DTA measure 1fazis Date: 2026324:1452 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.10 s Mass = 1191.400 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2533 -2.0696 207.4500 209.5196 247.8510 2.0505 -2.0692 207.5606 209.6298 247.7836 2.8683 -2.0676 207.6918 209.7594 247.7270 3.6348 -2.0618 207.8118 209.8736 247.6828 4.4935 -2.0583 208.0061 210.0644 247.6703 5.2395 -2.0542 208.1708 210.2250 247.6243 6.0880 -2.0486 208.3182 210.3667 247.5730 6.8548 -2.0454 208.4880 210.5334 247.5351 7.6835 -2.0425 208.6362 210.6787 247.4803 8.4808 -2.0444 208.7677 210.8121 247.4622 9.2775 -2.0430 208.9312 210.9741 247.4311 10.0955 -2.0389 209.0882 211.1271 247.3967 10.8725 -2.0321 209.2414 211.2735 247.3785 11.7210 -2.0313 209.3697 211.4010 247.3383 12.4768 -2.0325 209.5127 211.5452 247.2939 13.3155 -2.0276 209.6911 211.7187 247.2818 14.1025 -2.0190 209.8153 211.8342 247.2581 14.8998 -2.0207 209.9348 211.9554 247.2182 15.7278 -2.0190 210.0904 212.1094 247.1955 16.4943 -2.0232 210.1968 212.2200 247.1728 17.3223 -2.0203 210.3635 212.3838 247.1234 18.1093 -2.0141 210.4931 212.5072 247.0903 18.9475 -2.0071 210.6026 212.6097 247.0549 19.7038 -2.0006 210.7296 212.7302 247.0603 20.5318 -1.9953 210.8836 212.8789 247.0379 21.3290 -1.9884 211.0258 213.0142 247.0642 22.1263 -1.9815 211.2028 213.1843 247.0733 22.9543 -1.9746 211.3273 213.3019 247.0491 23.7105 -1.9699 211.4727 213.4425 247.0723 24.5795 -1.9660 211.6137 213.5797 247.0745 25.3463 -1.9630 211.7000 213.6630 247.1130 26.1745 -1.9590 211.8355 213.7944 247.1665 26.9615 -1.9578 211.9607 213.9185 247.2008 27.7693 -1.9505 212.1038 214.0543 247.2380 28.5870 -1.9427 212.2456 214.1884 247.3131 29.3535 -1.9377 212.3854 214.3231 247.3651 30.2125 -1.9332 212.5447 214.4779 247.3982 30.9790 -1.9258 212.6775 214.6033 247.4624 31.8070 -1.9162 212.8413 214.7574 247.5461 32.5940 -1.9116 212.9771 214.8886 247.6107 33.4015 -1.9036 213.1270 215.0307 247.6829 34.2193 -1.9040 213.2962 215.2002 247.7444 34.9858 -1.9043 213.4252 215.3295 247.8239 35.8350 -1.8986 213.5737 215.4724 247.9185 36.5915 -1.8926 213.7113 215.6039 247.9666 37.4605 -1.8949 213.8033 215.6982 248.0226 38.2168 -1.8870 213.9510 215.8381 248.1144 39.0448 -1.8807 214.0905 215.9712 248.2063 39.8420 -1.8739 214.1848 216.0587 248.3006 40.6393 -1.8636 214.3352 216.1988 248.4233 41.4673 -1.8614 214.4925 216.3539 248.5448 42.2235 -1.8585 214.6464 216.5048 248.6473 43.0925 -1.8573 214.7826 216.6399 248.7805 43.8490 -1.8533 214.8650 216.7184 248.9053 44.6778 -1.8465 214.9918 216.8383 249.0515 45.4750 -1.8435 215.0754 216.9189 249.1730 46.2723 -1.8391 215.1891 217.0282 249.2798 47.1003 -1.8303 215.3093 217.1396 249.4242 47.8565 -1.8308 215.4430 217.2738 249.5664 