DTA measure 3fut Date: 2026325:933 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.49 s Mass = 1155.600 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5185 -5.2182 464.2948 469.5130 432.4727 4.1374 -5.2258 464.2996 469.5255 432.7702 5.7459 -5.2328 464.2772 469.5100 432.9913 7.3543 -5.2426 464.1996 469.4422 433.1929 8.9629 -5.2515 464.1149 469.3664 433.3746 10.5663 -5.2616 464.0346 469.2962 433.4433 12.1799 -5.2698 463.9996 469.2694 433.4181 13.7680 -5.2771 463.9629 469.2400 433.2831 15.3814 -5.2865 463.9258 469.2123 433.0929 17.0004 -5.2891 463.9235 469.2125 432.8074 18.6141 -5.2898 463.9005 469.1903 432.4647 20.2173 -5.2907 463.8598 469.1505 432.0770 21.8208 -5.2982 463.8117 469.1099 431.6423 23.4241 -5.3008 463.7565 469.0573 431.1696 25.0120 -5.2987 463.7488 469.0475 430.6701 26.6204 -5.3000 463.6975 468.9974 430.1721 28.2238 -5.2996 463.5894 468.8890 429.7000 29.8426 -5.2985 463.5175 468.8161 429.2657 31.4509 -5.2948 463.4707 468.7655 428.8784 33.0543 -5.2916 463.3969 468.6884 428.5100 34.6626 -5.2822 463.3532 468.6355 428.1915 36.2660 -5.2785 463.2541 468.5326 427.9133 37.8746 -5.2733 463.2082 468.4815 427.7041 39.4779 -5.2690 463.1330 468.4020 427.5151 41.1070 -5.2707 463.0166 468.2873 427.4263 42.7105 -5.2685 462.9489 468.2174 427.3823 44.3240 -5.2680 462.8792 468.1472 427.4092 45.9275 -5.2698 462.7853 468.0551 427.4347 47.5413 -5.2677 462.7169 467.9847 427.4502 49.1444 -5.2675 462.6601 467.9276 427.4064 50.7530 -5.2665 462.5943 467.8608 427.3260 52.3768 -5.2653 462.5033 467.7686 427.2039 53.9801 -5.2670 462.4083 467.6753 427.1146 55.5680 -5.2677 462.3232 467.5909 426.9846 57.1714 -5.2658 462.2363 467.5021 426.8036 58.7748 -5.2697 462.1453 467.4150 426.5655 60.3779 -5.2666 462.0499 467.3166 426.3316 61.9814 -5.2670 461.9536 467.2206 426.0658 63.5898 -5.2609 461.8484 467.1093 425.7738 65.2085 -5.2510 461.7119 466.9630 425.4267 66.8171 -5.2446 461.6153 466.8599 425.0771 68.4104 -5.2461 461.4809 466.7270 424.7613 70.0188 -5.2491 461.3957 466.6448 424.4411 71.6224 -5.2452 461.2867 466.5318 424.0932 73.2358 -5.2475 461.2106 466.4580 423.7850 74.8394 -5.2446 461.1496 466.3942 423.4512 76.4530 -5.2418 461.0453 466.2871 423.1853 78.0409 -5.2316 460.9370 466.1686 422.9579 79.6599 -5.2249 460.8361 466.0609 422.7357 81.2736 -5.2241 460.7558 465.9798 422.5571 82.8770 -5.2204 460.6563 465.8767 422.4148 84.4855 -5.2176 460.5416 465.7592 422.2377 86.0890 -5.2102 460.4272 465.6374 422.1133 87.6769 -5.2078 460.2998 465.5076 421.9919 89.2804 -5.2026 460.1652 465.3678 421.8625 90.8786 -5.2018 460.0213 465.2232 421.7654 92.5024 -5.2049 459.8901 465.0951 421.6397 94.0905 -5.2059 459.7543 464.9602 421.5212 95.6991 -5.2036 459.6172 464.8208 