DTA measure 1olom2 Date: 2025114:1243 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1717.89 s Mass = 11.636 mg data_number = 1068 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5148 0.0061 231.0851 231.0790 217.7710 4.1349 0.0146 231.1546 231.1400 217.4634 5.7491 0.0193 231.2057 231.1864 217.1617 7.3536 0.0279 231.1752 231.1474 216.8444 8.9584 0.0408 231.1772 231.1364 216.5231 10.5578 0.0488 231.1958 231.1470 216.2192 12.1618 0.0531 231.2154 231.1624 215.9965 13.7716 0.0558 231.2552 231.1994 215.8584 15.3764 0.0660 231.2693 231.2033 215.7214 17.0059 0.0748 231.3226 231.2478 215.6830 18.6105 0.0791 231.3580 231.2789 215.7150 20.2204 0.0832 231.3703 231.2871 215.7987 21.8250 0.0904 231.3848 231.2944 216.0069 23.4186 0.0979 231.3732 231.2753 216.2906 25.0234 0.1045 231.4252 231.3208 216.6860 26.6281 0.1108 231.4734 231.3626 217.1712 28.2324 0.1056 231.4470 231.3414 217.7257 29.8469 0.1112 231.4557 231.3445 218.3331 31.4363 0.1151 231.4069 231.2918 218.9334 33.0406 0.1158 231.4285 231.3127 219.4966 34.6396 0.1192 231.4305 231.3113 220.0502 36.2393 0.1192 231.4781 231.3589 220.5474 37.8486 0.1174 231.5125 231.3951 220.9827 39.4529 0.1169 231.5481 231.4313 221.3328 41.0371 0.1175 231.5292 231.4117 221.6395 42.6419 0.1185 231.5677 231.4492 221.8693 44.2615 0.1127 231.6059 231.4932 221.9940 45.8709 0.1099 231.6214 231.5115 222.1012 47.4756 0.1073 231.6073 231.5000 222.1564 49.0804 0.1067 231.6532 231.5465 222.1594 50.6690 0.1025 231.6953 231.5928 222.1478 52.2786 0.0973 231.6854 231.5881 222.1035 53.8885 0.0972 231.6616 231.5643 222.0528 55.4923 0.0957 231.6613 231.5655 221.9764 57.1175 0.0952 231.7101 231.6149 221.8872 58.7221 0.0912 231.7399 231.6487 221.8521 60.3260 0.0922 231.7468 231.6546 221.8851 61.9359 0.0944 231.7975 231.7031 221.9694 63.5304 0.0924 231.8344 231.7420 222.0799 65.1393 0.0928 231.8330 231.7403 222.2278 66.7440 0.0937 231.8756 231.7819 222.4623 68.3539 0.0936 231.9057 231.8121 222.7030 69.9785 0.0902 231.9207 231.8305 223.0169 71.5880 0.0818 231.9842 231.9024 223.4309 73.1928 0.0795 232.0019 231.9224 223.8181 74.8026 0.0744 232.0284 231.9540 224.2868 76.4120 0.0682 232.0809 232.0127 224.7531 78.0214 0.0629 232.0946 232.0317 225.2059 79.6108 0.0587 232.1402 232.0814 225.6081 81.2309 0.0591 232.1535 232.0945 226.0325 82.8553 0.0582 232.1926 232.1344 226.3946 84.4599 0.0524 232.2206 232.1682 226.7208 86.0698 0.0502 232.2471 232.1969 226.9797 87.6741 0.0459 232.2472 232.2013 227.1836 89.2885 0.0449 232.2974 232.2525 227.3293 90.8933 0.0407 232.3444 232.3037 227.4502 92.5134 0.0356 232.3830 232.3474 227.4950 94.1123 0.0315 232.4248 232.3933 227.5357 95.6911 0.0267 232.4473 232.4206 227.5436 97.2959 0.0230 232.4740 232.4511 227.5369 98.9006 0.0236 232.5542 232.5306 227.5179 100.5000 0.0206 232.5809 232.5603 227.5537 102.1040 0.0163 232.6310 232.6148 227.5705 103.7088 0.0115 232.6719 