DTA measure 1olom_1 Date: 2025114:1122 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.46 s Mass = 11.636 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1785 0.4941 230.6287 230.1345 274.8291 1.9748 0.5016 230.8918 230.3902 275.0680 2.7715 0.5004 231.1942 230.6938 275.3109 3.5888 0.5008 231.4942 230.9933 275.5157 4.3543 0.4993 231.7480 231.2487 275.6749 5.1820 0.4983 232.0247 231.5264 275.8575 5.9375 0.4978 232.2681 231.7703 276.0243 6.7955 0.5009 232.5597 232.0588 276.1872 7.5615 0.5041 232.8297 232.3256 276.2895 8.3785 0.5049 233.0860 232.5810 276.3480 9.1850 0.5102 233.3306 232.8204 276.3944 9.9718 0.5123 233.5891 233.0768 276.4481 10.7888 0.5173 233.8745 233.3572 276.4617 11.5648 0.5183 234.1345 233.6161 276.4771 12.4125 0.5192 234.4106 233.8914 276.4377 13.1478 0.5185 234.6867 234.1683 276.4170 14.0055 0.5138 234.9754 234.4616 276.3592 14.7715 0.5078 235.2338 234.7261 276.2880 15.5990 0.5063 235.5144 235.0080 276.2198 16.3850 0.5026 235.7699 235.2673 276.1388 17.1920 0.5058 236.0315 235.5257 276.0770 18.0093 0.5075 236.2826 235.7751 276.0155 18.7748 0.5108 236.5164 236.0055 275.9427 19.6330 0.5089 236.7677 236.2588 275.8913 20.3785 0.5122 236.9995 236.4872 275.8520 21.2468 0.5124 237.3039 236.7915 275.8648 22.0025 0.5124 237.5676 237.0552 275.8730 22.8298 0.5134 237.8444 237.3310 275.9222 23.6263 0.5131 238.1029 237.5898 275.9817 24.4228 0.5134 238.3453 237.8319 276.0578 25.2503 0.5151 238.6038 238.0887 276.1698 26.0055 0.5142 238.8598 238.3456 276.3058 26.8740 0.5155 239.1344 238.6190 276.5046 27.6298 0.5157 239.3639 238.8483 276.6842 28.4568 0.5158 239.6273 239.1115 276.9532 29.2538 0.5123 239.8511 239.3388 277.2395 30.0503 0.5162 240.1182 239.6020 277.5417 30.8775 0.5205 240.3856 239.8651 277.8591 31.6333 0.5216 240.6275 240.1059 278.1472 32.5015 0.5222 240.9231 240.4008 278.5389 33.2570 0.5224 241.1785 240.6561 278.9141 34.0845 0.5243 241.4204 240.8961 279.2796 34.8810 0.5236 241.6694 241.1458 279.6233 35.6878 0.5182 241.9151 241.3969 279.9631 36.5053 0.5193 242.1742 241.6549 280.3161 37.2708 0.5229 242.4121 241.8892 280.6504 38.1288 0.5224 242.6994 242.1770 280.9821 38.9050 0.5223 242.9294 242.4071 281.2703 39.7220 0.5201 243.1782 242.6581 281.5357 40.5185 0.5211 243.4151 242.8939 281.7787 41.3153 0.5206 243.6404 243.1198 282.0022 42.1425 0.5162 243.8853 243.3691 282.2098 42.9083 0.5143 244.1141 243.5999 282.3566 43.7665 0.5132 244.3763 243.8632 282.4927 44.5323 0.5132 244.6144 244.1012 282.6008 45.3595 0.5085 244.8687 244.3602 282.6955 46.1563 0.5051 245.0974 244.5924 282.7687 46.9425 0.5050 245.3099 244.8049 282.8146 47.7803 0.5036 245.5711 245.0675 282.8244 48.5360 0.4979 245.7805 245.2827 282.8031 49.4040 0.4949 246.0789 245.5839 282.7973 50.1595 0.4949 246.3183 245.8234 282.7772 50.9973 0.4935 246.5610 246.0675 282.7273 51.7835 0.4957 246.7789 246.2832 282.6512 52.5800 0.4939 246.9994 246.5055 282.5582 