DTA measure 2lassumeres Date: 2026310:178 Lower limit = 20.0 C Upper limit = 300.0 C Rate = 5.00 C/min Mtime = 978.83 s Mass = 612.700 mg data_number = 1215 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1795 -0.7869 292.3109 293.0977 264.9102 2.0485 -0.7886 292.2415 293.0301 264.8730 2.8048 -0.7880 292.1791 292.9671 264.8245 3.6215 -0.7861 292.1357 292.9218 264.8115 4.4290 -0.7864 292.0972 292.8837 264.7815 5.2160 -0.7847 292.0397 292.8244 264.7517 6.0440 -0.7854 291.9857 292.7710 264.7220 6.8105 -0.7814 291.9477 292.7291 264.7299 7.6580 -0.7828 291.9033 292.6862 264.7579 8.4245 -0.7820 291.8701 292.6521 264.7375 9.2525 -0.7838 291.8265 292.6103 264.7193 10.0495 -0.7823 291.7823 292.5646 264.7067 10.8460 -0.7813 291.7563 292.5376 264.7027 11.6638 -0.7803 291.7299 292.5102 264.6806 12.4303 -0.7828 291.6793 292.4622 264.6618 13.2885 -0.7885 291.6503 292.4387 264.6537 14.0135 -0.7891 291.5893 292.3784 264.6640 14.8825 -0.7925 291.5428 292.3353 264.6724 15.6490 -0.7889 291.4926 292.2815 264.6690 16.4765 -0.7848 291.4159 292.2006 264.6528 17.2733 -0.7845 291.3653 292.1498 264.6261 18.0705 -0.7856 291.3272 292.1128 264.6056 18.8985 -0.7859 291.2841 292.0700 264.5527 19.6643 -0.7815 291.2472 292.0288 264.4962 20.4818 -0.7814 291.1885 291.9699 264.4449 21.2585 -0.7827 291.1109 291.8935 264.4035 22.1070 -0.7842 291.0534 291.8376 264.3484 22.8728 -0.7844 291.0217 291.8061 264.3245 23.7005 -0.7844 290.9742 291.7586 264.3059 24.4978 -0.7851 290.9372 291.7223 264.2714 25.2950 -0.7822 290.8906 291.6728 264.2066 26.1123 -0.7831 290.8389 291.6220 264.1633 26.9193 -0.7833 290.7879 291.5712 264.1347 27.7370 -0.7838 290.7301 291.5139 264.0800 28.5035 -0.7826 290.6732 291.4558 264.0181 29.3615 -0.7858 290.6403 291.4261 263.9799 30.1278 -0.7840 290.6024 291.3864 263.9638 30.9455 -0.7822 290.5712 291.3534 263.9272 31.7530 -0.7819 290.5539 291.3358 263.8644 32.5393 -0.7835 290.5216 291.3051 263.8014 33.3670 -0.7830 290.4959 291.2790 263.7427 34.1335 -0.7813 290.4545 291.2358 263.6932 35.0025 -0.7764 290.3889 291.1654 263.6357 35.7583 -0.7778 290.3396 291.1174 263.5905 36.6165 -0.7776 290.2693 291.0470 263.5143 37.3420 -0.7751 290.2246 290.9997 263.4572 38.1905 -0.7748 290.1723 290.9472 263.3891 38.9670 -0.7727 290.1363 290.9089 263.3225 39.7943 -0.7747 290.0576 290.8322 263.2775 40.5915 -0.7732 289.9847 290.7579 263.2375 41.3785 -0.7750 289.9350 290.7101 263.1927 42.2168 -0.7796 289.9054 290.6849 263.1300 42.9725 -0.7796 289.8537 290.6333 263.0873 43.8308 -0.7797 289.8158 290.5955 263.0458 44.5973 -0.7784 289.7881 290.5666 263.0128 45.4253 -0.7770 289.7495 290.5264 262.9628 46.2218 -0.7769 289.6892 290.4662 262.8752 47.0085 -0.7742 289.6650 290.4391 262.8279 47.8468 -0.7708 289.6131 290.3838 262.7822 48.6030 -0.7715 289.5875 290.3590 262.7044 49.4613 -0.7702 289.5333 290.3035 262.6695 50.2273 -0.7680 289.4954 290.2634 262.6438 51.0553 -0.7666 289.4290 290.1957 262.5930 51.8423 -0.7657 289.3763 290.1420 262.5600 52.6395 -0.7635 289.3234 290.0869 262.5263 53.4568 -0.7670 289.2907 290.0577 262.4818 