DTA measure 2pb_updown3 Date: 2025326:96 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.36 s Mass = 937.3 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1338 0.2137 203.1068 202.8931 260.4987 1.9523 0.2148 203.3643 203.1495 260.5050 2.7123 0.2174 203.5844 203.3670 260.5004 3.5630 0.2221 203.8433 203.6212 260.5111 4.3543 0.2195 204.1176 203.8982 260.5422 5.1455 0.2260 204.3625 204.1365 260.5455 5.9680 0.2341 204.6043 204.3702 260.5747 6.7298 0.2353 204.8239 204.5886 260.6147 7.5820 0.2393 205.0783 204.8389 260.6385 8.3438 0.2421 205.3194 205.0773 260.6598 9.1658 0.2421 205.5998 205.3577 260.7159 9.9578 0.2434 205.8309 205.5876 260.7609 10.7495 0.2489 206.0616 205.8127 260.8276 11.6018 0.2525 206.3302 206.0778 260.9127 12.3635 0.2576 206.5604 206.3028 260.9719 13.1858 0.2603 206.7945 206.5341 261.0547 13.9778 0.2601 207.0381 206.7780 261.1365 14.7695 0.2589 207.2729 207.0140 261.2357 15.6218 0.2618 207.5243 207.2626 261.3674 16.3835 0.2642 207.7672 207.5030 261.4426 17.2058 0.2647 208.0128 207.7482 261.5253 17.9975 0.2636 208.2400 207.9765 261.6401 18.7895 0.2659 208.4736 208.2076 261.7831 19.6423 0.2664 208.7204 208.4540 261.9220 20.4045 0.2692 208.9472 208.6779 262.0435 21.2265 0.2721 209.2004 208.9283 262.1773 22.0185 0.2792 209.4351 209.1559 262.2964 22.8105 0.2779 209.6683 209.3904 262.4481 23.6325 0.2782 209.9012 209.6230 262.6000 24.4245 0.2759 210.1325 209.8566 262.7741 25.2465 0.2719 210.3741 210.1022 262.9441 26.0385 0.2730 210.5998 210.3268 263.1158 26.8285 0.2730 210.8208 210.5477 263.2686 27.6468 0.2763 211.0768 210.8005 263.4523 28.4350 0.2779 211.3066 211.0287 263.6294 29.2538 0.2750 211.5089 211.2339 263.8147 30.0420 0.2764 211.7398 211.4634 263.9834 30.8300 0.2759 211.9851 211.7091 264.1736 31.6780 0.2751 212.2281 211.9530 264.3627 32.4365 0.2738 212.4393 212.1654 264.5362 33.2558 0.2802 212.6496 212.3695 264.7049 34.0445 0.2778 212.8754 212.5975 264.9086 34.8350 0.2766 213.1391 212.8625 265.0949 35.6865 0.2725 213.3953 213.1228 265.2808 36.4485 0.2687 213.5922 213.3235 265.4784 37.2705 0.2649 213.8204 213.5554 265.6840 38.0625 0.2658 214.0543 213.7884 265.8682 38.8545 0.2674 214.2587 213.9914 266.0567 39.7068 0.2656 214.4989 214.2333 266.2384 40.4685 0.2635 214.7429 214.4794 266.4233 41.2908 0.2641 214.9640 214.7000 266.6128 42.0825 0.2601 215.1860 214.9259 266.7945 42.8745 0.2583 215.3936 215.1353 266.9707 43.7265 0.2571 215.6096 215.3525 267.1503 44.4885 0.2571 215.8304 215.5734 267.3250 45.3105 0.2594 216.0610 215.8016 267.4952 46.1025 0.2568 216.2830 216.0262 267.6547 46.8945 0.2541 216.4964 216.2422 267.8223 47.7465 0.2533 216.7333 216.4800 268.0003 48.5085 0.2511 216.9391 216.6879 268.1516 49.3305 0.2461 217.1670 216.9209 268.3154 50.1525 0.2471 217.4054 217.1584 268.4666 50.9145 0.2464 217.6194 217.3731 268.6056 51.7665 0.2455 217.8485 217.6031 268.7838 52.5285 0.2441 218.0662 