DTA measure 1gyrss Date: 2024115:1457 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1102.13 s Mass = 960 mg data_number = 1368 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0673 -0.5947 242.8958 243.4904 238.3978 1.8560 -0.5881 242.8715 243.4596 238.4390 2.6745 -0.5848 242.8851 243.4699 238.4689 3.4633 -0.5842 242.8799 243.4641 238.4695 4.2830 -0.5842 242.8770 243.4612 238.4862 5.0720 -0.5832 242.8726 243.4558 238.5062 5.8665 -0.5802 242.8750 243.4552 238.5223 6.6943 -0.5818 242.8630 243.4448 238.5517 7.4578 -0.5836 242.8511 243.4347 238.5730 8.3083 -0.5851 242.8381 243.4232 238.5813 9.0978 -0.5791 242.8302 243.4093 238.6069 9.8880 -0.5782 242.8166 243.3948 238.6511 10.7085 -0.5805 242.8392 243.4197 238.6751 11.4728 -0.5826 242.8333 243.4160 238.7039 12.3298 -0.5827 242.8111 243.3938 238.7346 13.0938 -0.5892 242.7997 243.3889 238.7427 13.9155 -0.5793 242.7901 243.3694 238.7661 14.7413 -0.5813 242.7937 243.3750 238.8297 15.5045 -0.5850 242.7928 243.3778 238.8616 16.3568 -0.5841 242.7773 243.3614 238.9071 17.1200 -0.5863 242.7802 243.3665 238.9533 17.9455 -0.5872 242.7564 243.3437 239.0113 18.7413 -0.5889 242.7496 243.3384 239.0794 19.5368 -0.5862 242.7445 243.3307 239.1187 20.3668 -0.5835 242.7335 243.3170 239.1779 21.1285 -0.5853 242.7229 243.3083 239.2225 21.9805 -0.5878 242.7252 243.3129 239.2996 22.7725 -0.5886 242.7128 243.3013 239.3679 23.5643 -0.5993 242.7155 243.3148 239.4442 24.3860 -0.6016 242.7083 243.3098 239.5133 25.1475 -0.6011 242.7177 243.3188 239.5887 26.0000 -0.6003 242.6855 243.2858 239.6736 26.7920 -0.6053 242.6764 243.2817 239.7557 27.5835 -0.6088 242.6697 243.2785 239.8388 28.4068 -0.6109 242.6490 243.2599 239.9358 29.1685 -0.6113 242.6498 243.2610 240.0161 30.0210 -0.6096 242.6444 243.2540 240.1306 30.7830 -0.6125 242.6442 243.2567 240.2193 31.6058 -0.6122 242.6367 243.2489 240.3207 32.4280 -0.6107 242.6206 243.2313 240.4284 33.1895 -0.6132 242.6281 243.2413 240.5195 34.0455 -0.6172 242.6257 243.2429 240.6507 34.8100 -0.6170 242.6068 243.2238 240.7596 35.6325 -0.6147 242.6082 243.2229 240.8763 36.4303 -0.6151 242.5910 243.2061 240.9854 37.2268 -0.6217 242.6037 243.2254 241.1029 38.0808 -0.6329 242.5870 243.2199 241.2349 38.8450 -0.6331 242.5809 243.2140 241.3867 39.6685 -0.6411 242.5733 243.2144 241.5161 40.4605 -0.6393 242.5681 243.2074 241.6316 41.2525 -0.6443 242.5770 243.2213 241.7522 42.0703 -0.6438 242.5749 243.2187 241.8908 42.8540 -0.6462 242.5600 243.2061 242.0311 43.6703 -0.6455 242.5517 243.1972 242.1625 44.4615 -0.6450 242.5404 243.1853 242.3071 45.2510 -0.6467 242.5468 243.1935 242.4378 46.0720 -0.6671 242.5500 243.2171 242.5829 46.8340 -0.6650 242.5556 243.2206 242.6973 47.6878 -0.6548 242.5455 243.2003 242.8345 48.4538 -0.6551 242.5399 243.1951 242.9932 49.2810 -0.6518 242.5350 243.1868 243.1366 50.0700 -0.6533 242.5290 243.1823 243.2813 50.8598 -0.6623 242.5283 243.1906 243.4132 51.6788 -0.6767 242.5261 243.2027 243.5589 52.4375 -0.6701 242.5281 243.1982 243.7010 53.2903 -0.6702 242.5142 243.1845 243.8378 54.0490 -0.6809 242.5165 