DTA measure 2gyrss Date: 2024115:1522 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1362.64 s Mass = 960 mg data_number = 1696 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3410 -12.2279 390.9659 403.1938 407.3277 2.1655 -12.1001 391.1189 403.2190 407.3330 2.9575 -11.9762 391.2632 403.2395 407.3433 3.7495 -11.8579 391.4201 403.2780 407.3565 4.5735 -11.7348 391.5803 403.3151 407.3690 5.3655 -11.6165 391.7125 403.3290 407.3682 6.1875 -11.4929 391.8729 403.3658 407.3692 6.9795 -11.3813 391.9998 403.3811 407.3617 7.7715 -11.2666 392.1440 403.4106 407.3478 8.5935 -11.1489 392.2939 403.4427 407.3410 9.3610 -11.0393 392.4298 403.4691 407.2985 10.2028 -10.9280 392.5728 403.5009 407.2813 10.9880 -10.8276 392.7183 403.5458 407.2391 11.7765 -10.7252 392.8607 403.5860 407.2013 12.5988 -10.6164 392.9851 403.6015 407.1558 13.3570 -10.5174 393.1042 403.6216 407.1113 14.2045 -10.4038 393.2527 403.6564 407.0637 14.9620 -10.3123 393.3874 403.6997 407.0072 15.7830 -10.2097 393.5106 403.7203 406.9456 16.6013 -10.1084 393.6166 403.7250 406.8697 17.3590 -10.0152 393.7430 403.7582 406.8046 18.2073 -9.9172 393.8924 403.8096 406.7017 18.9963 -9.8237 394.0132 403.8370 406.6267 19.7860 -9.7353 394.1233 403.8586 406.5490 20.6043 -9.6409 394.2456 403.8866 406.4569 21.3625 -9.5551 394.3749 403.9300 406.3857 22.2128 -9.4634 394.4955 403.9589 406.2847 22.9778 -9.3796 394.5935 403.9731 406.1872 23.7970 -9.2917 394.7130 404.0047 406.0595 24.6158 -9.2067 394.8373 404.0440 405.9399 25.3745 -9.1262 394.9485 404.0746 405.8363 26.2255 -9.0530 395.0719 404.1249 405.7428 26.9855 -8.9842 395.1646 404.1487 405.6220 27.8033 -8.9086 395.2597 404.1683 405.5040 28.6543 -8.8263 395.3708 404.1971 405.3729 29.3833 -8.7540 395.4730 404.2270 405.2676 30.2320 -8.6755 395.5649 404.2404 405.1539 31.0205 -8.5985 395.6740 404.2725 405.0246 31.8110 -8.5252 395.7891 404.3143 404.9070 32.6343 -8.4473 395.8938 404.3410 404.7978 33.4310 -8.3656 395.9984 404.3640 404.6921 34.2500 -8.2898 396.0900 404.3799 404.5660 35.0385 -8.2139 396.1729 404.3868 404.4424 35.8270 -8.1337 396.2533 404.3870 404.3294 36.6780 -8.0572 396.3582 404.4154 404.1749 37.4363 -7.9904 396.4427 404.4330 404.0645 38.2550 -7.9219 396.5364 404.4583 403.9504 39.0750 -7.8522 396.6308 404.4830 403.8170 39.8345 -7.7880 396.7122 404.5002 403.6874 40.6858 -7.7213 396.7874 404.5087 403.5704 41.4760 -7.6613 396.8934 404.5546 403.4433 42.2668 -7.6017 396.9808 404.5825 403.3041 43.0860 -7.5377 397.0583 404.5960 403.1876 43.8775 -7.4803 397.1306 404.6109 403.0802 44.6985 -7.4188 397.2175 404.6362 402.9471 45.4908 -7.3616 397.2944 404.6560 402.8373 46.2825 -7.3017 397.3575 404.6592 402.7359 47.1050 -7.2436 397.4313 404.6750 402.5934 47.8675 -7.1940 397.4935 404.6875 402.4884 48.7198 -7.1342 397.5812 404.7154 402.3685 49.5115 -7.0801 397.6571 404.7373 402.2533 50.3035 -7.0285 