DTA measure 3fazis_pbupdown3 Date: 2026429:941 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.35 s Mass = 1149.800 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4010 -4.2604 424.4946 428.7550 406.3178 4.0049 -4.2692 424.5010 428.7702 406.3582 5.6095 -4.2776 424.5027 428.7803 406.3902 7.2186 -4.2876 424.5008 428.7883 406.4052 8.8180 -4.2970 424.4888 428.7858 406.4156 10.4225 -4.3043 424.4890 428.7932 406.4198 12.0316 -4.3117 424.4899 428.8016 406.4027 13.6363 -4.3191 424.4978 428.8169 406.3814 15.2350 -4.3256 424.5050 428.8306 406.3536 16.8446 -4.3352 424.4987 428.8339 406.2978 18.4486 -4.3442 424.4885 428.8326 406.2175 20.0584 -4.3513 424.4871 428.8384 406.1310 21.6469 -4.3565 424.4818 428.8384 406.0392 23.2568 -4.3614 424.4726 428.8340 405.9217 24.8764 -4.3682 424.4735 428.8417 405.8098 26.4806 -4.3762 424.4500 428.8261 405.6856 28.0905 -4.3828 424.4414 428.8243 405.5405 29.6944 -4.3878 424.4330 428.8208 405.3917 31.2939 -4.3934 424.4387 428.8321 405.2384 32.8979 -4.3989 424.4329 428.8318 405.0650 34.5075 -4.4044 424.4285 428.8330 404.8932 36.1115 -4.4097 424.4174 428.8270 404.7104 37.7365 -4.4137 424.3959 428.8096 404.5267 39.3458 -4.4160 424.3841 428.8001 404.3286 40.9399 -4.4204 424.3682 428.7886 404.1387 42.5440 -4.4238 424.3513 428.7750 403.9371 44.1484 -4.4267 424.3240 428.7507 403.7515 45.7631 -4.4301 424.2905 428.7206 403.5562 47.3671 -4.4307 424.2805 428.7111 403.3678 48.9770 -4.4315 424.2586 428.6901 403.1772 50.6014 -4.4324 424.2342 428.6666 402.9749 52.1958 -4.4343 424.2045 428.6389 402.7992 53.7998 -4.4384 424.1654 428.6038 402.6096 55.4094 -4.4410 424.1538 428.5948 402.4245 57.0134 -4.4417 424.1347 428.5764 402.2427 58.6179 -4.4413 424.1124 428.5537 402.0723 60.2378 -4.4441 424.0687 428.5128 401.8937 61.8213 -4.4464 424.0191 428.4654 401.7058 63.4363 -4.4471 423.9640 428.4111 401.5114 65.0401 -4.4492 423.9192 428.3684 401.3139 66.6448 -4.4498 423.8870 428.3368 401.1163 68.2436 -4.4502 423.8428 428.2930 400.9336 69.8481 -4.4507 423.7938 428.2445 400.7342 71.4526 -4.4522 423.7516 428.2038 400.5270 73.0618 -4.4546 423.6983 428.1529 400.3203 74.6509 -4.4569 423.6504 428.1072 400.1225 76.2703 -4.4573 423.6093 428.0666 399.9207 77.8799 -4.4576 423.5492 428.0067 399.7172 79.4839 -4.4574 423.4894 427.9469 399.5145 81.0938 -4.4575 423.4261 427.8837 399.3131 82.6975 -4.4580 423.3643 427.8223 399.1199 84.3074 -4.4592 423.3138 427.7730 398.9209 85.9113 -4.4600 423.2465 427.7065 398.7240 87.5313 -4.4597 423.1777 427.6374 398.5425 89.1250 -4.4596 423.1088 427.5684 398.3592 90.7295 -4.4596 423.0448 427.5044 398.1634 92.3385 -4.4588 422.9840 427.4428 397.9719 93.9431 -4.4618 422.9269 427.3887 397.7774 95.5525 -4.4613 422.8600 