421.3609 97.3024 -5.2009 459.4951 464.6960 421.1821 98.9059 -5.1997 459.3889 464.5886 420.9923 100.5145 -5.2015 459.2449 464.4464 420.8280 102.1176 -5.1979 459.0878 464.2857 420.6480 103.7263 -5.1927 458.9995 464.1921 420.3879 105.3453 -5.1894 458.8876 464.0770 420.1403 106.9536 -5.1847 458.7457 463.9304 419.8973 108.5621 -5.1797 458.6135 463.7933 419.5661 110.1705 -5.1795 458.4427 463.6222 419.2972 111.7740 -5.1730 458.3079 463.4809 418.9941 113.3878 -5.1670 458.1988 463.3658 418.7710 114.9910 -5.1653 458.0880 463.2533 418.5238 116.5893 -5.1693 457.9691 463.1384 418.2804 118.2081 -5.1668 457.8227 462.9895 418.0616 119.8064 -5.1620 457.6490 462.8111 417.8617 121.4098 -5.1571 457.4856 462.6427 417.6458 123.0133 -5.1550 457.3217 462.4767 417.4124 124.6165 -5.1506 457.1930 462.3435 417.2289 126.2251 -5.1467 457.0431 462.1898 417.0278 127.8284 -5.1466 456.8774 462.0241 416.8134 129.4523 -5.1422 456.7383 461.8806 416.6127 131.0558 -5.1348 456.5986 461.7333 416.4296 132.6640 -5.1261 456.4555 461.5816 416.2268 134.2676 -5.1264 456.3084 461.4348 416.0565 135.8813 -5.1190 456.1479 461.2669 415.8972 137.4845 -5.1160 455.9923 461.1083 415.7198 139.0931 -5.1138 455.8619 460.9757 415.5276 140.7169 -5.1106 455.7109 460.8214 415.3456 142.3049 -5.1098 455.5375 460.6473 415.1434 143.9135 -5.1066 455.3321 460.4387 414.9336 145.5374 -5.1003 455.1495 460.2499 414.7021 147.1458 -5.0962 454.9930 460.0892 414.5093 148.7391 -5.0932 454.8573 459.9505 414.3131 150.3423 -5.0882 454.6833 459.7715 414.0929 151.9458 -5.0881 454.5292 459.6173 413.8423 153.5646 -5.0831 454.3555 459.4386 413.6231 155.1678 -5.0778 454.2067 459.2845 413.4221 156.7559 -5.0732 454.0234 459.0967 413.2008 158.3644 -5.0642 453.8517 458.9158 412.9853 159.9678 -5.0617 453.7024 458.7641 412.7348 161.5764 -5.0607 453.5619 458.6226 412.5126 163.1798 -5.0546 453.3880 458.4426 412.2751 164.7934 -5.0477 453.2253 458.2730 412.0575 166.4121 -5.0442 453.0427 458.0868 411.8227 168.0000 -5.0397 452.8750 457.9146 411.6337 169.6088 -5.0353 452.6724 457.7077 411.4217 171.2174 -5.0389 452.5061 457.5450 411.1972 172.8259 -5.0322 452.3686 457.4008 411.0046 174.4293 -5.0189 452.1972 457.2161 410.8089 176.0429 -5.0206 452.0140 457.0347 410.6046 177.6463 -5.0193 451.8461 456.8654 410.4119 179.2394 -5.0196 451.6769 456.6965 410.2332 180.8583 -5.0155 451.5159 456.5313 410.0562 182.4666 -5.0150 451.3456 456.3605 409.8491 184.0649 -5.0082 451.1586 456.1668 409.6182 185.6684 -5.0033 451.0090 456.0123 409.3787 187.2716 -4.9941 450.8359 455.8300 409.1664 188.8598 -4.9829 450.6441 455.6270 408.9618 190.4580 -4.9807 450.4586 455.4393 408.7585 192.0664 -4.9717 450.2721 455.2438 408.5780 193.6853 -4.9625 450.0797 455.0422 408.3978 