DTA measure 1fazis_pbupdown3 Date: 2026429:911 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.61 s Mass = 1149.800 mg data_number = 1343 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2205 0.5576 196.1629 195.6053 248.1530 2.0075 0.5588 196.4272 195.8684 248.1600 2.8458 0.5600 196.7139 196.1540 248.1749 3.6015 0.5621 196.9693 196.4072 248.1876 4.4598 0.5627 197.2629 196.7002 248.2055 5.2160 0.5637 197.5228 196.9591 248.2166 6.0543 0.5642 197.8124 197.2482 248.2416 6.8208 0.5646 198.0775 197.5129 248.2589 7.6790 0.5637 198.3717 197.8080 248.2841 8.4143 0.5631 198.6193 198.0562 248.3145 9.2730 0.5633 198.9028 198.3396 248.3456 10.0293 0.5636 199.1516 198.5880 248.3680 10.8670 0.5639 199.4353 198.8713 248.3938 11.6535 0.5637 199.7030 199.1393 248.4230 12.4508 0.5648 199.9694 199.4046 248.4592 13.2788 0.5659 200.2405 199.6746 248.4931 14.0453 0.5657 200.4925 199.9268 248.5353 14.9033 0.5657 200.7770 200.2112 248.5884 15.6490 0.5655 201.0217 200.4562 248.6307 16.5078 0.5652 201.3165 200.7513 248.6863 17.2743 0.5664 201.5706 201.0043 248.7380 18.1118 0.5684 201.8570 201.2886 248.7995 18.8678 0.5685 202.1028 201.5344 248.8564 19.6958 0.5670 202.3724 201.8054 248.9211 20.4930 0.5654 202.6255 202.0601 249.0032 21.3005 0.5655 202.8808 202.3153 249.0909 22.1173 0.5653 203.1347 202.5694 249.1847 22.8838 0.5647 203.3818 202.8171 249.2701 23.7425 0.5646 203.6553 203.0906 249.3730 24.5090 0.5650 203.8918 203.3268 249.4597 25.3363 0.5642 204.1596 203.5955 249.5545 26.1128 0.5630 204.4127 203.8497 249.6526 26.9408 0.5626 204.6767 204.1140 249.7523 27.7073 0.5627 204.9203 204.3576 249.8728 28.5345 0.5637 205.1953 204.6315 249.9909 29.3623 0.5639 205.4613 204.8973 250.0997 30.1185 0.5621 205.6998 205.1377 250.2115 30.9875 0.5602 205.9686 205.4084 250.3365 31.7230 0.5585 206.2039 205.6454 250.4527 32.5810 0.5571 206.4784 205.9213 250.5933 33.3373 0.5561 206.7097 206.1536 250.7189 34.1755 0.5555 206.9638 206.4083 250.8633 34.9625 0.5539 207.2159 206.6620 250.9991 35.7700 0.5537 207.4734 206.9197 251.1508 36.5868 0.5535 207.7210 207.1675 251.3071 37.3635 0.5524 207.9476 207.3952 251.4558 38.2120 0.5515 208.2046 207.6531 251.6186 38.9785 0.5496 208.4326 207.8830 251.7599 39.8058 0.5470 208.6828 208.1359 251.9115 40.6028 0.5453 208.9253 208.3800 252.0601 41.3898 0.5438 209.1696 208.6258 252.2183 42.2178 0.5426 209.4170 208.8745 252.3741 42.9735 0.5409 209.6494 209.1085 252.5191 43.8010 0.5398 209.9014 209.3615 252.6859 44.5675 0.5383 210.1318 209.5935 252.8369 45.4160 0.5369 210.3841 209.8472 253.0083 46.1820 0.5351 210.6220 210.0869 253.1502 47.0095 0.5316 210.8682 210.3366 253.3055 47.8068 0.5285 211.1010 210.5725 253.4515 48.5938 0.5268 211.3377 210.8108 253.6050 49.4218 0.5251 211.5902 211.0651 253.7666 50.1873 0.5218 211.8316 211.3099 253.9345 51.0358 0.5195 212.0728 211.5533 254.1052 51.8023 0.5172 212.2830 211.7658 254.2695 52.6303 0.5129 212.5226 212.0096 254.4307 53.4165 0.5098 212.7529 212.2432 254.5861 54.2135 0.5063 212.9812 212.4749 254.7344 55.0415 0.5039 213.2289 212.7250 254.8897 