DTA measure 1lassu Date: 2024115:1551 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1549.56 s Mass = 960.000 mg data_number = 1929 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1418 0.0928 240.8412 240.7484 216.9688 1.9340 0.0964 240.7382 240.6418 216.8978 2.7255 0.0966 240.6485 240.5518 216.8048 3.5530 0.0942 240.5778 240.4836 216.7064 4.3165 0.0940 240.4916 240.3976 216.6313 5.1690 0.0947 240.3850 240.2903 216.5381 5.9633 0.0941 240.2915 240.1974 216.4558 6.7588 0.0966 240.2095 240.1129 216.3676 7.5548 0.0944 240.1080 240.0136 216.2971 8.3465 0.0950 240.0181 239.9231 216.2147 9.1990 0.0955 239.9318 239.8362 216.1359 9.9605 0.0964 239.8545 239.7581 216.0584 10.7825 0.0941 239.7557 239.6616 215.9779 11.5745 0.0946 239.6597 239.5651 215.8839 12.3688 0.0955 239.5831 239.4877 215.8158 13.2205 0.0969 239.5132 239.4163 215.7094 13.9830 0.0953 239.4206 239.3253 215.6283 14.8088 0.0973 239.3235 239.2262 215.5531 15.6015 0.0991 239.2223 239.1232 215.4860 16.3945 0.0969 239.1280 239.0312 215.3903 17.2183 0.0977 239.0261 238.9285 215.3029 17.9828 0.0987 238.9454 238.8467 215.2327 18.8345 0.0985 238.8611 238.7625 215.1278 19.6270 0.0988 238.7880 238.6892 215.0531 20.4205 0.1026 238.7093 238.6067 214.9699 21.2425 0.1017 238.6143 238.5126 214.8936 22.0045 0.1063 238.5368 238.4305 214.8186 22.8573 0.1043 238.4372 238.3329 214.7351 23.6150 0.1017 238.3498 238.2481 214.6482 24.4265 0.0996 238.2606 238.1610 214.5565 25.2420 0.0992 238.1755 238.0762 214.4970 25.9958 0.0978 238.0811 237.9832 214.4276 26.8433 0.1005 237.9919 237.8914 214.3335 27.6075 0.1045 237.9068 237.8023 214.2567 28.4300 0.1024 237.8047 237.7023 214.1825 29.2223 0.1011 237.7212 237.6200 214.0817 30.0170 0.1035 237.6275 237.5240 214.0006 30.8360 0.1067 237.5469 237.4402 213.9128 31.5945 0.1067 237.4643 237.3575 213.8315 32.4430 0.1083 237.3664 237.2581 213.7370 33.2305 0.1084 237.2870 237.1786 213.6667 34.0180 0.1089 237.2139 237.1050 213.5890 34.8370 0.1087 237.1215 237.0127 213.4971 35.5950 0.1092 237.0215 236.9124 213.4175 36.4433 0.1100 236.9259 236.8159 213.3460 37.2330 0.1134 236.8435 236.7301 213.2587 38.0210 0.1144 236.7467 236.6322 213.1893 38.8395 0.1158 236.6670 236.5512 213.1059 39.6273 0.1175 236.5822 236.4648 213.0287 40.4453 0.1183 236.4973 236.3790 212.9325 41.2343 0.1171 236.4184 236.3013 212.8562 42.0230 0.1150 236.3347 236.2197 212.7972 42.8723 0.1153 236.2273 236.1120 212.7101 43.6303 0.1223 236.1595 236.0373 212.6214 44.4490 0.1253 236.0675 235.9422 212.5447 45.2685 0.1230 235.9789 235.8559 212.4661 46.0270 0.1181 235.8905 235.7724 212.3939 46.8788 0.1174 235.8079 235.6905 212.3070 47.6675 0.1194 235.7121 235.5927 212.2201 48.4560 0.1192 235.6184 235.4991 212.1254 49.2760 0.1177 235.5235 235.4059 212.0469 50.0655 0.1179 235.4415 235.3237 211.9768 50.8873 0.1203 235.3527 235.2324 211.8863 51.6823 0.1235 235.2721 235.1485 211.8187 