48.7255 -1.8307 215.6125 217.4432 249.7541 49.4818 -1.8287 215.7227 217.5515 249.9012 50.3098 -1.8261 215.8588 217.6848 250.0578 51.1070 -1.8223 216.0003 217.8226 250.2408 51.9043 -1.8164 216.1372 217.9536 250.3608 52.7325 -1.8177 216.2602 218.0779 250.5190 53.4885 -1.8190 216.3899 218.2090 250.6817 54.3473 -1.8197 216.5410 218.3607 250.8575 55.1035 -1.8160 216.6667 218.4827 251.0348 55.9315 -1.8121 216.7729 218.5850 251.2188 56.7190 -1.8115 216.9048 218.7162 251.4016 57.5168 -1.8103 217.0660 218.8763 251.6089 58.3140 -1.8113 217.1897 219.0010 251.7846 59.1010 -1.8095 217.3083 219.1179 251.9802 59.9188 -1.8080 217.4285 219.2364 252.1505 60.6955 -1.8118 217.5521 219.3639 252.3290 61.5440 -1.8108 217.6859 219.4967 252.5329 62.3003 -1.8020 217.8135 219.6155 252.7099 63.1385 -1.7950 217.9455 219.7404 252.9117 63.8948 -1.7926 218.0632 219.8558 253.1088 64.7125 -1.7909 218.2195 220.0105 253.3178 65.5203 -1.7849 218.3201 220.1049 253.4862 66.3178 -1.7813 218.4586 220.2400 253.6534 67.1150 -1.7792 218.6051 220.3843 253.8609 67.9025 -1.7799 218.7402 220.5201 254.0294 68.7305 -1.7828 218.8819 220.6647 254.1713 69.4970 -1.7834 219.0633 220.8466 254.3561 70.3455 -1.7845 219.2409 221.0254 254.5434 71.1223 -1.7847 219.3755 221.1603 254.7474 71.9400 -1.7878 219.5365 221.3243 254.9641 72.7373 -1.7848 219.6617 221.4465 255.1416 73.5345 -1.7810 219.8044 221.5854 255.3122 74.3625 -1.7849 219.9242 221.7091 255.4924 75.1290 -1.7852 220.0195 221.8047 255.6553 75.9570 -1.7858 220.1550 221.9408 255.8123 76.7235 -1.7854 220.2781 222.0635 255.9725 77.5618 -1.7831 220.4077 222.1907 256.1673 78.3180 -1.7830 220.5220 222.3049 256.3538 79.1768 -1.7810 220.6453 222.4264 256.5195 79.9433 -1.7790 220.7710 222.5500 256.6895 80.7723 -1.7745 220.9127 222.6872 256.8852 81.5695 -1.7754 221.0399 222.8153 257.0832 82.3565 -1.7735 221.1986 222.9721 257.2787 83.1640 -1.7716 221.3701 223.1416 257.4207 83.9510 -1.7720 221.5074 223.2794 257.5685 84.7790 -1.7806 221.6334 223.4140 257.7310 85.5455 -1.7820 221.7534 223.5354 257.8599 86.4145 -1.7817 221.9288 223.7105 258.0374 87.1605 -1.7782 222.0462 223.8244 258.1560 88.0090 -1.7792 222.1856 223.9649 258.3227 88.7755 -1.7804 222.2885 224.0690 258.4664 89.6035 -1.7798 222.4459 224.2257 258.6206 90.4008 -1.7796 222.5927 224.3724 258.7944 91.1990 -1.7809 222.7211 224.5020 258.9501 92.0168 -1.7804 222.8410 224.6214 259.0958 92.7935 -1.7791 222.9692 224.7483 259.2557 93.6215 -1.7782 223.1152 224.8934 259.4195 94.3880 -1.7749 223.2157 224.9906 259.5589 95.2365 -1.7728 223.3796 225.1524 259.6850 96.0133 -1.7749 223.4977 225.2726 259.7948 96.8310 -1.7714 223.6392 225.4105 259.9114 97.6283 -1.7724 223.7760 225.5484 260.0279 98.4255 -1.7752 223.9039 