DTA measure 2olom_1 Date: 2025114:1152 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.89 s Mass = 11.636 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4404 -2.8058 459.6680 462.4737 433.9393 4.0486 -2.8173 459.7545 462.5718 434.3067 5.6521 -2.8286 459.8185 462.6471 434.5689 7.2505 -2.8309 459.8457 462.6766 434.7443 8.8589 -2.8334 459.8859 462.7193 434.8471 10.4624 -2.8408 459.9200 462.7608 434.8413 12.0556 -2.8496 459.9572 462.8068 434.7189 13.6640 -2.8525 459.9980 462.8505 434.4871 15.2880 -2.8596 460.0361 462.8958 434.1463 16.8965 -2.8648 460.0783 462.9431 433.7428 18.5049 -2.8711 460.1487 463.0199 433.2150 20.1084 -2.8789 460.1807 463.0596 432.6488 21.7168 -2.8817 460.1725 463.0542 432.1111 23.3099 -2.8825 460.1872 463.0697 431.5262 24.9134 -2.8830 460.2242 463.1072 430.9774 26.5218 -2.8862 460.2632 463.1494 430.4215 28.1456 -2.8825 460.2676 463.1501 429.8840 29.7538 -2.8824 460.2862 463.1686 429.3452 31.3573 -2.8847 460.2869 463.1716 428.9463 32.9709 -2.8823 460.3140 463.1962 428.6405 34.5743 -2.8788 460.2685 463.1473 428.4127 36.1828 -2.8822 460.3005 463.1827 428.2280 37.7911 -2.8846 460.2999 463.1845 428.1051 39.4151 -2.8905 460.2884 463.1789 428.0484 41.0186 -2.8930 460.2703 463.1633 428.1116 42.6270 -2.8867 460.2824 463.1692 428.1814 44.2356 -2.8851 460.2728 463.1579 428.3010 45.8440 -2.8827 460.2710 463.1538 428.4332 47.4525 -2.8838 460.2725 463.1564 428.5295 49.0610 -2.8898 460.2775 463.1673 428.5605 50.6694 -2.8960 460.2710 463.1670 428.5243 52.2729 -2.8953 460.2484 463.1437 428.4476 53.8764 -2.8981 460.1989 463.0970 428.2974 55.4744 -2.8974 460.1563 463.0536 428.1268 57.0779 -2.9005 460.1019 463.0024 427.8470 58.6760 -2.8995 460.0716 462.9711 427.4887 60.2794 -2.9036 460.0580 462.9616 427.1366 61.8878 -2.9046 460.0453 462.9499 426.7312 63.4910 -2.9075 460.0035 462.9110 426.3654 65.0944 -2.9103 460.0025 462.9129 425.9379 66.6978 -2.9069 459.9593 462.8662 425.5111 68.3011 -2.9086 459.9275 462.8361 425.1083 69.9096 -2.9093 459.8825 462.7918 424.6994 71.5129 -2.9069 459.8434 462.7503 424.3322 73.1165 -2.9006 459.8057 462.7063 424.0188 74.7250 -2.8974 459.7364 462.6337 423.7318 76.3284 -2.8985 459.6525 462.5511 423.4558 77.9370 -2.9017 459.6038 462.5056 423.2512 79.5455 -2.9017 459.5604 462.4620 423.1193 81.1539 -2.9026 459.5164 462.4189 423.0223 82.7575 -2.9013 459.4390 462.3404 422.9806 84.3709 -2.8966 459.3691 462.2658 422.9368 85.9744 -2.8955 459.3152 462.2107 422.9221 87.5830 -2.8983 459.2885 462.1867 422.8829 89.2018 -2.8982 459.2260 462.1243 422.7899 90.8053 -2.8963 459.1979 462.0942 422.7322 92.4139 -2.8971 459.1495 462.0467 422.6620 94.0170 -2.8970 459.0860 461.9830 422.5510 95.6256 -2.9036 459.0153 461.9189 