DTA measure 1Pb_updown3 Date: 2025312:90 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.18 s Mass = 936.600 mg data_number = 1258 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2530 -0.9233 201.3872 202.3105 260.6016 2.0423 -0.9197 201.6326 202.5523 260.6182 2.8333 -0.9175 201.8899 202.8075 260.6336 3.6550 -0.9096 202.1175 203.0271 260.6179 4.4468 -0.8992 202.3800 203.2793 260.6534 5.2688 -0.8881 202.6498 203.5379 260.6782 6.0610 -0.8840 202.8987 203.7827 260.7165 6.8525 -0.8834 203.1289 204.0124 260.7430 7.6750 -0.8790 203.3799 204.2589 260.7549 8.4365 -0.8744 203.6236 204.4980 260.8021 9.2890 -0.8696 203.8979 204.7676 260.8643 10.0810 -0.8635 204.1668 205.0303 260.9455 10.8725 -0.8537 204.3839 205.2376 261.0056 11.6950 -0.8501 204.6161 205.4663 261.0781 12.4565 -0.8492 204.8490 205.6982 261.1700 13.3090 -0.8458 205.1216 205.9674 261.2467 14.1010 -0.8401 205.3557 206.1959 261.3164 14.8925 -0.8377 205.5831 206.4208 261.4088 15.7150 -0.8333 205.8484 206.6817 261.5184 16.4765 -0.8283 206.0845 206.9128 261.6325 17.3288 -0.8284 206.3492 207.1776 261.7392 18.1208 -0.8238 206.5758 207.3996 261.8651 18.9125 -0.8193 206.8153 207.6346 261.9885 19.7355 -0.8194 207.0523 207.8716 262.1182 20.4985 -0.8112 207.3100 208.1212 262.2581 21.3513 -0.8060 207.5234 208.3294 262.4043 22.1135 -0.8033 207.7651 208.5684 262.5520 22.9355 -0.8028 208.0182 208.8210 262.7055 23.7575 -0.7999 208.2571 209.0569 262.8735 24.5195 -0.7967 208.4686 209.2654 263.0109 25.3715 -0.7927 208.7224 209.5152 263.1948 26.1635 -0.7901 208.9658 209.7559 263.3831 26.9520 -0.7821 209.1839 209.9660 263.5387 27.7698 -0.7815 209.4294 210.2109 263.7159 28.5280 -0.7775 209.6495 210.4270 263.8798 29.3770 -0.7772 209.8989 210.6761 264.0846 30.1353 -0.7770 210.1361 210.9131 264.2382 30.9540 -0.7722 210.3781 211.1503 264.4201 31.7725 -0.7689 210.6232 211.3921 264.6017 32.5310 -0.7696 210.8511 211.6207 264.7808 33.4103 -0.7686 211.0808 211.8493 265.0025 34.2308 -0.7664 211.3322 212.0986 265.1931 35.0215 -0.7669 211.5516 212.3186 265.3706 35.8125 -0.7626 211.7775 212.5400 265.5749 36.6635 -0.7620 212.0298 212.7918 265.7550 37.6358 -0.7551 212.3076 213.0627 265.9911 38.4865 -0.7550 212.5660 213.3209 266.2173 39.2785 -0.7529 212.7833 213.5363 266.3708 40.0705 -0.7542 212.9983 213.7525 266.5499 40.9228 -0.7507 213.2619 214.0126 266.7365 41.7745 -0.7495 213.4819 214.2314 266.9039 42.5665 -0.7508 213.6949 214.4457 267.0970 43.3585 -0.7496 213.9351 214.6847 267.2645 44.2108 -0.7516 214.1836 214.9352 267.4548 44.9725 -0.7500 214.4035 215.1535 267.6160 45.7945 -0.7496 214.6415 215.3910 267.7901 46.5865 -0.7491 214.8577 215.6068 267.9546 47.3785 -0.7458 215.0702 215.8160 268.0967 48.2305 -0.7459 215.3084 216.0543 268.2772 48.9925 -0.7436 215.5218 216.2654 268.4371 49.8145 -0.7384 215.7686 216.5070 268.5976 50.6065 -0.7389 215.9817 216.7206 