243.1974 243.9875 54.8693 -0.7143 242.5276 243.2418 244.1317 55.6910 -0.7109 242.5280 243.2389 244.2567 56.4533 -0.7064 242.5287 243.2351 244.3828 57.3045 -0.7068 242.5208 243.2275 244.5513 58.0945 -0.7207 242.5200 243.2407 244.6886 58.8830 -0.7334 242.5080 243.2414 244.8117 59.7315 -0.7381 242.5167 243.2548 244.9653 60.4955 -0.7257 242.5262 243.2519 245.0841 61.3148 -0.7314 242.5153 243.2466 245.2345 62.1035 -0.7452 242.5105 243.2557 245.3795 62.8940 -0.7372 242.5157 243.2529 245.5147 63.7455 -0.7142 242.5172 243.2314 245.6804 64.5075 -0.7169 242.5208 243.2378 245.8170 65.3298 -0.7201 242.5309 243.2510 245.9631 66.1185 -0.7234 242.5346 243.2580 246.0925 66.9080 -0.7260 242.5360 243.2620 246.2264 67.7593 -0.7291 242.5298 243.2589 246.3733 68.5180 -0.7333 242.5415 243.2748 246.4882 69.3368 -0.7397 242.5455 243.2852 246.6268 70.1560 -0.7410 242.5458 243.2867 246.7675 70.9148 -0.7419 242.5668 243.3086 246.8884 71.7650 -0.7482 242.5763 243.3244 247.0260 72.5540 -0.7520 242.5615 243.3134 247.1498 73.3440 -0.7551 242.5636 243.3187 247.2780 74.1640 -0.7649 242.5766 243.3416 247.4298 74.9280 -0.7837 242.5895 243.3731 247.5540 75.7865 -0.7949 242.6067 243.4016 247.6886 76.5488 -0.7992 242.6251 243.4242 247.8188 77.3708 -0.8019 242.6282 243.4301 247.9573 78.1930 -0.7901 242.6250 243.4150 248.0784 78.9553 -0.7895 242.6417 243.4312 248.1995 79.8080 -0.8006 242.6372 243.4378 248.3324 80.5700 -0.7947 242.6253 243.4200 248.4496 81.3918 -0.7965 242.6281 243.4246 248.6013 82.2140 -0.7986 242.6456 243.4442 248.7283 82.9755 -0.8069 242.6636 243.4706 248.8394 83.8280 -0.8230 242.6739 243.4969 248.9611 84.5898 -0.8256 242.6899 243.5155 249.0859 85.4118 -0.8216 242.7108 243.5324 249.2047 86.2048 -0.8207 242.7206 243.5413 249.3296 86.9975 -0.8230 242.7321 243.5551 249.4560 87.8495 -0.8295 242.7382 243.5677 249.5970 88.6160 -0.8438 242.7561 243.5998 249.7045 89.4415 -0.8503 242.7653 243.6156 249.8161 90.2360 -0.8578 242.7803 243.6381 249.9332 91.0320 -0.8602 242.8008 243.6610 250.0505 91.8545 -0.8639 242.8293 243.6931 250.1649 92.6165 -0.8620 242.8269 243.6889 250.2860 93.4685 -0.8602 242.8466 243.7069 250.4075 94.2310 -0.8556 242.8606 243.7162 250.5249 95.0550 -0.8536 242.8766 243.7302 250.6452 95.8778 -0.8569 242.8815 243.7384 250.7601 96.6420 -0.8665 242.8948 243.7613 250.8638 97.4945 -0.8717 242.9278 243.7994 250.9908 98.2585 -0.8771 242.9422 243.8193 251.0948 99.0805 -0.8913 242.9613 243.8526 251.2121 99.9025 -0.9026 242.9809 243.8835 251.3234 100.6650 -0.9060 242.9815 243.8874 251.4127 101.5185 -0.9127 243.0033 243.9160 251.5301 102.2803 -0.9071 243.0303 243.9374 251.6630 103.1020 -0.8968 243.0432 243.9400 251.7756 103.9240 -0.8918 243.0732 243.9649 251.9023 104.6858 -0.8958 243.0915 243.9873 252.0148 105.5420 -0.8966 243.1132 244.0098 252.1344 106.3050 -0.9015 243.1442 244.0457 252.2432 107.1215 -0.9039 243.1575 244.0614 252.3566 107.9060 -0.9097 243.1720 244.0817 252.4762 108.6905 -0.9157 243.1913 244.1070 252.5948 109.5358 -0.9200 243.2299 244.1499 252.7142 110.3275 -0.9236 243.2523 244.1759 