55.8080 0.5023 213.4433 212.9409 255.0289 56.6558 0.4995 213.6803 213.1808 255.1876 57.4015 0.4966 213.8967 213.4001 255.3285 58.2500 0.4925 214.1418 213.6493 255.4884 59.0473 0.4893 214.3734 213.8841 255.6318 59.8438 0.4869 214.6070 214.1200 255.7770 60.6715 0.4825 214.8443 214.3618 255.9091 61.4380 0.4793 215.0670 214.5877 256.0398 62.2558 0.4758 215.3015 214.8257 256.1800 63.0318 0.4717 215.5225 215.0509 256.3057 63.8800 0.4690 215.7749 215.3059 256.4512 64.6465 0.4662 215.9831 215.5169 256.5837 65.4745 0.4634 216.2143 215.7510 256.7214 66.2715 0.4601 216.4423 215.9822 256.8613 67.0680 0.4556 216.6690 216.2134 256.9858 67.8858 0.4514 216.8988 216.4474 257.1167 68.6625 0.4482 217.1272 216.6790 257.2382 69.5108 0.4448 217.3701 216.9252 257.3711 70.2765 0.4431 217.5858 217.1427 257.4930 71.1045 0.4402 217.8103 217.3701 257.6152 71.9018 0.4364 218.0287 217.5923 257.7379 72.6990 0.4333 218.2504 217.8172 257.8656 73.5158 0.4305 218.4881 218.0576 257.9967 74.2925 0.4279 218.7128 218.2849 258.1217 75.1410 0.4251 218.9616 218.5365 258.2577 75.9075 0.4227 219.1743 218.7516 258.3770 76.7353 0.4191 219.4049 218.9858 258.4988 77.5318 0.4150 219.6272 219.2122 258.6208 78.3290 0.4104 219.8469 219.4365 258.7408 79.1468 0.4068 220.0792 219.6724 258.8685 79.9235 0.4041 220.3090 219.9048 258.9991 80.7715 0.3995 220.5428 220.1433 259.1336 81.5375 0.3941 220.7471 220.3530 259.2594 82.3655 0.3895 220.9741 220.5846 259.3930 83.1628 0.3856 221.1867 220.8011 259.5251 83.9593 0.3810 221.3989 221.0179 259.6509 84.7768 0.3781 221.6350 221.2569 259.7769 85.5535 0.3741 221.8485 221.4744 259.8897 86.4020 0.3679 222.0764 221.7085 260.0137 87.1785 0.3647 222.2922 221.9275 260.1366 87.9955 0.3624 222.5166 222.1542 260.2595 88.8030 0.3576 222.7386 222.3810 260.3817 89.5900 0.3530 222.9509 222.5979 260.5044 90.4180 0.3484 223.1830 222.8346 260.6307 91.1838 0.3433 223.3941 223.0509 260.7499 92.0423 0.3406 223.6295 223.2889 260.8771 92.8088 0.3368 223.8382 223.5014 261.0008 93.6265 0.3311 224.0483 223.7172 261.1337 94.4330 0.3254 224.2613 223.9359 261.2575 95.2303 0.3214 224.4737 224.1522 261.3868 96.0583 0.3172 224.6905 224.3732 261.5208 96.8145 0.3143 224.8928 224.5785 261.6373 97.6830 0.3087 225.1135 224.8048 261.7616 98.4388 0.3044 225.3122 225.0078 261.8788 99.2668 0.2998 225.5255 225.2257 262.0066 100.0640 0.2951 225.7285 225.4334 262.1291 100.8613 0.2918 225.9491 225.6574 262.2460 101.6885 0.2883 226.1748 225.8865 262.3701 102.4548 0.2843 226.3708 226.0865 262.4846 103.3135 0.2799 226.5883 226.3084 262.6079 104.0493 0.2760 226.7872 226.5113 262.7241 104.8975 0.2699 227.0047 226.7348 262.8625 105.6633 0.2636 227.2123 226.9488 262.9721 106.4810 0.2584 227.4449 227.1865 263.0975 107.2783 0.2533 227.6540 227.4007 263.2185 108.0748 0.2499 227.8587 227.6088 263.3360 108.8923 0.2434 228.0900 227.8466 263.4500 109.6485 0.2390 228.3007 228.0618 263.5617 110.5175 0.2356 228.5275 228.2919 263.6942 111.2425 0.2336 228.7094 228.4759 263.8124 112.0905 0.2296 228.9251 228.6955 263.9430 112.8673 0.2247 229.1248 228.9001 264.0598 