195.2936 -4.9610 449.9195 454.8805 408.2222 196.8971 -4.9582 449.7707 454.7289 408.0328 198.5105 -4.9580 449.5888 454.5468 407.8369 200.1139 -4.9490 449.3958 454.3447 407.6328 201.7021 -4.9430 449.2110 454.1541 407.4184 203.3105 -4.9431 449.0155 453.9586 407.1901 204.9139 -4.9362 448.8718 453.8080 406.9668 206.5429 -4.9295 448.6772 453.6067 406.7050 208.1461 -4.9243 448.4803 453.4046 406.4688 209.7548 -4.9197 448.2823 453.2020 406.2291 211.3634 -4.9113 448.0804 452.9917 405.9834 212.9718 -4.9105 447.8994 452.8099 405.7427 214.5753 -4.9091 447.7495 452.6586 405.4832 216.1686 -4.9074 447.5745 452.4819 405.2301 217.7924 -4.9038 447.3907 452.2945 405.0296 219.3908 -4.8953 447.2262 452.1214 404.8418 220.9943 -4.8887 447.0720 451.9607 404.6489 222.5873 -4.8837 446.8454 451.7291 404.4699 224.1908 -4.8771 446.6281 451.5053 404.2824 225.7994 -4.8721 446.4452 451.3173 404.0978 227.4028 -4.8667 446.2715 451.1381 403.8964 229.0114 -4.8624 446.0933 450.9558 403.6786 230.6301 -4.8576 445.9083 450.7659 403.4822 232.2385 -4.8535 445.7256 450.5791 403.3066 233.8470 -4.8548 445.5133 450.3681 403.1030 235.4506 -4.8502 445.3473 450.1975 402.8785 237.0641 -4.8400 445.1705 450.0105 402.6842 238.6676 -4.8320 444.9392 449.7712 402.4834 240.2763 -4.8278 444.7024 449.5302 402.2885 241.9000 -4.8181 444.4926 449.3107 402.0757 243.5086 -4.8157 444.2829 449.0987 401.8849 245.1121 -4.8095 444.1067 448.9162 401.6889 246.7206 -4.8044 443.9549 448.7593 401.4549 248.3241 -4.8026 443.7852 448.5878 401.2145 249.9224 -4.7948 443.6071 448.4019 401.0072 251.5308 -4.7875 443.3971 448.1846 400.7572 253.1445 -4.7806 443.2183 447.9989 400.5337 254.7531 -4.7754 443.0221 447.7975 400.3214 256.3563 -4.7738 442.8662 447.6400 400.0905 257.9445 -4.7736 442.6513 447.4249 399.8414 259.5531 -4.7682 442.4285 447.1967 399.6113 261.1718 -4.7634 442.2100 446.9734 399.3957 262.7804 -4.7614 442.0116 446.7730 399.1788 264.3993 -4.7506 441.8126 446.5632 398.9577 266.0076 -4.7456 441.6264 446.3719 398.7301 267.6161 -4.7434 441.4044 446.1478 398.5639 269.2248 -4.7437 441.1861 445.9298 398.3736 270.8280 -4.7336 440.9940 445.7277 398.1534 272.4368 -4.7253 440.7941 445.5194 397.9237 274.0454 -4.7217 440.5752 445.2969 397.7742 275.6640 -4.7186 440.4099 445.1285 397.6070 277.2625 -4.7155 440.2082 444.9237 397.4291 278.8659 -4.7132 439.9933 444.7065 397.2227 280.4691 -4.7068 439.7742 444.4810 397.0233 282.0726 -4.7038 439.6113 444.3152 396.8251 283.6556 -4.6946 439.4532 444.1478 396.6006 285.2589 -4.6901 439.2436 443.9337 396.4231 286.8624 -4.6880 439.0378 443.7258 396.2001 288.4710 -4.6873 438.8696 443.5569 395.9816 290.0744 -4.6755 438.6796 443.3551 395.7716 291.6779 -4.6633 438.4625 443.1258 395.5577 293.2865 -4.6570 438.2933 442.9503 395.3560 294.8948 -4.6504 438.0900 442.7405 395.1169 296.5034 -4.6396 437.8901 442.5298 394.8492 298.1069 -4.6334 437.6510 442.2844 394.6031 299.7154 -4.6275 437.4240 442.0515 394.3938 301.3189 -4.6199 437.2139 441.8338 394.1819 302.9326 -4.6100 437.0135 441.6235 393.9082 304.5360 -4.6046 436.8038 441.4084 393.6809 306.1445 -4.6039 436.5966 441.2005 393.4835 307.7480 -4.6023 436.4495 441.0519 393.2931 309.3564 -4.5948 436.2336 440.8283 393.0783 310.9598 -4.5905 436.0177 440.6083 392.8808 312.5581 -4.5863 435.8172 440.4035 392.6818 314.1665 -4.5766 435.5776 440.1543 392.4599 315.7649 -4.5674 435.3620 439.9293 392.2480 317.3683 -4.5659 435.1735 439.7394 392.0265 318.9766 -4.5642 434.9661 439.5303 391.7991 320.5801 -4.5587 434.7637 439.3225 391.6088 322.1886 -4.5528 434.5628 439.1155 391.4291 323.7920 -4.5444 434.3342 438.8786 391.2576 325.3955 -4.5401 434.1144 438.6545 391.0709 327.0040 -4.5376 433.9109 438.4484 390.8562 328.6228 -4.5305 433.7311 438.2615 390.6582 330.2365 -4.5206 433.5295 438.0501 390.4434 331.8399 -4.5162 433.3188 437.8350 390.2339 333.4484 -4.5127 433.1083 437.6210 390.0350 335.0519 -4.5034 432.8956 437.3990 389.8539 336.6655 -4.4956 432.7051 437.2007 389.6385 338.2586 -4.4869 432.4992 436.9861 389.3858 339.8671 -4.4835 432.3010 436.7845 389.1582 341.4909 -4.4792 432.1041 436.5833 388.9361 343.0996 -4.4683 431.9265 436.3948 388.7100 344.6929 -4.4622 431.7325 436.1947 388.5202 346.2963 -4.4531 431.5092 435.9622 388.2984 347.9048 -4.4478 431.3431 435.7909 388.0640 349.5030 -4.4431 431.1290 435.5721 387.8691 351.1063 -4.4410 430.9048 435.3458 387.6515 352.7303 -4.4391 430.6689 435.1080 387.4275 354.3338 -4.4373 430.4749 434.9123 387.1991 355.9423 -4.4285 430.2443 434.6728 386.9703 357.5458 -4.4171 430.0252 434.4423 386.7501 359.1595 -4.4148 429.8381 434.2529 386.5188 360.7630 -4.4106 429.6107 434.0213 386.2917 362.3715 -4.4081 429.4082 433.8164 386.0794 363.9648 -4.4034 429.1681 433.5715 385.8850 365.5886 -4.3972 428.9807 433.3779 385.6972 367.1919 -4.3941 428.7581 433.1522 385.5106 368.8159 -4.3909 428.5153 432.9062 385.2974 370.4091 -4.3818 428.3110 432.6927 385.1105 372.0125 -4.3756 428.1290 432.5047 384.9532 373.6263 -4.3688 427.9238 432.2926 384.7516 375.2298 -4.3592 427.7312 432.0904 384.5367 376.8535 -4.3461 427.5211 431.8672 384.3184 378.4519 -4.3371 427.2949 431.6320 384.1258 380.0554 -4.3313 427.0755 431.4068 383.9294 381.6431 -4.3285 426.8827 431.2111 383.7276 383.2466 -4.3237 426.6477 430.9713 383.5217 384.8551 -4.3136 426.4615 430.7751 383.3069 386.4585 -4.3100 426.2938 430.6039 383.0923 388.0673 -4.3030 426.0902 430.3932 382.8887 389.6756 -4.2997 425.8425 430.1421 382.6567 391.2841 -4.2986 425.6316 429.9302 382.4321 392.8876 -4.2911 425.4072 429.6982 382.1960 394.4964 -4.2784 425.1821 429.4605 381.9504 396.1048 -4.2733 424.9995 429.2728 381.6805 397.7134 -4.2658 424.7910 429.0568 381.4744 399.3219 -4.2526 424.5740 428.8266 381.2619 400.9303 -4.2500 424.3674 428.6174 381.0535 402.5543 -4.2409 424.1739 428.4148 380.8347 404.1421 -4.2362 423.9585 428.1947 380.6194 405.7713 -4.2339 423.7269 427.9609 380.4518 407.3594 -4.2233 423.5216 427.7449 380.2519 408.9628 -4.2209 423.3253 427.5462 380.0385 410.5663 -4.2196 423.1152 427.3347 379.8090 412.1646 -4.2122 422.9332 427.1455 379.6315 413.7680 -4.2049 422.6995 426.9044 379.4406 415.3868 -4.1951 422.4621 426.6572 379.1976 416.9953 -4.1919 422.2349 426.4267 379.0071 418.5986 -4.1830 422.0548 426.2378 378.8119 420.2020 -4.1761 421.8466 426.0227 378.6291 421.8158 -4.1701 421.6242 425.7943 378.4312 423.4191 -4.1664 421.4168 425.5833 378.2203 425.0275 -4.1645 421.2011 425.3656 378.0095 426.6464 -4.1570 421.0061 425.1630 377.8327 428.2599 -4.1450 420.7937 424.9387 377.5997 429.8633 -4.1411 420.5775 424.7186 377.3939 431.4718 -4.1405 420.4112 424.5517 377.1986 433.0751 -4.1336 420.2005 424.3341 376.9884 434.6889 -4.1249 419.9829 424.1078 376.7851 436.2973 -4.1181 419.7733 423.8914 376.5719 437.9211 -4.1149 419.5753 423.6901 376.3294 439.5144 -4.1063 419.3539 423.4602 376.1101 441.1228 -4.0993 419.0960 423.1954 375.8946 442.7211 -4.0967 418.9004 422.9971 375.6569 444.3195 -4.0936 418.7058 422.7994 375.4157 445.9279 -4.0852 418.4810 422.5662 375.1897 447.5314 -4.0754 418.2674 422.3429 374.9683 449.1400 -4.0686 418.0489 422.1175 374.6982 450.7586 -4.0681 417.8177 421.8858 374.4680 452.3620 -4.0589 417.6128 421.6717 374.2499 453.9705 -4.0503 417.3988 421.4491 374.0593 455.5739 -4.0451 417.2145 421.2596 373.8622 457.1825 -4.0351 417.0095 421.0446 373.6478 458.7860 -4.0249 416.7614 420.7863 373.4413 460.3995 -4.0176 416.5058 420.5235 373.2013 462.0184 -4.0103 416.2970 420.3073 372.9690 463.6323 -4.0021 416.0821 420.0842 372.7770 465.2354 -3.9982 415.8974 419.8956 372.5888 466.8491 -3.9922 415.6935 419.6856 372.3903 468.4525 -3.9874 415.4738 419.4611 372.2087 470.0611 -3.9814 415.2356 419.2170 371.9759 471.6698 -3.9721 415.0103 418.9824 371.7632 473.2835 -3.9680 414.7884 418.7563 371.5748 474.8919 -3.9628 414.5875 418.5504 371.4113 476.4954 -3.9542 414.4197 418.3739 371.2490 478.0989 -3.9535 414.2072 418.1607 371.0789 479.7021 -3.9514 413.9883 417.9397 370.8708 481.3056 -3.9505 413.8019 417.7524 370.6754 482.9143 -3.9470 413.5698 417.5168 370.4858 484.5329 -3.9360 413.3618 417.2978 370.2704 486.1415 -3.9273 413.1246 417.0519 370.0492 487.7450 -3.9221 412.8973 416.8194 369.8705 489.3585 -3.9178 