52.4750 0.1263 235.1875 235.0612 211.7337 53.3010 0.1249 235.0958 234.9709 211.6591 54.0615 0.1257 235.0142 234.8885 211.5871 54.9198 0.1243 234.9188 234.7945 211.5045 55.6798 0.1252 234.8419 234.7166 211.4298 56.5018 0.1228 234.7456 234.6227 211.3421 57.3238 0.1263 234.6650 234.5387 211.2738 58.0855 0.1284 234.5834 234.4550 211.1969 58.9390 0.1322 234.4834 234.3512 211.1105 59.7058 0.1348 234.4018 234.2670 211.0212 60.5305 0.1378 234.3154 234.1776 210.9315 61.3258 0.1368 234.2184 234.0816 210.8650 62.1175 0.1370 234.1261 233.9891 210.7991 62.9453 0.1405 234.0286 233.8880 210.7085 63.7085 0.1391 233.9514 233.8123 210.6321 64.5605 0.1405 233.8612 233.7208 210.5465 65.3525 0.1388 233.7855 233.6466 210.4770 66.1445 0.1394 233.7001 233.5607 210.4058 66.9665 0.1410 233.5936 233.4526 210.3348 67.7308 0.1409 233.5235 233.3826 210.2621 68.5900 0.1388 233.4374 233.2986 210.1719 69.3535 0.1387 233.3601 233.2214 210.1338 70.1760 0.1407 233.2580 233.1173 210.0476 70.9995 0.1404 233.1762 233.0358 209.9721 71.7655 0.1425 233.1068 232.9643 209.9023 72.6195 0.1403 232.9949 232.8546 209.8350 73.3815 0.1395 232.9095 232.7700 209.7729 74.2045 0.1377 232.8209 232.6832 209.7141 75.0018 0.1376 232.7489 232.6113 209.6572 75.7955 0.1398 232.6640 232.5241 209.5823 76.6195 0.1408 232.5627 232.4220 209.5246 77.3840 0.1396 232.4880 232.3485 209.4723 78.2390 0.1418 232.3854 232.2436 209.4169 79.0018 0.1419 232.3073 232.1655 209.3612 79.8273 0.1437 232.2109 232.0672 209.3029 80.6285 0.1422 232.1246 231.9824 209.2585 81.4268 0.1399 232.0639 231.9240 209.2158 82.2500 0.1419 231.9689 231.8269 209.1743 83.0115 0.1430 231.9004 231.7574 209.1239 83.8650 0.1417 231.8148 231.6732 209.0915 84.6570 0.1395 231.7147 231.5752 209.0473 85.4485 0.1382 231.6241 231.4859 209.0167 86.2708 0.1401 231.5268 231.3867 209.0051 87.0325 0.1411 231.4383 231.2972 208.9666 87.8845 0.1413 231.3501 231.2088 208.9312 88.6715 0.1407 231.2765 231.1358 208.9231 89.4535 0.1397 231.1932 231.0535 208.8996 90.2685 0.1385 231.1068 230.9683 208.8934 91.0550 0.1402 231.0297 230.8895 208.8749 91.8728 0.1402 230.9311 230.7910 208.8740 92.6630 0.1395 230.8637 230.7242 208.8657 93.4540 0.1390 230.7749 230.6359 208.8693 94.2705 0.1400 230.7036 230.5636 208.8656 95.0590 0.1386 230.6231 230.4845 208.8580 95.8770 0.1382 230.5501 230.4119 208.8814 96.6678 0.1399 230.4538 230.3139 208.8973 97.4580 0.1381 230.3772 230.2391 208.9106 98.2760 0.1363 230.2813 230.1450 208.9310 99.0640 0.1381 230.1960 230.0579 208.9598 99.8820 0.1330 230.1088 229.9758 208.9879 100.6700 0.1377 230.0328 229.8951 209.0119 101.4618 0.1468 229.9477 229.8009 209.0338 102.2810 0.1466 229.8606 229.7140 209.0702 103.0690 0.1445 229.7902 229.6457 209.1161 103.8870 0.1434 229.7190 229.5756 209.1779 104.6800 0.1432 229.6123 229.4692 209.2260 105.4690 0.1456 229.5230 229.3774 209.2507 106.2948 0.1420 229.4689 229.3269 209.3048 