422.3602 97.2343 -2.9087 458.9498 461.8585 422.1576 98.8426 -2.9111 458.8622 461.7733 421.9390 100.4308 -2.9121 458.7562 461.6684 421.6973 102.0598 -2.9146 458.6907 461.6053 421.4219 103.6630 -2.9144 458.6195 461.5339 421.1143 105.2716 -2.9110 458.5301 461.4412 420.7731 106.8748 -2.9131 458.4364 461.3495 420.4425 108.4885 -2.9128 458.3699 461.2827 420.0938 110.0919 -2.9101 458.2823 461.1924 419.7548 111.7003 -2.9082 458.1941 461.1023 419.4526 113.3243 -2.9107 458.0932 461.0039 419.1522 114.9121 -2.9103 458.0009 460.9112 418.8706 116.5206 -2.9105 457.8852 460.7957 418.5980 118.1239 -2.9097 457.7937 460.7033 418.3729 119.7221 -2.9073 457.6879 460.5952 418.1318 121.3256 -2.9010 457.5897 460.4907 417.9033 122.9289 -2.9023 457.4766 460.3788 417.7400 124.5221 -2.9000 457.3852 460.2853 417.5761 126.1255 -2.9004 457.3121 460.2125 417.4379 127.7390 -2.8997 457.2364 460.1361 417.3340 129.3476 -2.8998 457.1740 460.0738 417.2467 130.9510 -2.9031 457.0751 459.9782 417.1451 132.5594 -2.9013 456.9676 459.8689 416.9990 134.1629 -2.9006 456.8697 459.7704 416.9254 135.7711 -2.9004 456.7273 459.6277 416.8098 137.3644 -2.9050 456.5805 459.4856 416.6648 138.9729 -2.9034 456.4671 459.3705 416.4727 140.5915 -2.8963 456.3055 459.2018 416.2905 142.1950 -2.8980 456.1654 459.0633 416.1118 143.8035 -2.8978 456.0629 458.9607 415.8953 145.4068 -2.8985 455.9781 458.8767 415.6278 147.0153 -2.8970 455.8548 458.7518 415.3786 148.6185 -2.8921 455.7258 458.6179 415.1074 150.2321 -2.8906 455.5799 458.4706 414.8197 151.8508 -2.8879 455.4325 458.3204 414.5715 153.4645 -2.8846 455.3195 458.2041 414.2826 155.0679 -2.8842 455.2158 458.1001 414.0059 156.6814 -2.8815 455.0513 457.9329 413.7430 158.2849 -2.8820 454.9614 457.8434 413.4689 159.8934 -2.8840 454.8831 457.7671 413.1842 161.5120 -2.8739 454.7761 457.6500 412.8785 163.1051 -2.8765 454.6464 457.5229 412.6370 164.7289 -2.8754 454.4988 457.3742 412.4056 166.3375 -2.8723 454.3435 457.2158 412.1956 167.9405 -2.8695 454.1903 457.0598 411.9912 169.5491 -2.8679 454.0225 456.8904 411.7771 171.1576 -2.8699 453.8744 456.7442 411.6377 172.7661 -2.8678 453.7237 456.5915 411.5244 174.3696 -2.8643 453.6195 456.4838 411.3385 175.9985 -2.8587 453.5042 456.3629 411.1804 177.6019 -2.8621 453.3609 456.2231 411.0503 179.2156 -2.8625 453.2106 456.0731 410.9160 180.7931 -2.8623 453.0560 455.9183 410.7407 182.3966 -2.8527 452.9109 455.7637 410.5820 184.0051 -2.8501 452.7953 455.6455 410.4538 185.6034 -2.8510 452.6945 455.5455 410.3363 187.1864 -2.8532 452.5328 455.3860 410.1536 188.7948 -2.8534 452.3753 455.2287 409.9219 190.4135 -2.8533 452.1905 455.0438 409.6937 192.0169 -2.8573 452.0480 454.9053 409.4504 193.6201 -2.8575 451.8649 454.7224 409.1775 