217.8221 268.9395 53.3505 0.2415 218.2765 218.0350 269.0953 54.1725 0.2394 218.5105 218.2711 269.2392 54.9343 0.2345 218.7224 218.4880 269.3817 55.7865 0.2346 218.9623 218.7277 269.5215 56.5783 0.2347 219.1682 218.9335 269.6516 57.3698 0.2304 219.3813 219.1509 269.7842 58.1923 0.2308 219.6092 219.3784 269.9099 58.9838 0.2258 219.8200 219.5942 270.0539 59.8045 0.2246 220.0451 219.8206 270.1944 60.5923 0.2255 220.2760 220.0505 270.3165 61.3803 0.2257 220.4792 220.2535 270.4162 62.1993 0.2215 220.7279 220.5064 270.5640 62.9875 0.2176 220.9158 220.6982 270.6833 63.8068 0.2180 221.1244 220.9064 270.7812 64.5953 0.2147 221.3579 221.1432 270.8985 65.3850 0.2125 221.5508 221.3383 271.0240 66.2338 0.2111 221.8025 221.5914 271.1427 66.9933 0.2104 221.9964 221.7860 271.2240 67.8145 0.2125 222.1992 221.9866 271.3601 68.6058 0.2104 222.4066 222.1962 271.4701 69.3975 0.2034 222.6050 222.4016 271.5939 70.2495 0.2057 222.8417 222.6360 271.7066 71.0115 0.2020 223.0386 222.8366 271.7805 71.8335 0.2021 223.2641 223.0620 271.8890 72.6255 0.1971 223.4861 223.2890 272.0106 73.4175 0.1926 223.6937 223.5010 272.1269 74.2695 0.1940 223.9268 223.7328 272.2411 75.0315 0.1898 224.1253 223.9354 272.3431 75.8535 0.1838 224.3383 224.1546 272.4712 76.6455 0.1844 224.5212 224.3368 272.5666 77.4375 0.1844 224.7274 224.5430 272.6681 78.2895 0.1853 224.9799 224.7946 272.7898 79.0513 0.1846 225.1676 224.9830 272.9028 79.8728 0.1809 225.3639 225.1830 273.0052 80.6673 0.1797 225.5670 225.3873 273.1282 81.4608 0.1771 225.7700 225.5929 273.2784 82.3135 0.1726 225.9843 225.8117 273.3815 83.0758 0.1741 226.1830 226.0089 273.4989 83.8978 0.1785 226.3820 226.2035 273.6084 84.6900 0.1792 226.6057 226.4265 273.7299 85.4815 0.1746 226.8058 226.6312 273.8424 86.3345 0.1709 227.0298 226.8589 274.0064 87.0968 0.1697 227.2135 227.0438 274.0986 87.9188 0.1675 227.4434 227.2758 274.2314 88.7110 0.1649 227.6429 227.4779 274.3761 89.5025 0.1632 227.8528 227.6897 274.5001 90.3555 0.1598 228.0533 227.8935 274.6422 91.1175 0.1581 228.2453 228.0872 274.7607 91.9360 0.1557 228.4504 228.2947 274.8884 92.7238 0.1530 228.6434 228.4904 275.0189 93.5110 0.1563 228.8371 228.6808 275.1402 94.3293 0.1583 229.0394 228.8811 275.2799 95.0870 0.1555 229.2506 229.0951 275.4182 95.9350 0.1531 229.4682 229.3151 275.5750 96.7233 0.1503 229.6705 229.5202 275.7231 97.5120 0.1471 229.8656 229.7185 275.8357 98.3303 0.1439 230.0669 229.9231 275.9832 99.0880 0.1456 230.2383 230.0928 276.1115 99.9370 0.1435 230.4716 230.3281 276.2621 100.7255 0.1429 230.6642 230.5213 276.3952 101.5155 0.1388 230.8561 230.7173 276.5495 102.3380 0.1377 231.0750 230.9373 276.6974 103.0995 0.1315 231.2737 231.1423 276.8147 103.9520 0.1319 231.4685 231.3366 276.9696 104.7138 0.1301 231.6476 231.5175 277.1248 105.5358 0.1318 231.8454 231.7137 277.2768 106.3283 0.1280 232.0585 231.9306 277.4132 107.1205 0.1290 