397.7356 404.7642 402.1256 51.1260 -6.9690 397.7985 404.7675 402.0163 51.8885 -6.9175 397.8663 404.7838 401.9102 52.7405 -6.8619 397.9349 404.7968 401.7929 53.5038 -6.8198 398.0103 404.8300 401.6993 54.3265 -6.7676 398.0663 404.8339 401.5976 55.1485 -6.7165 398.1284 404.8449 401.4912 55.9125 -6.6717 398.1887 404.8605 401.4011 56.7653 -6.6234 398.2577 404.8810 401.2923 57.5275 -6.5795 398.2951 404.8746 401.1910 58.3495 -6.5314 398.3586 404.8900 401.0922 59.1753 -6.4822 398.4136 404.8958 400.9856 59.9385 -6.4395 398.4717 404.9113 400.8953 60.7963 -6.3904 398.5279 404.9183 400.7818 61.5590 -6.3524 398.5845 404.9369 400.6903 62.3835 -6.3080 398.6323 404.9403 400.6136 63.1558 -6.2723 398.6777 404.9499 400.5103 63.9858 -6.2285 398.7228 404.9513 400.4171 64.7785 -6.1858 398.7729 404.9588 400.3222 65.5725 -6.1430 398.8328 404.9758 400.2477 66.3950 -6.1051 398.8679 404.9730 400.1588 67.1595 -6.0723 398.9027 404.9750 400.0971 68.0120 -6.0281 398.9757 405.0039 399.9987 68.7865 -5.9932 399.0065 404.9997 399.9180 69.6215 -5.9543 399.0474 405.0018 399.8251 70.4140 -5.9169 399.0919 405.0088 399.7249 71.2055 -5.8780 399.1532 405.0311 399.6455 72.0313 -5.8430 399.1792 405.0221 399.5671 72.7945 -5.8062 399.2313 405.0375 399.4686 73.6500 -5.7673 399.2550 405.0223 399.3774 74.4055 -5.7331 399.2953 405.0284 399.2951 75.2233 -5.6997 399.3426 405.0423 399.2177 76.0073 -5.6694 399.3695 405.0390 399.1266 76.7960 -5.6344 399.3996 405.0340 399.0278 77.6455 -5.5925 399.4298 405.0223 398.9250 78.4078 -5.5613 399.4744 405.0356 398.8424 79.2270 -5.5320 399.4979 405.0299 398.7533 80.0175 -5.5027 399.5343 405.0370 398.6924 80.8090 -5.4742 399.5939 405.0681 398.5982 81.6290 -5.4470 399.6008 405.0478 398.5104 82.3890 -5.4188 399.6227 405.0414 398.4151 83.2370 -5.3874 399.6429 405.0303 398.3276 84.0250 -5.3594 399.6740 405.0333 398.2486 84.8130 -5.3322 399.6918 405.0240 398.1682 85.6310 -5.3052 399.7286 405.0339 398.0751 86.3890 -5.2762 399.7433 405.0195 397.9901 87.2390 -5.2487 399.7884 405.0372 397.8971 88.0273 -5.2197 399.8047 405.0244 397.8046 88.8150 -5.1939 399.8224 405.0162 397.7031 89.6330 -5.1673 399.8168 404.9841 397.6315 90.4210 -5.1409 399.8635 405.0043 397.5592 91.2390 -5.1165 399.8961 405.0126 397.4541 92.0270 -5.0920 399.9049 404.9969 397.3806 92.8150 -5.0679 399.9147 404.9826 397.2799 93.6635 -5.0398 399.9409 404.9807 397.1781 94.4220 -5.0151 399.9496 404.9647 397.0848 95.2408 -4.9910 399.9718 404.9628 397.0021 96.0593 -4.9686 399.9852 404.9538 396.9120 96.8180 -4.9480 399.9832 404.9312 396.8139 97.6665 -4.9215 400.0070 404.9286 396.6935 98.4553 -4.9005 400.0283 404.9288 396.6036 99.2450 -4.8773 400.0366 404.9139 396.5219 100.0705 -4.8565 400.0450 404.9015 396.4358 100.8310 -4.8341 400.0645 404.8986 396.3532 101.6813 -4.8133 400.0673 404.8806 396.2641 102.4700 -4.7929 400.0962 404.8891 396.1699 103.2590 -4.7691 400.1023 404.8715 396.0620 104.0773 -4.7519 400.1042 404.8562 395.9657 104.8418 -4.7321 400.1160 404.8481 395.8951 105.6935 -4.7108 400.1137 404.8245 395.7886 106.4855 -4.6942 400.1233 404.8175 395.6977 107.2775 -4.6753 400.1355 404.8108 395.6087 108.0990 -4.6561 400.1264 404.7825 395.4812 108.8605 -4.6355 400.1232 404.7586 395.3768 109.7135 -4.6143 400.1326 404.7469 395.3027 110.5065 -4.5949 400.1571 404.7521 395.2169 111.2980 -4.5744 400.1504 404.7248 395.1092 112.1210 -4.5568 400.1500 404.7068 394.9951 112.8825 -4.5407 400.1558 404.6965 394.8921 113.7350 -4.5202 400.1534 404.6736 394.7936 114.4998 -4.5035 400.1621 404.6656 394.7072 115.3218 -4.4848 400.1650 404.6498 394.6043 116.1440 -4.4675 400.1630 404.6305 394.4908 116.9068 -4.4512 400.1520 404.6032 394.3909 117.7620 -4.4302 400.1606 404.5908 394.3001 118.5238 -4.4172 400.1459 404.5631 394.2054 119.3458 -4.3947 400.1382 404.5329 394.0928 120.1680 -4.3786 400.1414 404.5200 394.0070 120.9295 -4.3627 400.1372 404.4999 393.9195 121.7820 -4.3463 400.1176 404.4639 393.8214 122.5438 -4.3309 400.1214 404.4524 393.7118 123.3658 -4.3146 400.1282 404.4427 393.6227 124.1928 -4.3006 400.1170 404.4176 393.5124 124.9565 -4.2864 400.1095 404.3959 393.4229 125.8088 -4.2706 400.0852 404.3558 393.3346 126.5728 -4.2561 400.0755 404.3316 393.2337 127.3955 -4.2413 400.0830 404.3242 393.1211 128.1875 -4.2247 400.0732 404.2979 393.0261 128.9795 -4.2101 400.0569 404.2669 392.9512 129.8373 -4.1961 400.0529 404.2490 392.8534 130.5723 -4.1845 400.0327 404.2172 392.7586 131.4323 -4.1700 400.0231 404.1931 392.6551 132.1945 -4.1550 400.0033 404.1582 392.5531 133.0165 -4.1409 399.9770 404.1179 392.4513 133.8385 -4.1259 399.9778 404.1037 392.3572 134.6005 -4.1140 399.9779 404.0919 392.2631 135.4555 -4.1000 399.9684 404.0684 392.1373 136.2175 -4.0851 399.9423 404.0273 392.0474 137.0395 -4.0717 399.9339 404.0056 391.9498 137.8615 -4.0567 399.9118 403.9685 391.8401 138.6225 -4.0466 399.8816 403.9282 391.7468 139.4678 -4.0319 399.8591 403.8911 391.6481 140.2235 -4.0196 399.8467 403.8664 391.5543 141.0425 -4.0074 399.8264 403.8338 391.4561 141.8283 -3.9933 399.8138 403.8071 391.3468 142.6190 -3.9796 399.7932 403.7728 391.2482 143.4673 -3.9648 399.7571 403.7219 391.1241 144.2253 -3.9531 399.7570 403.7100 391.0293 145.0438 -3.9419 399.7391 403.6810 390.9369 145.8333 -3.9305 399.7112 403.6417 390.8304 146.6210 -3.9175 399.6811 403.5986 390.7281 147.4698 -3.9042 399.6675 403.5716 390.6163 148.2288 -3.8947 399.6361 403.5307 390.5042 149.0485 -3.8830 399.6064 403.4894 390.4047 149.8363 -3.8723 399.5867 403.4590 390.3092 150.6240 -3.8611 399.5601 403.4213 390.2097 151.4730 -3.8521 399.5390 403.3911 390.1002 152.2313 -3.8401 399.5105 403.3505 389.9992 153.0493 -3.8302 399.4944 403.3246 389.9091 153.8675 -3.8177 399.4809 403.2986 389.8011 154.6250 -3.8050 399.4444 