232.6604 227.6434 105.2981 0.0041 232.7611 232.7570 227.7333 106.9175 0.0004 232.7870 232.7866 227.8623 108.5271 0.0026 232.8397 232.8371 228.0460 110.1165 -0.0045 232.8827 232.8873 228.2549 111.7255 -0.0093 232.9225 232.9318 228.5716 113.3301 -0.0106 233.0020 233.0126 228.9051 114.9400 -0.0158 233.0575 233.0733 229.2570 116.5448 -0.0217 233.1173 233.1389 229.6450 118.1486 -0.0230 233.1773 233.2003 230.0352 119.7738 -0.0278 233.1962 233.2240 230.4407 121.3631 -0.0300 233.2374 233.2674 230.8372 122.9724 -0.0312 233.2978 233.3290 231.2322 124.5768 -0.0328 233.3641 233.3970 231.6060 126.1866 -0.0374 233.4613 233.4987 231.9000 127.7910 -0.0443 233.5207 233.5650 232.1663 129.4054 -0.0472 233.5676 233.6148 232.4054 131.0101 -0.0564 233.6493 233.7058 232.5986 132.5994 -0.0636 233.6565 233.7201 232.7608 134.2238 -0.0653 233.6998 233.7651 232.8663 135.8336 -0.0649 233.7683 233.8332 232.9857 137.4433 -0.0654 233.8601 233.9255 233.0517 139.0473 -0.0674 233.9298 233.9972 233.0532 140.6571 -0.0638 234.0284 234.0922 233.0260 142.2616 -0.0661 234.0885 234.1546 233.0874 143.8708 -0.0665 234.1073 234.1738 233.1241 145.4909 -0.0660 234.1789 234.2448 233.1639 147.0803 -0.0718 234.2740 234.3458 233.2380 148.6900 -0.0761 234.3498 234.4260 233.3688 150.2939 -0.0756 234.4144 234.4900 233.5714 151.9038 -0.0767 234.5209 234.5976 233.7718 153.5085 -0.0814 234.6061 234.6875 234.0324 155.1225 -0.0839 234.6710 234.7549 234.3063 156.7273 -0.0852 234.7289 234.8141 234.6402 158.3371 -0.0862 234.7589 234.8451 234.9817 159.9460 -0.0814 234.8458 234.9271 235.3964 161.5405 -0.0857 234.9547 235.0405 235.8028 163.1453 -0.0911 235.0505 235.1416 236.2270 164.7500 -0.0955 235.1577 235.2532 236.6141 166.3541 -0.0966 235.2361 235.3326 236.9814 167.9534 -0.0978 235.3363 235.4341 237.3345 169.5786 -0.0982 235.4171 235.5153 237.6167 171.1828 -0.1055 235.4806 235.5861 237.8536 172.7820 -0.1091 235.5805 235.6896 238.0671 174.3919 -0.1108 235.6991 235.8099 238.2084 175.9913 -0.1140 235.8205 235.9345 238.3229 177.6004 -0.1132 235.9117 236.0250 238.4149 179.2051 -0.1165 236.0006 236.1171 238.4851 180.8253 -0.1169 236.1124 236.2293 238.5523 182.4350 -0.1211 236.1796 236.3007 238.6020 184.0235 -0.1246 236.2793 236.4039 238.6560 185.6334 -0.1244 236.4045 236.5289 238.6634 187.2381 -0.1204 236.5221 236.6425 238.7102 188.8480 -0.1220 236.6025 236.7245 238.8056 190.4520 -0.1171 236.6844 236.8015 238.9206 192.0616 -0.1217 236.7869 236.9086 239.0721 193.6818 -0.1169 236.9086 237.0255 239.2730 195.2865 -0.1161 237.0221 237.1382 239.5439 196.8960 -0.1217 237.1436 237.2653 239.8061 198.5001 -0.1249 237.2718 237.3967 240.1622 200.1151 -0.1218 237.3903 237.5121 240.5377 201.7199 -0.1252 237.4826 237.6078 240.9003 203.3295 -0.1261 237.5657 237.6918 241.2572 204.9335 -0.1282 237.6665 237.7947 241.6756 206.5383 -0.1310 237.7394 237.8705 242.0648 208.1481 -0.1307 237.8685 237.9992 