232.2302 232.1012 277.5603 107.9430 0.1266 232.4518 232.3252 277.7157 108.7348 0.1198 232.6545 232.5347 277.8519 109.5568 0.1166 232.8473 232.7307 277.9937 110.3490 0.1105 233.0400 232.9295 278.1314 111.1405 0.1094 233.2287 233.1194 278.2788 111.9630 0.1064 233.4233 233.3169 278.4327 112.7245 0.1008 233.6081 233.5072 278.5794 113.5770 0.0997 233.8271 233.7273 278.7259 114.3690 0.0984 234.0285 233.9301 278.8704 115.1605 0.0934 234.2017 234.1083 278.9911 115.9830 0.0934 234.4113 234.3179 279.1461 116.7445 0.0886 234.5837 234.4951 279.2911 117.5970 0.0870 234.7842 234.6972 279.4411 118.3888 0.0854 234.9864 234.9010 279.5879 119.1805 0.0807 235.1904 235.1098 279.7408 120.0030 0.0782 235.3786 235.3005 279.8909 120.7655 0.0717 235.5704 235.4987 280.0229 121.6175 0.0720 235.7788 235.7068 280.1651 122.4098 0.0732 235.9616 235.8885 280.3256 123.2025 0.0692 236.1519 236.0827 280.4608 124.0228 0.0657 236.3477 236.2820 280.6077 124.7835 0.0608 236.5186 236.4578 280.7389 125.6343 0.0571 236.7444 236.6874 280.8812 126.4250 0.0539 236.9139 236.8599 281.0125 127.2155 0.0539 237.1085 237.0546 281.1430 128.0370 0.0501 237.2974 237.2473 281.2919 128.7988 0.0502 237.4814 237.4312 281.4166 129.6510 0.0444 237.6935 237.6491 281.5587 130.4430 0.0425 237.8721 237.8296 281.6670 131.2345 0.0393 238.0489 238.0096 281.8002 132.0570 0.0379 238.2408 238.2029 281.9313 132.8185 0.0351 238.4509 238.4158 282.0471 133.6710 0.0315 238.6422 238.6107 282.2119 134.4328 0.0332 238.8138 238.7806 282.3221 135.2548 0.0241 239.0123 238.9882 282.4410 136.0770 0.0244 239.1963 239.1719 282.5729 136.8385 0.0210 239.3848 239.3638 282.6775 137.6910 0.0170 239.6042 239.5872 282.7884 138.4528 0.0116 239.7696 239.7580 282.9100 139.2748 0.0112 239.9547 239.9435 283.0434 140.0970 0.0108 240.1335 240.1227 283.1834 140.8585 0.0073 240.3243 240.3170 283.2989 141.7108 0.0049 240.5101 240.5052 283.4243 142.4725 0.0003 240.6713 240.6710 283.5402 143.2948 0.0005 240.8856 240.8850 283.6668 144.0868 0.0015 241.0759 241.0744 283.7688 144.8785 0.0031 241.2530 241.2499 283.8912 145.7308 -0.0016 241.4420 241.4435 284.0179 146.4925 -0.0056 241.6234 241.6290 284.1137 147.3145 -0.0081 241.8208 241.8289 284.2584 148.1368 -0.0106 241.9990 242.0096 284.3839 148.8985 -0.0138 242.1532 242.1670 284.4951 149.7505 -0.0130 242.3740 242.3870 284.6246 150.5125 -0.0070 242.5564 242.5634 284.7333 151.3345 -0.0051 242.7423 242.7474 284.8689 152.1570 -0.0070 242.9286 242.9356 284.9819 152.9195 -0.0085 243.0964 243.1049 285.1024 153.7715 -0.0120 243.3129 243.3248 285.2284 154.5335 -0.0181 243.4692 243.4873 285.3381 155.3555 -0.0197 243.6474 243.6672 285.4840 156.1775 -0.0218 243.8514 243.8732 285.6187 156.9395 -0.0266 244.0344 244.0611 285.7367 157.7915 -0.0299 244.2241 244.2540 285.8923 158.5835 -0.0395 244.3990 244.4384 286.0308 159.3748 -0.0433 244.5527 244.5961 286.1527 160.1973 -0.0468 