195.2083 -2.8591 451.7372 454.5963 408.9132 196.8168 -2.8525 451.5229 454.3755 408.6645 198.4201 -2.8482 451.4156 454.2638 408.4130 200.0286 -2.8416 451.2661 454.1077 408.1470 201.6318 -2.8422 451.1325 453.9747 407.9082 203.2404 -2.8424 450.9934 453.8358 407.6866 204.8488 -2.8406 450.8192 453.6598 407.4551 206.4521 -2.8390 450.6545 453.4935 407.1888 208.0606 -2.8449 450.4565 453.3014 406.8979 209.6639 -2.8441 450.3101 453.1542 406.6291 211.2776 -2.8382 450.1278 452.9660 406.4046 212.8810 -2.8316 449.9788 452.8105 406.2109 214.4945 -2.8318 449.8100 452.6417 406.0201 216.0980 -2.8308 449.6500 452.4809 405.8134 217.7064 -2.8282 449.5093 452.3375 405.6242 219.3150 -2.8228 449.3938 452.2166 405.4416 220.9236 -2.8212 449.2141 452.0353 405.2713 222.5269 -2.8238 449.0360 451.8598 405.1088 224.1355 -2.8187 448.8641 451.6829 404.8905 225.7441 -2.8169 448.6941 451.5109 404.6990 227.3525 -2.8153 448.5252 451.3404 404.5225 228.9714 -2.8099 448.3678 451.1777 404.3651 230.5853 -2.8112 448.1828 450.9941 404.1942 232.2499 -2.8082 448.0164 450.8245 403.9865 233.8841 -2.8020 447.8437 450.6457 403.7952 235.6156 -2.8029 447.6337 450.4367 403.5700 237.2394 -2.8040 447.4380 450.2420 403.3568 238.8480 -2.8000 447.2853 450.0853 403.1567 240.4821 -2.7926 447.1357 449.9283 402.9284 242.0906 -2.7853 446.9304 449.7157 402.6892 243.6941 -2.7839 446.7543 449.5382 402.4488 245.2924 -2.7802 446.5435 449.3238 402.2396 246.8804 -2.7775 446.3787 449.1563 402.0443 248.4839 -2.7733 446.2280 449.0013 401.7850 250.0873 -2.7694 446.0717 448.8411 401.5475 251.6908 -2.7671 445.8879 448.6550 401.2954 253.3044 -2.7631 445.7352 448.4983 401.1027 254.9129 -2.7621 445.5493 448.3114 400.8619 256.5161 -2.7612 445.3473 448.1086 400.6792 258.1196 -2.7630 445.1489 447.9120 400.4475 259.7280 -2.7644 444.9852 447.7496 400.2051 261.3315 -2.7627 444.8513 447.6140 399.9192 262.9399 -2.7589 444.6920 447.4509 399.7160 264.5586 -2.7580 444.5335 447.2916 399.5280 266.1671 -2.7523 444.3089 447.0612 399.3250 267.7703 -2.7445 444.1215 446.8660 399.1565 269.3738 -2.7439 443.9063 446.6502 398.9962 270.9820 -2.7397 443.7098 446.4495 398.8190 272.5855 -2.7344 443.4917 446.2260 398.6089 274.1943 -2.7342 443.3484 446.0826 398.4351 275.8179 -2.7303 443.1804 445.9106 398.2383 277.4111 -2.7291 443.0266 445.7557 398.0167 279.0146 -2.7260 442.8577 445.5837 397.8059 280.6229 -2.7248 442.7094 445.4342 397.5959 282.2315 -2.7254 442.5602 445.2856 397.3522 283.8400 -2.7216 442.3481 445.0697 397.1167 285.4433 -2.7185 442.1188 444.8373 396.9012 287.0570 -2.7148 441.9307 444.6455 396.6513 288.6756 -2.7110 441.7476 444.4586 396.4490 290.2791 -2.7062 441.5753 444.2816 396.2725 291.8775 -2.7085 441.3729 444.0813 396.0570 