107.0830 0.1422 229.3917 229.2495 209.3705 107.9010 0.1439 229.3186 229.1747 209.4429 108.6895 0.1423 229.2279 229.0856 209.5001 109.4790 0.1394 229.1502 229.0108 209.5532 110.3308 0.1399 229.0580 228.9181 209.6394 111.0995 0.1400 228.9790 228.8390 209.7035 111.9198 0.1400 228.8959 228.7559 209.7758 112.7140 0.1364 228.8195 228.6831 209.8383 113.5040 0.1351 228.7594 228.6243 209.9231 114.3230 0.1351 228.6785 228.5434 210.0232 115.1125 0.1303 228.5998 228.4695 210.0864 115.9328 0.1298 228.5191 228.3894 210.1722 116.7210 0.1268 228.4303 228.3035 210.2498 117.5100 0.1241 228.3486 228.2245 210.3416 118.3625 0.1173 228.2762 228.1589 210.4327 119.1213 0.1184 228.2071 228.0887 210.5381 119.9410 0.1164 228.1228 228.0064 210.6492 120.7625 0.1143 228.0445 227.9302 210.7382 121.5250 0.1120 227.9742 227.8622 210.8268 122.3828 0.1089 227.8967 227.7878 210.9472 123.1473 0.1066 227.8145 227.7079 211.0462 123.9730 0.1039 227.7238 227.6199 211.1531 124.7655 0.0987 227.6422 227.5435 211.2504 125.5588 0.0959 227.5918 227.4959 211.3555 126.3820 0.0916 227.5240 227.4324 211.4684 127.1435 0.0903 227.4466 227.3563 211.5810 127.9980 0.0876 227.3835 227.2959 211.6869 128.7900 0.0824 227.3219 227.2395 211.7906 129.5815 0.0762 227.2526 227.1764 211.9008 130.4040 0.0739 227.1612 227.0873 212.0129 131.1655 0.0728 227.0977 227.0250 212.1346 132.0190 0.0677 227.0091 226.9413 212.2469 132.8110 0.0603 226.9508 226.8904 212.3702 133.6043 0.0566 226.9027 226.8460 212.4762 134.4308 0.0387 226.8173 226.7786 212.6002 135.1925 0.0400 226.7608 226.7208 212.7058 136.0508 0.0517 226.6760 226.6243 212.8442 136.8128 0.0415 226.6144 226.5729 212.9541 137.6348 0.0321 226.5582 226.5261 213.0502 138.4565 0.0305 226.4820 226.4515 213.1805 139.2185 0.0297 226.4228 226.3931 213.3053 140.0705 0.0288 226.3446 226.3159 213.4128 140.8325 0.0241 226.2860 226.2619 213.5267 141.6545 0.0165 226.2129 226.1963 213.6424 142.4765 0.0114 226.1464 226.1350 213.7622 143.2385 0.0062 226.0903 226.0841 213.8778 144.0918 0.0015 226.0099 226.0084 213.9826 144.8535 -0.0013 225.9633 225.9646 214.1031 145.6755 -0.0083 225.9134 225.9216 214.2250 146.4975 -0.0092 225.8366 225.8458 214.3464 147.2603 -0.0119 225.7782 225.7901 214.4417 148.1158 -0.0160 225.7166 225.7326 214.5615 148.8828 -0.0178 225.6701 225.6879 214.6814 149.7055 -0.0200 225.6005 225.6205 214.7807 150.4975 -0.0228 225.5381 225.5609 214.9065 151.2895 -0.0244 225.4766 225.5010 215.0232 152.1400 -0.0289 225.4304 225.4594 215.1254 152.8970 -0.0326 225.3700 225.4026 215.2214 153.7158 -0.0378 225.2874 225.3253 215.3195 154.5025 -0.0437 225.2398 225.2835 215.4459 155.2895 -0.0468 225.1755 225.2224 215.5558 156.1065 -0.0531 225.1338 225.1869 215.6641 156.8963 -0.0569 225.0708 225.1277 215.7737 157.7163 -0.0605 225.0265 225.0869 215.8597 158.5053 -0.0649 224.9844 225.0492 215.9562 159.2940 -0.0687 224.9250 224.9936 216.0430 160.1130 -0.0713 224.8575 224.9288 216.1524 160.8723 -0.0774 224.8052 224.8826 216.2436 161.7260 -0.0793 224.7588 224.8381 216.3595 162.4898 -0.0877 224.6999 224.7876 216.4755 163.3120 -0.0895 224.6350 224.7245 216.5783 164.1038 -0.1031 224.5937 224.6968 216.6604 164.8925 -0.1163 224.5363 224.6526 216.7322 165.7150 -0.1242 224.4952 224.6194 216.8184 166.4743 -0.1226 224.4482 224.5708 216.9010 167.3240 -0.1270 224.3874 224.5144 217.0074 168.1135 -0.1323 224.3449 224.4772 217.0990 168.9010 -0.1350 224.3216 224.4566 217.1893 169.7288 -0.1414 224.2533 224.3947 217.2672 170.4883 -0.1453 224.1983 224.3436 217.3594 171.3378 -0.1447 224.1562 224.3009 217.4572 172.0970 -0.1478 224.1068 224.2546 217.5274 172.9170 -0.1572 224.0388 224.1960 217.6222 173.7363 -0.1570 224.0128 224.1698 217.7327 174.5900 -0.1572 223.9600 224.1172 217.8341 175.4408 -0.1555 223.9106 224.0661 217.9067 176.2005 -0.1581 223.8745 224.0326 217.9865 177.0520 -0.1617 223.8239 223.9856 218.0795 177.8435 -0.1666 223.7892 223.9558 218.1623 178.6320 -0.1827 223.7368 223.9195 218.2489 179.4508 -0.1915 223.6916 223.8832 218.3432 180.2393 -0.1963 223.6446 223.8409 218.4419 181.0590 -0.2051 223.6020 223.8070 218.5374 181.8475 -0.2155 223.5794 223.7949 218.6048 182.6378 -0.2145 223.5263 223.7408 218.6737 183.4898 -0.2137 223.4925 223.7062 218.7667 184.2498 -0.2175 223.4428 223.6603 218.8600 185.0718 -0.2234 223.4020 223.6255 218.9372 185.8628 -0.2259 223.3838 223.6097 219.0190 186.6543 -0.2395 223.3373 223.5768 219.1020 187.5095 -0.2305 223.3092 223.5397 219.1940 188.2728 -0.2232 223.2559 223.4790 219.2645 189.0945 -0.2241 223.2133 223.4374 219.3488 189.8855 -0.2246 223.1892 223.4138 219.4462 190.6775 -0.2305 223.1405 223.3710 219.5520 191.5895 -0.2428 223.1104 223.3532 219.6360 192.4715 -0.2574 223.0695 223.3270 219.7367 193.2935 -0.2642 223.0384 223.3026 219.8092 194.0888 -0.2667 223.0048 223.2715 219.8973 194.9145 -0.2724 222.9507 223.2231 219.9983 195.7078 -0.2769 222.9405 223.2173 220.0745 196.5325 -0.2812 222.9009 223.1821 220.1676 197.3270 -0.2795 222.8712 223.1507 220.2515 198.1223 -0.2792 222.8432 223.1225 220.3508 198.9813 -0.2763 222.8004 223.0767 220.4527 199.7135 -0.2756 222.7687 223.0444 220.5272 200.5700 -0.2798 222.7350 223.0148 220.6127 201.3625 -0.2839 222.7092 222.9931 220.7118 202.1545 -0.2878 222.6720 222.9598 220.8014 202.9770 -0.2936 222.6462 222.9398 220.8928 203.7460 -0.3010 222.6261 222.9271 220.9959 204.5990 -0.2997 222.5821 222.8818 221.1041 205.3625 -0.3045 222.5572 222.8617 221.1993 206.1850 -0.3087 222.5376 222.8463 221.2808 207.0070 -0.3173 222.5135 222.8308 221.3764 207.7685 -0.3256 222.4928 222.8184 221.4764 208.6230 -0.3299 222.4595 222.7894 221.5879 209.3850 -0.3316 222.4215 222.7532 221.6793 210.2085 -0.3344 222.4047 222.7391 221.7691 211.0010 -0.3323 222.3849 222.7171 221.8831 211.7940 -0.3364 222.3482 222.6846 221.9833 212.6200 -0.3417 222.3176 222.6593 222.0628 213.4130 -0.3461 222.3044 222.6505 222.1478 214.2375 -0.3533 222.2918 222.6451 222.2563 215.0298 -0.3568 222.2667 222.6235 222.3547 215.8215 -0.3589 222.2488 222.6077 222.4379 216.6393 -0.3623 222.2165 222.5788 222.5646 217.3975 -0.3675 222.1893 222.5568 222.6452 218.2425 -0.3722 222.1771 222.5493 222.7458 219.0295 -0.3779 222.1547 222.5325 222.8553 219.8185 -0.3830 222.1357 222.5187 222.9264 220.6385 -0.3840 222.1033 222.4873 223.0256 221.3980 -0.3850 222.0792 222.4642 223.1213 222.2443 -0.3878 222.0621 222.4499 223.2079 223.0335 -0.3909 222.0513 222.4422 223.3189 223.8230 -0.3945 222.0221 222.4165 223.4232 224.6410 -0.4001 222.0191 222.4192 223.5195 225.3990 -0.4021 222.0103 222.4124 223.6138 226.2470 -0.4089 221.9922 222.4011 223.7316 227.0350 -0.4105 221.9836 222.3942 223.8219 227.8230 -0.4121 221.9819 222.3939 223.9270 228.6448 -0.4166 221.9456 222.3622 224.0368 229.4083 -0.4228 221.9382 222.3610 224.1310 230.2613 -0.4272 221.9355 222.3627 224.2345 231.0190 -0.4301 221.9158 222.3459 224.3321 231.8370 -0.4322 221.8904 222.3226 224.4247 232.6550 -0.4368 221.8835 222.3203 224.5437 233.4170 -0.4391 221.8743 222.3134 224.6338 234.2688 -0.4414 221.8511 222.2925 224.7514 235.0290 -0.4464 221.8423 222.2887 224.8589 235.8508 -0.4521 221.8276 222.2797 224.9607 236.6693 -0.4569 221.8151 222.2721 225.0573 237.4280 -0.4601 221.7955 222.2555 225.1596 238.2765 -0.4597 221.7886 222.2482 225.2734 239.0650 -0.4641 221.7678 222.2320 225.3635 239.8540 -0.4692 221.7607 222.2300 225.4551 240.6723 -0.4709 221.7616 222.2325 225.5719 241.4630 -0.4744 221.7602 222.2345 225.6688 242.2828 -0.4792 221.7388 222.2180 225.7776 243.0800 -0.4834 221.7231 222.2065 225.8887 243.8770 -0.4874 221.7179 222.2052 225.9833 244.6953 -0.4892 221.7135 222.2027 226.0819 245.4540 -0.4928 221.7087 222.2016 226.1860 246.3028 -0.4999 221.7137 222.2136 226.2970 247.0993 -0.5054 221.6922 222.1976 226.4071 247.8920 -0.5109 221.7062 222.2172 226.4985 248.7115 -0.5099 221.6971 222.2070 226.5910 249.4710 -0.5130 221.6842 222.1972 226.6873 250.3265 -0.5173 221.6887 222.2061 226.7834 251.0885 -0.5195 221.6834 222.2029 226.8770 251.9105 -0.5247 221.6758 222.2005 226.9931 252.7323 -0.5279 221.6870 222.2150 227.0965 253.4943 -0.5304 221.6816 222.2119 227.1842 254.3463 -0.5336 221.6597 222.1933 227.2994 255.1080 -0.5392 221.6621 222.2013 227.4078 255.9298 -0.5436 221.6747 222.2183 227.4997 256.7520 -0.5661 221.6707 222.2368 227.5914 257.5143 -0.5957 221.6883 222.2841 227.6998 258.3670 -0.5933 221.6795 222.2727 227.7909 259.1288 -0.5753 221.6785 222.2539 227.8741 259.9508 -0.5779 221.6868 222.2648 227.9741 260.7760 -0.5877 221.6943 222.2820 228.0701 261.5385 -0.5955 221.7000 222.2956 228.1721 262.3910 -0.5867 221.7063 222.2930 228.2690 263.1528 -0.5881 221.7050 222.2931 228.3502 263.9758 -0.5748 221.6855 222.2602 228.4588 264.7680 -0.5709 