2885 213.6655 232.2972 227.2969 0.6183 214.3988 213.7805 232.4877 228.8955 0.6153 214.5533 213.9379 232.7070 230.5241 0.6131 214.6771 214.0640 232.9325 232.1234 0.6110 214.8041 214.1931 233.1537 233.7261 0.6109 214.9292 214.3183 233.3624 235.3248 0.6067 215.0454 214.4387 233.5793 236.9238 0.6041 215.1729 214.5688 233.7682 238.5529 0.6040 215.3120 214.7080 234.0052 240.1519 0.6021 215.4382 214.8361 234.1993 241.7658 0.6018 215.5755 214.9737 234.4282 243.3648 0.6026 215.7038 215.1012 234.6273 244.9638 0.5983 215.8362 215.2379 234.8343 246.5928 0.5944 215.9631 215.3687 235.0437 248.2068 0.5938 216.0996 215.5057 235.2493 249.8056 0.5925 216.2443 215.6518 235.4398 251.4046 0.5925 216.3704 215.7779 235.6486 253.0185 0.5893 216.5116 215.9223 235.8483 254.6475 0.5841 216.6506 216.0665 236.0626 256.2465 0.5827 216.8008 216.2180 236.2783 257.8455 0.5789 216.9338 216.3549 236.4696 259.4595 0.5776 217.0853 216.5076 236.6665 261.0735 0.5781 217.2227 216.6445 236.8616 262.6874 0.5774 217.3602 216.7827 237.0646 264.2861 0.5782 217.4923 216.9141 237.2608 265.8998 0.5768 217.6304 217.0536 237.4515 267.4988 0.5755 217.7790 217.2035 237.6666 269.1279 0.5795 217.9119 217.3323 237.8351 270.7420 0.5848 218.0679 217.4831 238.0483 272.3413 0.5751 218.2101 217.6351 238.2432 273.9340 0.5700 218.3536 217.7835 238.4316 275.5258 0.5685 218.4909 217.9224 238.6409 277.1471 0.5688 218.6388 218.0700 238.8646 278.7383 0.5661 218.7846 218.2185 239.0484 280.3301 0.5609 218.9340 218.3731 239.2683 281.9366 0.5583 219.0965 218.5382 239.4878 283.5331 0.5574 219.2364 218.6789 239.6824 285.1421 0.5540 219.4004 218.8464 239.9057 286.7346 0.5506 219.5382 218.9875 240.1093 288.3585 0.5500 219.6805 219.1305 240.3218 289.9544 0.5463 219.8344 219.2880 240.5452 291.5518 0.5448 219.9973 219.4525 240.7646 293.1499 0.5417 220.1386 219.5969 240.9814 294.7486 0.5463 220.2857 219.7394 241.2150 296.3775 0.5451 220.4367 219.8916 241.4485 297.9766 0.5434 220.5988 220.0555 241.6585 299.5755 0.5375 220.7574 220.2199 241.8674 301.1745 0.5352 220.9156 220.3804 242.0821 302.7885 0.5343 221.0809 220.5466 242.3198 304.3875 0.5335 221.2209 220.6874 242.5296 306.0015 0.5310 221.3905 220.8594 242.7388 307.6155 0.5288 221.5500 221.0212 242.9702 309.2145 0.5258 221.7076 221.1818 243.1953 310.8144 0.5232 221.8661 221.3429 243.4000 312.4145 0.5181 222.0342 221.5160 243.6288 314.0443 0.5147 222.1922 221.6774 243.8512 315.6429 0.5153 222.3518 221.8365 244.0714 317.2568 0.5114 222.5019 221.9905 244.2593 318.8558 0.5039 222.6835 222.1796 244.4821 320.4548 0.5023 222.8353 222.3330 244.6895 322.0839 0.4998 222.9929 222.4931 244.9181 323.6828 0.4935 223.1409 222.6473 245.1089 325.2849 0.4922 223.3093 222.8172 245.3168 326.8956 0.4892 223.4982 223.0090 245.5198 328.5100 0.4886 223.6471 223.1585 