427.3213 397.5930 97.1568 -4.4611 422.7889 427.2500 397.4270 98.7610 -4.4614 422.7091 427.1705 397.2499 100.3909 -4.4624 422.6245 427.0869 397.0797 101.9955 -4.4628 422.5487 427.0115 396.9098 103.6045 -4.4626 422.4809 426.9435 396.7410 105.1939 -4.4628 422.4062 426.8690 396.5678 106.8028 -4.4627 422.3217 426.7845 396.3881 108.4075 -4.4600 422.2368 426.6968 396.1992 110.0164 -4.4596 422.1479 426.6075 396.0104 111.6211 -4.4589 422.0669 426.5257 395.8353 113.2408 -4.4599 421.9843 426.4441 395.6552 114.8399 -4.4593 421.9025 426.3618 395.4708 116.4443 -4.4593 421.8094 426.2687 395.2819 118.0535 -4.4584 421.7231 426.1815 395.0904 119.6631 -4.4579 421.6453 426.1032 394.9099 121.2723 -4.4569 421.5732 426.0302 394.7271 122.8769 -4.4558 421.4831 425.9389 394.5261 124.4859 -4.4551 421.3937 425.8488 394.3407 126.0800 -4.4544 421.2872 425.7416 394.1486 127.6790 -4.4540 421.1848 425.6388 393.9592 129.2781 -4.4536 421.0845 425.5382 393.7802 130.8875 -4.4517 420.9785 425.4303 393.5954 132.4865 -4.4519 420.8790 425.3309 393.4134 134.0858 -4.4509 420.7679 425.2188 393.2300 135.6899 -4.4504 420.6671 425.1174 393.0542 137.2943 -4.4498 420.5561 425.0058 392.8703 138.9035 -4.4500 420.4360 424.8860 392.6846 140.5079 -4.4480 420.3282 424.7762 392.4912 142.1120 -4.4467 420.2217 424.6684 392.3016 143.7215 -4.4465 420.1116 424.5581 392.1144 145.3258 -4.4456 419.9923 424.4379 391.9157 146.9351 -4.4429 419.8725 424.3154 391.7304 148.5345 -4.4418 419.7566 424.1984 391.5275 150.1385 -4.4405 419.6483 424.0889 391.3484 151.7634 -4.4391 419.5527 423.9918 391.1482 153.3675 -4.4389 419.4440 423.8829 390.9607 154.9769 -4.4374 419.3277 423.7651 390.7627 156.5811 -4.4361 419.2217 423.6578 390.5623 158.1905 -4.4328 419.1089 423.5417 390.3707 159.7948 -4.4309 418.9886 423.4195 390.1681 161.3993 -4.4295 418.8685 423.2979 389.9581 163.0238 -4.4280 418.7482 423.1762 389.7569 164.6285 -4.4265 418.6253 423.0519 389.5591 166.2374 -4.4256 418.4986 422.9242 389.3680 167.8421 -4.4257 418.3786 422.8043 389.1664 169.4513 -4.4226 418.2645 422.6871 388.9733 171.0558 -4.4220 418.1329 422.5549 388.7862 172.6655 -4.4216 417.9996 422.4212 388.5866 174.2900 -4.4197 417.8746 422.2943 388.3898 175.8946 -4.4176 417.7471 422.1647 388.2023 177.5038 -4.4159 417.6207 422.0366 388.0134 179.1083 -4.4142 417.4931 421.9072 387.8275 180.7178 -4.4131 417.3709 421.7840 387.6319 182.3219 -4.4093 417.2432 421.6525 387.4381 183.9365 -4.4063 417.1300 421.5363 387.2569 185.5560 -4.4022 417.0036 421.4058 387.0671 187.1659 -4.3984 416.8688 421.2672 386.8760 188.7646 -4.3977 416.7218 421.1195 386.6939 190.3539 -4.3973 416.5843 420.9816 386.5086 191.9578 -4.3972 416.4547 420.8519 386.3295 193.5573 -4.3957 416.3141 420.7098 