252.8383 111.1180 -0.9267 243.2700 244.1967 252.9522 111.9350 -0.9332 243.3040 244.2372 253.0513 112.6940 -0.9313 243.3169 244.2481 253.1844 113.5423 -0.9359 243.3373 244.2732 253.3074 114.3303 -0.9405 243.3646 244.3051 253.4263 115.1180 -0.9357 243.3833 244.3190 253.5393 115.9365 -0.9358 243.4001 244.3360 253.6609 116.6940 -0.9390 243.4320 244.3710 253.7794 117.5423 -0.9428 243.4631 244.4060 253.9161 118.3303 -0.9479 243.4799 244.4278 254.0325 119.1180 -0.9524 243.4920 244.4443 254.1558 119.9363 -0.9599 243.5444 244.5043 254.2838 120.7243 -0.9651 243.5874 244.5525 254.3950 121.5420 -0.9714 243.6022 244.5737 254.5322 122.3315 -0.9659 243.6210 244.5870 254.6743 123.1200 -0.9671 243.6508 244.6179 254.7972 123.9383 -0.9753 243.6606 244.6359 254.9165 124.7268 -0.9798 243.6997 244.6795 255.0518 125.5460 -0.9812 243.7475 244.7287 255.1863 126.3343 -0.9866 243.7571 244.7437 255.3110 127.1220 -0.9874 243.7955 244.7829 255.4515 127.9708 -0.9855 243.8214 244.8070 255.5847 128.7293 -0.9900 243.8593 244.8492 255.7051 129.5478 -1.0029 243.8965 244.8994 255.8447 130.3678 -1.0019 243.9369 244.9387 255.9641 131.1270 -1.0004 243.9515 244.9518 256.0942 131.9755 -1.0054 243.9894 244.9948 256.2406 132.7645 -1.0115 244.0099 245.0214 256.3615 133.5540 -1.0176 244.0279 245.0455 256.4871 134.3738 -1.0194 244.0903 245.1097 256.6406 135.1635 -1.0248 244.1209 245.1457 256.7576 135.9838 -1.0275 244.1426 245.1701 256.8814 136.7725 -1.0321 244.1768 245.2088 257.0259 137.5668 -1.0363 244.2078 245.2441 257.1529 138.3895 -1.0353 244.2432 245.2785 257.2988 139.1823 -1.0394 244.2907 245.3301 257.4050 140.0065 -1.0436 244.3259 245.3695 257.5369 140.7978 -1.0440 244.3579 245.4019 257.6971 141.5895 -1.0495 244.3862 245.4357 257.8364 142.4125 -1.0494 244.4190 245.4684 257.9546 143.2040 -1.0530 244.4589 245.5119 258.0666 144.0255 -1.0550 244.4961 245.5510 258.2056 144.8178 -1.0578 244.5385 245.5963 258.3399 145.6105 -1.0605 244.5925 245.6530 258.4810 146.4325 -1.0632 244.6325 245.6957 258.5920 147.1945 -1.0700 244.6574 245.7274 258.7052 148.0468 -1.0735 244.6971 245.7706 258.8382 148.8385 -1.0741 244.7451 245.8191 258.9621 149.6305 -1.0745 244.7800 245.8545 259.0876 150.4600 -1.0778 244.8219 245.8997 259.2237 151.2255 -1.0811 244.8448 245.9259 259.3494 152.0775 -1.0831 244.8890 245.9721 259.4821 152.8395 -1.0874 244.9432 246.0306 259.5915 153.6620 -1.0925 244.9942 246.0868 259.7283 154.4540 -1.0925 245.0461 246.1386 259.8387 155.2455 -1.0928 245.0716 246.1644 259.9741 156.1000 -1.0995 245.1352 246.2347 260.0964 156.8398 -1.1032 245.1620 246.2652 260.2019 157.6930 -1.1058 245.2119 246.3177 260.3447 158.4598 -1.1094 245.2479 246.3573 260.4659 159.2828 -1.1094 245.2883 246.3977 260.5827 160.1095 -1.1083 245.3240 246.4323 260.7139 160.8745 -1.1076 245.3746 246.4821 260.8200 161.7290 -1.1094 245.4263 246.5357 260.9476 162.4918 -1.1101 245.4733 246.5833 261.0728 163.3138 -1.1130 245.5298 246.6428 261.2018 164.1060 -1.1148 245.5635 246.6783 261.3241 164.8978 -1.1173 245.6118 246.7290 261.4261 165.7498 -1.1195 245.6587 246.7782 