54.2125 -0.7682 289.2617 290.0299 262.4462 55.0713 -0.7640 289.2314 289.9954 262.4003 55.8275 -0.7625 289.1941 289.9566 262.3564 56.6553 -0.7617 289.1653 289.9271 262.2903 57.4518 -0.7620 289.1075 289.8694 262.2704 58.2388 -0.7594 289.0374 289.7967 262.2342 59.0668 -0.7573 289.0122 289.7696 262.1896 59.8230 -0.7572 288.9826 289.7398 262.1661 60.6713 -0.7591 288.9036 289.6627 262.1308 61.4473 -0.7582 288.8632 289.6213 262.1091 62.2650 -0.7592 288.8300 289.5891 262.0659 63.0623 -0.7574 288.7909 289.5483 262.0373 63.8595 -0.7574 288.7425 289.5000 262.0067 64.6763 -0.7561 288.6920 289.4481 261.9756 65.4428 -0.7557 288.6512 289.4069 261.9601 66.3015 -0.7539 288.6065 289.3605 261.9368 67.0578 -0.7470 288.5880 289.3350 261.9300 67.8858 -0.7490 288.5355 289.2845 261.8946 68.6820 -0.7520 288.4927 289.2447 261.8687 69.4793 -0.7506 288.4301 289.1806 261.8260 70.2765 -0.7536 288.3965 289.1501 261.7803 71.0635 -0.7531 288.3465 289.0997 261.7649 71.8910 -0.7516 288.3144 289.0660 261.7426 72.6570 -0.7501 288.2779 289.0280 261.7299 73.5055 -0.7490 288.1800 288.9290 261.6611 74.2823 -0.7468 288.1744 288.9212 261.6503 75.1000 -0.7438 288.1456 288.8894 261.6167 75.8963 -0.7446 288.1086 288.8532 261.5899 76.6935 -0.7440 288.0955 288.8395 261.5684 77.5215 -0.7448 288.0562 288.8010 261.5234 78.2878 -0.7445 288.0223 288.7668 261.4848 79.1355 -0.7423 287.9522 288.6945 261.4547 79.9123 -0.7425 287.8874 288.6299 261.4061 80.7300 -0.7420 287.8534 288.5954 261.4022 81.5270 -0.7413 287.8153 288.5566 261.3509 82.3235 -0.7391 287.7673 288.5064 261.3044 83.1515 -0.7393 287.7330 288.4723 261.2338 83.9180 -0.7382 287.6848 288.4230 261.1732 84.7353 -0.7381 287.6342 288.3723 261.1368 85.5115 -0.7371 287.6177 288.3547 261.0985 86.3600 -0.7355 287.5719 288.3074 261.0732 87.1060 -0.7363 287.5449 288.2812 261.0597 87.9853 -0.7342 287.4743 288.2085 261.0045 88.7508 -0.7338 287.4332 288.1670 260.9596 89.5685 -0.7408 287.3792 288.1200 260.8978 90.3760 -0.7382 287.3434 288.0816 260.8513 91.1630 -0.7328 287.2898 288.0226 260.8173 91.9910 -0.7273 287.2640 287.9913 260.7879 92.7565 -0.7252 287.2098 287.9350 260.7672 93.6153 -0.7273 287.1683 287.8956 260.7187 94.3510 -0.7285 287.1535 287.8821 260.6855 95.2098 -0.7264 287.0802 287.8066 260.5728 95.9763 -0.7273 287.0366 287.7639 260.5301 96.8033 -0.7283 286.9776 287.7059 260.4773 97.5800 -0.7269 286.9655 287.6924 260.4067 98.4285 -0.7241 286.9079 287.6320 260.3531 99.2155 -0.7218 286.8553 287.5771 260.3133 100.0120 -0.7173 286.8134 287.5307 260.2549 100.8398 -0.7224 286.7839 287.5062 260.2148 101.6063 -0.7213 286.7164 287.4377 260.1805 102.4650 -0.7203 286.6366 287.3569 260.1101 103.2213 -0.7180 286.6159 287.3338 260.0445 104.0585 -0.7130 286.5934 287.3064 260.0027 104.8455 -0.7106 286.5556 287.2662 259.9482 105.6428 -0.7089 286.5083 287.2171 259.9314 106.4708 -0.7090 286.4495 287.1584 259.8780 107.2373 -0.7070 286.3973 287.1042 259.8376 108.1060 -0.7045 286.3550 287.0596 259.8057 108.8513 -0.7057 286.3162 287.0218 259.7530 109.7100 -0.7061 286.2549 286.9610 259.7134 110.4663 -0.7050 