242.3990 209.7523 -0.1316 237.9980 238.1296 242.7316 211.3618 -0.1300 238.0839 238.2139 243.0170 212.9665 -0.1299 238.2059 238.3358 243.2585 214.5759 -0.1293 238.3050 238.4342 243.4704 216.1801 -0.1279 238.4446 238.5725 243.6727 217.8003 -0.1257 238.6196 238.7453 243.7912 219.4101 -0.1287 238.7727 238.9013 243.8813 221.0143 -0.1254 238.8645 238.9899 243.9707 222.6135 -0.1218 238.9535 239.0753 244.0068 224.1978 -0.1218 239.0995 239.2213 244.0434 225.8024 -0.1255 239.2159 239.3413 244.0720 227.3960 -0.1315 239.3826 239.5141 244.1067 229.0059 -0.1349 239.5327 239.6676 244.1895 230.6260 -0.1326 239.6331 239.7657 244.3199 232.2099 -0.1303 239.7568 239.8870 244.4587 233.8191 -0.1300 239.8808 240.0108 244.6132 235.4239 -0.1302 240.0165 240.1467 244.8026 237.0335 -0.1261 240.1611 240.2871 245.0530 238.6375 -0.1270 240.2980 240.4251 245.3327 240.2320 -0.1289 240.4241 240.5530 245.6197 241.8368 -0.1319 240.5648 240.6966 246.0036 243.4359 -0.1301 240.6657 240.7958 246.3728 245.0606 -0.1288 240.8059 240.9347 246.7871 246.6654 -0.1297 240.9566 241.0862 247.1908 248.2753 -0.1327 241.1274 241.2601 247.5595 249.8800 -0.1292 241.2935 241.4227 247.9183 251.4684 -0.1220 241.4020 241.5240 248.2216 253.0936 -0.1213 241.5432 241.6645 248.5085 254.6830 -0.1239 241.6864 241.8103 248.7229 256.2923 -0.1231 241.8473 241.9704 248.9041 257.9120 -0.1196 242.0028 242.1223 249.0756 259.5219 -0.1162 242.1673 242.2836 249.2167 261.1619 -0.1137 242.3000 242.4137 249.3262 262.8944 -0.1099 242.4728 242.5827 249.4249 264.4991 -0.1093 242.6436 242.7529 249.4582 266.1193 -0.1046 242.8358 242.9404 249.4868 267.7188 -0.1040 242.9896 243.0937 249.5275 269.3226 -0.1042 243.0941 243.1983 249.6015 270.9325 -0.1131 243.2450 243.3581 249.6601 272.5373 -0.1130 243.4028 243.5158 249.7474 274.1464 -0.1103 243.5358 243.6461 249.9053 275.7509 -0.1084 243.6923 243.8007 250.0834 277.3659 -0.1069 243.8603 243.9673 250.2944 278.9706 -0.1021 244.0090 244.1111 250.5459 280.5848 -0.0911 244.1901 244.2811 250.8950 282.1894 -0.0740 244.3467 244.4208 251.2900 283.7990 -0.0634 244.4862 244.5497 251.6556 285.3979 -0.0416 244.6481 244.6897 252.0396 286.9975 -0.0393 244.8137 244.8529 252.4434 288.5920 -0.0427 244.9799 245.0227 252.8387 290.1908 -0.0534 245.1046 245.1581 253.2375 291.7903 -0.0626 245.2398 245.3024 253.5947 293.4053 -0.0670 245.4247 245.4917 253.8901 295.0151 -0.0724 245.6149 245.6873 254.1641 296.6139 -0.0759 245.8012 245.8771 254.3833 298.2236 -0.0689 245.9985 246.0674 254.5511 299.8233 -0.0708 246.1497 246.2205 254.6840 301.4276 -0.0751 246.2959 246.3710 254.7985 303.0369 -0.0757 246.4522 246.5279 254.8311 304.6519 -0.0762 246.5675 246.6437 254.8440 306.2566 -0.0756 246.7795 246.8551 254.8568 307.8658 -0.0746 246.9510 247.0255 254.8745 309.4703 -0.0661 247.1557 247.2218 254.9192 311.0648 -0.0766 247.3078 247.3844 254.9642 312.6691 -0.0801 247.4995 