261.5480 166.5115 -1.1348 245.7127 246.8476 261.6701 167.3355 -1.1318 245.7641 246.8959 261.8079 168.1278 -1.1275 245.8162 246.9438 261.9421 168.9208 -1.1320 245.8444 246.9764 262.0712 169.7725 -1.1704 245.9005 247.0709 262.2009 170.5388 -1.1784 245.9489 247.1274 262.3133 171.3588 -1.1714 246.0003 247.1717 262.4467 172.1735 -1.1517 246.0481 247.1998 262.5642 172.9628 -1.1466 246.0997 247.2463 262.6957 173.7853 -1.1468 246.1662 247.3131 262.8319 174.5725 -1.1498 246.1973 247.3471 262.9702 175.3610 -1.1538 246.2551 247.4089 263.0831 176.1813 -1.1570 246.2814 247.4384 263.2173 176.9413 -1.1596 246.3404 247.5000 263.3192 177.7685 -1.1626 246.3921 247.5547 263.4784 178.5580 -1.1651 246.4517 247.6168 263.5887 179.3770 -1.1670 246.5094 247.6764 263.7241 180.1700 -1.1705 246.5538 247.7243 263.8512 180.9580 -1.1720 246.6095 247.7815 263.9911 181.7760 -1.1801 246.6736 247.8536 264.1034 182.5640 -1.1878 246.7240 247.9117 264.2166 183.3820 -1.1890 246.7725 247.9615 264.3633 184.1708 -1.1920 246.8260 248.0180 264.4931 184.9610 -1.1957 246.8634 248.0591 264.6091 185.7813 -1.1975 246.9369 248.1343 264.7416 186.5700 -1.2005 246.9935 248.1940 264.8851 187.3880 -1.2028 247.0456 248.2484 265.0071 188.1760 -1.2066 247.1072 248.3138 265.1263 188.9640 -1.2085 247.1818 248.3903 265.2418 189.8125 -1.2085 247.2476 248.4561 265.4054 190.5743 -1.2117 247.2941 248.5057 265.5164 191.3955 -1.2161 247.3479 248.5641 265.6470 192.2213 -1.2160 247.4098 248.6258 265.7805 192.9810 -1.2192 247.4750 248.6942 265.8989 193.8295 -1.2199 247.5112 248.7311 266.0217 194.5883 -1.2238 247.5674 248.7911 266.1429 195.4078 -1.2274 247.6259 248.8533 266.2724 196.2275 -1.2291 247.6917 248.9208 266.4045 196.9870 -1.2364 247.7592 248.9956 266.5127 197.8365 -1.2373 247.8160 249.0533 266.6407 198.6258 -1.2344 247.8845 249.1189 266.7799 199.4170 -1.2355 247.9363 249.1718 266.8881 200.2353 -1.2361 247.9922 249.2284 267.0008 201.0243 -1.2420 248.0481 249.2900 267.1303 201.8433 -1.2429 248.1210 249.3639 267.2513 202.6333 -1.2477 248.1652 249.4130 267.3808 203.4235 -1.2509 248.2191 249.4699 267.4947 204.2758 -1.2515 248.3039 249.5554 267.6310 205.0358 -1.2557 248.3744 249.6301 267.7547 205.8578 -1.2595 248.4404 249.6999 267.8995 206.6500 -1.2621 248.4871 249.7491 268.0140 207.4415 -1.2672 248.5608 249.8280 268.1403 208.2940 -1.2718 248.6281 249.9000 268.2721 209.0558 -1.2744 248.6795 249.9539 268.3857 209.8795 -1.2738 248.7513 250.0251 268.5174 210.7020 -1.2746 248.8119 250.0865 268.6584 211.4635 -1.2782 248.8600 250.1382 268.7763 212.3160 -1.2823 248.9397 250.2221 268.9376 213.1080 -1.2849 249.0086 250.2936 269.0466 213.8995 -1.2887 249.0719 250.3605 269.1775 214.7263 -1.2917 249.1474 250.4390 269.3216 215.4875 -1.2944 249.2245 250.5189 269.4458 216.3463 -1.2959 249.2827 250.5786 269.5756 217.1140 -1.2956 249.3462 250.6418 269.7267 217.9368 -1.2980 249.4128 250.7108 269.8660 218.7288 -1.3053 249.4725 250.7778 269.9862 219.5205 -1.3082 249.5618 250.8700 270.1233 220.3738 -1.3115 249.6252 250.9367 270.2481 221.1385 -1.3134 249.6915 