DTA measure 1fazis_pbupdown4 Date: 2026429:1025 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.96 s Mass = 1149.800 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4071 -0.6448 205.0133 205.6581 196.2755 4.0119 -0.6451 205.0125 205.6576 196.2941 5.6074 -0.6462 205.0056 205.6518 196.2974 7.2121 -0.6470 205.0007 205.6477 196.2992 8.8120 -0.6498 204.9982 205.6480 196.3140 10.4175 -0.6515 204.9942 205.6458 196.3180 12.0224 -0.6536 204.9906 205.6442 196.3286 13.6229 -0.6550 204.9985 205.6535 196.3469 15.2276 -0.6537 205.0039 205.6576 196.3727 16.8378 -0.6555 204.9887 205.6443 196.3966 18.4279 -0.6559 204.9699 205.6258 196.4351 20.0275 -0.6559 204.9751 205.6311 196.4797 21.6484 -0.6559 204.9953 205.6511 196.5341 23.2534 -0.6571 205.0055 205.6626 196.5926 24.8636 -0.6577 204.9964 205.6541 196.6541 26.4690 -0.6592 204.9929 205.6521 196.7377 28.0584 -0.6615 204.9890 205.6505 196.8177 29.6635 -0.6627 204.9888 205.6515 196.9056 31.2689 -0.6643 204.9811 205.6454 197.0124 32.8788 -0.6634 204.9811 205.6445 197.1280 34.4998 -0.6652 204.9890 205.6542 197.2521 36.1046 -0.6669 204.9863 205.6532 197.3800 37.6993 -0.6674 204.9965 205.6639 197.5171 39.3049 -0.6663 205.0015 205.6678 197.6466 40.9148 -0.6652 205.0038 205.6691 197.7752 42.5204 -0.6688 205.0102 205.6789 197.9223 44.1304 -0.6703 205.0162 205.6864 198.0788 45.7359 -0.6725 205.0213 205.6938 198.2387 47.3563 -0.6758 205.0268 205.7026 198.4187 48.9714 -0.6769 205.0223 205.6992 198.5864 50.5770 -0.6768 205.0256 205.7024 198.7649 52.1869 -0.6778 205.0332 205.7111 198.9239 53.7923 -0.6786 205.0397 205.7183 199.0854 55.4025 -0.6792 205.0581 205.7373 199.2570 57.0078 -0.6810 205.0718 205.7528 199.4383 58.6335 -0.6840 205.0800 205.7640 199.6195 60.2386 -0.6847 205.0833 205.7680 199.8084 61.8338 -0.6870 205.0951 205.7821 199.9978 63.4440 -0.6887 205.1087 205.7974 200.1889 65.0443 -0.6896 205.1225 205.8122 200.3723 66.6543 -0.6905 205.1335 205.8240 200.5572 68.2494 -0.6904 205.1384 205.8288 200.7480 69.8544 -0.6927 205.1536 205.8464 200.9418 71.4496 -0.6943 205.1702 205.8645 201.1455 73.0649 -0.6956 205.1798 205.8754 201.3388 74.6699 -0.6985 205.2007 205.8993 201.5296 76.2754 -0.7015 205.2183 205.9198 201.7107 77.8803 -0.7033 205.2457 205.9490 201.9052 79.4808 -0.7052 205.2755 205.9807 202.0826 81.0855 -0.7064 205.2948 206.0012 202.2731 82.6910 -0.7070 205.3124 206.0194 202.4731 84.3063 -0.7102 205.3542 206.0644 202.6609 85.9009 -0.7131 205.3786 206.0917 202.8341 87.5065 -0.7149 205.4102 206.1251 203.0232 89.1164 -0.7135 205.4319 206.1454 203.2170 90.7220 -0.7155 205.4542 206.1697 203.3960 92.3218 -0.7175 205.4873 206.2048 203.5672 93.9318 -0.7200 205.5180 206.2380 203.7424 95.5374 -0.7216 205.5460 