53.4075 0.4931 247.2456 246.7526 282.4727 54.1733 0.4909 247.4682 246.9773 282.4001 55.0313 0.4901 247.7091 247.2189 282.3088 55.7873 0.4887 247.9179 247.4292 282.2416 56.6245 0.4840 248.1586 247.6745 282.1700 57.4113 0.4820 248.3940 247.9121 282.1271 58.2180 0.4843 248.6576 248.1733 282.0986 59.0043 0.4842 248.8941 248.4099 282.0964 59.8113 0.4848 249.1414 248.6566 282.0846 60.6385 0.4787 249.4055 248.9268 282.1002 61.4040 0.4767 249.6219 249.1451 282.1587 62.2520 0.4743 249.8433 249.3690 282.2443 63.0283 0.4719 250.0419 249.5701 282.3639 63.8453 0.4736 250.2851 249.8114 282.5298 64.6420 0.4732 250.5345 250.0613 282.6775 65.4385 0.4744 250.7708 250.2964 282.8712 66.2658 0.4683 251.0452 250.5769 283.1181 67.0215 0.4619 251.2455 250.7836 283.3962 67.8795 0.4587 251.4995 251.0407 283.7378 68.6145 0.4572 251.7317 251.2745 283.9742 69.4730 0.4580 251.9685 251.5105 284.3396 70.2283 0.4576 252.1821 251.7245 284.6720 71.0660 0.4603 252.4096 251.9493 285.0580 71.8525 0.4575 252.6343 252.1767 285.4531 72.6388 0.4558 252.8839 252.4281 285.8400 73.4458 0.4518 253.1210 252.6692 286.2300 74.2320 0.4510 253.3248 252.8739 286.6113 75.0493 0.4474 253.5308 253.0834 287.0211 75.8255 0.4392 253.7469 253.3076 287.3472 76.6730 0.4352 253.9924 253.5572 287.6924 77.4393 0.4290 254.2139 253.7850 287.9749 78.2665 0.4224 254.4593 254.0370 288.2510 79.0630 0.4201 254.6666 254.2465 288.4867 79.8598 0.4181 254.8916 254.4735 288.7081 80.6768 0.4153 255.1093 254.6940 288.8900 81.4528 0.4127 255.3143 254.9016 289.0460 82.2803 0.4099 255.5658 255.1559 289.1714 83.0358 0.4067 255.8020 255.3953 289.2411 83.8940 0.4042 256.0445 255.6403 289.2906 84.6600 0.4013 256.2578 255.8565 289.3121 85.4873 0.3975 256.4318 256.0343 289.3063 86.2738 0.3920 256.6316 256.2396 289.2792 87.0805 0.3850 256.8338 256.4488 289.2505 87.8978 0.3776 257.0831 256.7054 289.2298 88.6638 0.3734 257.3261 256.9527 289.1971 89.5215 0.3708 257.5644 257.1936 289.1158 90.2568 0.3713 257.7660 257.3947 289.0451 91.1150 0.3742 257.9841 257.6099 288.9462 91.8705 0.3773 258.2046 257.8273 288.8566 92.7083 0.3756 258.4478 258.0722 288.7026 93.4945 0.3717 258.6780 258.3063 288.5786 94.2913 0.3717 258.9207 258.5489 288.4822 95.1188 0.3692 259.1188 258.7496 288.3994 95.8843 0.3679 259.2971 258.9292 288.3373 96.7428 0.3680 259.5126 259.1446 288.2898 97.4983 0.3657 259.7114 259.3457 288.2694 98.3360 0.3626 259.9247 259.5621 288.3127 99.1225 0.3604 260.1213 259.7609 288.3606 99.9188 0.3582 260.3295 259.9713 288.4112 100.7465 0.3600 260.5588 260.1988 288.5193 101.5123 0.3548 260.7568 260.4020 288.6386 102.3703 0.3498 260.9898 260.6399 288.8313 103.1363 0.3518 261.2330 260.8812 289.0520 103.9635 0.3518 261.4505 261.0987 289.2937 104.7600 0.3492 261.6419 261.2927 289.5351 105.5568 0.3471 261.8371 261.4900 289.8370 106.3533 0.3460 262.0450 261.6990 290.1497 107.1498 0.3406 262.2529 261.9123 290.5237 107.9773 