403.2494 389.7172 155.4748 -3.7914 399.4234 403.2148 389.6029 156.2385 -3.7816 399.3801 403.1618 389.5074 157.0593 -3.7688 399.3685 403.1373 389.4052 157.8778 -3.7595 399.3344 403.0939 389.2995 158.6360 -3.7491 399.2990 403.0481 389.2201 159.4850 -3.7378 399.2775 403.0153 389.1147 160.2735 -3.7275 399.2380 402.9655 389.0221 161.0620 -3.7199 399.2118 402.9317 388.9226 161.8815 -3.7097 399.1732 402.8829 388.8426 162.6703 -3.6982 399.1455 402.8437 388.7474 163.4900 -3.6880 399.1172 402.8052 388.6423 164.2793 -3.6773 399.1064 402.7836 388.5391 165.0690 -3.6676 399.0572 402.7248 388.4390 165.9188 -3.6582 399.0070 402.6653 388.3386 166.6815 -3.6501 398.9687 402.6188 388.2453 167.5040 -3.6426 398.9422 402.5849 388.1662 168.3233 -3.6340 398.9131 402.5471 388.0606 169.0820 -3.6220 398.8836 402.5056 387.9657 169.9313 -3.6129 398.8479 402.4608 387.8637 170.7210 -3.6028 398.8265 402.4293 387.7682 171.5123 -3.5954 398.7938 402.3892 387.6767 172.3325 -3.5863 398.7647 402.3510 387.6055 173.0940 -3.5761 398.7249 402.3010 387.5164 173.9455 -3.5650 398.6666 402.2316 387.4004 174.7375 -3.5569 398.6294 402.1862 387.3055 175.5300 -3.5487 398.5939 402.1426 387.1975 176.3535 -3.5426 398.5501 402.0927 387.1246 177.1155 -3.5331 398.5072 402.0403 387.0271 177.9725 -3.5247 398.4585 401.9832 386.9198 178.7345 -3.5155 398.4397 401.9552 386.8370 179.5565 -3.5092 398.4015 401.9108 386.7393 180.3493 -3.5014 398.3658 401.8672 386.6447 181.1408 -3.4916 398.3416 401.8332 386.5447 181.9925 -3.4834 398.3042 401.7876 386.4240 182.7545 -3.4749 398.2530 401.7279 386.3353 183.5765 -3.4670 398.2022 401.6692 386.2302 184.3715 -3.4589 398.1728 401.6317 386.1359 185.1645 -3.4501 398.1263 401.5764 386.0427 186.0215 -3.4414 398.0740 401.5155 385.9407 186.7835 -3.4350 398.0352 401.4702 385.8508 187.6055 -3.4298 397.9991 401.4288 385.7502 188.3975 -3.4201 397.9549 401.3750 385.6458 189.1908 -3.4132 397.8927 401.3058 385.5529 190.0208 -3.4059 397.8535 401.2594 385.4301 190.7875 -3.3960 397.8059 401.2019 385.3388 191.6430 -3.3886 397.7641 401.1527 385.2327 192.4048 -3.3807 397.7242 401.1049 385.1629 193.2268 -3.3706 397.6683 401.0388 385.0579 194.0193 -3.3640 397.6189 400.9828 384.9470 194.8105 -3.3587 397.5850 400.9436 384.8438 195.6630 -3.3504 397.5269 400.8773 384.7600 196.4248 -3.3415 397.4919 400.8335 384.6976 197.2498 -3.3348 397.4543 400.7891 384.5799 198.0420 -3.3269 397.4107 400.7376 384.4730 198.8335 -3.3203 397.3412 400.6615 384.3706 199.6860 -3.3095 397.3037 400.6132 384.2790 200.4500 -3.3060 397.2515 400.5574 384.1736 201.2765 -3.2963 397.2131 400.5094 384.0738 202.0678 -3.2919 397.1802 400.4721 383.9745 202.8508 -3.2890 397.1019 400.3908 383.8582 203.6570 -3.2808 397.0643 400.3451 383.7615 204.4353 -3.2743 397.0157 400.2900 383.6736 205.2445 -3.2671 396.9527 400.2198 383.5753 206.0263 -3.2601 396.9220 400.1821 383.4809 