286.2245 286.9295 259.6721 111.3045 -0.7023 286.1954 286.8978 259.6239 112.0908 -0.7036 286.1595 286.8631 259.6110 112.8878 -0.7029 286.1173 286.8202 259.5894 113.7158 -0.6995 286.0503 286.7498 259.5539 114.4823 -0.6955 286.0077 286.7031 259.4959 115.3405 -0.6988 285.9607 286.6596 259.4850 116.0655 -0.7002 285.9367 286.6369 259.4714 116.9345 -0.6989 285.8881 286.5870 259.4359 117.6908 -0.6966 285.8506 286.5472 259.4050 118.5388 -0.6936 285.8189 286.5125 259.3790 119.2945 -0.6915 285.7808 286.4723 259.3457 120.1225 -0.6913 285.7451 286.4364 259.2870 120.8890 -0.6873 285.7043 286.3915 259.2516 121.7065 -0.6848 285.6578 286.3426 259.2000 122.5030 -0.6853 285.6161 286.3013 259.1701 123.3003 -0.6841 285.5755 286.2596 259.1489 124.1283 -0.6798 285.5263 286.2061 259.1121 124.8845 -0.6808 285.4928 286.1736 259.0865 125.7430 -0.6816 285.4774 286.1590 259.0414 126.5088 -0.6826 285.4414 286.1240 258.9954 127.3265 -0.6798 285.4115 286.0914 258.9715 128.1545 -0.6782 285.3668 286.0450 258.9424 129.1260 -0.6785 285.3096 285.9881 258.9115 129.9125 -0.6771 285.2575 285.9346 258.8674 130.7400 -0.6742 285.2083 285.8825 258.8250 131.5065 -0.6736 285.1411 285.8148 258.7898 132.3653 -0.6757 285.1058 285.7815 258.7520 133.1215 -0.6771 285.0798 285.7569 258.7102 133.9490 -0.6784 285.0125 285.6910 258.6895 134.7458 -0.6780 284.9673 285.6454 258.6730 135.5430 -0.6765 284.9288 285.6053 258.6384 136.3608 -0.6764 284.8940 285.5704 258.5906 137.1375 -0.6789 284.8544 285.5333 258.5519 137.9850 -0.6752 284.8122 285.4874 258.5212 138.7208 -0.6708 284.7876 285.4585 258.4719 139.5795 -0.6709 284.7275 285.3984 258.4603 140.3460 -0.6724 284.6530 285.3254 258.4349 141.1733 -0.6690 284.5938 285.2627 258.3850 141.9600 -0.6701 284.5706 285.2407 258.3519 142.7675 -0.6701 284.5325 285.2026 258.3168 143.5853 -0.6712 284.4861 285.1572 258.2569 144.3510 -0.6687 284.4452 285.1139 258.2218 145.2095 -0.6667 284.4134 285.0801 258.1302 145.9760 -0.6664 284.3652 285.0316 258.0629 146.8040 -0.6684 284.3301 284.9985 258.0326 147.5908 -0.6692 284.2783 284.9475 257.9931 148.3975 -0.6680 284.2279 284.8959 257.9311 149.2153 -0.6669 284.1802 284.8471 257.8717 149.9818 -0.6678 284.1247 284.7924 257.8157 150.8405 -0.6667 284.0885 284.7553 257.7564 151.6063 -0.6608 284.0268 284.6876 257.7263 152.4340 -0.6598 283.9910 284.6508 257.6636 153.2210 -0.6574 283.9616 284.6190 257.6106 154.0285 -0.6570 283.9388 284.5958 257.5427 154.8460 -0.6612 283.9182 284.5794 257.5121 155.6118 -0.6616 283.8862 284.5478 257.4912 156.4705 -0.6626 283.8336 284.4963 257.4643 157.2370 -0.6626 283.8215 284.4842 257.4307 158.0650 -0.6599 283.7449 284.4048 257.3882 158.8930 -0.6585 283.6889 284.3474 257.3538 159.8533 -0.6596 283.6262 284.2858 257.3083 160.6505 -0.6568 283.5857 284.2425 257.2728 161.4785 -0.6574 283.5636 284.2211 257.2489 162.2450 -0.6549 283.4946 284.1495 257.1870 163.0925 -0.6559 283.4428 284.0987 257.1539 163.8693 -0.6555 283.4322 284.0877 257.1094 164.6870 -0.6580 283.3986 284.0566 257.0662 165.4843 -0.6612 283.3659 284.0271 257.0253 166.2810 -0.6570 