0.3379 262.4756 262.1377 290.9181 108.7430 0.3333 262.6559 262.3225 291.2352 109.5908 0.3286 262.8923 262.5637 291.7212 110.3670 0.3245 263.0865 262.7620 292.1270 111.1943 0.3250 263.2747 262.9497 292.5478 111.9908 0.3250 263.4674 263.1424 292.9345 112.7775 0.3198 263.6349 263.3152 293.3161 113.6148 0.3156 263.8494 263.5338 293.6829 114.3805 0.3090 264.0821 263.7731 293.9888 115.2390 0.3054 264.3161 264.0108 294.3112 115.9943 0.2971 264.5033 264.2062 294.5810 116.8320 0.2917 264.7470 264.4553 294.8044 117.6185 0.2897 264.9811 264.6914 295.0094 118.4150 0.2879 265.1662 264.8783 295.1872 119.2425 0.2822 265.3846 265.1023 295.3748 120.0083 0.2793 265.5898 265.3105 295.5186 120.8665 0.2765 265.7979 265.5214 295.6089 121.6223 0.2743 265.9841 265.7098 295.6836 122.4595 0.2721 266.1938 265.9218 295.7216 123.2563 0.2673 266.4014 266.1341 295.7284 124.0530 0.2641 266.6062 266.3421 295.7170 124.8698 0.2618 266.8446 266.5828 295.6613 125.6463 0.2589 267.0688 266.8099 295.6045 126.4940 0.2558 267.2567 267.0009 295.4889 127.2600 0.2530 267.4486 267.1957 295.4169 128.0875 0.2506 267.6895 267.4389 295.3266 128.8838 0.2459 267.8824 267.6365 295.2403 129.6808 0.2451 268.0782 267.8332 295.1348 130.4978 0.2437 268.2701 268.0264 295.0162 131.2635 0.2415 268.4545 268.2130 294.9030 132.1118 0.2423 268.6739 268.4316 294.8247 132.8773 0.2416 268.8782 268.6366 294.7442 133.7048 0.2434 269.0837 268.8403 294.6544 134.4913 0.2396 269.2948 269.0552 294.6292 135.2878 0.2330 269.4813 269.2484 294.6093 136.1153 0.2284 269.6979 269.4695 294.6167 136.8810 0.2278 269.8753 269.6475 294.6374 137.7288 0.2255 270.0570 269.8315 294.6821 138.4640 0.2263 270.2316 270.0053 294.7751 139.3220 0.2218 270.4569 270.2351 294.9239 140.0775 0.2194 270.6503 270.4309 295.0753 140.9153 0.2162 270.8504 270.6342 295.2748 141.7015 0.2144 271.0195 270.8051 295.5081 142.4980 0.2082 271.2197 271.0115 295.7711 143.3255 0.2040 271.4190 271.2151 296.0768 144.0913 0.2028 271.6198 271.4170 296.4000 144.9495 0.2005 271.8260 271.6254 296.7728 145.7050 0.1995 272.0323 271.8329 297.1113 146.5425 0.1994 272.2342 272.0349 297.5165 147.3288 0.1950 272.4216 272.2266 297.9044 148.1258 0.1925 272.6302 272.4377 298.3002 148.9528 0.1841 272.8199 272.6358 298.7028 149.7188 0.1820 273.0152 272.8332 299.0532 150.5768 0.1819 273.2298 273.0479 299.4666 151.3323 0.1775 273.3973 273.2198 299.8075 152.1698 0.1728 273.6014 273.4286 300.1826 152.9563 0.1704 273.8099 273.6395 300.4976 153.7528 0.1655 273.9996 273.8341 300.7901 154.5803 0.1625 274.2094 274.0469 301.0815 155.3463 0.1586 274.4056 274.2470 301.3336 156.2040 0.1515 274.6151 274.4636 301.5392 156.9598 0.1469 274.7927 274.6457 301.6913 157.7975 0.1432 274.9869 274.8437 301.8914 158.5838 0.1372 275.2033 275.0661 301.9746 159.3805 0.1346 275.4058 275.2712 302.0303 160.2078 0.1340 275.6171 275.4831 302.0707 160.9738 0.1281 275.8027 275.6746 302.0960 161.8320 