268.7371 51.3985 -0.7409 216.1909 216.9318 268.9040 52.2505 -0.7320 216.4455 217.1775 269.0575 53.0125 -0.7344 216.6613 217.3957 269.1903 53.8345 -0.7342 216.8882 217.6224 269.3294 54.6265 -0.7329 217.0941 217.8270 269.4856 55.4185 -0.7400 217.3304 218.0704 269.6016 56.2705 -0.7343 217.5745 218.3088 269.7593 57.0333 -0.7347 217.7657 218.5004 269.8723 57.8553 -0.7357 218.0079 218.7436 270.0139 58.6450 -0.7373 218.2247 218.9620 270.1405 59.4340 -0.7331 218.4390 219.1720 270.2620 60.2513 -0.7340 218.6740 219.4079 270.3975 61.0405 -0.7308 218.8915 219.6223 270.4947 61.8598 -0.7295 219.1357 219.8652 270.6046 62.6478 -0.7297 219.3246 220.0543 270.7218 63.4360 -0.7274 219.5449 220.2722 270.8440 64.2853 -0.7257 219.7647 220.4905 270.9688 65.0440 -0.7244 219.9810 220.7054 271.0700 65.8630 -0.7219 220.2047 220.9265 271.1608 66.6520 -0.7182 220.4001 221.1183 271.2542 67.4418 -0.7143 220.6340 221.3482 271.3687 68.2923 -0.7146 220.8577 221.5723 271.4885 69.0535 -0.7162 221.0573 221.7735 271.6035 69.8755 -0.7151 221.2897 222.0048 271.7099 70.6678 -0.7142 221.5025 222.2167 271.8160 71.4605 -0.7146 221.7068 222.4213 271.9301 72.2825 -0.7100 221.9594 222.6694 272.0261 73.1345 -0.7106 222.1654 222.8759 272.1611 73.9265 -0.7094 222.3671 223.0765 272.2804 74.7485 -0.7076 222.5927 223.3003 272.4048 75.5705 -0.7087 222.8118 223.5205 272.4945 76.3325 -0.7120 223.0037 223.7157 272.5983 77.1845 -0.7123 223.2242 223.9365 272.7265 77.9465 -0.7085 223.4310 224.1396 272.8265 78.7685 -0.7042 223.6379 224.3421 272.9280 79.5605 -0.7116 223.8497 224.5612 273.0386 80.3525 -0.7129 224.0511 224.7640 273.1563 81.2045 -0.7088 224.2806 224.9893 273.2644 82.0563 -0.7058 224.5126 225.2183 273.4168 82.8483 -0.7063 224.7237 225.4300 273.5395 83.6700 -0.7073 224.9395 225.6468 273.6629 84.4933 -0.7071 225.1454 225.8525 273.7994 85.3153 -0.7024 225.3645 226.0670 273.9177 86.0765 -0.7063 225.5813 226.2876 274.0458 86.9290 -0.7062 225.8033 226.5095 274.1920 87.6908 -0.7079 226.0053 226.7132 274.2971 88.5135 -0.7016 226.1912 226.8928 274.4093 89.3060 -0.6997 226.3852 227.0849 274.5419 90.0975 -0.6995 226.5909 227.2904 274.6803 90.9455 -0.7016 226.8249 227.5265 274.8114 91.7043 -0.7043 227.0283 227.7325 274.9239 92.5220 -0.7068 227.2440 227.9509 275.0540 93.3103 -0.6992 227.4411 228.1404 275.1811 94.2183 -0.7011 227.6799 228.3809 275.3490 95.0363 -0.6985 227.8618 228.5602 275.4919 95.7943 -0.6994 228.0590 228.7584 275.6242 96.6425 -0.7017 228.2756 228.9773 275.7842 97.4305 -0.7018 228.4761 229.1780 275.9157 98.2243 -0.7062 228.6684 229.3747 276.0506 99.0193 -0.7053 228.8781 229.5834 276.1799 99.8115 -0.7059 229.0722 229.7780 276.3098 100.6635 -0.7052 229.2787 229.9839 276.4678 101.4255 -0.7083 229.4640 230.1723 276.6079 102.2475 -0.7066 229.6783 230.3850 276.7479 103.0395 -0.7047 229.8960 230.6007 276.8850 103.8313 -0.7028 230.0807 