293.4808 -2.7042 441.1809 443.8850 395.8468 295.0946 -2.6980 441.0300 443.7280 395.6400 296.6981 -2.6951 440.7994 443.4945 395.3982 298.3118 -2.6951 440.5955 443.2906 395.2126 299.9203 -2.6906 440.4236 443.1142 395.0148 301.5289 -2.6874 440.2407 442.9281 394.7742 303.1374 -2.6826 440.0199 442.7026 394.5480 304.7510 -2.6818 439.8243 442.5061 394.3096 306.3495 -2.6836 439.6384 442.3220 394.1040 307.9528 -2.6776 439.4348 442.1124 393.8737 309.5560 -2.6685 439.2555 441.9239 393.6599 311.1544 -2.6646 439.0768 441.7414 393.4401 312.7576 -2.6638 438.8853 441.5491 393.2672 314.3611 -2.6587 438.6554 441.3142 393.0595 315.9645 -2.6562 438.4698 441.1260 392.8311 317.5678 -2.6526 438.2459 440.8984 392.6393 319.1711 -2.6495 438.0611 440.7106 392.4664 320.7743 -2.6438 437.8835 440.5273 392.2759 322.3778 -2.6483 437.7259 440.3742 392.0650 323.9863 -2.6450 437.5361 440.1811 391.8772 325.5895 -2.6385 437.3357 439.9742 391.6910 327.1981 -2.6318 437.1217 439.7535 391.4763 328.7860 -2.6312 436.8688 439.5000 391.2913 330.4100 -2.6307 436.6307 439.2614 391.1066 332.0134 -2.6330 436.4515 439.0844 390.8932 333.6166 -2.6329 436.2824 438.9153 390.6763 335.2253 -2.6349 436.1383 438.7732 390.4639 336.8284 -2.6378 435.9085 438.5463 390.2512 338.4370 -2.6380 435.7352 438.3732 390.0163 340.0405 -2.6390 435.5269 438.1659 389.7830 341.6693 -2.6368 435.3391 437.9759 389.5677 343.2728 -2.6321 435.1266 437.7587 389.3192 344.8761 -2.6270 434.9961 437.6232 389.0993 346.4846 -2.6180 434.7967 437.4147 388.8892 348.0933 -2.6073 434.5993 437.2065 388.6334 349.6966 -2.6040 434.3855 436.9895 388.3913 351.3101 -2.6057 434.1400 436.7457 388.1784 352.9136 -2.6035 433.9399 436.5434 387.9545 354.5374 -2.5967 433.7409 436.3376 387.7120 356.1511 -2.5952 433.5656 436.1608 387.5059 357.7595 -2.5909 433.4035 435.9944 387.2847 359.3628 -2.5885 433.1551 435.7436 387.0699 360.9764 -2.5859 432.9355 435.5214 386.8948 362.5848 -2.5842 432.7360 435.3202 386.7522 364.1934 -2.5812 432.5092 435.0904 386.5186 365.8019 -2.5720 432.3079 434.8800 386.2797 367.4103 -2.5658 432.1188 434.6846 386.1240 369.0189 -2.5599 431.9217 434.4816 385.9443 370.6273 -2.5584 431.7131 434.2715 385.7752 372.2308 -2.5547 431.5502 434.1049 385.6111 373.8391 -2.5522 431.3591 433.9114 385.4087 375.4323 -2.5485 431.1859 433.7344 385.2183 377.0358 -2.5472 430.9599 433.5070 385.0171 378.6391 -2.5442 430.7529 433.2971 384.7941 380.2425 -2.5446 430.5322 433.0768 384.6112 381.8460 -2.5412 430.3488 432.8900 384.3730 383.4493 -2.5314 430.1447 432.6762 384.1366 385.0374 -2.5248 429.9043 432.4290 383.9260 386.6459 -2.5245 429.7286 432.2531 383.6543 388.2490 -2.5252 429.5205 432.0457 383.4412 389.8576 -2.5199 429.3045 431.8244 383.2240 391.4504 -2.5157 429.0774 431.5931 383.0316 393.0539 -2.5158 428.8920 431.4078 382.8060 394.6778 -2.5107 428.6903 431.2010 382.5480 396.2811 -2.5069 428.4670 430.9739 382.2710 397.8898 -2.5041 428.2713 430.7754 382.0230 399.4929 -2.5049 428.0800 430.5849 381.8222 401.1015 -2.5044 427.8715 430.3760 381.6161 402.7050 -2.5003 427.6547 430.1550 381.4433 404.3135 -2.4964 427.4952 429.9916 381.2489 405.9066 -2.4929 427.3088 429.8017 381.0651 407.5253 -2.4903 427.0362 429.5265 380.8296 409.1388 -2.4858 426.7940 429.2798 380.6060 410.8036 -2.4829 426.5975 429.0804 380.3977 412.4325 -2.4764 426.4083 428.8847 380.2134 414.0359 -2.4707 426.1801 428.6508 380.0149 415.6441 -2.4660 425.9348 428.4008 379.8522 417.2528 -2.4650 425.7620 428.2271 379.6375 418.8613 -2.4627 425.5571 428.0198 379.4195 420.4698 -2.4610 425.3789 427.8398 379.2122 422.0784 -2.4528 425.1889 427.6417 378.9903 423.6971 -2.4517 424.9283 427.3800 378.8000 425.3106 -2.4491 424.7486 427.1977 378.5883 426.9143 -2.4458 424.5667 427.0125 378.3497 428.5226 -2.4426 424.3505 426.7931 378.0877 430.1313 -2.4369 424.1334 426.5702 377.8897 431.7398 -2.4317 423.9322 426.3639 377.7056 433.3328 -2.4269 423.7278 426.1548 377.4951 434.9414 -2.4249 423.5213 425.9462 377.2681 436.5603 -2.4206 423.2991 425.7198 377.0374 438.1584 -2.4156 423.0954 425.5110 376.8052 439.7670 -2.4174 422.9067 425.3241 376.5774 441.3651 -2.4114 422.6791 425.0904 376.3340 442.9685 -2.4093 422.4359 424.8452 376.0986 444.5668 -2.4057 422.2737 424.6794 375.9356 446.1649 -2.3976 422.0825 424.4801 375.7707 447.7838 -2.3912 421.8812 424.2724 375.5429 449.3871 -2.3861 421.6545 424.0405 375.3326 450.9903 -2.3837 421.4751 423.8588 375.1084 452.5988 -2.3828 421.2445 423.6273 374.8795 454.2020 -2.3833 421.0439 423.4272 374.7011 455.8055 -2.3819 420.8313 423.2132 374.5065 457.4140 -2.3793 420.6101 422.9893 374.2897 459.0328 -2.3703 420.4201 422.7904 374.0615 460.6413 -2.3594 420.2160 422.5754 373.8197 462.2448 -2.3577 419.9890 422.3467 373.6266 463.8533 -2.3568 419.7753 422.1321 373.3915 465.4568 -2.3580 419.5980 421.9559 373.1796 467.0701 -2.3533 419.4127 421.7659 372.9939 468.6736 -2.3452 419.1877 421.5328 372.7751 470.2924 -2.3359 418.9391 421.2750 372.5708 471.9006 -2.3345 418.7326 421.0670 372.4120 473.5093 -2.3284 418.5301 420.8585 372.2161 475.1176 -2.3295 418.2859 420.6154 371.9928 476.7261 -2.3253 418.0619 420.3872 371.7773 478.3344 -2.3169 417.8343 420.1512 371.5726 479.9430 -2.3143 417.6311 419.9454 371.3758 481.5670 -2.3081 417.4893 419.7974 371.1295 483.1754 -2.3055 417.2875 419.5931 370.9114 484.7839 -2.2996 417.0637 419.3633 370.7121 486.3873 -2.2938 416.8703 419.1641 370.5109 487.9958 -2.2916 416.6745 418.9661 370.3155 489.6044 -2.2900 