244.7357 244.7825 286.2817 160.9890 -0.0534 244.9092 244.9627 286.4061 161.8115 -0.0543 245.1108 245.1651 286.5532 162.6040 -0.0566 245.2847 245.3413 286.6909 163.3965 -0.0588 245.4660 245.5248 286.8024 164.2190 -0.0592 245.6583 245.7176 286.9471 165.0108 -0.0629 245.8563 245.9192 287.0992 165.8328 -0.0650 246.0341 246.0991 287.2122 166.6250 -0.0679 246.1925 246.2603 287.3417 167.4165 -0.0716 246.3705 246.4421 287.4829 168.2690 -0.0714 246.5480 246.6194 287.6413 169.0308 -0.0758 246.7266 246.8025 287.7662 169.8528 -0.0766 246.9181 246.9948 287.8840 170.6450 -0.0820 247.0931 247.1752 288.0265 171.4375 -0.0860 247.2740 247.3600 288.1659 172.2903 -0.0848 247.4529 247.5377 288.3243 173.0525 -0.0893 247.5934 247.6827 288.4531 173.8755 -0.0947 247.7999 247.8946 288.5993 174.6980 -0.0984 248.0077 248.1061 288.7311 175.4605 -0.1006 248.1954 248.2960 288.8748 176.3133 -0.1031 248.3623 248.4654 289.0196 177.0755 -0.1041 248.5267 248.6308 289.1316 177.8975 -0.1079 248.7146 248.8225 289.2421 178.7195 -0.1074 248.8889 248.9963 289.4105 179.4815 -0.1102 249.0583 249.1685 289.5405 180.3340 -0.1146 249.2433 249.3579 289.6854 181.0965 -0.1179 249.4033 249.5213 289.8262 181.9185 -0.1186 249.5898 249.7084 289.9807 182.7405 -0.1181 249.7723 249.8904 290.1073 183.5025 -0.1248 249.9321 250.0569 290.2411 184.3550 -0.1232 250.1315 250.2547 290.3961 185.1475 -0.1290 250.3179 250.4469 290.5177 185.9405 -0.1289 250.4667 250.5956 290.6568 186.7625 -0.1318 250.6555 250.7872 290.8088 187.5228 -0.1377 250.8289 250.9667 290.9329 188.3725 -0.1451 251.0014 251.1465 291.0644 189.1605 -0.1439 251.1648 251.3087 291.2047 189.9483 -0.1412 251.3443 251.4855 291.3486 190.7665 -0.1459 251.5252 251.6711 291.4823 191.5240 -0.1530 251.6787 251.8318 291.6060 192.3728 -0.1571 251.8641 252.0212 291.7683 193.1303 -0.1629 252.0386 252.2015 291.9050 193.9495 -0.1652 252.2027 252.3679 292.0468 194.7680 -0.1648 252.3727 252.5375 292.1811 195.5258 -0.1671 252.5537 252.7208 292.3170 196.3738 -0.1697 252.7253 252.8950 292.4584 197.1313 -0.1722 252.8887 253.0609 292.5820 197.9510 -0.1736 253.0790 253.2526 292.7167 198.7698 -0.1810 253.2575 253.4385 292.8579 199.5283 -0.1826 253.4056 253.5882 292.9689 200.3780 -0.1838 253.5982 253.7821 293.1383 201.1365 -0.1873 253.7573 253.9446 293.2746 201.9568 -0.1892 253.9200 254.1092 293.4102 202.7765 -0.1888 254.1076 254.2964 293.5666 203.5360 -0.1917 254.2732 254.4648 293.6800 204.3863 -0.1943 254.4654 254.6596 293.8330 205.1470 -0.2019 254.6217 254.8236 293.9631 205.9683 -0.2068 254.7964 255.0032 294.0983 206.7600 -0.2095 254.9664 255.1759 294.2215 207.5515 -0.2070 255.1588 255.3658 294.3655 208.4040 -0.2094 255.3303 255.5397 294.5060 209.1658 -0.2120 255.4752 255.6872 294.6337 209.9878 -0.2169 255.6446 255.8615 294.7854 210.7800 -0.2209 255.8135 256.0344 294.9118 211.5718 -0.2234 255.9720 256.1954 295.0539 212.3940 -0.2248 