245.7373 330.1108 0.4837 223.8095 223.3258 245.9375 331.7255 0.4831 223.9832 223.5001 246.1569 333.3395 0.4806 224.1412 223.6605 246.3648 334.9386 0.4777 224.3155 223.8378 246.5647 336.5526 0.4757 224.4717 223.9960 246.7693 338.1446 0.4769 224.6555 224.1786 246.9770 339.7359 0.4777 224.8240 224.3463 247.1665 341.3564 0.4708 224.9982 224.5274 247.3642 342.9480 0.4692 225.1649 224.6957 247.5729 344.5540 0.4647 225.3368 224.8720 247.7818 346.1450 0.4627 225.4924 225.0296 247.9572 347.7668 0.4600 225.6702 225.2102 248.1702 349.3749 0.4569 225.8537 225.3968 248.3535 350.9676 0.4532 226.0163 225.5631 248.5482 352.5754 0.4501 226.1782 225.7280 248.7532 354.1696 0.4469 226.3612 225.9143 248.9532 355.7845 0.4455 226.5194 226.0739 249.1460 357.4005 0.4434 226.7096 226.2662 249.3533 358.9991 0.4373 226.8690 226.4318 249.5437 360.5979 0.4362 227.0295 226.5933 249.7710 362.2118 0.4337 227.2159 226.7822 249.9343 363.8259 0.4304 227.3905 226.9601 250.1240 365.4399 0.4310 227.5680 227.1371 250.3227 367.0388 0.4281 227.7420 227.3139 250.5211 368.6378 0.4231 227.9164 227.4933 250.7146 370.2518 0.4213 228.0922 227.6709 250.9069 371.8809 0.4180 228.2773 227.8593 251.1177 373.4798 0.4146 228.4464 228.0318 251.3363 375.0788 0.4120 228.6290 228.2170 251.5357 376.6926 0.4107 228.8225 228.4117 251.7524 378.3066 0.4083 228.9934 228.5851 251.9703 379.9206 0.4068 229.1703 228.7635 252.1648 381.5195 0.4011 229.3567 228.9556 252.4055 383.1335 0.4034 229.5244 229.1210 252.6364 384.7325 0.3976 229.7114 229.3139 252.8492 386.3615 0.3957 229.8955 229.4998 253.0766 387.9605 0.3925 230.0689 229.6763 253.2965 389.5743 0.3904 230.2500 229.8596 253.5131 391.1730 0.3847 230.4301 230.0454 253.7524 392.7719 0.3836 230.6107 230.2271 253.9733 394.4016 0.3827 230.7914 230.4087 254.1736 396.0018 0.3793 230.9792 230.5998 254.4132 397.6158 0.3751 231.1888 230.8138 254.6358 399.2148 0.3731 231.3602 230.9871 254.8630 400.8141 0.3706 231.5316 231.1610 255.0801 402.4240 0.3683 231.7187 231.3504 255.3067 404.0303 0.3641 231.8986 231.5345 255.5075 405.6224 0.3638 232.0817 231.7179 255.7465 407.2290 0.3606 232.2585 231.8979 255.9751 408.8211 0.3560 232.4596 232.1037 256.1871 410.4298 0.3502 232.6261 232.2759 256.4033 412.0371 0.3506 232.8063 232.4557 256.6286 413.6449 0.3497 233.0004 232.6507 256.8580 415.2400 0.3418 233.1954 232.8536 257.0673 416.8486 0.3395 233.3807 233.0411 257.2835 418.4604 0.3359 233.5690 233.2331 257.4819 420.0738 0.3325 233.7588 233.4263 257.6534 421.6726 0.3332 233.9609 233.6278 257.8565 423.2716 0.3288 234.1361 233.8073 258.0576 424.8708 0.3258 234.3219 233.9961 258.2483 426.4999 0.3244 234.5232 234.1988 258.4215 428.0995 0.3241 234.7256 234.4014 258.5957 429.6985 0.3203 234.9143 234.5940 258.7944 431.3125 0.3182 235.1025 234.7843 258.9732 432.9115 