230.7836 277.0360 104.6535 -0.6987 230.2882 230.9870 277.1961 105.5053 -0.7004 230.5146 231.2151 277.3443 106.2968 -0.6988 230.7208 231.4196 277.4852 107.1200 -0.7011 230.9266 231.6277 277.6270 107.9723 -0.7027 231.1117 231.8143 277.7703 108.7640 -0.7051 231.3153 232.0204 277.9299 109.5558 -0.7032 231.5154 232.2185 278.0722 110.3783 -0.7015 231.7005 232.4020 278.2129 111.1398 -0.7016 231.8894 232.5910 278.3646 111.9920 -0.7036 232.1256 232.8292 278.5178 112.7840 -0.7009 232.3214 233.0223 278.6449 113.5755 -0.7090 232.5140 233.2229 278.8131 114.3983 -0.7123 232.7220 233.4343 278.9540 115.1595 -0.7133 232.9061 233.6194 279.0756 116.0120 -0.7105 233.1297 233.8402 279.2262 116.8040 -0.7082 233.3251 234.0333 279.3551 117.6268 -0.7109 233.5075 234.2184 279.5074 118.4488 -0.7124 233.7365 234.4489 279.6436 119.2410 -0.7117 233.9138 234.6255 279.7823 120.0325 -0.7125 234.0863 234.7988 279.9376 120.8548 -0.7133 234.3012 235.0145 280.0897 121.6465 -0.7154 234.4885 235.2039 280.2493 122.4688 -0.7176 234.6916 235.4092 280.4018 123.2605 -0.7198 234.8986 235.6183 280.5392 124.0500 -0.7195 235.0723 235.7918 280.6705 124.8683 -0.7191 235.2640 235.9831 280.8024 125.6260 -0.7197 235.4598 236.1795 280.9434 126.4743 -0.7206 235.6624 236.3829 281.1020 127.2623 -0.7195 235.8416 236.5611 281.2574 128.0518 -0.7225 236.0442 236.7667 281.3640 128.8713 -0.7224 236.2725 236.9950 281.5144 129.6300 -0.7264 236.3930 237.1194 281.6351 130.4788 -0.7281 236.6171 237.3452 281.7753 131.2678 -0.7257 236.8108 237.5365 281.8954 132.0585 -0.7298 237.0048 237.7346 282.0347 132.8795 -0.7316 237.2056 237.9372 282.1779 133.6405 -0.7333 237.3708 238.1041 282.2923 134.4930 -0.7265 237.5904 238.3169 282.4320 135.2548 -0.7267 237.7660 238.4927 282.5473 136.0768 -0.7303 237.9688 238.6991 282.7001 136.8690 -0.7303 238.1395 238.8698 282.8231 137.6605 -0.7306 238.3465 239.0772 282.9545 138.5130 -0.7233 238.5475 239.2708 283.0805 139.2748 -0.7224 238.7227 239.4450 283.1957 140.0968 -0.7290 238.9158 239.6449 283.3304 140.8890 -0.7342 239.0856 239.8198 283.4701 141.6805 -0.7360 239.2828 240.0188 283.5632 142.5330 -0.7379 239.5015 240.2394 283.6861 143.2948 -0.7366 239.6768 240.4134 283.8184 144.1198 -0.7355 239.8665 240.6020 283.9606 144.9120 -0.7407 240.0550 240.7958 284.0770 145.7035 -0.7411 240.2347 240.9758 284.2050 146.5558 -0.7419 240.4369 241.1788 284.3262 147.3175 -0.7471 240.6189 241.3660 284.4479 148.1398 -0.7458 240.8192 241.5650 284.5704 148.9318 -0.7446 240.9966 241.7412 284.6793 149.7235 -0.7414 241.1971 241.9385 284.7770 150.5758 -0.7450 241.3772 242.1222 284.9402 151.3375 -0.7455 241.5416 242.2871 285.0505 152.1605 -0.7434 241.7288 242.4722 285.1857 152.9825 -0.7453 241.9395 242.6848 285.3005 153.7445 -0.7449 242.1144 242.8593 285.4201 154.5965 -0.7454 242.3182 243.0636 285.5511 155.3585 -0.7474 242.5057 243.2532 285.6647 156.1778 -0.7491 242.6888 243.4378 285.7840 156.9960 -0.7483 242.8620 243.6104 285.9047 157.7540 -0.7547 243.0358 243.7905 286.0335 158.6030 -0.7545 243.2278 243.9823 286.1646 159.3635 -0.7562 243.4123 244.1686 286.2851 160.1910 -0.7527 243.6006 244.3533 286.3904 160.9790 -0.7514 243.7828 244.5343 286.5290 161.7670 -0.7534 243.9571 244.7105 286.6552 162.7060 -0.7580 244.1800 244.9380 286.8105 163.5858 -0.7533 244.3969 245.1502 286.9464 164.3750 -0.7553 244.5853 245.3406 287.0859 165.2848 -0.7632 244.7698 245.5331 287.2595 166.0465 -0.7610 244.9364 245.6975 287.3816 166.9308 -0.7628 245.1389 245.9018 287.5361 167.7828 -0.7674 245.3249 246.0923 287.6628 168.5745 -0.7722 245.5190 246.2912 287.7774 169.3968 -0.7703 245.7049 246.4751 287.9313 170.1585 -0.7648 245.8776 246.6424 288.0650 171.0108 -0.7611 246.0629 246.8240 288.2235 171.8025 -0.7622 246.2387 247.0009 288.3697 172.5945 -0.7613 246.3940 247.1554 288.4810 173.4168 -0.7613 246.5883 247.3496 288.6234 174.1785 -0.7621 246.7680 247.5302 288.7551 175.0305 -0.7732 246.9588 247.7320 288.8838 175.8225 -0.7719 247.1355 247.9075 289.0501 176.6148 -0.7699 247.3093 248.0791 289.1861 177.4365 -0.7702 247.4904 248.2606 289.3409 178.1985 -0.7767 247.6584 248.4351 289.4735 179.0505 -0.7811 247.8690 248.6501 289.6257 179.8425 -0.7830 248.0410 248.8240 289.7717 180.6345 -0.7829 248.2293 249.0122 289.9051 181.4565 -0.7793 248.4095 249.1889 290.0653 182.2185 -0.7768 248.5650 249.3418 290.1667 183.0705 -0.7640 248.7415 249.5055 290.2947 183.8325 -0.7607 248.9172 249.6779 290.4331 184.7145 -0.7618 249.1218 249.8836 290.6156 185.5065 -0.7604 249.2960 250.0564 290.7470 186.3590 -0.7623 249.4650 250.2273 290.8960 187.1513 -0.7655 249.6550 250.4205 291.0283 188.0275 -0.7748 249.8412 250.6159 291.1613 188.7863 -0.7836 250.0209 250.8045 291.3083 189.6343 -0.7813 250.2241 251.0054 291.4675 190.3923 -0.7801 250.3885 251.1686 291.5819 191.2120 -0.7888 250.5556 251.3443 291.7436 192.0303 -0.7965 250.7352 251.5317 291.8837 192.7890 -0.7961 250.8959 251.6920 292.0279 193.6375 -0.7939 251.0902 251.8841 292.1846 194.4260 -0.7962 251.2456 252.0418 292.3351 195.2158 -0.7984 251.4265 252.2249 292.4655 196.0360 -0.8031 251.6182 252.4213 292.5876 196.7975 -0.8074 251.7889 252.5963 292.7344 197.6488 -0.8053 251.9514 252.7567 292.8907 198.4095 -0.8063 252.1278 252.9341 292.9971 199.2315 -0.8072 252.3029 253.1101 293.1337 200.0235 -0.8052 252.4642 253.2695 293.2759 200.8155 -0.8072 252.6471 253.4543 293.3933 201.6678 -0.8061 252.8180 253.6240 293.5376 202.4295 -0.8144 252.9766 253.7910 293.6697 203.2515 -0.8175 253.1706 253.9881 293.7898 204.0738 -0.8178 253.3487 254.1666 293.9130 204.9555 -0.8189 253.5635 254.3823 294.0463 205.7475 -0.8184 253.7185 254.5368 294.1706 206.5395 -0.8202 253.8951 254.7154 294.3023 207.3915 -0.8253 254.0675 254.8928 294.4221 208.1535 -0.8258 254.2222 