DTA measure 3meres Date: 2025916:162 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.36 s Mass = 5000.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4704 -4.6188 447.2878 451.9065 433.5667 4.0688 -4.6291 447.3593 451.9885 433.6594 5.6619 -4.6416 447.4577 452.0994 433.6615 7.2651 -4.6458 447.5353 452.1812 433.6108 8.8685 -4.6599 447.6038 452.2637 433.4106 10.4820 -4.6700 447.6905 452.3605 433.1188 12.0906 -4.6777 447.7812 452.4589 432.7673 13.6889 -4.6839 447.8263 452.5102 432.3292 15.2973 -4.6908 447.8844 452.5752 431.8207 16.9213 -4.6934 447.9596 452.6530 431.2973 18.5295 -4.6903 448.0451 452.7354 430.7574 20.1381 -4.6921 448.0971 452.7893 430.2011 21.7466 -4.6948 448.1748 452.8696 429.7009 23.3398 -4.6974 448.2522 452.9496 429.2127 24.9484 -4.7026 448.3180 453.0206 428.8194 26.5569 -4.7009 448.3619 453.0628 428.4852 28.1654 -4.7021 448.3506 453.0527 428.2136 29.7843 -4.7027 448.4034 453.1061 428.0236 31.3823 -4.7029 448.4462 453.1491 427.8879 32.9755 -4.7034 448.4773 453.1807 427.8388 34.5790 -4.7027 448.4856 453.1883 427.8678 36.1771 -4.7029 448.5101 453.2130 427.9482 37.7856 -4.7034 448.5225 453.2260 427.9831 39.3890 -4.7077 448.5068 453.2145 428.0524 40.9975 -4.7139 448.5269 453.2408 428.0845 42.6164 -4.7210 448.5848 453.3058 428.0910 44.2300 -4.7289 448.6155 453.3444 428.0473 45.8334 -4.7347 448.6476 453.3823 427.9596 47.4420 -4.7415 448.6880 453.4295 427.7960 49.0453 -4.7486 448.6981 453.4466 427.5831 50.6488 -4.7588 448.7129 453.4717 427.3281 52.2625 -4.7693 448.7352 453.5045 427.0069 53.8810 -4.7712 448.7227 453.4939 426.6518 55.4896 -4.7708 448.7431 453.5139 426.2937 57.0983 -4.7750 448.7076 453.4826 425.8780 58.7066 -4.7730 448.6977 453.4707 425.5129 60.3101 -4.7700 448.6957 453.4658 425.0908 61.9189 -4.7695 448.6896 453.4591 424.6610 63.5220 -4.7708 448.6657 453.4365 424.3015 65.1204 -4.7711 448.6462 453.4173 423.9452 66.7239 -4.7680 448.6336 453.4016 423.6190 68.3323 -4.7664 448.6184 453.3847 423.4123 69.9356 -4.7685 448.6297 453.3982 423.2403 71.5390 -4.7699 448.5962 453.3661 423.1171 73.1475 -4.7703 448.5447 453.3149 423.0373 74.7510 -4.7713 448.4792 453.2505 422.9779 76.3595 -4.7788 448.4139 453.1927 422.9577 77.9629 -4.7816 448.3939 453.1755 422.8951 79.5869 -4.7811 448.3634 453.1445 422.8095 81.1953 -4.7864 448.3084 453.0949 422.7035 82.8038 -4.7914 448.2371 453.0284 422.5692 84.3969 -4.7956 448.1602 452.9558 422.4554 86.0104 -4.7972 448.0907 452.8879 422.3223 87.6139 -4.7975 448.0609 452.8583 422.1636 89.2274 -4.8023 448.0362 452.8385 421.9895 90.8308 -4.8045 447.9990 452.8035 421.7920 92.4289 -4.8079 447.9222 452.7301 421.5317 94.0476 -4.8155 447.8789 452.6944 421.2329 95.6460 -4.8124 447.8104 452.6227 420.9281 97.2491 -4.8160 447.7678 452.5837 420.5637 98.8526 -4.8170 447.7219 452.5388 420.2461 100.4613 -4.8197 447.6707 452.4904 419.9110 102.0490 -4.8206 447.6208 452.4413 419.6711 