206.2676 203.9120 97.1626 -0.7234 205.5849 206.3083 204.1040 98.7526 -0.7260 205.6139 206.3399 204.2770 100.3629 -0.7275 205.6546 206.3821 204.4552 101.9681 -0.7288 205.6838 206.4126 204.6424 103.5785 -0.7300 205.7168 206.4468 204.8365 105.1889 -0.7296 205.7579 206.4875 205.0410 106.7941 -0.7301 205.7870 206.5171 205.2373 108.4041 -0.7322 205.8223 206.5545 205.4444 109.9944 -0.7347 205.8585 206.5932 205.6242 111.6196 -0.7339 205.9036 206.6375 205.8136 113.2253 -0.7360 205.9499 206.6858 206.0207 114.8353 -0.7381 205.9932 206.7313 206.2144 116.4405 -0.7411 206.0545 206.7956 206.4214 118.0406 -0.7419 206.0955 206.8374 206.6134 119.6456 -0.7425 206.1368 206.8793 206.8094 121.2511 -0.7427 206.1868 206.9295 206.9980 122.8616 -0.7436 206.2536 206.9972 207.1790 124.4821 -0.7459 206.3179 207.0637 207.3607 126.0924 -0.7484 206.3676 207.1160 207.5582 127.6978 -0.7502 206.4290 207.1792 207.7486 129.2924 -0.7526 206.4890 207.2416 207.9244 130.8980 -0.7525 206.5281 207.2806 208.1174 132.4926 -0.7537 206.5751 207.3288 208.2997 134.0983 -0.7542 206.6334 207.3876 208.4797 135.6979 -0.7544 206.6978 207.4522 208.6703 137.3036 -0.7542 206.7616 207.5158 208.8396 138.9186 -0.7541 206.8386 207.5926 209.0242 140.5239 -0.7533 206.9100 207.6633 209.2282 142.1138 -0.7535 206.9575 207.7110 209.4205 143.7189 -0.7548 207.0237 207.7785 209.6193 145.3243 -0.7561 207.0962 207.8523 209.8204 146.9341 -0.7577 207.1559 207.9137 210.0155 148.5396 -0.7595 207.2275 207.9870 210.2151 150.1498 -0.7592 207.2946 208.0539 210.4242 151.7649 -0.7572 207.3571 208.1143 210.6463 153.3705 -0.7575 207.4293 208.1868 210.8602 154.9804 -0.7594 207.4943 208.2538 211.0681 156.5856 -0.7548 207.5614 208.3162 211.2744 158.1806 -0.7444 207.6296 208.3740 211.4791 159.7856 -0.7356 207.7037 208.4393 211.6837 161.3911 -0.7395 207.8067 208.5462 211.8974 163.0011 -0.7475 207.8905 208.6379 212.1008 164.6221 -0.7537 207.9747 208.7284 212.3081 166.2320 -0.7562 208.0492 208.8054 212.5082 167.8378 -0.7571 208.1262 208.8833 212.7023 169.4476 -0.7590 208.2061 208.9651 212.9013 171.0534 -0.7603 208.2845 209.0448 213.0939 172.6581 -0.7607 208.3574 209.1181 213.2912 174.2689 -0.7637 208.4342 209.1979 213.4884 175.8891 -0.7639 208.5112 209.2751 213.6851 177.4994 -0.7657 208.5963 209.3620 213.8801 179.1099 -0.7669 208.6911 209.4580 214.0758 180.7151 -0.7651 208.7854 209.5505 214.2693 182.3255 -0.7643 208.8770 209.6413 214.4669 183.9355 -0.7649 208.9616 209.7264 214.6513 185.5411 -0.7636 209.0569 209.8205 214.8298 187.1459 -0.7620 209.1543 209.9162 215.0251 188.7568 -0.7616 209.2536 210.0152 215.2049 190.3615 -0.7616 209.3573 210.1188 215.3832 191.9718 -0.7623 209.4548 210.2171 215.5688 193.5771 -0.7635 209.5562 210.3198 