206.8095 -3.2533 396.8738 400.1270 383.4003 207.6528 -3.2456 396.8183 400.0640 383.2846 208.4080 -3.2403 396.7625 400.0028 383.1761 209.2215 -3.2330 396.7096 399.9426 383.0800 210.0085 -3.2290 396.6630 399.8920 382.9820 210.7970 -3.2198 396.6191 399.8389 382.8685 211.6468 -3.2107 396.5650 399.7757 382.7606 212.4065 -3.2049 396.5117 399.7166 382.6508 213.2300 -3.1983 396.4486 399.6470 382.5454 214.0180 -3.1914 396.3907 399.5821 382.4538 214.8060 -3.1851 396.3265 399.5116 382.3729 215.6543 -3.1791 396.2784 399.4575 382.2333 216.4140 -3.1730 396.2260 399.3990 382.1279 217.2380 -3.1669 396.1701 399.3370 382.0135 218.0260 -3.1616 396.1167 399.2784 381.9181 218.8140 -3.1558 396.0766 399.2324 381.8233 219.6625 -3.1483 396.0228 399.1711 381.7227 220.4213 -3.1417 395.9643 399.1060 381.6054 221.2408 -3.1354 395.8988 399.0342 381.5069 222.0600 -3.1294 395.8523 398.9816 381.3952 222.8198 -3.1235 395.7954 398.9190 381.3188 223.6723 -3.1189 395.7327 398.8517 381.1981 224.4363 -3.1145 395.6868 398.8013 381.1062 225.2570 -3.1061 395.6266 398.7327 381.0052 226.0785 -3.1012 395.5582 398.6594 380.9011 226.8405 -3.0942 395.5109 398.6051 380.8037 227.6963 -3.0893 395.4564 398.5457 380.7042 228.4585 -3.0824 395.3784 398.4608 380.6145 229.2805 -3.0754 395.3182 398.3936 380.5018 230.0725 -3.0697 395.2661 398.3358 380.4063 230.8645 -3.0641 395.2151 398.2792 380.3097 231.7208 -3.0564 395.1461 398.2026 380.2144 232.4838 -3.0526 395.0920 398.1446 380.1120 233.3098 -3.0469 395.0471 398.0940 380.0109 234.1015 -3.0420 394.9726 398.0145 379.9159 234.8910 -3.0334 394.9111 397.9445 379.8248 235.7095 -3.0265 394.8785 397.9050 379.7299 236.4973 -3.0203 394.8156 397.8360 379.6289 237.3160 -3.0159 394.7468 397.7628 379.5254 238.1045 -3.0095 394.6947 397.7042 379.4359 238.8930 -3.0041 394.6132 397.6173 379.3389 239.7420 -2.9962 394.5495 397.5457 379.2541 240.5008 -2.9902 394.5037 397.4938 379.1497 241.3200 -2.9854 394.4342 397.4196 379.0385 242.1388 -2.9823 394.3698 397.3522 378.9494 242.8990 -2.9756 394.3213 397.2968 378.8619 243.7495 -2.9671 394.2317 397.1988 378.7442 244.5083 -2.9595 394.1958 397.1553 378.6718 245.3313 -2.9586 394.1187 397.0773 378.5712 246.1285 -2.9578 394.0559 397.0137 378.4684 246.9193 -2.9514 393.9738 396.9252 378.3703 247.7708 -2.9441 393.9173 396.8614 378.2586 248.5310 -2.9401 393.8774 396.8175 378.1834 249.3515 -2.9298 393.8193 396.7491 378.0860 250.1438 -2.9239 393.7548 396.6787 377.9797 250.9375 -2.9228 393.6783 396.6010 377.8703 251.7658 -2.9228 393.6136 396.5364 377.7687 252.5298 -2.9139 393.5610 396.4750 377.6818 253.3838 -2.9092 393.4727 396.3819 377.5554 254.1755 -2.9009 393.4187 396.3196 377.4668 254.9683 -2.8954 393.3577 396.2531 377.3799 255.7923 -2.8907 393.2889 396.1797 377.2649 256.6155 -2.8856 393.2118 396.0974 377.1486 257.4075 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