256.1625 256.3872 295.1910 213.1555 -0.2240 256.3140 256.5379 295.3184 214.0080 -0.2259 256.5184 256.7443 295.4735 214.7698 -0.2298 256.6721 256.9019 295.5815 215.5918 -0.2345 256.8731 257.1076 295.7166 216.4140 -0.2365 257.0469 257.2834 295.8559 217.1755 -0.2425 257.1900 257.4325 295.9982 218.0280 -0.2457 257.3601 257.6059 296.1512 218.7898 -0.2495 257.5103 257.7597 296.2692 219.6118 -0.2527 257.6910 257.9438 296.3989 220.4040 -0.2572 257.8854 258.1426 296.5276 221.1955 -0.2602 258.0293 258.2895 296.6485 222.0478 -0.2605 258.2093 258.4698 296.7897 222.8095 -0.2661 258.3676 258.6336 296.9273 223.6318 -0.2669 258.5369 258.8038 297.0576 224.4235 -0.2696 258.7079 258.9775 297.2007 225.2155 -0.2700 258.8896 259.1596 297.3329 226.0675 -0.2754 259.0696 259.3450 297.4786 226.8295 -0.2923 259.2149 259.5072 297.6082 227.6515 -0.2954 259.3760 259.6714 297.7378 228.4435 -0.2947 259.5497 259.8444 297.8711 229.2355 -0.2962 259.7150 260.0111 298.0064 230.0575 -0.2963 259.8825 260.1788 298.1141 230.8495 -0.3009 260.0461 260.3470 298.2469 231.6715 -0.3064 260.2074 260.5138 298.3776 232.4635 -0.3097 260.3819 260.6916 298.5192 233.2555 -0.3124 260.5418 260.8542 298.6557 234.0775 -0.3122 260.7144 261.0266 298.7925 234.8695 -0.3143 260.8766 261.1909 298.9199 235.6913 -0.3167 261.0353 261.3521 299.0520 236.4833 -0.3179 261.2104 261.5283 299.1912 237.2750 -0.3212 261.3776 261.6988 299.3138 238.1275 -0.3268 261.5559 261.8828 299.4433 238.8890 -0.3284 261.7299 262.0583 299.5767 239.7108 -0.3319 261.8865 262.2184 299.7294 240.5033 -0.3335 262.0553 262.3888 299.8452 241.2945 -0.3380 262.2079 262.5459 299.9886 242.1470 -0.3456 262.3945 262.7401 300.1173 242.9088 -0.3576 262.5380 262.8956 300.2470 243.7308 -0.3510 262.6894 263.0404 300.3720 244.5230 -0.3498 262.8700 263.2198 300.5014 245.3145 -0.3528 263.0620 263.4148 300.6373 246.1675 -0.3548 263.2231 263.5779 300.7666 246.9298 -0.3564 263.3732 263.7295 300.8827 247.7518 -0.3599 263.5399 263.8999 301.0246 248.5438 -0.3619 263.6986 264.0606 301.1542 249.3355 -0.3628 263.8531 264.2159 301.2874 250.1885 -0.3671 264.0431 264.4102 301.4251 250.9505 -0.3693 264.2021 264.5713 301.5518 251.7735 -0.3691 264.3586 264.7278 301.6731 252.5653 -0.3711 264.5165 264.8876 301.8021 253.3540 -0.3774 264.6930 265.0704 301.9670 254.2020 -0.3776 264.8613 265.2390 302.0889 254.9600 -0.3803 265.0334 265.4137 302.2006 255.7780 -0.3825 265.2083 265.5908 302.3359 256.5660 -0.3836 265.3671 265.7508 302.4693 257.3540 -0.3873 265.4960 265.8832 302.5998 258.2020 -0.3890 265.6768 266.0658 302.7314 258.9600 -0.3943 265.8211 266.2154 302.8671 259.7785 -0.3959 265.9837 266.3796 302.9960 260.5970 -0.3990 266.1685 266.5675 303.1491 261.3550 -0.4063 266.3098 266.7161 303.2766 262.2035 -0.4052 266.4707 266.8759 303.3904 262.9920 -0.4129 266.6310 267.0438 303.5046 263.7800 -0.4172 266.8010 267.2183 303.6522 264.5988 -0.4177 