412.7146 416.6324 369.6400 490.9619 -3.9124 412.4814 416.3938 369.4196 492.5603 -3.9061 412.2612 416.1674 369.1925 494.1636 -3.9017 412.0620 415.9637 368.9099 495.7721 -3.8974 411.8451 415.7425 368.6626 497.3909 -3.8929 411.6572 415.5500 368.4466 498.9944 -3.8840 411.4498 415.3338 368.1936 500.6440 -3.8751 411.2279 415.1030 367.9669 502.2525 -3.8687 410.9894 414.8582 367.7670 503.8559 -3.8574 410.7866 414.6440 367.5536 505.4748 -3.8525 410.5931 414.4456 367.3213 507.0783 -3.8463 410.3687 414.2150 367.1147 508.6815 -3.8373 410.1439 413.9812 366.8944 510.2748 -3.8292 409.9306 413.7598 366.7009 511.8834 -3.8204 409.7017 413.5221 366.4871 513.4918 -3.8124 409.4803 413.2927 366.2634 515.0953 -3.8017 409.2362 413.0379 366.0547 516.6989 -3.7936 409.0158 412.8094 365.8409 518.3225 -3.7832 408.8000 412.5832 365.6321 519.9260 -3.7847 408.5978 412.3824 365.4496 521.5346 -3.7819 408.3726 412.1545 365.2686 523.1430 -3.7718 408.2182 411.9899 365.0428 524.7516 -3.7652 408.0414 411.8066 364.8686 526.3551 -3.7557 407.8098 411.5654 364.6968 527.9635 -3.7518 407.5665 411.3183 364.4889 529.5875 -3.7508 407.3348 411.0856 364.2941 531.1959 -3.7484 407.1255 410.8740 364.0801 532.8044 -3.7403 406.9181 410.6584 363.8842 534.4130 -3.7352 406.7134 410.4487 363.6690 536.0215 -3.7276 406.4672 410.1948 363.4459 537.6248 -3.7253 406.2713 409.9966 363.2427 539.2281 -3.7163 406.0774 409.7937 363.0175 540.8109 -3.7067 405.8930 409.5997 362.7536 542.4349 -3.7051 405.6908 409.3960 362.5332 544.0380 -3.6992 405.4476 409.1468 362.3297 545.6415 -3.6972 405.2274 408.9246 362.1202 547.2501 -3.6891 405.0388 408.7279 361.9178 548.8535 -3.6812 404.8355 408.5167 361.7221 550.4620 -3.6710 404.6246 408.2957 361.4909 552.0706 -3.6689 404.3632 408.0320 361.2290 553.6944 -3.6655 404.1406 407.8062 360.9565 555.2979 -3.6556 403.9275 407.5831 360.7452 556.9116 -3.6504 403.7207 407.3711 360.4889 558.5149 -3.6446 403.4813 407.1259 360.2676 560.1235 -3.6375 403.2469 406.8845 360.0922 561.7270 -3.6302 403.0655 406.6957 359.9144 563.3355 -3.6208 402.8563 406.4770 359.7361 564.9595 -3.6108 402.6476 406.2584 359.5344 566.5629 -3.6104 402.4254 406.0358 359.3876 568.1764 -3.6049 402.2342 405.8391 359.2085 569.7748 -3.5976 402.0380 405.6356 359.0217 571.3783 -3.5860 401.8212 405.4072 358.8393 572.9661 -3.5807 401.6309 405.2116 358.5898 574.5645 -3.5791 401.4246 405.0038 358.3666 576.1731 -3.5745 401.2090 404.7836 358.1616 577.7918 -3.5718 400.9951 404.5669 357.9384 579.4004 -3.5672 400.7756 404.3428 357.7369 581.0038 -3.5618 400.5515 404.1133 357.5256 582.6071 -3.5557 400.3441 403.8998 357.3012 584.2158 -3.5473 400.1348 403.6821 357.0659 585.8193 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