255.0480 294.5456 208.9755 -0.8262 254.4085 255.2347 294.6703 209.7675 -0.8267 254.5790 255.4057 294.7920 210.5595 -0.8293 254.7627 255.5921 294.9156 211.4115 -0.8296 254.9478 255.7774 295.0557 212.1735 -0.8313 255.1061 255.9374 295.1433 212.9953 -0.8295 255.2721 256.1015 295.2654 213.7875 -0.8280 255.4381 256.2660 295.3893 214.6395 -0.8320 255.6173 256.4493 295.5298 215.4305 -0.8339 255.8188 256.6527 295.6310 216.2533 -0.8362 255.9818 256.8180 295.7406 217.0155 -0.8391 256.1216 256.9608 295.8634 217.8680 -0.8416 256.3225 257.1641 295.9939 218.6600 -0.8388 256.4944 257.3332 296.1179 219.4510 -0.8423 256.6489 257.4912 296.2274 220.2693 -0.8455 256.8422 257.6877 296.3598 221.0270 -0.8487 256.9831 257.8317 296.4988 221.8740 -0.8482 257.1608 258.0091 296.6222 222.6935 -0.8483 257.3207 258.1690 296.7621 223.4815 -0.8458 257.5029 258.3487 296.8896 224.3003 -0.8476 257.6920 258.5397 297.0347 225.0893 -0.8507 257.8530 258.7037 297.1442 225.8780 -0.8546 258.0255 258.8800 297.2560 226.6968 -0.8573 258.1968 259.0540 297.3880 227.4880 -0.8565 258.3620 259.2185 297.5309 228.3078 -0.8578 258.5193 259.3772 297.6507 229.0975 -0.8614 258.7049 259.5662 297.7917 229.8895 -0.8633 258.8598 259.7232 297.9340 230.7115 -0.8662 259.0313 259.8974 298.0660 231.4735 -0.8701 259.1924 260.0625 298.1922 232.3253 -0.8677 259.3792 260.2469 298.3476 233.1175 -0.8690 259.5453 260.4142 298.4766 233.9095 -0.8729 259.7031 260.5759 298.6017 234.7315 -0.8721 259.8711 260.7431 298.7395 235.4935 -0.8763 260.0418 260.9182 298.8430 236.3455 -0.8793 260.2186 261.0979 298.9836 237.1373 -0.8790 260.3889 261.2679 299.1340 237.9288 -0.8825 260.5609 261.4434 299.2529 238.7513 -0.8825 260.7166 261.5991 299.3916 239.5128 -0.8815 260.8716 261.7532 299.5178 240.3650 -0.8837 261.0531 261.9368 299.6553 241.1570 -0.8865 261.2144 262.1009 299.7933 241.9488 -0.8866 261.3986 262.2852 299.9191 242.7710 -0.8878 261.5736 262.4614 300.0641 243.5325 -0.8984 261.7328 262.6312 300.1729 244.3850 -0.9097 261.8974 262.8071 300.3176 245.1770 -0.9138 262.0454 262.9592 300.4495 245.9685 -0.9260 262.2073 263.1333 300.5810 246.7913 -0.9358 262.3666 263.3023 300.7517 247.5525 -0.9395 262.5319 263.4715 300.8825 248.4050 -0.9387 262.7234 263.6621 300.9945 249.1970 -0.9430 262.8977 263.8407 301.1319 249.9885 -0.9435 263.0406 263.9841 301.2767 250.8108 -0.9418 263.2210 264.1628 301.4008 251.5725 -0.9444 263.3714 264.3158 301.5184 252.4228 -0.9451 263.5445 264.4896 301.6495 253.2110 -0.9475 263.7090 264.6566 301.7816 253.9990 -0.9475 263.8568 264.8043 301.9313 254.8173 -0.9512 264.0361 264.9872 302.0673 255.8160 -0.9502 264.2266 265.1768 302.1974 256.5743 -0.9528 264.3992 265.3520 302.3293 257.3920 -0.9553 264.5475 265.5028 302.4726 258.1805 -0.9612 264.7289 265.6902 302.6029 258.9690 -0.9624 264.8955 265.8579 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