103.6525 -4.8177 447.5564 452.3741 419.4351 105.2610 -4.8192 447.4578 452.2770 419.1476 106.8694 -4.8210 447.3559 452.1769 418.9054 108.4883 -4.8207 447.2463 452.0670 418.6662 110.0969 -4.8207 447.1961 452.0168 418.4294 111.7003 -4.8201 447.1204 451.9405 418.2405 113.3140 -4.8228 447.0485 451.8713 418.0425 114.9173 -4.8191 446.9738 451.7928 417.8329 116.5258 -4.8177 446.8570 451.6748 417.6599 118.1344 -4.8189 446.7751 451.5940 417.5016 119.7426 -4.8266 446.6833 451.5099 417.3280 121.3513 -4.8274 446.5682 451.3956 417.2095 122.9596 -4.8325 446.4662 451.2987 417.1075 124.5731 -4.8328 446.4157 451.2485 416.9768 126.1764 -4.8361 446.3583 451.1944 416.8132 127.7798 -4.8412 446.2571 451.0983 416.6535 129.3780 -4.8407 446.1308 450.9715 416.4263 130.9710 -4.8403 446.0108 450.8511 416.2486 132.5745 -4.8437 445.8753 450.7189 416.0973 134.1930 -4.8438 445.7352 450.5790 415.9069 135.8016 -4.8412 445.6100 450.4513 415.7083 137.4051 -4.8465 445.5223 450.3688 415.4549 139.0134 -4.8493 445.3981 450.2474 415.2182 140.6220 -4.8503 445.3200 450.1703 414.9887 142.2203 -4.8505 445.2104 450.0609 414.7480 143.8235 -4.8524 445.1049 449.9572 414.4573 145.4320 -4.8567 445.0117 449.8684 414.1131 147.0506 -4.8587 444.8832 449.7419 413.8352 148.6643 -4.8608 444.7715 449.6324 413.5794 150.2675 -4.8593 444.6380 449.4973 413.3602 151.8811 -4.8574 444.5547 449.4120 413.0929 153.4848 -4.8542 444.4763 449.3304 412.8571 155.0983 -4.8538 444.3035 449.1573 412.6179 156.7068 -4.8535 444.1502 449.0037 412.4455 158.3048 -4.8525 443.9924 448.8449 412.2885 159.8930 -4.8522 443.8673 448.7195 412.1462 161.5066 -4.8504 443.7463 448.5967 411.9516 163.1099 -4.8445 443.6045 448.4489 411.7606 164.7133 -4.8494 443.4842 448.3336 411.5629 166.3219 -4.8472 443.3768 448.2240 411.4132 167.9251 -4.8458 443.2599 448.1057 411.2655 169.5184 -4.8455 443.1169 447.9624 411.1460 171.1216 -4.8490 443.0077 447.8566 410.9262 172.7353 -4.8504 442.8864 447.7368 410.7319 174.3541 -4.8513 442.7293 447.5806 410.5454 175.9625 -4.8465 442.5729 447.4193 410.3664 177.5558 -4.8479 442.4492 447.2970 410.1008 179.1695 -4.8464 442.3312 447.1777 409.8864 180.7728 -4.8495 442.1747 447.0242 409.6594 182.3813 -4.8454 442.0500 446.8954 409.3941 183.9898 -4.8429 441.9061 446.7489 409.1924 185.5930 -4.8385 441.7929 446.6315 408.9684 187.2170 -4.8375 441.6119 446.4495 408.7345 188.8254 -4.8404 441.4382 446.2786 408.4954 190.4339 -4.8380 441.2786 446.1166 408.2720 192.0164 -4.8386 441.1733 446.0118 408.0747 193.6148 -4.8349 441.0510 445.8858 407.8490 195.2180 -4.8290 440.8877 445.7167 407.6291 196.8214 -4.8207 440.7328 445.5535 407.3911 198.4300 -4.8181 440.5695 445.3876 407.1307 200.0331 -4.8106 440.4609 445.2715 406.8621 201.6418 -4.8100 440.2657 445.0757 406.6704 203.2501 -4.8076 440.1049 444.9125 406.4793 204.8535 -4.8036 439.9628 444.7664 406.3055 206.4723 -4.8024 439.8076 444.6101 406.1109 