225.6791 260.1634 99.2535 -1.7769 224.0274 225.8044 260.2853 100.0200 -1.7768 224.1706 225.9474 260.3607 100.8685 -1.7781 224.2791 226.0571 260.4976 101.6150 -1.7773 224.3554 226.1327 260.6514 102.4640 -1.7827 224.4888 226.2715 260.7565 103.2613 -1.7860 224.6318 226.4178 260.8509 104.0585 -1.7867 224.7751 226.5618 260.9593 104.8558 -1.7851 224.8954 226.6805 261.0675 105.6530 -1.7842 224.9948 226.7790 261.1988 106.4708 -1.7834 225.1407 226.9241 261.3522 107.2475 -1.7820 225.2799 227.0619 261.4867 108.1063 -1.7798 225.4430 227.2228 261.6123 108.8728 -1.7786 225.5726 227.3512 261.7183 109.6905 -1.7813 225.6881 227.4694 261.8176 110.4980 -1.7827 225.8374 227.6202 261.9316 111.2850 -1.7838 225.9910 227.7748 262.0090 112.1133 -1.7817 226.1386 227.9203 262.1340 112.8805 -1.7815 226.3046 228.0861 262.2509 113.7393 -1.7809 226.4450 228.2259 262.3811 114.5058 -1.7778 226.5708 228.3486 262.4780 115.3235 -1.7792 226.7095 228.4887 262.5763 116.1310 -1.7788 226.8376 228.6164 262.6841 116.9180 -1.7794 226.9723 228.7516 262.7953 117.7358 -1.7801 227.0855 228.8655 262.9293 118.5125 -1.7791 227.2032 228.9823 263.0362 119.3610 -1.7787 227.3430 229.1217 263.1584 120.1173 -1.7787 227.4890 229.2678 263.2520 120.9453 -1.7788 227.6319 229.4108 263.3620 121.7015 -1.7813 227.7980 229.5793 263.4695 122.5303 -1.7812 227.9529 229.7341 263.6025 123.3278 -1.7812 228.0570 229.8382 263.7149 124.1148 -1.7799 228.1284 229.9082 263.8235 124.9428 -1.7781 228.3057 230.0837 263.9248 125.6990 -1.7774 228.4280 230.2055 264.0072 126.5578 -1.7742 228.5254 230.2997 264.1008 127.3243 -1.7721 228.6742 230.4463 264.1579 128.1420 -1.7694 228.8212 230.5905 264.2697 128.9393 -1.7672 228.9828 230.7499 264.3408 129.7365 -1.7675 229.0936 230.8611 264.4559 130.5648 -1.7695 229.1976 230.9671 264.5648 131.3218 -1.7739 229.2796 231.0535 264.7113 132.1805 -1.7767 229.4286 231.2053 264.8162 132.9470 -1.7756 229.5544 231.3299 264.8912 133.7750 -1.7764 229.7081 231.4845 264.9106 134.5620 -1.7740 229.8707 231.6447 265.0097 135.3593 -1.7739 229.9783 231.7521 265.1639 136.1873 -1.7769 230.1152 231.8921 265.2903 136.9435 -1.7776 230.2793 232.0569 265.3935 137.8023 -1.7751 230.4503 232.2254 265.4993 138.5693 -1.7780 230.5850 232.3629 265.6237 139.3875 -1.7789 230.7162 232.4952 265.7457 140.1950 -1.7766 230.8383 232.6148 265.8559 140.9820 -1.7726 230.9560 232.7287 265.9809 141.8100 -1.7675 231.0718 232.8393 266.1075 142.5765 -1.7694 231.2160 232.9854 266.1945 143.4250 -1.7669 231.3812 233.1482 266.2992 144.1915 -1.7627 231.4945 233.2572 266.4305 145.0195 -1.7586 231.6391 233.3977 266.5838 145.8168 -1.7601 231.7572 233.5173 266.7267 146.6140 -1.7606 231.8812 233.6418 266.8566 147.4318 -1.7610 231.9960 233.7570 