247.5796 255.0402 314.2784 -0.0798 247.6740 247.7538 255.1216 315.8831 -0.0822 247.8238 247.9060 255.2783 317.5030 -0.0870 247.9812 248.0682 255.5142 319.1121 -0.0928 248.1916 248.2843 255.7728 320.7169 -0.0954 248.3774 248.4728 256.0868 322.3268 -0.0967 248.5560 248.6527 256.4225 323.9311 -0.0962 248.7191 248.8153 256.8132 325.5404 -0.1005 248.8774 248.9778 257.2119 327.1451 -0.1036 249.0489 249.1525 257.6652 328.7653 -0.1043 249.2528 249.3571 258.1105 330.3745 -0.1081 249.4455 249.5535 258.4797 331.9789 -0.1043 249.6199 249.7242 258.8769 333.5888 -0.1063 249.7871 249.8935 259.2684 335.1935 -0.1034 249.9379 250.0413 259.5440 336.8083 -0.1008 250.1200 250.2208 259.7769 338.4123 -0.1032 250.3110 250.4142 259.9829 340.0375 -0.1062 250.4830 250.5892 260.1017 341.6423 -0.1037 250.7182 250.8219 260.1612 343.2464 -0.1009 250.8877 250.9885 260.2331 344.8559 -0.1002 251.0839 251.1841 260.2677 346.4606 -0.1017 251.2661 251.3678 260.2765 348.0705 -0.1015 251.3782 251.4797 260.2973 349.6749 -0.0999 251.5606 251.6605 260.3250 351.2636 -0.1016 251.7597 251.8613 260.3368 352.8786 -0.0951 251.9408 252.0359 260.3944 354.4725 -0.0927 252.1190 252.2118 260.4778 356.0769 -0.0945 252.2893 252.3838 260.6025 357.6765 -0.0929 252.5188 252.6118 260.7757 359.2811 -0.0931 252.6987 252.7918 260.9905 360.8850 -0.0931 252.8751 252.9682 261.3028 362.4744 -0.0909 253.0599 253.1509 261.6345 364.0790 -0.0905 253.2278 253.3183 262.0192 365.6983 -0.0928 253.4093 253.5021 262.4307 367.3081 -0.0936 253.6280 253.7216 262.8948 368.9129 -0.0939 253.8413 253.9352 263.3561 370.5218 -0.0946 254.0060 254.1005 263.7993 372.1111 -0.0962 254.1754 254.2716 264.1754 373.7108 -0.0936 254.3797 254.4732 264.5320 375.3205 -0.0959 254.6026 254.6985 264.8521 376.9244 -0.1002 254.8007 254.9009 265.0380 378.5496 -0.1010 255.0022 255.1032 265.2029 380.1544 -0.1038 255.2253 255.3291 265.3490 381.7634 -0.1095 255.4119 255.5215 265.4306 383.3680 -0.1114 255.5740 255.6854 265.4995 384.9728 -0.1137 255.7114 255.8251 265.5331 386.5818 -0.1191 255.9283 256.0474 265.5921 388.1710 -0.1145 256.1390 256.2535 265.6300 389.7809 -0.1115 256.3420 256.4535 265.6329 391.4056 -0.1087 256.5776 256.6862 265.6451 393.0150 -0.1129 256.7582 256.8711 265.7187 394.6198 -0.1140 256.9296 257.0436 265.8383 396.2450 -0.1156 257.1450 257.2606 266.0123 397.8489 -0.1193 257.3297 257.4490 266.1886 399.4484 -0.1183 257.5599 257.6782 266.4292 401.0531 -0.1176 257.8015 257.9191 266.6822 402.6729 -0.1189 257.9897 258.1085 267.0278 404.2821 -0.1170 258.1763 258.2933 267.3554 405.8920 -0.1236 258.3863 258.5099 267.7496 407.5019 -0.1230 258.5790 258.7020 268.1633 409.1060 -0.1229 258.7816 258.9044 268.5540 410.7155 -0.1219 259.0070 259.1289 268.9295 412.3203 -0.1263 259.2353 259.3616 269.3008 413.9403 -0.1296 259.4599 259.5894 269.7091 415.5441 -0.1299 259.6467 259.7766 270.0412 417.1438 -0.1256 259.8059 