0.1273 276.0031 275.8758 302.0910 162.5875 0.1218 276.2072 276.0854 302.0393 163.4253 0.1138 276.3873 276.2734 301.9941 164.2115 0.1105 276.5714 276.4609 301.9492 165.0083 0.1099 276.7587 276.6488 301.9020 165.8358 0.1087 276.9576 276.8489 301.8325 166.6015 0.1031 277.1363 277.0332 301.7237 167.4598 0.1002 277.3606 277.2604 301.5958 168.2153 0.0958 277.5124 277.4166 301.4715 169.0530 0.0935 277.7065 277.6130 301.3599 169.8395 0.0909 277.8865 277.7957 301.2405 170.6358 0.0876 278.0906 278.0030 301.1324 171.4635 0.0866 278.2713 278.1846 301.0468 172.2395 0.0872 278.4237 278.3365 300.9666 173.0565 0.0863 278.6229 278.5366 300.9508 173.8225 0.0842 278.8223 278.7381 300.9233 174.6805 0.0822 279.0425 278.9603 300.9327 175.4463 0.0772 279.2199 279.1427 300.9673 176.2738 0.0761 279.4107 279.3347 301.0108 177.0600 0.0729 279.6305 279.5576 301.1133 177.8670 0.0665 279.8334 279.7669 301.2443 178.6843 0.0549 279.9792 279.9242 301.3997 179.4600 0.0478 280.1392 280.0914 301.6018 180.3080 0.0495 280.3393 280.2898 301.8549 181.0843 0.0461 280.5010 280.4549 302.1143 181.9010 0.0425 280.6934 280.6509 302.3968 182.6978 0.0406 280.8842 280.8436 302.7485 183.4945 0.0374 281.0386 281.0012 303.1167 184.3013 0.0384 281.2406 281.2021 303.5273 185.0878 0.0392 281.4641 281.4248 303.9229 185.9150 0.0372 281.6738 281.6365 304.3393 186.6808 0.0322 281.8272 281.7950 304.7669 187.5393 0.0312 282.0166 281.9854 305.2070 188.3048 0.0308 282.1830 282.1522 305.6197 189.1323 0.0294 282.3616 282.3322 306.0736 189.9290 0.0303 282.5650 282.5347 306.4578 190.7255 0.0280 282.7430 282.7150 306.7770 191.5530 0.0224 282.9305 282.9081 307.1135 192.3085 0.0224 283.1087 283.0863 307.3808 193.1768 0.0179 283.3063 283.2883 307.6424 193.9328 0.0143 283.4779 283.4636 307.8812 194.7598 0.0116 283.6440 283.6324 308.0937 195.5258 0.0071 283.8314 283.8244 308.2262 196.3430 0.0020 284.0241 284.0221 308.3448 197.1395 -0.0032 284.2053 284.2085 308.4036 197.9363 -0.0115 284.3945 284.4060 308.4674 198.7635 -0.0170 284.5658 284.5828 308.4745 199.5190 -0.0242 284.7341 284.7583 308.4610 200.3773 -0.0261 284.9438 284.9699 308.4501 201.1430 -0.0258 285.1147 285.1405 308.4598 201.9600 -0.0243 285.3092 285.3336 308.3791 202.7568 -0.0322 285.5026 285.5348 308.3034 203.5533 -0.0422 285.6788 285.7210 308.1835 204.3498 -0.0470 285.8217 285.8687 308.0741 205.1363 -0.0478 286.0066 286.0544 307.9731 205.9635 -0.0511 286.2023 286.2534 307.8567 206.7293 -0.0548 286.4333 286.4881 307.7610 207.5773 -0.0594 286.6443 286.7037 307.6708 208.3533 -0.0627 286.8252 286.8880 307.5873 209.1703 -0.0624 286.9852 287.0476 307.4697 209.9670 -0.0604 287.1204 287.1808 307.4067 210.7635 -0.0581 287.2807 287.3388 307.3269 211.5908 -0.0582 287.4694 287.5276 307.2773 212.3568 -0.0587 287.6554 287.7140 307.2629 213.2045 -0.0577 287.8830 287.9407 307.2831 213.9805 -0.0605 288.0698 288.1304 307.3381 214.7980 -0.0621 288.2624 