267.0054 148.2085 -1.7583 232.1369 233.8952 267.1072 149.0570 -1.7597 232.2823 234.0420 267.2233 149.8235 -1.7590 232.3835 234.1425 267.3264 150.6515 -1.7565 232.5255 234.2820 267.4499 151.4488 -1.7575 232.6816 234.4391 267.5834 152.2460 -1.7591 232.7893 234.5483 267.7094 153.0638 -1.7590 232.9330 234.6920 267.8195 153.8405 -1.7594 233.0912 234.8506 267.9301 154.6890 -1.7563 233.2026 234.9588 268.0638 155.4555 -1.7537 233.3239 235.0776 268.2053 156.2835 -1.7522 233.4773 235.2294 268.3612 157.0808 -1.7551 233.6524 235.4075 268.4885 157.8780 -1.7597 233.7977 235.5574 268.6123 158.6753 -1.7544 233.9367 235.6911 268.7467 159.4725 -1.7530 234.0832 235.8362 268.8729 160.3005 -1.7542 234.2256 235.9798 268.9653 161.0670 -1.7517 234.3449 236.0967 269.0789 161.9155 -1.7512 234.4665 236.2177 269.1827 162.6923 -1.7473 234.6120 236.3593 269.3267 163.5100 -1.7465 234.7477 236.4942 269.4554 164.3073 -1.7423 234.8842 236.6265 269.5767 165.1045 -1.7474 234.9677 236.7150 269.7004 165.9325 -1.7456 235.0533 236.7989 269.8446 166.6990 -1.7436 235.1778 236.9214 269.9417 167.5475 -1.7463 235.3517 237.0981 270.1098 168.2935 -1.7506 235.4730 237.2236 270.2470 169.1625 -1.7550 235.6010 237.3560 270.4010 169.9393 -1.7551 235.7298 237.4849 270.5201 170.7570 -1.7502 235.8815 237.6317 270.6537 171.5543 -1.7485 235.9964 237.7448 270.8057 172.3515 -1.7487 236.1465 237.8951 270.9379 173.1795 -1.7426 236.2763 238.0189 271.0904 173.9460 -1.7393 236.4173 238.1565 271.2438 174.7638 -1.7381 236.5209 238.2590 271.3797 175.5405 -1.7386 236.6733 238.4119 271.5199 176.3890 -1.7437 236.8390 238.5828 271.7033 177.1555 -1.7391 236.9690 238.7081 271.8646 177.9835 -1.7389 237.1206 238.8594 272.0292 178.7603 -1.7380 237.2314 238.9694 272.1313 179.5985 -1.7386 237.3224 239.0610 272.2969 180.3958 -1.7373 237.4120 239.1493 272.4600 181.1828 -1.7366 237.5243 239.2610 272.5892 182.0108 -1.7387 237.6917 239.4304 272.7538 182.7670 -1.7399 237.7990 239.5389 272.8741 183.6155 -1.7388 237.9250 239.6637 273.0583 184.3615 -1.7384 238.0475 239.7859 273.2071 185.2100 -1.7381 238.2141 239.9523 273.3695 185.9663 -1.7414 238.3607 240.1021 273.5027 186.7943 -1.7390 238.5129 240.2519 273.6325 187.5915 -1.7391 238.6540 240.3931 273.7535 188.3785 -1.7401 238.8103 240.5505 273.8616 189.2065 -1.7394 238.9785 240.7179 273.9881 189.9738 -1.7400 239.0710 240.8109 274.1397 190.8225 -1.7375 239.1926 240.9301 274.3202 191.5890 -1.7402 239.3321 241.0724 274.4876 192.4170 -1.7378 239.4831 241.2209 274.6553 193.1733 -1.7320 239.5886 241.3206 274.7953 194.0115 -1.7343 239.7414 241.4756 274.9440 194.7985 -1.7349 239.8957 241.6306 275.1082 195.5855 -1.7351 240.0010 241.7361 275.2540 196.4238 -1.7362 240.1276 241.8638 275.3757 