113.6850 0.2194 229.3316 229.1123 264.2026 114.4815 0.2138 229.5288 229.3151 264.3331 115.2785 0.2090 229.7388 229.5298 264.4641 116.0963 0.2061 229.9497 229.7437 264.6030 116.8628 0.2030 230.1515 229.9485 264.7355 117.7215 0.1984 230.3817 230.1833 264.8838 118.4568 0.1941 230.5743 230.3803 265.0111 119.3048 0.1875 230.7803 230.5928 265.1681 120.0713 0.1819 230.9627 230.7808 265.3073 120.8993 0.1768 231.1783 231.0015 265.4654 121.6965 0.1729 231.3817 231.2089 265.6141 122.4828 0.1671 231.5817 231.4147 265.7534 123.3208 0.1615 231.7848 231.6233 265.9139 124.0770 0.1565 231.9708 231.8142 266.0488 124.9358 0.1528 232.1834 232.0306 266.2078 125.7018 0.1487 232.3752 232.2264 266.3532 126.5293 0.1448 232.5890 232.4442 266.5169 127.2958 0.1392 232.7758 232.6366 266.6705 128.1135 0.1359 232.9812 232.8453 266.8263 128.9210 0.1322 233.1778 233.0456 266.9722 129.7073 0.1290 233.3773 233.2483 267.1102 130.5350 0.1244 233.5822 233.4578 267.2614 131.3015 0.1193 233.7813 233.6620 267.4028 132.1603 0.1143 233.9969 233.8826 267.5601 132.9258 0.1102 234.1847 234.0744 267.7052 133.7435 0.1047 234.3908 234.2861 267.8599 134.5510 0.1007 234.5870 234.4863 268.0153 135.3380 0.0963 234.7751 234.6788 268.1677 136.1660 0.0911 234.9781 234.8871 268.3199 136.9315 0.0862 235.1655 235.0793 268.4583 137.7903 0.0824 235.3761 235.2937 268.6084 138.5260 0.0811 235.5509 235.4699 268.7419 139.3743 0.0766 235.7609 235.6843 268.8984 140.1503 0.0723 235.9579 235.8856 269.0359 140.9680 0.0692 236.1723 236.1031 269.1780 141.7653 0.0677 236.3637 236.2960 269.3036 142.5623 0.0696 236.5599 236.4903 269.4380 143.3895 0.0678 236.7689 236.7012 269.5841 144.1560 0.0599 236.9529 236.8930 269.7099 145.0148 0.0528 237.1559 237.1031 269.8511 145.7813 0.0474 237.3403 237.2930 269.9825 146.6083 0.0395 237.5418 237.5023 270.1240 147.4055 0.0328 237.7484 237.7156 270.2516 148.1925 0.0266 237.9402 237.9136 270.3686 149.0308 0.0214 238.1373 238.1159 270.5023 149.7865 0.0162 238.3148 238.2986 270.6324 150.6550 0.0098 238.5328 238.5231 270.7577 151.4113 0.0053 238.7240 238.7188 270.8732 152.2495 0.0011 238.9247 238.9236 271.0020 153.0363 -0.0025 239.1162 239.1187 271.1264 153.8328 -0.0079 239.3116 239.3195 271.2518 154.6608 -0.0134 239.5085 239.5219 271.3772 155.4273 -0.0189 239.6902 239.7092 271.4949 156.2860 -0.0237 239.8874 239.9111 271.6245 157.0415 -0.0293 240.0643 240.0936 271.7504 157.8795 -0.0340 240.2626 240.2967 271.8790 158.6665 -0.0375 240.4454 240.4829 271.9924 159.4638 -0.0403 240.6360 240.6763 272.1161 160.2918 -0.0456 240.8332 240.8788 272.2389 161.0573 -0.0492 241.0114 241.0607 272.3589 161.9160 -0.0537 241.2134 241.2671 272.4869 162.6723 -0.0586 241.3912 241.4498 272.5937 163.5105 -0.0633 241.5803 241.6436 272.7222 164.3073 -0.0669 241.7745 241.8414 272.8374 165.1040 -0.0706 241.9785 242.0491 272.9572 165.9218 -0.0750 242.1720 242.2470 273.0802 166.6985 -0.0788 242.3506 242.4294 273.1998 167.5463 -0.0804 242.5463 242.6267 273.3186 168.3125 -0.0855 242.7260 242.8115 273.4209 169.1405 -0.0904 242.9236 243.0140 273.5472 