288.3245 307.4071 215.5943 -0.0679 288.4308 288.4987 307.5147 216.3910 -0.0739 288.6063 288.6802 307.6547 217.2183 -0.0801 288.7899 288.8700 307.8343 217.9840 -0.0804 288.9602 289.0406 308.0280 218.8318 -0.0812 289.1063 289.1875 308.2978 219.5775 -0.0792 289.2650 289.3442 308.5968 220.4455 -0.0827 289.4806 289.5632 308.9425 221.2013 -0.0855 289.6902 289.7758 309.2345 222.0288 -0.0913 289.8638 289.9550 309.6083 222.8250 -0.0956 290.0052 290.1008 309.9816 223.6218 -0.0983 290.1706 290.2689 310.3563 224.4493 -0.0985 290.3293 290.4278 310.7863 225.2148 -0.1019 290.4759 290.5779 311.1806 226.0730 -0.1073 290.6375 290.7448 311.6417 226.8390 -0.1107 290.7795 290.8903 312.0344 227.6663 -0.1168 290.9916 291.1084 312.4430 228.4633 -0.1185 291.1509 291.2695 312.8276 229.2595 -0.1228 291.3169 291.4397 313.1710 230.0870 -0.1315 291.5300 291.6614 313.5090 230.8530 -0.1370 291.7282 291.8651 313.7799 231.7005 -0.1412 291.9249 292.0661 314.0513 232.4770 -0.1424 292.1005 292.2429 314.2522 233.2940 -0.1490 292.2874 292.4364 314.4335 234.1008 -0.1561 292.4768 292.6330 314.6162 234.8875 -0.1645 292.6943 292.8588 314.7470 235.7248 -0.1687 292.8714 293.0401 314.8658 236.4805 -0.1720 293.0102 293.1822 314.9160 237.3388 -0.1767 293.2097 293.3864 314.9524 238.1043 -0.1785 293.3771 293.5555 314.9515 238.9320 -0.1819 293.5791 293.7610 314.9141 239.7285 -0.1775 293.7705 293.9479 314.8755 240.5150 -0.1789 293.9436 294.1225 314.8101 241.3528 -0.1821 294.1230 294.3051 314.7107 242.1183 -0.1852 294.2968 294.4820 314.6082 242.9768 -0.1913 294.4446 294.6360 314.4491 243.7323 -0.1935 294.6028 294.7964 314.3342 244.5698 -0.1957 294.8023 294.9980 314.1897 245.3565 -0.1997 294.9736 295.1733 314.0661 246.1630 -0.2012 295.1473 295.3484 313.9185 246.9800 -0.2027 295.3296 295.5323 313.8086 247.7563 -0.2043 295.5077 295.7121 313.6964 248.6040 -0.2063 295.6839 295.8902 313.5993 249.3700 -0.2051 295.8516 296.0567 313.5501 250.1973 -0.2060 296.0138 296.2198 313.5390 251.0040 -0.2123 296.2057 296.4180 313.5134 251.7905 -0.2152 296.3683 296.5836 313.5319 252.6180 -0.2158 296.5071 296.7229 313.5791 253.3835 -0.2150 296.6550 296.8700 313.6764 254.2520 -0.2141 296.8413 297.0553 313.7951 255.0078 -0.2145 297.0222 297.2367 313.9606 255.8348 -0.2145 297.2123 297.4267 314.1909 256.6008 -0.2167 297.4074 297.6240 314.4515 257.4385 -0.2221 297.5810 297.8031 314.7887 258.2245 -0.2222 297.7767 297.9989 315.0753 259.0113 -0.2245 297.9469 298.1715 315.4322 259.8488 -0.2303 298.1106 298.3409 315.8525 260.6043 -0.2327 298.2712 298.5039 316.1909 261.4525 -0.2347 298.4413 298.6759 316.5835 262.2283 -0.2353 298.5752 298.8106 317.0169 263.0455 -0.2371 298.7205 298.9577 317.4679 263.8115 -0.2372 298.9066 299.1438 317.8642 264.6385 -0.2383 299.1178 299.3562 318.2845 265.4253 -0.2436 299.3110 299.5546 318.6703 266.2218 -0.2458 299.4854 299.7312 319.0324 267.0493 -0.2472 299.6569 299.9041 319.3972 