259.9315 270.3075 418.7383 -0.1278 260.0036 260.1313 270.5196 420.3479 -0.1308 260.1941 260.3249 270.6944 421.9468 -0.1363 260.4382 260.5745 270.8511 423.5464 -0.1370 260.6572 260.7943 270.9630 425.1716 -0.1408 260.8849 261.0258 271.0213 426.7706 -0.1435 261.1096 261.2531 271.0296 428.3750 -0.1470 261.2869 261.4339 271.0823 429.9849 -0.1481 261.5126 261.6607 271.0784 431.5895 -0.1529 261.6904 261.8433 271.0998 433.1934 -0.1510 261.9030 262.0540 271.1364 434.7981 -0.1500 262.0693 262.2193 271.2126 436.4183 -0.1529 262.2007 262.3536 271.3223 438.0273 -0.1533 262.4265 262.5799 271.5065 439.6319 -0.1525 262.6587 262.8112 271.6889 441.2416 -0.1583 262.9077 263.0661 271.9350 442.8455 -0.1593 263.1010 263.2603 272.2568 444.4554 -0.1557 263.3185 263.4742 272.6088 446.0601 -0.1595 263.5326 263.6921 272.9478 447.6793 -0.1644 263.7861 263.9506 273.3708 449.2891 -0.1623 264.0128 264.1752 273.7969 450.8939 -0.1641 264.2236 264.3878 274.2344 452.5038 -0.1719 264.4005 264.5724 274.6153 454.1078 -0.1737 264.6113 264.7849 274.9519 455.7174 -0.1705 264.8111 264.9816 275.3175 457.3221 -0.1717 265.0347 265.2064 275.6010 458.9520 -0.1764 265.2257 265.4021 275.8425 460.5409 -0.1760 265.4631 265.6391 276.0101 462.1610 -0.1754 265.6925 265.8678 276.1310 463.7758 -0.1772 265.8949 266.0721 276.2356 465.3798 -0.1770 266.1267 266.3037 276.3021 466.9896 -0.1773 266.3060 266.4834 276.3204 468.5944 -0.1762 266.5516 266.7278 276.3554 470.2241 -0.1777 266.8158 266.9935 276.4038 471.8285 -0.1717 267.0491 267.2208 276.4490 473.4384 -0.1775 267.2522 267.4297 276.4618 475.0428 -0.1804 267.4395 267.6199 276.5203 476.6571 -0.1814 267.6547 267.8361 276.6416 478.2516 -0.1815 267.8821 268.0637 276.8142 479.8513 -0.1824 268.1059 268.2883 276.9817 481.4660 -0.1836 268.3402 268.5238 277.2687 483.0598 -0.1844 268.5651 268.7495 277.5656 484.6645 -0.1829 268.7400 268.9229 277.9367 486.2693 -0.1847 268.9691 269.1538 278.3170 487.8526 -0.1901 269.1912 269.3813 278.7154 489.4573 -0.1868 269.3634 269.5502 279.1391 491.0671 -0.1826 269.5532 269.7358 279.5881 492.6719 -0.1804 269.7604 269.9409 280.0305 494.2763 -0.1805 269.9972 270.1778 280.3911 495.8958 -0.1835 270.2059 270.3894 280.6963 497.4903 -0.1849 270.4141 270.5989 281.0069 499.1001 -0.1887 270.6330 270.8217 281.1646 500.7039 -0.1868 270.8604 271.0472 281.3362 502.3138 -0.1864 271.1134 271.2998 281.4573 503.9185 -0.1872 271.3231 271.5102 281.5472 505.5281 -0.1894 271.5537 271.7432 281.5797 507.1321 -0.1962 271.8014 271.9976 281.6062 508.7215 -0.1986 271.9488 272.1474 281.5977 510.3620 -0.1991 272.1877 272.3868 281.6375 511.9659 -0.2026 272.3901 272.5927 281.6234 513.5604 -0.1995 272.5990 272.7985 281.7005 515.1651 -0.1957 272.8206 273.0163 281.7477 516.7745 -0.1922 273.0727 273.2649 281.9015 518.3788 -0.1905 273.2993 273.4898 282.0966 519.9835 -0.1899 273.5632 273.7531 282.3291 521.6088 -0.1911 273.7791 