215.7530 195.1718 -0.7615 209.6550 210.4164 215.9484 196.7774 -0.7609 209.7445 210.5054 216.1404 198.3770 -0.7600 209.8410 210.6010 216.3239 199.9666 -0.7580 209.9529 210.7109 216.5130 201.5824 -0.7576 210.0681 210.8257 216.7182 203.1769 -0.7562 210.1669 210.9230 216.9140 204.7774 -0.7572 210.2594 211.0166 217.1112 206.3874 -0.7566 210.3605 211.1172 217.3087 207.9876 -0.7562 210.4750 211.2312 217.5147 209.5876 -0.7552 210.5900 211.3452 217.7183 211.1976 -0.7546 210.6891 211.4437 217.9355 212.7879 -0.7548 210.7974 211.5522 218.1391 214.3978 -0.7538 210.9012 211.6549 218.3420 216.0189 -0.7533 211.0093 211.7626 218.5516 217.6236 -0.7537 211.1215 211.8753 218.7567 219.2336 -0.7529 211.2332 211.9860 218.9653 220.8239 -0.7516 211.3460 212.0976 219.1755 222.4338 -0.7495 211.4656 212.2152 219.3828 224.0391 -0.7493 211.5842 212.3335 219.5793 225.6494 -0.7502 211.6999 212.4500 219.7790 227.2545 -0.7495 211.8153 212.5648 219.9788 228.8650 -0.7469 211.9342 212.6811 220.1793 230.4544 -0.7444 212.0565 212.8009 220.3724 232.0806 -0.7458 212.1762 212.9221 220.5776 233.6854 -0.7450 212.2940 213.0390 220.7770 235.3064 -0.7431 212.4026 213.1457 220.9720 236.9164 -0.7414 212.5214 213.2628 221.1869 238.5216 -0.7391 212.6464 213.3856 221.3851 240.1320 -0.7396 212.7776 213.5172 221.5735 241.7370 -0.7391 212.9121 213.6512 221.7609 243.3323 -0.7371 213.0379 213.7750 221.9431 244.9421 -0.7377 213.1584 213.8961 222.1257 246.5478 -0.7368 213.2915 214.0283 222.3195 248.1578 -0.7370 213.4184 214.1554 222.5105 249.7783 -0.7347 213.5454 214.2801 222.7058 251.3836 -0.7332 213.6825 214.4157 222.9170 252.9936 -0.7309 213.8121 214.5430 223.1040 254.6044 -0.7306 213.9580 214.6886 223.3050 256.2143 -0.7294 214.0818 214.8112 223.4926 257.8199 -0.7278 214.2236 214.9513 223.6783 259.4248 -0.7266 214.3690 215.0956 223.8456 261.0405 -0.7250 214.5092 215.2342 224.0455 262.6404 -0.7237 214.6396 215.3633 224.2403 264.2404 -0.7228 214.7767 215.4995 224.4377 265.8458 -0.7221 214.9148 215.6370 224.6434 267.4354 -0.7211 215.0390 215.7602 224.8466 269.0409 -0.7201 215.1794 215.8995 225.0556 270.6456 -0.7178 215.3166 216.0344 225.2621 272.2513 -0.7153 215.4517 216.1670 225.4749 273.8715 -0.7135 215.5953 216.3088 225.6918 275.4768 -0.7109 215.7402 216.4511 225.9114 277.0769 -0.7101 215.8851 216.5952 226.1238 278.6869 -0.7100 216.0239 216.7339 226.3425 280.2925 -0.7100 216.1845 216.8944 226.5592 281.9024 -0.7084 216.3248 217.0332 226.7810 283.4928 -0.7072 216.4548 217.1620 226.9950 285.0975 -0.7051 216.5921 217.2972 227.2162 286.7230 -0.7052 216.7384 217.4436 227.4402 288.3285 -0.7033 216.8836 217.5869 227.6488 289.9230 -0.7020 217.0289 217.7309 227.8647 291.5284 -0.7006 217.1757 217.8763 228.0918 