386.1384 195.1560 -4.3930 416.1696 420.5626 385.9387 196.7504 -4.3897 416.0272 420.4170 385.7503 198.3546 -4.3878 415.8942 420.2820 385.5681 199.9691 -4.3851 415.7654 420.1505 385.3746 201.5789 -4.3819 415.6202 420.0021 385.1663 203.1674 -4.3800 415.4736 419.8536 384.9526 204.7721 -4.3781 415.3274 419.7055 384.7439 206.3760 -4.3754 415.1909 419.5663 384.5436 207.9806 -4.3743 415.0575 419.4319 384.3555 209.5896 -4.3730 414.9173 419.2903 384.1564 211.1789 -4.3707 414.7739 419.1447 383.9513 212.7880 -4.3678 414.6298 418.9975 383.7543 214.4079 -4.3654 414.4809 418.8463 383.5527 216.0123 -4.3631 414.3452 418.7083 383.3655 217.6215 -4.3586 414.2016 418.5602 383.1791 219.2259 -4.3555 414.0570 418.4125 382.9682 220.8351 -4.3539 413.9051 418.2590 382.7718 222.4396 -4.3492 413.7600 418.1092 382.5798 224.0539 -4.3458 413.6057 417.9515 382.3809 225.6433 -4.3423 413.4515 417.7938 382.1934 227.2675 -4.3407 413.3048 417.6455 382.0135 228.8723 -4.3397 413.1604 417.5001 381.8212 230.4763 -4.3376 412.9996 417.3372 381.6392 232.0859 -4.3364 412.8627 417.1992 381.4617 233.6899 -4.3332 412.7079 417.0411 381.2678 235.3046 -4.3300 412.5581 416.8881 381.0833 236.9140 -4.3289 412.4049 416.7338 380.8978 238.5183 -4.3262 412.2475 416.5737 380.7170 240.1430 -4.3219 412.0881 416.4101 380.5276 241.7473 -4.3197 411.9321 416.2518 380.3382 243.3518 -4.3167 411.7756 416.0923 380.1547 244.9660 -4.3151 411.6102 415.9253 379.9604 246.5708 -4.3144 411.4522 415.7666 379.7730 248.1695 -4.3110 411.2909 415.6019 379.5857 249.7844 -4.3060 411.1384 415.4444 379.3811 251.3885 -4.3053 410.9798 415.2852 379.1827 253.0031 -4.3028 410.8199 415.1227 378.9825 254.6021 -4.2990 410.6647 414.9637 378.7866 256.2065 -4.2957 410.5148 414.8104 378.6055 257.8058 -4.2935 410.3599 414.6535 378.4071 259.4048 -4.2894 410.1972 414.4866 378.2009 261.0093 -4.2855 410.0429 414.3284 377.9965 262.6133 -4.2841 409.8707 414.1548 377.7928 264.2283 -4.2783 409.7032 413.9815 377.5900 265.8371 -4.2754 409.5389 413.8143 377.3958 267.4265 -4.2732 409.3706 413.6437 377.2076 269.0355 -4.2699 409.2085 413.4785 377.0020 270.6401 -4.2690 409.0407 413.3097 376.7996 272.2491 -4.2661 408.8841 413.1502 376.6013 273.8486 -4.2619 408.7129 412.9748 376.4153 275.4529 -4.2559 408.5535 412.8094 376.2229 277.0776 -4.2513 408.3925 412.6438 376.0258 278.6821 -4.2491 408.2265 412.4756 375.8357 280.2913 -4.2444 408.0680 412.3125 375.6429 281.8958 -4.2394 407.9045 412.1439 375.4477 283.4998 -4.2356 407.7403 411.9759 375.2561 285.1095 -4.2336 407.5662 411.7999 375.0688 286.7134 -4.2327 407.4025 411.6352 374.8884 288.3386 -4.2307 407.2355 411.4662 374.6988 289.9424 -4.2284 407.0621 411.2905 374.5010 291.5523 -4.2240 406.8967 411.1208 374.3040 