283.3254 283.9824 256.9852 167.1085 -0.6567 283.2802 283.9369 256.9473 167.8750 -0.6627 283.2279 283.8906 256.9343 168.7235 -0.6560 283.1822 283.8382 256.8858 169.5003 -0.6521 283.1602 283.8123 256.8439 170.3175 -0.6504 283.1450 283.7953 256.8071 171.1143 -0.6521 283.0895 283.7416 256.7727 171.9115 -0.6521 283.0502 283.7022 256.7366 172.7395 -0.6503 283.0358 283.6861 256.7259 173.5058 -0.6489 282.9964 283.6453 256.6792 174.3535 -0.6484 282.9588 283.6072 256.6413 175.1303 -0.6459 282.9179 283.5639 256.6028 175.9480 -0.6455 282.8643 283.5097 256.5870 176.7453 -0.6452 282.8141 283.4593 256.5548 177.5423 -0.6448 282.7731 283.4179 256.5223 178.3798 -0.6414 282.7027 283.3441 256.4959 179.1360 -0.6356 282.6720 283.3076 256.4816 179.9743 -0.6363 282.6283 283.2646 256.4369 180.7305 -0.6342 282.5736 283.2078 256.3859 181.5885 -0.6351 282.5452 283.1803 256.3565 182.3548 -0.6380 282.5216 283.1596 256.3075 183.1725 -0.6377 282.4922 283.1299 256.2497 183.9390 -0.6366 282.4524 283.0890 256.2045 184.7568 -0.6381 282.3951 283.0332 256.1616 185.5533 -0.6359 282.3695 283.0054 256.1116 186.3400 -0.6367 282.3217 282.9583 256.0854 187.1680 -0.6356 282.2669 282.9025 256.0739 187.9345 -0.6336 282.1950 282.8287 256.0503 188.7823 -0.6337 282.1643 282.7980 256.0203 189.5280 -0.6299 282.1281 282.7580 255.9857 190.3868 -0.6260 282.1021 282.7281 255.9551 191.1533 -0.6190 282.0676 282.6866 255.9288 191.9813 -0.6154 282.0273 282.6427 255.8201 192.7673 -0.6191 282.0054 282.6245 255.7258 193.5645 -0.6197 281.9587 282.5784 255.6706 194.3925 -0.6232 281.8933 282.5164 255.6437 195.1590 -0.6226 281.8111 282.4337 255.6091 196.0073 -0.6251 281.7697 282.3948 255.5799 196.7730 -0.6263 281.7304 282.3567 255.5537 197.5908 -0.6232 281.6610 282.2842 255.4934 198.3880 -0.6207 281.6196 282.2403 255.4465 199.1853 -0.6211 281.5931 282.2142 255.4084 200.0125 -0.6267 281.5721 282.1988 255.3804 200.7890 -0.6283 281.5410 282.1693 255.3184 201.6068 -0.6309 281.5045 282.1353 255.3022 202.3835 -0.6272 281.4670 282.0942 255.2717 203.2320 -0.6254 281.4688 282.0942 255.1913 203.9978 -0.6188 281.4225 282.0413 255.1534 204.8255 -0.6165 281.3828 281.9993 255.1246 205.6228 -0.6153 281.3414 281.9567 255.0733 206.4198 -0.6130 281.3094 281.9224 255.0382 207.2368 -0.6120 281.2823 281.8943 255.0164 208.0135 -0.6140 281.2448 281.8588 254.9715 208.8313 -0.6102 281.2111 281.8213 254.9248 209.5978 -0.6113 281.1816 281.7929 254.8796 210.4763 -0.6122 281.1254 281.7376 254.8412 211.2015 -0.6111 281.0619 281.6731 254.7798 212.0705 -0.6112 281.0244 281.6356 254.7238 212.8268 -0.6151 280.9670 281.5821 254.6775 213.6645 -0.6167 280.9162 281.5330 254.6442 214.4510 -0.6144 280.8769 281.4912 254.6117 215.2585 -0.6144 280.8176 281.4320 254.5627 216.0763 -0.6141 280.7801 281.3942 254.5126 216.8428 -0.6125 280.7429 281.3555 254.4697 217.7005 -0.6131 280.6772 281.2902 254.4391 218.4670 -0.6110 280.6381 281.2491 254.3951 219.2950 -0.6107 280.5919 281.2026 254.3584 220.0820 -0.6106 280.5907 281.2013 254.3319 220.9095 -0.6097 280.5526 281.1623 254.2932 221.6653 -0.6091 280.5266 