416.4576 418.7476 370.0904 491.2126 -2.2832 416.2044 418.4876 369.8720 492.8316 -2.2802 416.0016 418.2818 369.6395 494.4454 -2.2744 415.7548 418.0292 369.4102 496.0538 -2.2650 415.5205 417.7855 369.2018 497.6623 -2.2638 415.3162 417.5800 369.0216 499.2658 -2.2637 415.1482 417.4119 368.8034 500.8740 -2.2582 414.9521 417.2103 368.5850 502.4775 -2.2540 414.7406 416.9946 368.3602 504.0603 -2.2561 414.5300 416.7861 368.1714 505.6739 -2.2509 414.2898 416.5407 367.9648 507.2773 -2.2477 414.0960 416.3437 367.7699 508.8804 -2.2426 413.8477 416.0903 367.5556 510.4890 -2.2374 413.6351 415.8724 367.3216 512.0921 -2.2346 413.4091 415.6437 367.0970 513.7008 -2.2328 413.2239 415.4567 366.8656 515.2888 -2.2338 412.9964 415.2302 366.6230 516.8921 -2.2317 412.7801 415.0118 366.3903 518.5160 -2.2291 412.5982 414.8274 366.1881 520.1194 -2.2249 412.4165 414.6414 365.9463 521.7279 -2.2234 412.2024 414.4258 365.7114 523.3314 -2.2224 411.9510 414.1734 365.4595 524.9398 -2.2209 411.7188 413.9397 365.2650 526.5433 -2.2211 411.4881 413.7092 365.0799 528.1568 -2.2162 411.2884 413.5046 364.8841 529.7755 -2.2115 411.0781 413.2896 364.6817 531.3790 -2.2057 410.8463 413.0520 364.4725 532.9875 -2.2006 410.6474 412.8479 364.3142 534.5909 -2.2002 410.4308 412.6310 364.1387 536.1994 -2.2002 410.2417 412.4419 363.9785 537.8026 -2.2018 409.9937 412.1954 363.7625 539.4164 -2.2031 409.7637 411.9668 363.5640 541.0351 -2.2048 409.5644 411.7692 363.4040 542.6435 -2.1981 409.3858 411.5839 363.2125 544.2470 -2.1982 409.1832 411.3814 362.9950 545.8604 -2.1995 408.9475 411.1470 362.7628 547.4639 -2.1923 408.7395 410.9318 362.5340 549.0775 -2.1856 408.5072 410.6929 362.3094 550.6808 -2.1798 408.2963 410.4761 362.0764 552.3048 -2.1758 408.0902 410.2660 361.8706 553.9133 -2.1675 407.8712 410.0387 361.6795 555.5216 -2.1645 407.6416 409.8062 361.4681 557.1303 -2.1605 407.4433 409.6038 361.2014 558.7386 -2.1579 407.2166 409.3745 360.8787 560.3473 -2.1568 406.9713 409.1281 360.6888 561.9611 -2.1520 406.7231 408.8751 360.4893 563.5540 -2.1410 406.4822 408.6232 360.2811 565.1575 -2.1344 406.2858 408.4202 360.0932 566.7713 -2.1245 406.0552 408.1798 359.8964 568.3696 -2.1228 405.8502 407.9729 359.6770 569.9781 -2.1182 405.6735 407.7917 359.4337 571.5815 -2.1153 405.4934 407.6087 359.1876 573.1848 -2.1100 405.3120 407.4220 358.9893 574.7831 -2.1042 405.1018 407.2061 358.8302 576.3865 -2.0982 404.8911 406.9893 358.6379 578.0053 -2.0890 404.6656 406.7545 358.4381 579.5934 -2.0856 404.4126 406.4982 358.2163 581.2018 -2.0799 404.2730 406.3529 358.0351 582.8051 -2.0671 404.0373 406.1044 357.8974 584.4086 -2.0642 403.8129 405.8771 357.6638 586.0170 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