251.0050 270.3568 221.9605 -1.3180 249.7680 251.0861 270.5145 222.7525 -1.3195 249.8158 251.1353 270.6492 223.5445 -1.3196 249.8796 251.1992 270.7763 224.3680 -1.3218 249.9688 251.2905 270.9040 225.1605 -1.3268 250.0401 251.3669 271.0418 225.9825 -1.3298 250.1140 251.4439 271.1694 226.7745 -1.3323 250.1840 251.5164 271.3160 227.5665 -1.3360 250.2561 251.5922 271.4472 228.3900 -1.3390 250.3161 251.6551 271.5735 229.1825 -1.3401 250.3896 251.7297 271.7080 230.0043 -1.3465 250.4689 251.8154 271.8487 230.7963 -1.3525 250.5392 251.8916 271.9634 231.5878 -1.3548 250.6195 251.9742 272.0974 232.4100 -1.3561 250.6978 252.0538 272.2353 233.2018 -1.3552 250.7705 252.1257 272.3674 234.0238 -1.3546 250.8318 252.1865 272.4928 234.8138 -1.3569 250.9199 252.2767 272.6304 235.5955 -1.3617 250.9932 252.3549 272.7396 236.4440 -1.3667 251.0649 252.4316 272.8673 237.1975 -1.3672 251.1256 252.4927 272.9979 238.0160 -1.3672 251.1943 252.5615 273.1511 238.8028 -1.3687 251.2777 252.6464 273.2517 239.5920 -1.3696 251.3583 252.7279 273.3918 240.4385 -1.3731 251.4339 252.8069 273.5231 241.1973 -1.3735 251.4943 252.8678 273.6422 242.0150 -1.3762 251.5754 252.9516 273.7724 242.8333 -1.3803 251.6615 253.0419 273.9008 243.5910 -1.3824 251.7305 253.1129 274.0185 244.4393 -1.3842 251.8151 253.1993 274.1520 245.2273 -1.3858 251.8960 253.2817 274.2822 246.0150 -1.3866 251.9666 253.3532 274.4014 246.8355 -1.3902 252.0586 253.4488 274.5266 247.5940 -1.3909 252.1334 253.5243 274.6434 248.4423 -1.3931 252.2080 253.6012 274.7742 249.2303 -1.3957 252.2905 253.6862 274.9004 250.0180 -1.3962 252.3530 253.7492 275.0030 250.8363 -1.4003 252.4322 253.8324 275.1318 251.6243 -1.4009 252.5073 253.9082 275.2660 252.4430 -1.4027 252.5818 253.9845 275.3758 253.2313 -1.4068 252.6652 254.0720 275.5143 254.0190 -1.4108 252.7590 254.1698 275.6376 254.8680 -1.4110 252.8368 254.2479 275.7472 255.6263 -1.4103 252.9135 254.3238 275.8707 256.4450 -1.4092 252.9858 254.3950 275.9913 257.2635 -1.4146 253.0691 254.4837 276.1264 258.0220 -1.4203 253.1369 254.5571 276.2414 258.8708 -1.4272 253.2215 254.6487 276.3801 259.6593 -1.4285 253.2990 254.7275 276.4894 260.4480 -1.4307 253.3951 254.8258 276.6239 261.2665 -1.4317 253.4860 254.9177 276.7415 262.0553 -1.4324 253.5591 254.9915 276.8716 262.8748 -1.4333 253.6437 255.0771 277.0135 263.6630 -1.4375 253.7287 255.1663 277.1335 264.4520 -1.4400 253.8085 255.2484 277.2651 265.3025 -1.4454 253.8864 255.3318 277.4207 266.0618 -1.4446 253.9750 255.4197 277.5524 266.8828 -1.4396 254.0639 255.5035 277.6836 267.7030 -1.4350 254.1359 255.5710 277.8145 268.4648 -1.4412 254.2199 255.6611 277.9441 269.3195 -1.4510 254.3132 255.7642 278.0987 270.0815 -1.4519 254.3902 255.8421 278.2061 270.9058 -1.4539 254.4772 255.9311 278.3349 271.6995 -1.4528 254.5644 256.0172 278.4856 272.4965 -1.4569 254.6546 256.1115 278.6220 273.3485 -1.4624 254.7310 256.1934 278.7585 274.1123 -1.4685 254.8045 256.2730 278.8862 274.9355 -1.4737 254.8919 256.3656 279.0418 275.7575 -1.4780 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