0.3167 235.2766 234.9599 259.1395 434.5255 0.3149 235.4805 235.1656 259.3282 436.1395 0.3111 235.6591 235.3480 259.5272 437.7535 0.3146 235.8532 235.5386 259.7126 439.3524 0.3103 236.0401 235.7298 259.8900 440.9509 0.3042 236.2288 235.9246 260.0862 442.5801 0.2998 236.4219 236.1221 260.2859 444.1789 0.2983 236.6208 236.3225 260.4636 445.7928 0.2979 236.7931 236.4952 260.6827 447.3918 0.2930 236.9907 236.6978 260.8778 449.0058 0.2911 237.1996 236.9085 261.0550 450.6199 0.2920 237.3768 237.0848 261.2451 452.2338 0.2826 237.5846 237.3020 261.4487 453.8329 0.2787 237.7679 237.4892 261.6675 455.4476 0.2782 237.9637 237.6855 261.8591 457.0466 0.2770 238.1407 237.8637 262.0961 458.6764 0.2723 238.3508 238.0785 262.3378 460.2755 0.2726 238.5428 238.2702 262.5369 461.8899 0.2707 238.7229 238.4522 262.7559 463.4900 0.2670 238.9193 238.6522 262.9963 465.1050 0.2625 239.1364 238.8739 263.2268 466.7148 0.2626 239.3096 239.0470 263.4603 468.3063 0.2586 239.5095 239.2509 263.6875 469.9133 0.2553 239.6937 239.4384 263.9207 471.5068 0.2521 239.9064 239.6543 264.1426 473.1146 0.2530 240.0879 239.8349 264.3754 474.7210 0.2486 240.2945 240.0459 264.6067 476.3281 0.2435 240.4975 240.2540 264.8351 477.9211 0.2394 240.6709 240.4315 265.0857 479.5301 0.2312 240.8664 240.6352 265.2879 481.1420 0.2275 241.0755 240.8480 265.5138 482.7535 0.2276 241.2661 241.0385 265.7528 484.3506 0.2250 241.4626 241.2376 265.9687 485.9490 0.2195 241.6723 241.4528 266.1797 487.5630 0.2161 241.8706 241.6545 266.3737 489.1770 0.2140 242.0701 241.8561 266.5762 490.7909 0.2117 242.2567 242.0450 266.7818 492.3900 0.2095 242.4571 242.2475 266.9806 493.9888 0.2073 242.6655 242.4582 267.1693 495.6028 0.2009 242.8572 242.6563 267.3631 497.2169 0.1988 243.0535 242.8547 267.5627 498.8308 0.1984 243.2565 243.0580 267.7533 500.4298 0.1949 243.4413 243.2464 267.9209 502.0436 0.1940 243.6620 243.4679 268.1069 503.6426 0.1871 243.8484 243.6613 268.2874 505.2716 0.1853 244.0576 243.8723 268.4824 506.8706 0.1873 244.2489 244.0616 268.6809 508.4846 0.1781 244.4602 244.2821 268.8937 510.0835 0.1747 244.6573 244.4825 269.0789 511.7125 0.1758 244.8546 244.6788 269.2850 513.3115 0.1702 245.0569 244.8867 269.4966 514.9255 0.1632 245.2619 245.0987 269.6987 516.5245 0.1620 245.4556 245.2936 269.9186 518.1385 0.1569 245.6575 245.5006 270.1318 519.7523 0.1558 245.8552 245.6994 270.3541 521.3659 0.1493 246.0710 245.9217 270.5488 522.9648 0.1493 246.2548 246.1055 270.7591 524.5788 0.1455 246.4517 246.3062 270.9859 526.1929 0.1447 246.6672 246.5224 271.1961 527.8069 0.1390 246.8676 246.7286 271.4099 529.4211 0.1399 247.0708 246.9308 271.6295 531.0140 0.1345 247.2813 247.1468 271.8404 532.6050 0.1349 247.4906 247.3557 272.0737 534.2268 0.1295 247.6946 247.5651 272.2936 535.8181 0.1255 247.8990 