197.1800 -1.7374 240.2625 241.9999 275.4963 198.0388 -1.7403 240.3815 242.1218 275.6296 198.8053 -1.7395 240.4624 242.2019 275.7441 199.6333 -1.7371 240.5862 242.3233 275.8704 200.4305 -1.7404 240.7238 242.4642 275.9845 201.2175 -1.7409 240.8682 242.6091 276.1318 202.0250 -1.7407 241.0286 242.7693 276.2639 202.8120 -1.7397 241.1762 242.9159 276.4055 203.6400 -1.7388 241.2986 243.0373 276.5104 204.4065 -1.7371 241.4161 243.1532 276.6410 205.2653 -1.7335 241.5629 243.2963 276.7846 206.0325 -1.7348 241.6846 243.4194 276.9276 206.8505 -1.7379 241.8403 243.5782 277.0789 207.6580 -1.7371 241.9430 243.6801 277.1856 208.4450 -1.7325 242.0814 243.8138 277.3115 209.2423 -1.7301 242.2270 243.9571 277.4206 210.0395 -1.7325 242.3721 244.1046 277.5755 210.8675 -1.7272 242.5304 244.2577 277.7282 211.6340 -1.7249 242.6455 244.3704 277.8475 212.4825 -1.7327 242.8034 244.5361 278.0245 213.2593 -1.7351 242.9227 244.6578 278.1482 214.0770 -1.7318 243.0689 244.8007 278.3055 214.8743 -1.7291 243.2364 244.9654 278.4392 215.6715 -1.7292 243.3699 245.0991 278.5567 216.4995 -1.7327 243.5145 245.2472 278.6696 217.2660 -1.7354 243.6352 245.3707 278.7940 218.1145 -1.7368 243.7991 245.5358 278.9339 218.8913 -1.7369 243.9237 245.6606 279.0594 219.7090 -1.7340 244.0960 245.8301 279.1956 220.5063 -1.7386 244.2028 245.9414 279.3272 221.3035 -1.7370 244.3401 246.0771 279.4475 222.1315 -1.7327 244.4775 246.2102 279.5543 222.8980 -1.7308 244.6010 246.3318 279.6407 223.7465 -1.7284 244.7719 246.5003 279.7391 224.5233 -1.7268 244.9196 246.6464 279.8232 225.3410 -1.7225 245.0628 246.7853 279.9669 226.1383 -1.7210 245.1792 246.9003 280.1061 226.9355 -1.7206 245.2877 247.0083 280.1994 227.7635 -1.7157 245.4015 247.1172 280.3202 228.5300 -1.7143 245.5219 247.2362 280.4585 229.3785 -1.7185 245.6855 247.4041 280.5512 230.1553 -1.7206 245.8174 247.5380 280.6809 230.9730 -1.7245 245.9552 247.6797 280.7917 231.7710 -1.7245 246.0835 247.8080 280.9128 232.5685 -1.7174 246.2334 247.9508 281.0274 233.3965 -1.7167 246.3873 248.1040 281.1480 234.1630 -1.7158 246.5079 248.2238 281.2659 235.0115 -1.7195 246.6237 248.3431 281.3835 235.7883 -1.7176 246.7330 248.4506 281.4796 236.6060 -1.7159 246.8860 248.6019 281.5932 237.4033 -1.7095 247.0420 248.7515 281.7165 238.2005 -1.7062 247.1888 248.8950 281.8623 239.0285 -1.7047 247.3179 249.0226 281.9843 239.7950 -1.7042 247.4538 249.1581 282.0924 240.6435 -1.6983 247.5760 249.2743 282.2171 241.4110 -1.6971 247.7171 249.4143 282.2944 242.2288 -1.6930 247.8391 249.5321 282.3996 243.0055 -1.6902 247.9610 249.6512 282.5181 243.8540 -1.6854 248.0698 249.7552 282.6509 244.6205 -1.6868 248.2065 249.8932 282.7772 245.4485 -1.6885 248.3591 250.0475 282.9317 