273.9702 282.5826 523.2125 -0.1869 274.0249 274.2119 282.9063 524.8224 -0.1885 274.2722 274.4607 283.3101 526.4271 -0.1913 274.4566 274.6478 283.6978 528.0366 -0.1918 274.6517 274.8434 284.1592 529.6408 -0.1969 274.8257 275.0226 284.5959 531.2506 -0.1987 275.0662 275.2649 285.0491 532.8759 -0.1962 275.2949 275.4911 285.4600 534.4799 -0.1997 275.5282 275.7279 285.8106 536.0895 -0.2053 275.7481 275.9534 286.1245 537.6943 -0.2064 275.9946 276.2010 286.3685 539.3084 -0.2111 276.2003 276.4114 286.5153 540.9130 -0.2144 276.4285 276.6429 286.6639 542.5126 -0.2226 276.6768 276.8994 286.7344 544.1171 -0.2209 276.9076 277.1284 286.7452 545.7160 -0.2262 277.1563 277.3825 286.7962 547.3156 -0.2350 277.3706 277.6056 286.8082 548.9204 -0.2378 277.5929 277.8306 286.8315 550.5191 -0.2382 277.8527 278.0909 286.8291 552.1238 -0.2354 278.0298 278.2652 286.8916 553.7285 -0.2336 278.2663 278.4999 286.9387 555.3328 -0.2324 278.5000 278.7325 287.0332 556.9473 -0.2336 278.7170 278.9506 287.1853 558.5623 -0.2324 278.9205 279.1529 287.3949 560.1669 -0.2324 279.1527 279.3852 287.6547 561.7759 -0.2293 279.4011 279.6304 287.9699 563.3806 -0.2251 279.6416 279.8668 288.3481 564.9905 -0.2314 279.8850 280.1164 288.7491 566.5953 -0.2362 280.0393 280.2755 289.2125 568.1888 -0.2389 280.2601 280.4989 289.6642 569.8089 -0.2429 280.5224 280.7653 290.0897 571.4136 -0.2456 280.7371 280.9827 290.5108 573.0280 -0.2445 280.9720 281.2165 290.8983 574.6324 -0.2401 281.1741 281.4142 291.2057 576.2423 -0.2399 281.4171 281.6570 291.4825 577.8515 -0.2414 281.6471 281.8885 291.6654 579.4661 -0.2458 281.8808 282.1266 291.8163 581.0709 -0.2472 282.1033 282.3505 291.9457 582.6956 -0.2501 282.3213 282.5714 292.0112 584.2999 -0.2541 282.5530 282.8072 292.0364 585.8995 -0.2590 282.8206 283.0796 291.9656 587.5040 -0.2619 283.0483 283.3102 291.9025 589.1131 -0.2573 283.2527 283.5100 291.8949 590.7179 -0.2598 283.4598 283.7196 291.8955 592.3278 -0.2641 283.7049 283.9690 291.9591 593.9475 -0.2677 283.9520 284.2197 292.0592 595.5516 -0.2701 284.1923 284.4624 292.2127 597.1666 -0.2708 284.4102 284.6810 292.4198 598.7714 -0.2735 284.6327 284.9062 292.7348 600.3810 -0.2781 284.8525 285.1306 293.1013 601.9850 -0.2800 285.0848 285.3648 293.5034 603.5949 -0.2841 285.3065 285.5906 293.9072 605.2150 -0.2836 285.5600 285.8436 294.3564 606.8244 -0.2831 285.8051 286.0882 294.8260 608.4235 -0.2879 286.0730 286.3609 295.2591 610.0231 -0.2921 286.2538 286.5459 295.6837 611.6228 -0.2969 286.4813 286.7782 296.0688 613.2275 -0.2972 286.6750 286.9723 296.3430 614.8265 -0.3003 286.8773 287.1777 296.6000 616.4463 -0.3041 287.1344 287.4385 296.8161 618.0510 -0.3106 287.3862 287.6968 297.0376 619.6555 -0.3109 287.6031 287.9140 297.1195 621.2646 -0.3093 287.8662 288.1755 297.1266 622.8643 -0.3118 288.1023 288.4141 297.0302 624.4689 -0.3137 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