169.9375 -0.0942 243.1200 243.2141 273.6606 170.7238 -0.0987 243.3030 243.4017 273.7733 171.5518 -0.1037 243.4984 243.6020 273.8889 172.3080 -0.1085 243.6839 243.7924 273.9995 173.1565 -0.1135 243.8825 243.9960 274.1256 173.9023 -0.1164 244.0586 244.1750 274.2354 174.7500 -0.1192 244.2508 244.3700 274.3685 175.5165 -0.1242 244.4270 244.5512 274.4861 176.3445 -0.1277 244.6276 244.7554 274.6127 177.1315 -0.1315 244.8145 244.9461 274.7410 177.9283 -0.1359 244.9998 245.1357 274.8656 178.7558 -0.1421 245.1915 245.3336 274.9962 179.5120 -0.1465 245.3618 245.5083 275.1152 180.3708 -0.1492 245.5572 245.7064 275.2525 181.1363 -0.1538 245.7348 245.8886 275.3791 181.9643 -0.1598 245.9240 246.0838 275.5178 182.7615 -0.1617 246.1067 246.2684 275.6598 183.5485 -0.1648 246.2881 246.4529 275.7965 184.3553 -0.1708 246.4677 246.6385 275.9499 185.1420 -0.1760 246.6543 246.8303 276.0801 185.9700 -0.1814 246.8491 247.0305 276.2100 186.7365 -0.1863 247.0264 247.2126 276.3384 187.5950 -0.1915 247.2137 247.4052 276.4836 188.3505 -0.1962 247.3881 247.5843 276.6138 189.1785 -0.2015 247.5880 247.7895 276.7618 189.9758 -0.2045 247.7701 247.9746 276.9005 190.7730 -0.2097 247.9370 248.1468 277.0400 191.5898 -0.2149 248.1156 248.3305 277.1778 192.3665 -0.2177 248.2913 248.5090 277.3143 193.2150 -0.2221 248.4872 248.7093 277.4602 193.9815 -0.2271 248.6652 248.8924 277.6033 194.8088 -0.2300 248.8506 249.0806 277.7473 195.6058 -0.2342 249.0393 249.2735 277.8852 196.4030 -0.2379 249.2253 249.4633 278.0159 197.2208 -0.2424 249.4146 249.6569 278.1561 197.9975 -0.2467 249.5828 249.8295 278.2877 198.8450 -0.2507 249.7705 250.0212 278.4335 199.6115 -0.2557 249.9471 250.2028 278.5753 200.4395 -0.2611 250.1365 250.3976 278.7296 201.2368 -0.2659 250.3087 250.5746 278.8690 202.0333 -0.2681 250.4806 250.7487 279.0086 202.8508 -0.2734 250.6562 250.9295 279.1522 203.6275 -0.2785 250.8323 251.1108 279.2909 204.4555 -0.2833 251.0258 251.3090 279.4400 205.2213 -0.2875 251.1948 251.4823 279.5798 206.0695 -0.2920 251.3812 251.6732 279.7335 206.8463 -0.2953 251.5575 251.8528 279.8725 207.6640 -0.2985 251.7322 252.0308 280.0167 208.4610 -0.3039 251.9021 252.2060 280.1606 209.2575 -0.3088 252.0786 252.3873 280.3070 210.0855 -0.3135 252.2563 252.5698 280.4643 210.8520 -0.3182 252.4254 252.7437 280.6066 211.7005 -0.3226 252.6176 252.9402 280.7512 212.4458 -0.3278 252.7774 253.1052 280.8681 213.2940 -0.3321 252.9633 253.2953 281.0112 214.0605 -0.3360 253.1279 253.4639 281.1524 214.8885 -0.3404 253.3128 253.6532 281.3042 215.6858 -0.3461 253.4874 253.8335 281.4459 216.4828 -0.3499 253.6650 254.0149 281.5860 217.2998 -0.3548 253.8411 254.1959 281.7200 218.0765 -0.3586 254.0206 254.3792 281.8523 218.9250 -0.3614 254.2111 254.5725 282.0012 219.7018 -0.3661 254.3789 254.7449 282.1367 220.5193 -0.3720 254.5577 254.9296 282.2751 221.3260 -0.3762 254.7397 255.1158 282.4127 222.1130 -0.3813 254.9106 255.2919 282.5359 222.9103 -0.3859 255.0898 255.4757 282.6700 223.7075 -0.3907 255.2602 255.6509 282.7988 224.5348 -0.3952 255.4473 255.8425 282.9325 225.3010 -0.3995 255.6299 256.0293 283.0628 226.1495 -0.4037 255.8232 256.2269 283.2094 226.9263 -0.4089 255.9910 256.3999 283.3353 227.7435 -0.4131 256.1697 256.5828 283.4756 228.5403 -0.4168 256.3399 256.7568 283.6164 229.3375 -0.4196 256.5111 256.9307 283.7474 230.1758 -0.4250 256.6967 257.1218 283.8841 230.9315 -0.4286 256.8525 257.2811 284.0132 231.7898 -0.4328 257.0367 257.4695 284.1512 232.5563 -0.4380 257.1986 257.6366 284.2827 233.3740 -0.4444 257.3809 257.8253 284.4316 234.1713 -0.4508 257.5565 258.0073 284.5668 234.9675 -0.4557 257.7369 258.1926 284.7055 235.7545 -0.4601 257.9144 258.3745 284.8427 236.5415 -0.4617 258.0805 258.5422 284.9704 237.3695 -0.4662 258.2565 258.7227 285.1080 238.1355 -0.4696 258.4150 258.8846 285.2338 238.9835 -0.4730 258.6000 259.0730 285.3787 239.7603 -0.4772 258.7655 259.2427 285.5112 240.5780 -0.4803 258.9406 259.4210 285.6460 241.3443 -0.4835 259.0998 259.5833 285.7785 242.1715 -0.4887 259.2732 259.7619 285.9153 242.9688 -0.4931 259.4450 259.9380 286.0444 243.7660 -0.4976 259.6201 260.1176 286.1703 244.5833 -0.5032 259.7989 260.3021 286.3093 245.3595 -0.5068 259.9612 260.4680 286.4355 246.2080 -0.5113 260.1413 260.6526 286.5699 246.9643 -0.5154 260.2935 260.8089 286.6896 247.8020 -0.5200 260.4689 260.9889 286.8229 248.5885 -0.5230 260.6484 261.1714 286.9567 249.3858 -0.5265 260.8155 261.3420 287.0879 250.2138 -0.5320 261.0001 261.5321 287.2219 250.9900 -0.5362 261.1603 261.6965 287.3532 251.8073 -0.5394 261.3291 261.8685 287.4942 252.5738 -0.5432 261.4872 262.0304 287.6100 253.4325 -0.5479 261.6769 262.2248 287.7372 254.1888 -0.5532 261.8471 262.4003 287.8464 255.0158 -0.5589 262.0245 262.5834 287.9797 255.8130 -0.5636 262.1936 262.7572 288.1072 256.6103 -0.5683 262.3587 262.9270 288.2293 257.4383 -0.5734 262.5310 263.1044 288.3655 258.1935 -0.5789 262.6892 263.2680 288.4821 259.0625 -0.5818 262.8762 263.4580 288.6237 259.8188 -0.5860 263.0428 263.6288 288.7356 260.6465 -0.5912 263.2162 263.8074 288.8615 261.4430 -0.5963 263.3803 263.9765 288.9829 262.2403 -0.5994 263.5448 264.1442 289.1152 263.0683 -0.6024 263.7167 264.3192 289.2403 263.8245 -0.6075 263.8748 264.4823 289.3576 264.6928 -0.6121 264.0601 264.6722 289.4947 265.4488 -0.6166 264.2339 264.8506 289.6148 266.2768 -0.6224 264.4126 265.0350 289.7467 267.0740 -0.6282 264.5772 265.2054 289.8655 267.8808 -0.6330 264.7534 265.3864 289.9893 268.6983 -0.6374 264.9235 265.5609 290.1231 269.4648 -0.6407 265.0837 265.7244 290.2473 270.3233 -0.6455 265.2595 265.9050 290.3930 271.0890 -0.6499 265.4212 266.0710 290.5183 271.9170 -0.6536 265.6084 266.2620 290.6571 272.7040 -0.6579 265.7722 266.4300 290.7807 273.5115 -0.6618 265.9571 266.6188 290.9081 274.3285 -0.6668 266.1265 266.7933 291.0312 275.0948 -0.6707 266.2820 266.9527 291.1531 275.9535 -0.6757 266.4670 267.1427 291.2827 276.7200 -0.6805 266.6168 267.2973 291.3924 277.5480 -0.6850 266.7835 267.4685 291.5150 278.3340 -0.6889 266.9404 267.6293 291.6330 279.1415 -0.6928 267.1073 267.8001 291.7586 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