267.8153 -0.2504 299.8207 300.0711 319.7332 268.6730 -0.2536 299.9994 300.2530 320.0564 269.3983 -0.2568 300.1494 300.4061 320.2563 270.2563 -0.2594 300.3179 300.5773 320.5143 271.0220 -0.2585 300.4701 300.7286 320.6801 271.8393 -0.2597 300.6501 300.9098 320.8604 272.6460 -0.2662 300.8437 301.1099 320.9954 273.4320 -0.2695 301.0063 301.2758 321.0876 274.2595 -0.2735 301.1454 301.4189 321.1665 275.0255 -0.2737 301.3239 301.5976 321.2065 275.8835 -0.2791 301.5092 301.7884 321.1886 276.6495 -0.2783 301.6643 301.9426 321.1488 277.4665 -0.2789 301.8527 302.1316 321.1288 278.2733 -0.2826 302.0268 302.3094 321.0703 279.0598 -0.2868 302.1684 302.4552 320.9861 279.8870 -0.2883 302.3542 302.6425 320.8778 280.6528 -0.2958 302.5238 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391.8581 393.4359 735.7418 -1.7771 390.2338 392.0109 393.5603 736.5688 -1.8376 390.3172 392.1547 393.7522 737.3350 -1.9006 390.3685 392.2691 393.9769 738.1930 -1.9698 390.4362 392.4060 394.2255 738.9588 -2.0324 390.4866 392.5190 394.5177 739.7863 -2.1040 390.5480 392.6520 394.8333 740.5828 -2.1772 390.6027 392.7799 395.2087 741.3793 -2.2477 390.6612 392.9088 395.6085 742.1965 -2.3185 390.7200 393.0385 396.0292 742.9725 -2.3891 390.7707 393.1598 396.4345 743.8308 -2.4674 390.8350 393.3023 396.9061 744.5968 -2.5444 390.9027 393.4471 397.3054 745.4135 -2.6277 390.9574 393.5851 397.7156 746.1898 -2.7035 391.0206 393.7241 398.1098 747.0070 -2.7811 391.1176 393.8987 398.5248 747.7830 -2.8583 391.1845 394.0428 398.9389 748.6413 -2.9487 391.2137 394.1624 399.3115 749.4070 -3.0296 391.2755 394.3052 399.6019 750.2343 -3.1192 391.3188 394.4380 399.8857 751.0310 -3.2080 391.3435 394.5516 400.1247 751.8275 -3.2987 391.3917 394.6904 400.2949 752.6548 -3.3943 391.4595 394.8538 400.4389 753.4208 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399.3861 771.9165 -6.0444 392.0112 398.0556 399.5064 772.7440 -6.1747 391.9999 398.1745 399.6775 773.5095 -6.2892 391.9768 398.2660 399.8571 774.3573 -6.4195 392.0172 398.4367 400.1426 775.1235 -6.5426 392.0369 398.5795 400.4336 775.9505 -6.6728 392.0191 398.6920 400.7753 776.7370 -6.7940 392.0271 398.8212 401.1281 777.5338 -6.9178 392.0162 398.9339 401.4804 778.3608 -7.0532 392.0206 399.0738 401.9432 779.1165 -7.1838 391.9941 399.1778 402.3571 779.9748 -7.3426 391.9913 399.3338 402.8273 780.7095 -7.4761 391.9680 399.4440 403.2357 781.5578 -7.6298 391.9456 399.5754 403.6772 782.3235 -7.7707 391.9356 399.7063 404.0737 783.1508 -7.9267 391.9150 399.8417 404.4791 783.9478 -8.0659 391.9056 399.9714 404.8397 784.7440 -8.2018 391.8657 400.0675 405.1841 785.5613 -8.3415 391.8410 400.1825 405.5005 786.3375 -8.4698 391.8404 400.3102 405.7765 787.1545 -8.6050 391.8344 400.4394 406.0465 787.9205 -8.7298 391.8489 400.5786 406.2531 788.7785 -8.8689 391.8517 400.7206 406.4185 789.5445 -8.9866 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