293.1386 -0.7000 217.3317 218.0317 228.3164 294.7435 -0.6994 217.4893 218.1886 228.5414 296.3491 -0.6969 217.6423 218.3392 228.7506 297.9590 -0.6955 217.7933 218.4888 228.9593 299.5491 -0.6957 217.9491 218.6448 229.1735 301.1798 -0.6939 218.0969 218.7909 229.3938 302.7848 -0.6910 218.2595 218.9504 229.6046 304.3954 -0.6911 218.4068 219.0979 229.8233 305.9848 -0.6901 218.5546 219.2447 230.0258 307.5951 -0.6904 218.7003 219.3907 230.2234 309.2004 -0.6895 218.8536 219.5431 230.4412 310.8055 -0.6892 219.0159 219.7051 230.6398 312.4160 -0.6894 219.1827 219.8721 230.8523 314.0363 -0.6876 219.3447 220.0323 231.0541 315.6265 -0.6853 219.5024 220.1877 231.2538 317.2466 -0.6858 219.6698 220.3556 231.4588 318.8524 -0.6860 219.8355 220.5215 231.6729 320.4623 -0.6842 220.0084 220.6926 231.8742 322.0675 -0.6816 220.1638 220.8454 232.0808 323.6676 -0.6804 220.3239 221.0042 232.2906 325.2521 -0.6797 220.4766 221.1563 232.4852 326.8525 -0.6784 220.6299 221.3083 232.6933 328.4521 -0.6787 220.7999 221.4786 232.9029 330.0681 -0.6784 220.9712 221.6497 233.1032 331.6780 -0.6763 221.1358 221.8121 233.3067 333.2784 -0.6752 221.3004 221.9756 233.5120 334.8783 -0.6726 221.4573 222.1299 233.7131 336.4889 -0.6705 221.6249 222.2954 233.9048 338.0836 -0.6710 221.7811 222.4522 234.0981 339.6888 -0.6697 221.9546 222.6243 234.2916 341.2941 -0.6674 222.1303 222.7977 234.4986 342.8989 -0.6672 222.3013 222.9685 234.6987 344.5096 -0.6670 222.4796 223.1466 234.8908 346.1248 -0.6656 222.6456 223.3112 235.0715 347.7149 -0.6657 222.8040 223.4697 235.2577 349.3353 -0.6635 222.9792 223.6427 235.4472 350.9456 -0.6605 223.1536 223.8141 235.6412 352.5509 -0.6605 223.3351 223.9956 235.8401 354.1610 -0.6607 223.5024 224.1632 236.0245 355.7665 -0.6591 223.6703 224.3294 236.2219 357.3764 -0.6574 223.8523 224.5097 236.4174 358.9819 -0.6557 224.0219 224.6776 236.6127 360.6023 -0.6540 224.1967 224.8507 236.8046 362.2128 -0.6534 224.3695 225.0229 236.9855 363.8179 -0.6520 224.5451 225.1970 237.1635 365.4280 -0.6530 224.7306 225.3836 237.3472 367.0335 -0.6521 224.9123 225.5645 237.5403 368.6434 -0.6498 225.0889 225.7387 237.7165 370.2490 -0.6480 225.2743 225.9224 237.9012 371.8693 -0.6442 225.4527 226.0969 238.1035 373.4794 -0.6435 225.6379 226.2814 238.3098 375.0849 -0.6419 225.8234 226.4653 238.5197 376.6948 -0.6407 226.0005 226.6412 238.7259 378.3004 -0.6418 226.1729 226.8146 238.9336 379.9104 -0.6391 226.3583 226.9974 239.1440 381.5159 -0.6372 226.5369 227.1741 239.3532 383.1363 -0.6369 226.7184 227.3552 239.5794 384.7464 -0.6378 226.8888 227.5266 239.7941 386.3570 -0.6390 227.0626 227.7016 240.0278 387.9464 -0.6403 227.2552 227.8955 240.2387 389.5419 -0.6392 227.4546 228.0937 240.4524 391.1466 -0.6378 227.6323 228.2701 240.6735 392.7519 -0.6380 227.8120 228.4500 240.8821 394.3366 -0.6377 227.9918 228.6295 241.1011 395.9414 -0.6354 228.1735 228.8089 241.3127 397.5574 -0.6366 228.3576 228.9942 241.5277 399.1621 -0.6368 228.5403 229.1771 241.7431 400.7675 -0.6367 228.7333 229.3700 241.9659 402.3726 -0.6369 228.9158 229.5528 242.1680 403.9574 -0.6380 229.1002 229.7382 242.3678 405.5626 -0.6372 229.2968 229.9340 242.5863 407.1728 -0.6371 229.4930 230.1300 242.7949 408.7783 -0.6348 229.6725 230.3073 243.0050 410.4036 -0.6359 229.8522 230.4881 243.2215 412.0041 -0.6378 230.0371 230.6749 243.4281 413.6089 -0.6377 230.2293 230.8670 243.6265 415.2194 -0.6384 230.4216 231.0600 243.8327 416.8245 -0.6367 230.6085 231.2452 244.0342 418.4350 -0.6381 230.8104 231.4485 244.2411 420.0401 -0.6406 230.9977 231.6383 244.4493 421.6604 -0.6404 231.1920 231.8324 244.6485 423.2711 -0.6416 231.3828 232.0245 244.8516 424.8759 -0.6403 231.5709 232.2113 245.0561 426.4859 -0.6395 231.7567 232.3961 245.2558 428.0761 -0.6406 231.9419 232.5825 245.4546 429.7014 -0.6411 232.1302 232.7713 245.6618 431.3066 -0.6421 232.3263 232.9684 245.8592 432.9119 -0.6431 232.5162 233.1593 246.0524 434.5374 -0.6455 232.7058 233.3513 246.2528 436.1326 -0.6466 232.8998 233.5465 246.4429 437.7374 -0.6456 233.0854 233.7309 246.6388 439.3584 -0.6451 233.2808 233.9259 246.8392 440.9684 -0.6462 233.4855 234.1317 247.0304 442.5635 -0.6491 233.6819 234.3309 247.2109 444.1738 -0.6490 233.8823 234.5313 247.4031 445.7941 -0.6503 234.0778 234.7281 247.5956 447.3996 -0.6509 234.2798 234.9307 247.7816 449.0095 -0.6520 234.4797 235.1316 247.9715 450.6151 -0.6510 234.6753 235.3262 248.1562 452.2251 -0.6527 234.8728 235.5255 248.3295 453.8204 -0.6512 235.0673 235.7184 248.5144 455.4254 -0.6531 235.2590 235.9121 248.7132 457.0153 -0.6562 235.4601 236.1163 248.9043 458.6308 -0.6585 235.6666 236.3251 249.0869 460.2306 -0.6596 235.8504 236.5099 249.2817 461.8361 -0.6620 236.0466 236.7086 249.4773 463.4410 -0.6635 236.2368 236.9002 249.6775 465.0415 -0.6650 236.4422 237.1073 249.8869 466.6514 -0.6664 236.6493 237.3157 250.1012 468.2568 -0.6667 236.8489 237.5156 250.3264 469.8773 -0.6674 237.0411 237.7085 250.5631 471.4874 -0.6675 237.2518 237.9192 250.7823 473.0878 -0.6684 237.4441 238.1125 250.9974 474.6976 -0.6703 237.6436 238.3139 251.2180 476.3030 -0.6725 237.8412 238.5137 251.4458 477.9081 -0.6733 238.0471 238.7204 251.6786 479.5188 -0.6733 238.2445 238.9178 251.9038 481.1391 -0.6743 238.4500 239.1243 252.1421 482.7493 -0.6747 238.6445 239.3193 252.3782 484.3496 -0.6766 238.8470 239.5236 252.6071 485.9544 -0.6776 239.0435 239.7211 252.8370 487.5653 -0.6774 239.2448 239.9222 253.0634 489.1700 -0.6800 239.4401 240.1201 253.2948 490.7806 -0.6819 239.6369 240.3188 253.5242 492.4010 -0.6844 239.8394 240.5238 253.7402 494.0113 -0.6873 240.0486 240.7359 253.9610 495.6166 -0.6875 240.2493 240.9368 254.1852 497.2214 -0.6895 240.4535 241.1430 254.4087 498.8319 -0.6922 240.6621 241.3543 254.6295 500.4370 -0.6931 240.8715 241.5646 254.8549 502.0469 -0.6954 241.0922 241.7876 255.0823 503.6680 -0.6996 241.2886 241.9881 255.3039 505.2779 -0.7017 241.4738 242.1755 255.5209 506.8834 -0.7034 241.6730 242.3763 255.7357 508.4884 -0.7041 241.8852 242.5894 255.9560 510.0989 -0.7060 242.1037 242.8097 256.1825 511.7040 -0.7070 242.3038 243.0108 256.4025 513.3146 -0.7081 242.5019 243.2100 256.6101 514.9350 -0.7109 242.7158 243.4267 256.8418 516.5201 -0.7121 242.9263 243.6385 257.0439 518.1250 -0.7146 243.1321 243.8468 257.2514 519.7254 -0.7177 243.3248 244.0425 257.4593 521.3253 -0.7186 243.5266 244.2451 257.6757 522.9354 -0.7197 243.7339 244.4536 257.8766 524.5358 -0.7229 243.9460 244.6689 258.0701 526.1356 -0.7236 244.1514 244.8750 258.2711 527.7616 -0.7256 244.3715 245.0971 258.4784 529.3613 -0.7299 244.5773 245.3072 258.6821 530.9668 -0.7320 244.7838 245.5159 258.8914 532.5718 -0.7338 244.9953 245.7291 259.0939 534.1771 -0.7335 245.2078 245.9413 259.3103 535.7823 -0.7334 245.4230 246.1565 259.5030 537.3870 -0.7351 245.6477 246.3828 259.6901 539.0030 -0.7386 245.8540 246.5925 259.8961 540.6129 -0.7402 246.0623 246.8025 260.0948 542.2184 -0.7415 246.2576 246.9992 260.3039 543.8234 -0.7428 246.4679 247.2107 260.4984 545.4334 -0.7440 246.6774 247.4214 260.6967 547.0236 -0.7462 246.8779 247.6241 260.8987 548.6335 -0.7484 247.0900 247.8383 261.1013 550.2386 -0.7499 247.3025 248.0523 261.2903 551.8645 -0.7502 247.5185 248.2687 261.4932 553.4693 -0.7513 247.7358 248.4871 261.6924 555.0749 -0.7542 247.9413 248.6955 261.8912 556.6849 -0.7571 248.1507 248.9077 262.0734 558.2905 -0.7570 248.3546 249.1116 262.2693 559.9005 -0.7586 248.5743 249.3329 262.4749 561.5061 -0.7600 248.7959 249.5558 262.6823 563.1315 -0.7603 249.0274 249.7877 262.8747 564.7369 -0.7642 249.2317 249.9959 263.0693 566.3420 -0.7661 249.4376 250.2038 263.2592 567.9526 -0.7665 249.6474 250.4138 263.4519 569.5576 -0.7686 249.8554 250.6240 263.6404 571.1679 -0.7717 250.0879 250.8596 263.8269 572.7886 -0.7747 250.2982 251.0728 264.0055 574.4140 -0.7762 250.5102 251.2864 264.1952 576.0196 -0.7789 250.7180 251.4969 264.3854 577.6193 -0.7797 250.9287 251.7084 264.5740 579.2194 -0.7807 251.1411 251.9218 264.7649 580.8195 -0.7819 251.3520 252.1339 264.9491 582.4243 -0.7855 251.5636 252.3491 265.1368 584.0249 -0.7884 251.7784 252.5669 265.3173 585.6450 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