221.6877 222.2586 228.5496 265.5605 -0.5729 221.7103 222.2832 228.6381 266.4155 -0.5769 221.7020 222.2789 228.7538 267.1775 -0.5813 221.7211 222.3024 228.8494 267.9995 -0.5858 221.7205 222.3063 228.9376 268.7915 -0.5888 221.7220 222.3108 229.0285 269.5835 -0.5929 221.7327 222.3256 229.1249 270.4373 -0.5952 221.7424 222.3375 229.2282 271.1995 -0.5985 221.7486 222.3471 229.3281 272.0215 -0.6014 221.7522 222.3536 229.4082 272.8163 -0.6030 221.7471 222.3501 229.5099 273.6115 -0.6046 221.7609 222.3655 229.6038 274.4455 -0.6118 221.7753 222.3872 229.6997 275.2105 -0.6173 221.7944 222.4117 229.7820 276.0675 -0.6205 221.7920 222.4125 229.9020 276.8295 -0.6210 221.7981 222.4191 230.0022 277.6515 -0.6265 221.7979 222.4244 230.1238 278.4448 -0.6301 221.8273 222.4574 230.2036 279.2375 -0.6306 221.8462 222.4768 230.3115 280.0625 -0.6344 221.8505 222.4849 230.4090 280.8155 -0.6390 221.8596 222.4986 230.4890 281.6610 -0.6461 221.8638 222.5099 230.5944 282.4440 -0.6488 221.8787 222.5275 230.6981 283.2358 -0.6508 221.8889 222.5398 230.7953 284.0523 -0.6536 221.8920 222.5456 230.8787 284.8110 -0.6564 221.9161 222.5725 230.9645 285.6603 -0.6578 221.9483 222.6061 231.0712 286.4470 -0.6577 221.9638 222.6215 231.1609 287.2368 -0.6617 221.9649 222.6266 231.2587 288.0575 -0.6676 221.9735 222.6412 231.3611 288.8150 -0.6703 221.9888 222.6591 231.4823 289.6633 -0.6725 222.0067 222.6792 231.5613 290.4515 -0.6750 222.0134 222.6884 231.6434 291.2390 -0.6806 222.0210 222.7016 231.7474 292.0573 -0.6847 222.0537 222.7384 231.8417 292.8183 -0.6861 222.0745 222.7606 231.9430 293.6735 -0.6904 222.0968 222.7872 232.0346 294.4313 -0.6901 222.1050 222.7951 232.1136 295.2510 -0.6924 222.1103 222.8028 232.2153 296.0708 -0.6976 222.1286 222.8262 232.3197 296.8280 -0.6996 222.1425 222.8421 232.4032 297.6770 -0.7018 222.1702 222.8720 232.5099 298.4665 -0.7061 222.1829 222.8890 232.5916 299.2625 -0.7115 222.2231 222.9346 232.7077 300.0578 -0.7123 222.2546 222.9669 232.8008 300.8470 -0.7137 222.2596 222.9733 232.9117 301.6970 -0.7181 222.2830 223.0012 233.0110 302.4645 -0.7206 222.3004 223.0211 233.1106 303.2910 -0.7235 222.3185 223.0421 233.2175 304.0825 -0.7297 222.3567 223.0864 233.3149 304.8710 -0.7325 222.3486 223.0812 233.4210 305.6898 -0.7356 222.3894 223.1250 233.5342 306.4785 -0.7409 222.4261 223.1670 233.6398 307.2990 -0.7434 222.4287 223.1721 233.7374 308.0903 -0.7469 222.4591 223.2061 233.8460 308.8843 -0.7489 222.4726 223.2216 233.9288 309.7073 -0.7518 222.5030 223.2548 234.0391 310.4980 -0.7540 222.5227 223.2766 234.1402 311.3203 -0.7542 222.5611 223.3153 234.2560 312.1130 -0.7582 222.5841 223.3422 234.3467 312.9023 -0.7611 222.5982 223.3593 234.4589 313.7243 -0.7637 222.6306 223.3943 234.5672 314.5160 -0.7703 222.6485 223.4188 234.6828 315.3375 -0.7772 222.6864 223.4636 234.7730 316.1625 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