266.9572 267.3749 303.7776 265.3880 -0.4186 267.1177 267.5363 303.9097 266.2073 -0.4225 267.2988 267.7213 304.0592 266.9965 -0.4282 267.4672 267.8954 304.1839 267.7875 -0.4272 267.6358 268.0629 304.3031 268.6095 -0.4282 267.7802 268.2083 304.4206 269.4008 -0.4317 267.9640 268.3957 304.5581 270.2210 -0.4336 268.1264 268.5600 304.7077 271.0115 -0.4373 268.2582 268.6955 304.8243 271.8023 -0.4437 268.4215 268.8651 304.9391 272.6235 -0.4497 268.5871 269.0368 305.0804 273.4148 -0.4519 268.7536 269.2055 305.2041 274.2365 -0.4548 268.9083 269.3631 305.3498 275.0285 -0.4569 269.0738 269.5308 305.4863 275.8205 -0.4609 269.2263 269.6872 305.6009 276.6425 -0.4656 269.3958 269.8613 305.7360 277.4345 -0.4653 269.5495 270.0148 305.8649 278.2565 -0.4712 269.7076 270.1788 305.9963 279.0485 -0.4713 269.8683 270.3396 306.1234 279.8405 -0.4736 270.0214 270.4951 306.2819 280.6625 -0.4699 270.1932 270.6631 306.3931 281.4545 -0.4752 270.3707 270.8459 306.5322 282.2765 -0.4772 270.5186 270.9958 306.6473 283.0685 -0.4832 270.6626 271.1458 306.7747 283.8605 -0.4823 270.8254 271.3077 306.8949 284.6825 -0.4846 270.9888 271.4734 307.0311 285.4743 -0.4885 271.1479 271.6364 307.1623 286.2960 -0.4914 271.3221 271.8135 307.2871 287.0883 -0.4934 271.4589 271.9524 307.4119 287.8800 -0.4950 271.6293 272.1243 307.5486 288.7020 -0.4979 271.7886 272.2865 307.6970 289.4938 -0.5018 271.9619 272.4637 307.8160 290.3158 -0.5059 272.1223 272.6282 307.9293 291.1080 -0.5100 272.2701 272.7801 308.0577 291.8995 -0.5096 272.4218 272.9314 308.1859 292.7520 -0.5073 272.5834 273.0907 308.3113 293.5138 -0.5147 272.7346 273.2493 308.4351 294.3358 -0.5154 272.9144 273.4299 308.5960 295.1280 -0.5222 273.0797 273.6019 308.7122 295.9195 -0.5235 273.2331 273.7566 308.8144 296.7720 -0.5286 273.3896 273.9182 308.9746 297.5338 -0.5309 273.5368 274.0677 309.0984 298.3558 -0.5339 273.6924 274.2263 309.2022 299.1480 -0.5413 273.8550 274.3962 309.3337 299.9395 -0.5470 274.0098 274.5568 309.4529 300.7918 -0.5481 274.1819 274.7299 309.5906 301.5535 -0.5472 274.3320 274.8793 309.7150 302.3758 -0.5445 274.4937 275.0382 309.8409 303.1675 -0.5492 274.6356 275.1848 309.9717 303.9595 -0.5500 274.7773 275.3273 310.0882 304.8115 -0.5578 274.9715 275.5293 310.2192 305.5735 -0.5620 275.1190 275.6809 310.3278 306.3955 -0.5616 275.2859 275.8475 310.4662 307.1875 -0.5629 275.4334 275.9963 310.5716 307.9795 -0.5624 275.5780 276.1404 310.6929 308.8315 -0.5629 275.7548 276.3178 310.8470 309.5935 -0.5683 275.8980 276.4663 310.9693 310.4163 -0.5745 276.0680 276.6425 311.0858 311.2085 -0.5766 276.2180 276.7946 311.2208 312.0005 -0.5793 276.3606 276.9400 311.3278 312.8228 -0.5794 276.5214 277.1008 311.4706 313.6155 -0.5822 276.6820 277.2642 311.6107 314.4383 -0.5845 276.8412 277.4258 311.7500 315.2315 -0.5869 276.9868 277.5737 311.8853 316.0240 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