247.7735 272.5242 537.4254 0.1210 248.0873 247.9663 272.7293 539.0191 0.1171 248.2889 248.1718 272.9342 540.6261 0.1142 248.4845 248.3703 273.1590 542.2485 0.1101 248.7005 248.5904 273.3813 543.8426 0.1064 248.8852 248.7787 273.5885 545.4508 0.1020 249.0881 248.9861 273.8002 547.0486 0.0956 249.2931 249.1974 274.0101 548.6618 0.0912 249.5145 249.4233 274.2242 550.2756 0.0874 249.7045 249.6171 274.4317 551.8746 0.0847 249.9262 249.8415 274.6517 553.4735 0.0805 250.1241 250.0436 274.8536 555.0875 0.0768 250.3265 250.2497 275.0615 556.6865 0.0744 250.5233 250.4489 275.2585 558.3155 0.0721 250.7218 250.6497 275.4742 559.9145 0.0662 250.9392 250.8729 275.6853 561.5135 0.0646 251.1378 251.0733 275.8981 563.1275 0.0632 251.3572 251.2940 276.0835 564.7265 0.0583 251.5506 251.4922 276.2965 566.3555 0.0550 251.7533 251.6983 276.5014 567.9540 0.0522 251.9760 251.9239 276.7260 569.5678 0.0475 252.1756 252.1281 276.9197 571.1700 0.0447 252.3682 252.3235 277.1234 572.7698 0.0408 252.5802 252.5394 277.3228 574.3990 0.0373 252.7996 252.7623 277.5153 575.9976 0.0346 253.0028 252.9682 277.7118 577.5968 0.0271 253.1839 253.1568 277.9126 579.2108 0.0314 253.4211 253.3896 278.1290 580.8246 0.0281 253.5982 253.5701 278.3284 582.4388 0.0317 253.8305 253.7989 278.4997 584.0375 0.0319 254.0321 254.0002 278.6921 585.6515 0.0298 254.2321 254.2023 278.8924 587.2510 0.0245 254.4472 254.4227 279.1069 588.8805 0.0174 254.6520 254.6346 279.3088 590.4795 0.0080 254.8778 254.8697 279.5210 592.0935 0.0042 255.0688 255.0646 279.7417 593.6911 -0.0049 255.2860 255.2908 279.9594 595.2829 -0.0094 255.4993 255.5087 280.1870 596.9048 -0.0085 255.6899 255.6985 280.4190 598.4965 -0.0119 255.8856 255.8975 280.6608 600.1040 -0.0180 256.1214 256.1394 280.8764 601.6955 -0.0175 256.3206 256.3381 281.0997 603.3026 -0.0243 256.5250 256.5493 281.3332 604.9111 -0.0282 256.7273 256.7555 281.5780 606.5198 -0.0336 256.9398 256.9733 281.7970 608.1133 -0.0355 257.1482 257.1837 282.0319 609.7108 -0.0425 257.3407 257.3832 282.2681 611.3223 -0.0471 257.5621 257.6092 282.4883 612.9353 -0.0504 257.7881 257.8385 282.7196 614.5483 -0.0563 257.9740 258.0303 282.9408 616.1473 -0.0615 258.1864 258.2479 283.1446 617.7459 -0.0633 258.4199 258.4832 283.3418 619.3598 -0.0667 258.6132 258.6799 283.5619 620.9739 -0.0724 258.8295 258.9020 283.7566 622.5729 -0.0746 259.0289 259.1035 283.9728 624.1868 -0.0767 259.2286 259.3053 284.1654 625.7858 -0.0843 259.4525 259.5368 284.3485 627.3848 -0.0850 259.6719 259.7569 284.5515 629.0138 -0.0846 259.8713 259.9559 284.7450 630.6278 -0.0896 260.0708 260.1604 284.9254 632.2311 -0.0924 260.2960 260.3883 285.1039 633.8346 -0.0937 260.4998 260.5935 285.2946 635.4336 -0.0993 260.7140 260.8134 285.4983 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