246.2355 -1.6832 248.5017 250.1849 283.0423 247.0328 -1.6805 248.6659 250.3464 283.1826 247.8608 -1.6782 248.7930 250.4712 283.3372 248.6170 -1.6729 248.9143 250.5871 283.4657 249.4655 -1.6696 249.0419 250.7114 283.6098 250.2115 -1.6735 249.1749 250.8484 283.7360 251.0600 -1.6718 249.3376 251.0093 283.8667 251.8265 -1.6655 249.4546 251.1201 283.9749 252.6545 -1.6630 249.5979 251.2610 284.0880 253.4518 -1.6630 249.7341 251.3971 284.1883 254.2388 -1.6624 249.8670 251.5294 284.2933 255.0668 -1.6601 249.9981 251.6582 284.4091 255.8333 -1.6611 250.1431 251.8042 284.5467 256.6818 -1.6576 250.3088 251.9664 284.6770 257.4483 -1.6506 250.4304 252.0809 284.8206 258.2763 -1.6495 250.5541 252.2037 284.9890 259.0633 -1.6538 250.6880 252.3418 285.1375 259.8605 -1.6528 250.7797 252.4325 285.2346 260.6885 -1.6526 250.8780 252.5306 285.3476 261.4550 -1.6519 251.0253 252.6772 285.5137 262.3035 -1.6476 251.2080 252.8555 285.6445 263.0495 -1.6439 251.3248 252.9687 285.7623 263.8980 -1.6419 251.4561 253.0980 285.8850 264.6645 -1.6390 251.5921 253.2311 286.0013 265.4925 -1.6370 251.7172 253.3542 286.1045 266.2898 -1.6335 251.8513 253.4848 286.2248 267.0870 -1.6322 251.9858 253.6180 286.3565 267.9048 -1.6290 252.1265 253.7555 286.5160 268.6815 -1.6263 252.2519 253.8782 286.6391 269.5300 -1.6228 252.4227 254.0455 286.7794 270.2965 -1.6185 252.5741 254.1926 286.9300 271.1245 -1.6154 252.6774 254.2928 287.1076 271.9218 -1.6164 252.8268 254.4432 287.2189 272.7193 -1.6164 252.9823 254.5987 287.3491 273.5375 -1.6171 253.1194 254.7365 287.4714 274.3145 -1.6182 253.2496 254.8677 287.6153 275.1630 -1.6145 253.3937 255.0082 287.7638 275.9295 -1.6138 253.5234 255.1372 287.8711 276.7575 -1.6118 253.6480 255.2598 288.0113 277.5240 -1.6110 253.8111 255.4222 288.1472 278.3520 -1.6136 253.9419 255.5555 288.2815 279.1390 -1.6125 254.0806 255.6932 288.3761 279.9465 -1.6107 254.1941 255.8048 288.4969 280.7643 -1.6107 254.3593 255.9699 288.6447 281.5308 -1.6116 254.5182 256.1299 288.7715 282.3895 -1.6105 254.6796 256.2901 288.9187 283.1560 -1.6068 254.8257 256.4325 289.0385 283.9840 -1.6048 254.9878 256.5926 289.1634 284.7710 -1.6038 255.1573 256.7611 289.2833 285.5785 -1.6057 255.3124 256.9181 289.4534 286.3963 -1.6051 255.4940 257.0992 289.5967 287.1628 -1.6020 255.6376 257.2396 289.7334 288.0220 -1.6010 255.7794 257.3804 289.9058 288.7583 -1.6004 255.9093 257.5097 290.0279 289.6170 -1.5977 256.0223 257.6199 290.1304 290.3733 -1.5920 256.1001 257.6921 290.2340 291.2115 -1.5891 256.2453 257.8343 290.3406 291.9985 -1.5853 256.3761 257.9614 290.4390 292.7958 -1.5827 256.5113 258.0940 290.5804 293.6238 -1.5818 256.6186 258.2005 290.6922 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