293.1560 -4.2200 406.7264 410.9463 374.1103 294.7659 -4.2150 406.5555 410.7705 373.9236 296.3750 -4.2107 406.3810 410.5917 373.7303 297.9641 -4.2067 406.2319 410.4386 373.5384 299.5785 -4.2011 406.0697 410.2708 373.3284 301.1983 -4.1983 405.8896 410.0879 373.1289 302.8078 -4.1943 405.7081 409.9024 372.9293 304.4119 -4.1902 405.5432 409.7334 372.7184 306.0110 -4.1864 405.3698 409.5562 372.5123 307.6153 -4.1833 405.1966 409.3800 372.2968 309.2248 -4.1806 405.0266 409.2072 372.0848 310.8289 -4.1756 404.8485 409.0242 371.8955 312.4385 -4.1716 404.6817 408.8533 371.6875 314.0425 -4.1674 404.5193 408.6867 371.4775 315.6524 -4.1593 404.3437 408.5030 371.2836 317.2564 -4.1552 404.1787 408.3340 371.0841 318.8558 -4.1529 404.0023 408.1552 370.8657 320.4549 -4.1478 403.8279 407.9757 370.6597 322.0591 -4.1421 403.6635 407.8056 370.4512 323.6635 -4.1392 403.4856 407.6247 370.2534 325.2471 -4.1367 403.3033 407.4400 370.0544 326.8568 -4.1335 403.1257 407.2592 369.8588 328.4710 -4.1305 402.9474 407.0779 369.6589 330.0756 -4.1279 402.7735 406.9014 369.4665 331.6795 -4.1242 402.5988 406.7230 369.2607 333.2841 -4.1190 402.4292 406.5482 369.0665 334.8931 -4.1156 402.2552 406.3708 368.8643 336.4979 -4.1129 402.0837 406.1966 368.6604 338.1070 -4.1073 401.9024 406.0097 368.4662 339.7269 -4.1039 401.7146 405.8186 368.2721 341.3158 -4.0989 401.5363 405.6353 368.0753 342.9251 -4.0947 401.3500 405.4447 367.8800 344.5295 -4.0923 401.1695 405.2619 367.6831 346.1388 -4.0881 400.9801 405.0682 367.4789 347.7430 -4.0829 400.8089 404.8918 367.2760 349.3524 -4.0793 400.6314 404.7107 367.0885 350.9619 -4.0752 400.4523 404.5276 366.9087 352.5865 -4.0687 400.2734 404.3420 366.7229 354.1806 -4.0637 400.1053 404.1690 366.5378 355.8053 -4.0612 399.9181 403.9793 366.3535 357.4096 -4.0578 399.7315 403.7893 366.1665 359.0138 -4.0525 399.5526 403.6051 365.9723 360.6233 -4.0499 399.3732 403.4231 365.7832 362.2274 -4.0457 399.1904 403.2361 365.5917 363.8526 -4.0429 398.9908 403.0337 365.3925 365.4564 -4.0389 398.7962 402.8350 365.1921 367.0661 -4.0325 398.6182 402.6507 364.9958 368.6751 -4.0274 398.4414 402.4688 364.7980 370.2848 -4.0230 398.2834 402.3064 364.5828 371.8939 -4.0188 398.1019 402.1207 364.3747 373.5036 -4.0150 397.9229 401.9379 364.1686 375.1229 -4.0099 397.7312 401.7411 363.9768 376.7276 -4.0059 397.5493 401.5552 363.7744 378.3419 -4.0029 397.3710 401.3739 363.5625 379.9464 -4.0006 397.1861 401.1867 363.3515 381.5454 -3.9959 397.0026 400.9985 363.1557 383.1446 -3.9921 396.8266 400.8188 362.9499 384.7386 -3.9870 396.6378 400.6248 362.7365 386.3429 -3.9815 396.4552 400.4368 362.5407 387.9419 -3.9748 396.2816 400.2564 362.3415 389.5616 -3.9700 396.0930 400.0630 362.1279 391.1504 -3.9674 395.9112 399.8786 361.9241 392.7496 -3.9634 395.7213 399.6848 361.7241 394.3594 -3.9595 395.5305 399.4900 361.5202 395.9633 -3.9550 395.3527 399.3077 361.3195 397.5731 -3.9499 395.1659 399.1158 361.1178 399.1616 -3.9464 394.9827 398.9291 360.9176 400.7714 -3.9405 394.7908 398.7312 360.7148 402.3754 -3.9355 394.6080 398.5435 360.5287 403.9953 -3.9325 394.4129 398.3454 360.3302 405.6043 -3.9288 394.2430 398.1719 360.1277 407.1935 -3.9237 394.0635 397.9872 359.9306 408.8026 -3.9195 393.8723 397.7918 359.7347 410.4071 -3.9138 393.6910 397.6048 359.5314 412.0168 -3.9098 393.4950 397.4047 359.3431 413.6208 -3.9069 393.3060 397.2129 359.1552 415.2255 -3.9026 393.1251 397.0277 358.9673 416.8499 -3.8991 392.9382 396.8373 358.7731 418.4545 -3.8945 392.7451 396.6396 358.6009 420.0634 -3.8906 392.5540 396.4446 358.4128 421.6733 -3.8863 392.3819 396.2682 358.2237 423.2823 -3.8822 392.1868 396.0690 358.0320 424.8869 -3.8752 391.9888 395.8640 357.8448 426.4961 -3.8696 391.7945 395.6641 357.6471 428.1159 -3.8631 391.6197 395.4828 357.4473 429.7205 -3.8588 391.4366 395.2954 357.2524 431.3295 -3.8562 391.2319 395.0881 357.0469 432.9343 -3.8533 391.0426 394.8959 356.8461 434.5433 -3.8492 390.8492 394.6985 356.6396 436.1479 -3.8454 390.6563 394.5017 356.4328 437.7569 -3.8406 390.4624 394.3030 356.2345 439.3769 -3.8370 390.2657 394.1027 356.0176 440.9811 -3.8345 390.0853 393.9198 355.8032 442.5905 -3.8292 389.9045 393.7338 355.6094 444.2001 -3.8253 389.7270 393.5523 355.4052 445.8041 -3.8207 389.5446 393.3653 355.2028 447.4085 -3.8158 389.3583 393.1741 354.9749 449.0024 -3.8131 389.1644 392.9775 354.7616 450.6121 -3.8090 388.9671 392.7760 354.5474 452.2161 -3.8043 388.7781 392.5824 354.3340 453.8156 -3.7991 388.5899 392.3890 354.1284 455.4246 -3.7955 388.3987 392.1942 353.9333 457.0291 -3.7911 388.2092 392.0003 353.7201 458.6381 -3.7856 388.0095 391.7950 353.5120 460.2429 -3.7793 387.8189 391.5982 353.3030 461.8520 -3.7733 387.6319 391.4052 353.0975 463.4668 -3.7690 387.4398 391.2088 352.8922 465.0708 -3.7650 387.2564 391.0214 352.6836 466.6804 -3.7602 387.0727 390.8329 352.4768 468.2848 -3.7555 386.8868 390.6423 352.2790 469.8940 -3.7520 386.6869 390.4389 352.0911 471.4986 -3.7474 386.5015 390.2489 351.8904 473.0871 -3.7429 386.3108 390.0538 351.6844 474.6969 -3.7379 386.1230 389.8609 351.4754 476.3161 -3.7356 385.9187 389.6543 351.2757 477.9260 -3.7295 385.7313 389.4608 351.0737 479.5299 -3.7246 385.5477 389.2722 350.8726 481.1396 -3.7176 385.3540 389.0716 350.6723 482.7435 -3.7137 385.1609 388.8746 350.4706 484.3533 -3.7100 384.9686 388.6787 350.2714 485.9625 -3.7070 384.7820 388.4890 350.0752 487.5823 -3.7021 384.5988 388.3009 349.8967 489.1916 -3.6990 384.4126 388.1116 349.7179 490.7959 -3.6974 384.2086 387.9059 349.5192 492.4054 -3.6938 384.0029 387.6967 349.3272 494.0095 -3.6898 383.8029 387.4927 349.1331 495.6190 -3.6848 383.6151 387.2999 348.9382 497.2231 -3.6801 383.4207 387.1007 348.7435 498.8433 -3.6747 383.2212 386.8960 348.5626 500.4680 -3.6708 383.0354 386.7062 348.3710 502.0774 -3.6650 382.8427 386.5077 348.1775 503.6921 -3.6584 382.6449 386.3033 347.9882 505.2910 -3.6556 382.4437 386.0993 347.8087 506.9009 -3.6505 382.2481 385.8986 347.6129 508.5098 -3.6453 382.0490 385.6942 347.4059 510.1248 -3.6396 381.8496 385.4892 347.1987 511.7235 -3.6358 381.6544 385.2902 346.9986 513.3128 -3.6335 381.4637 385.0972 346.7957 514.9168 -3.6291 381.2618 384.8909 346.5880 516.5161 -3.6236 381.0804 384.7040 346.3953 518.1256 -3.6206 380.8997 384.5202 346.1755 519.7298 -3.6159 380.7042 384.3201 345.9589 521.3288 -3.6119 380.5062 384.1181 345.7585 522.9536 -3.6067 380.3091 383.9157 345.5472 524.5528 -3.6025 380.1229 383.7254 345.3297 526.1570 -3.5980 379.9363 383.5343 345.1343 527.7615 -3.5918 379.7367 383.3285 344.9374 529.3655 -3.5877 379.5366 383.1243 344.7272 530.9751 -3.5823 379.3337 382.9160 344.5150 532.5791 -3.5771 379.1440 382.7211 344.3116 534.1988 -3.5728 378.9490 382.5218 344.1135 535.8081 -3.5691 378.7487 382.3178 343.9295 537.4129 -3.5640 378.5569 382.1209 343.7237 539.0218 -3.5589 378.3665 381.9254 343.5196 540.6265 -3.5536 378.1765 381.7302 343.3046 542.2356 -3.5485 377.9819 381.5304 343.1018 543.8401 -3.5434 377.7765 381.3199 342.8963 545.4701 -3.5407 377.5813 381.1220 342.6895 547.0743 -3.5356 377.3785 380.9141 342.4879 548.6790 -3.5311 377.1890 380.7201 342.2987 550.2880 -3.5260 376.9947 380.5208 342.1170 551.8978 -3.5218 376.8042 380.3260 341.9013 553.5073 -3.5168 376.6053 380.1221 341.6987 555.1114 -3.5094 376.4132 379.9226 341.5065 556.7366 -3.5048 376.2161 379.7208 341.3120 558.3404 -3.5014 376.0214 379.5228 341.1186 559.9554 -3.4959 375.8341 379.3300 340.9369 561.5593 -3.4912 375.6456 379.1368 340.7392 563.1690 -3.4859 375.4362 378.9221 340.5363 564.7733 -3.4803 375.2314 378.7117 340.3491 566.3826 -3.4771 375.0400 378.5170 340.1553 568.0074 -3.4718 374.8491 378.3209 339.9536 569.6116 -3.4693 374.6572 378.1265 339.7638 571.2214 -3.4658 374.4543 377.9201 339.5791 572.8253 -3.4605 374.2615 377.7220 339.3951 574.4198 -3.4539 374.0643 377.5182 339.2029 576.0134 -3.4496 373.8580 377.3076 339.0034 577.6180 -3.4440 373.6693 377.1134 338.8025 579.2223 -3.4378 373.4716 376.9094 338.6076 580.8368 -3.4345 373.2769 376.7113 338.4104 582.4413 -3.4329 373.0895 376.5224 338.2093 584.0453 -3.4290 372.8916 376.3206 338.0027 585.6295 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