208.0653 -4.8008 439.6648 444.4656 405.9190 209.6688 -4.8029 439.4896 444.2925 405.7389 211.2821 -4.7988 439.3367 444.1355 405.5471 212.8856 -4.7963 439.1549 443.9512 405.3815 214.4993 -4.7974 438.9319 443.7293 405.1746 216.1178 -4.8016 438.7653 443.5669 404.9937 217.7314 -4.7986 438.6362 443.4348 404.8205 219.3244 -4.7940 438.4753 443.2693 404.6154 220.9330 -4.7866 438.3253 443.1119 404.4238 222.5361 -4.7884 438.1389 442.9273 404.2275 224.1395 -4.7857 437.9745 442.7603 403.9976 225.7429 -4.7807 437.8355 442.6162 403.7641 227.3410 -4.7784 437.6647 442.4431 403.5245 228.9650 -4.7758 437.4968 442.2726 403.2545 230.5631 -4.7690 437.3771 442.1462 403.0116 232.1716 -4.7667 437.2047 441.9714 402.7648 233.7749 -4.7650 437.0294 441.7944 402.5115 235.3783 -4.7588 436.8463 441.6051 402.2911 236.9866 -4.7584 436.6856 441.4440 402.0553 238.5900 -4.7622 436.5424 441.3046 401.8770 240.2036 -4.7585 436.3485 441.1070 401.6790 241.8223 -4.7540 436.1386 440.8926 401.4735 243.4309 -4.7582 435.9689 440.7272 401.3015 245.0344 -4.7535 435.7715 440.5250 401.1153 246.6478 -4.7488 435.5940 440.3428 400.9243 248.2513 -4.7450 435.4280 440.1729 400.7306 249.8649 -4.7390 435.2547 439.9937 400.5414 251.4529 -4.7340 435.1097 439.8437 400.3859 253.0974 -4.7307 434.9336 439.6643 400.1389 254.6854 -4.7302 434.7537 439.4839 399.9126 256.2785 -4.7309 434.5717 439.3026 399.6861 257.8870 -4.7255 434.4052 439.1307 399.4406 259.4903 -4.7235 434.2442 438.9677 399.2129 261.0936 -4.7184 434.0232 438.7416 399.0442 262.6816 -4.7129 433.8470 438.5599 398.8510 264.2850 -4.7113 433.6764 438.3876 398.6070 265.9089 -4.7105 433.5279 438.2383 398.3634 267.5124 -4.7053 433.3279 438.0332 398.1617 269.1208 -4.7063 433.1275 437.8338 397.9346 270.7243 -4.6992 432.9531 437.6523 397.7258 272.3274 -4.6928 432.7656 437.4584 397.5452 273.9360 -4.6906 432.6274 437.3180 397.2988 275.5445 -4.6918 432.4477 437.1395 397.1040 277.1684 -4.6888 432.2521 436.9409 396.9398 278.7615 -4.6811 432.0780 436.7591 396.7711 280.3698 -4.6711 431.9182 436.5893 396.5943 281.9784 -4.6705 431.7341 436.4046 396.3771 283.5869 -4.6730 431.5138 436.1868 396.1393 285.1903 -4.6708 431.3258 435.9966 395.9289 286.7989 -4.6657 431.1864 435.8521 395.7164 288.3869 -4.6615 430.9939 435.6554 395.4766 289.9850 -4.6567 430.7925 435.4492 395.2044 291.6039 -4.6536 430.6256 435.2792 394.9566 293.2071 -4.6558 430.4138 435.0696 394.7021 294.8156 -4.6505 430.1998 434.8504 394.5013 296.4036 -4.6480 430.0183 434.6663 394.2698 298.0070 -4.6457 429.8494 434.4951 394.0906 299.6156 -4.6423 429.6586 434.3009 393.9370 301.2241 -4.6399 429.4642 434.1040 393.6909 302.8325 -4.6432 429.2751 433.9183 393.4850 304.4566 -4.6386 429.1227 433.7612 393.2848 306.0498 -4.6258 428.9644 433.5903 393.1167 307.6531 -4.6206 428.7937 433.4142 392.8897 309.2669 -4.6169 428.6335 433.2504 392.7033 310.8703 -4.6137 428.4351 433.0488 392.5554 312.4839 -4.6093 428.2457 432.8550 392.3752 314.0873 -4.6032 428.0218 432.6251 392.1735 315.6956 -4.6069 427.8356 432.4425 391.9450 317.3196 -4.6019 427.6635 432.2655 391.6964 318.9280 -4.6016 427.4689 432.0705 391.5233 320.5313 -4.5971 427.2722 431.8692 391.3287 322.1243 -4.5943 427.0941 431.6883 391.1203 323.7173 -4.5856 426.8892 431.4748 390.9123 325.3206 -4.5819 426.6938 431.2757 390.6829 326.9189 -4.5749 426.5108 431.0857 390.4209 328.5274 -4.5707 426.3094 430.8801 390.1534 330.1410 -4.5684 426.1157 430.6841 389.9199 331.7495 -4.5670 425.9203 430.4873 389.6978 333.3529 -4.5641 425.7219 430.2861 389.5240 334.9614 -4.5630 425.5616 430.1246 389.3143 336.5648 -4.5592 425.3994 429.9587 389.0808 338.1731 -4.5539 425.1998 429.7536 388.8655 339.7765 -4.5481 424.9800 429.5281 388.6771 341.3901 -4.5396 424.7507 429.2902 388.4617 343.0090 -4.5329 424.5431 429.0760 388.2686 344.6226 -4.5269 424.3117 428.8386 388.0681 346.2261 -4.5200 424.1360 428.6560 387.8411 347.8396 -4.5150 423.9437 428.4587 387.6308 349.4430 -4.5149 423.7690 428.2839 387.4490 351.0565 -4.5136 423.5185 428.0320 387.2538 352.6546 -4.5129 423.3061 427.8190 387.0293 354.2684 -4.5077 423.1327 427.6404 386.8101 355.8613 -4.4987 422.9382 427.4369 386.6048 357.4750 -4.4965 422.7685 427.2650 386.4144 359.0630 -4.4958 422.6249 427.1207 386.1954 360.6714 -4.4962 422.4536 426.9498 386.0134 362.2748 -4.4904 422.2495 426.7399 385.7696 363.8833 -4.4859 422.0586 426.5445 385.5497 365.4868 -4.4787 421.8299 426.3085 385.3789 367.1108 -4.4668 421.6564 426.1232 385.1393 368.7191 -4.4622 421.4668 425.9291 384.9299 370.3279 -4.4611 421.2564 425.7175 384.6767 371.9210 -4.4521 421.0305 425.4826 384.4822 373.5294 -4.4536 420.8197 425.2733 384.2420 375.1329 -4.4490 420.6417 425.0907 383.9989 376.7466 -4.4472 420.4296 424.8768 383.8116 378.3499 -4.4494 420.2215 424.6709 383.5964 379.9686 -4.4437 419.9796 424.4234 383.3864 381.5823 -4.4377 419.7663 424.2040 383.1631 383.1856 -4.4346 419.5627 423.9973 382.9878 384.7891 -4.4257 419.3785 423.8042 382.7815 386.3771 -4.4191 419.1843 423.6034 382.5829 387.9754 -4.4142 419.0187 423.4329 382.3804 389.5788 -4.4126 418.8296 423.2422 382.1560 391.1821 -4.4102 418.6609 423.0712 381.8985 392.8061 -4.4036 418.4250 422.8287 381.6796 394.4095 -4.4019 418.2231 422.6249 381.5100 395.9974 -4.3953 418.0148 422.4102 381.2393 397.6214 -4.3892 417.8026 422.1918 381.0634 399.2146 -4.3806 417.5955 421.9761 380.8624 400.8230 -4.3769 417.4096 421.7865 380.6849 402.4316 -4.3715 417.2245 421.5960 380.5148 404.0401 -4.3703 417.0106 421.3809 380.3147 405.6640 -4.3696 416.8258 421.1954 380.0907 407.2726 -4.3635 416.5983 420.9619 379.8789 408.8761 -4.3632 416.3922 420.7554 379.6261 410.4845 -4.3588 416.1935 420.5523 379.3832 412.0880 -4.3561 415.9970 420.3530 379.1653 413.6966 -4.3525 415.7673 420.1198 378.8801 415.2999 -4.3491 415.5532 419.9022 378.6652 416.9034 -4.3455 415.3724 419.7179 378.4707 418.5223 -4.3438 415.1806 419.5245 378.2570 420.1204 -4.3398 415.0150 419.3547 378.0557 421.7341 -4.3327 414.8136 419.1463 377.8522 423.3325 -4.3320 414.5969 418.9289 377.6921 424.9409 -4.3302 414.4086 418.7388 377.4754 426.5444 -4.3278 414.1699 418.4977 377.2792 428.1528 -4.3306 414.0249 418.3555 377.0946 429.7716 -4.3222 413.8250 418.1472 376.9044 431.3803 -4.3171 413.6071 417.9243 376.6869 432.9889 -4.3140 413.4320 417.7460 376.4691 434.5920 -4.3084 413.2444 417.5529 376.2538 436.2006 -4.3009 413.0481 417.3490 376.0249 437.8040 -4.2987 412.8113 417.1101 375.7902 439.4125 -4.2922 412.6003 416.8925 375.5581 441.0365 -4.2874 412.3856 416.6730 375.3401 442.6450 -4.2811 412.1547 416.4358 375.1316 444.2484 -4.2761 411.9401 416.2162 374.9375 445.8620 -4.2710 411.7423 416.0133 374.7231 447.4653 -4.2612 411.5491 415.8103 374.5367 449.0686 -4.2556 411.3898 415.6454 374.3646 450.6720 -4.2561 411.1548 415.4109 374.1506 452.2804 -4.2548 410.9252 415.1800 373.9331 453.8735 -4.2494 410.7237 414.9731 373.7602 455.4716 -4.2418 410.5174 414.7592 373.5211 457.0905 -4.2343 410.2302 414.4645 373.2896 458.6990 -4.2334 410.0089 414.2423 373.0432 460.3024 -4.2324 409.8551 414.0876 372.8237 461.9109 -4.2294 409.6741 413.9036 372.6395 463.5193 -4.2229 409.4617 413.6847 372.4382 465.1279 -4.2215 409.2550 413.4764 372.1932 466.7311 -4.2162 409.0780 413.2942 371.9747 468.3499 -4.2158 408.9056 413.1214 371.7465 469.9638 -4.2101 408.6962 412.9063 371.5499 471.5670 -4.2066 408.4931 412.6997 371.3431 473.1806 -4.2017 408.2776 412.4793 371.1361 474.7841 -4.1987 408.0592 412.2580 370.9226 476.3926 -4.1944 407.8670 412.0615 370.7373 478.0011 -4.1839 407.6451 411.8290 370.5011 479.6251 -4.1790 407.4854 411.6644 370.3377 481.2234 -4.1745 407.2402 411.4147 370.1421 482.8319 -4.1676 407.0356 411.2033 369.9075 484.4354 -4.1644 406.8359 411.0003 369.6846 486.0336 -4.1644 406.6553 410.8197 369.5192 487.6421 -4.1629 406.4380 410.6010 369.3111 489.2456 -4.1589 406.2506 410.4095 369.1070 490.8695 -4.1544 405.9672 410.1216 368.8758 492.4729 -4.1551 405.7297 409.8848 368.6625 494.0764 -4.1524 405.5252 409.6776 368.4708 495.6900 -4.1516 405.2913 409.4429 368.1995 497.2780 -4.1454 405.1249 409.2703 367.9759 498.8866 -4.1402 404.9320 409.0723 367.7346 500.4900 -4.1344 404.7554 408.8899 367.4855 502.0985 -4.1307 404.5738 408.7045 367.3347 503.7225 -4.1262 404.3984 408.5246 367.1383 505.3361 -4.1247 404.2183 408.3431 366.9053 506.9394 -4.1198 403.9927 408.1125 366.7070 508.5480 -4.1155 403.7707 407.8861 366.5153 510.1513 -4.1081 403.5438 407.6518 366.3095 511.7651 -4.0988 403.3224 407.4212 366.1104 513.3685 -4.0975 403.0966 407.1941 365.8925 514.9821 -4.0891 402.8760 406.9650 365.6939 516.5906 -4.0827 402.6539 406.7366 365.4853 518.1890 -4.0785 402.4707 406.5492 365.2944 519.7976 -4.0754 402.2570 406.3324 365.0603 521.4010 -4.0725 402.0782 406.1507 364.8603 523.0044 -4.0683 401.9158 405.9841 364.6136 524.6128 -4.0594 401.7254 405.7848 364.3569 526.2163 -4.0512 401.5347 405.5859 364.1410 527.8403 -4.0457 401.3072 405.3530 363.9411 529.4435 -4.0406 401.0850 405.1256 363.7317 531.0521 -4.0337 400.8856 404.9192 363.5076 532.6608 -4.0306 400.6500 404.6806 363.3276 534.2536 -4.0233 400.4306 404.4538 363.1192 535.8725 -4.0160 400.1995 404.2155 362.9339 537.4705 -4.0105 399.9708 403.9812 362.7157 539.0894 -4.0055 399.7830 403.7885 362.5132 540.6926 -4.0057 399.5880 403.5937 362.2887 542.3011 -3.9971 399.3898 403.3869 362.1415 543.9250 -3.9967 399.1554 403.1521 361.9501 545.5128 -3.9944 398.9574 402.9518 361.7343 547.1163 -3.9925 398.7808 402.7733 361.5346 548.7148 -3.9829 398.5697 402.5527 361.3107 550.3334 -3.9713 398.3175 402.2888 361.0619 551.9369 -3.9651 398.1503 402.1153 360.8711 553.5454 -3.9647 397.8800 401.8447 360.6558 555.1486 -3.9591 397.6606 401.6197 360.3912 556.7523 -3.9510 397.4516 401.4027 360.1678 558.3660 -3.9473 397.2404 401.1878 359.9573 559.9691 -3.9447 397.0365 400.9811 359.7858 561.5625 -3.9403 396.8510 400.7913 359.5268 563.1965 -3.9382 396.6060 400.5441 359.2540 564.8051 -3.9319 396.3833 400.3152 358.9920 566.3983 -3.9278 396.1992 400.1270 358.7692 568.0066 -3.9242 396.0118 399.9360 358.5379 569.6100 -3.9195 395.8237 399.7432 358.3230 571.2238 -3.9189 395.6529 399.5718 358.0872 572.8271 -3.9084 395.4644 399.3728 357.8651 574.4511 -3.8971 395.2491 399.1462 357.6638 576.0599 -3.8892 395.0557 398.9449 357.5227 577.6685 -3.8854 394.8578 398.7432 357.3587 579.2665 -3.8814 394.6422 398.5236 357.1731 580.8649 -3.8775 394.4219 398.2994 357.0217 582.4734 -3.8694 394.2023 398.0716 356.8467 584.0614 -3.8644 393.9893 397.8537 356.6613 585.6649 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1595.2986 -1.5706 261.2800 262.8506 224.1156 1596.9031 -1.5721 261.0703 262.6424 223.8537 1598.5181 -1.5648 260.8818 262.4466 223.6004 1600.1219 -1.5622 260.6466 262.2088 223.4131 1601.7318 -1.5564 260.4459 262.0024 223.2013 1603.3513 -1.5532 260.2430 261.7962 223.0028 1604.9556 -1.5505 260.0503 261.6008 222.8302 1606.5654 -1.5489 259.8563 261.4051 222.6181 1608.1693 -1.5485 259.6597 261.2082 222.4180 1609.7791 -1.5470 259.4574 261.0044 222.1886 1611.3830 -1.5448 259.2160 260.7608 221.9745 1612.9774 -1.5421 258.9819 260.5241 221.7795 1614.6021 -1.5380 258.7715 260.3095 221.5461 1616.2064 -1.5314 258.5665 260.0980 221.3134 1617.8161 -1.5249 258.3158 259.8408 221.0972 1619.4046 -1.5198 258.0912 259.6110 220.9052 1621.0094 -1.5189 257.8915 259.4104 220.7038 1622.6190 -1.5196 257.6753 259.1949 220.4589 1624.2230 -1.5212 257.4992 259.0204 220.2256 1625.8329 -1.5259 257.2859 258.8118 220.0122 1627.4526 -1.5217 257.0617 258.5834 219.8143 1629.0619 -1.5138 256.8611 258.3749 219.6046 1630.6666 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