281.1357 254.2438 222.5035 -0.6077 280.4732 281.0809 254.1789 223.2905 -0.6097 280.4428 281.0524 254.1389 224.0873 -0.6083 280.3818 280.9901 254.1012 224.9148 -0.6075 280.3445 280.9520 254.0665 225.6813 -0.6080 280.2827 280.8907 254.0330 226.5400 -0.6042 280.2257 280.8299 254.0081 227.2963 -0.6026 280.1822 280.7848 253.9938 228.1335 -0.6006 280.1564 280.7570 253.9799 228.9308 -0.6008 280.1170 280.7178 253.9087 229.7178 -0.5976 280.0805 280.6781 253.8364 230.5765 -0.5966 280.0433 280.6400 253.7977 231.3423 -0.5962 280.0041 280.6002 253.7742 232.1700 -0.5964 279.9885 280.5849 253.7462 232.9570 -0.5991 279.9284 280.5275 253.7379 233.7645 -0.5965 279.8565 280.4530 253.7260 234.5515 -0.5950 279.8267 280.4217 253.7024 235.3483 -0.5907 279.7855 280.3762 253.6591 236.1758 -0.5882 279.7377 280.3259 253.6335 236.9525 -0.5887 279.6862 280.2749 253.5940 237.8010 -0.5876 279.6358 280.2235 253.5672 238.5675 -0.5861 279.5944 280.1805 253.5445 239.3945 -0.5864 279.5536 280.1399 253.5468 240.1918 -0.5864 279.5124 280.0988 253.5100 240.9890 -0.5863 279.4693 280.0556 253.4402 241.8065 -0.5879 279.4378 280.0257 253.4366 242.5825 -0.5924 279.3985 279.9908 253.4174 243.4413 -0.5890 279.3741 279.9631 253.3810 244.2078 -0.5879 279.3382 279.9262 253.3206 245.0253 -0.5871 279.3016 279.8887 253.2836 245.7910 -0.5865 279.2372 279.8238 253.2503 246.6088 -0.5874 279.1881 279.7755 253.1928 247.4060 -0.5865 279.1337 279.7202 253.1323 248.1930 -0.5855 279.0740 279.6595 253.0957 249.0103 -0.5813 279.0264 279.6077 253.0318 249.7763 -0.5808 278.9673 279.5481 252.9838 250.6350 -0.5752 278.9239 279.4991 252.9135 251.3913 -0.5751 278.8857 279.4608 252.8926 252.2193 -0.5746 278.8434 279.4181 252.8527 253.0155 -0.5755 278.8131 279.3886 252.8233 253.8025 -0.5789 278.7695 279.3484 252.7802 254.6100 -0.5797 278.7272 279.3070 252.7210 255.3970 -0.5799 278.6729 279.2527 252.6533 256.2348 -0.5832 278.6049 279.1881 252.6013 256.9905 -0.5852 278.5585 279.1436 252.5635 257.8493 -0.5836 278.5307 279.1143 252.5307 258.5850 -0.5824 278.5087 279.0912 252.5020 259.4335 -0.5787 278.4863 279.0650 252.4729 260.2093 -0.5778 278.4423 279.0201 252.4378 261.0270 -0.5804 278.3733 278.9537 252.3949 261.8243 -0.5827 278.3208 278.9035 252.3368 262.6215 -0.5848 278.2865 278.8713 252.2808 263.4495 -0.5838 278.2544 278.8382 252.2204 264.2153 -0.5813 278.2250 278.8063 252.1916 265.0635 -0.5801 278.1873 278.7675 252.1619 265.8403 -0.5810 278.1623 278.7433 252.1277 266.6580 -0.5785 278.1323 278.7109 252.0861 267.4343 -0.5751 278.0864 278.6616 252.0662 268.2515 -0.5742 278.0232 278.5975 252.0305 269.0488 -0.5715 277.9776 278.5492 251.9882 269.8460 -0.5725 277.9435 278.5160 251.9397 270.6738 -0.5696 277.9209 278.4905 251.8883 271.4395 -0.5706 277.8986 278.4692 251.8541 272.2983 -0.5757 277.8595 278.4352 251.7873 273.0648 -0.5776 277.8274 278.4050 251.7106 273.8823 -0.5730 277.7712 278.3442 251.6400 274.6788 -0.5707 277.7450 278.3157 251.6150 275.4760 -0.5710 277.7310 278.3020 251.6064 276.2938 -0.5706 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