DTA measure 2lassu Date: 2026324:1549 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.58 s Mass = 1191.400 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2005 -1.1816 217.7257 218.9074 248.9281 1.9978 -1.1836 217.8342 219.0178 248.9040 2.8160 -1.1884 217.9221 219.1105 248.8751 3.5825 -1.1929 218.0087 219.2016 248.8146 4.4310 -1.1916 218.1245 219.3161 248.7591 5.1975 -1.1913 218.2472 219.4385 248.7248 6.0255 -1.1910 218.3462 219.5372 248.6854 6.8228 -1.1866 218.4409 219.6275 248.6502 7.6095 -1.1843 218.5530 219.7373 248.6042 8.4378 -1.1819 218.6717 219.8535 248.5523 9.2038 -1.1810 218.7442 219.9252 248.5139 10.0215 -1.1824 218.8536 220.0359 248.4591 10.7878 -1.1814 218.9601 220.1415 248.3958 11.6468 -1.1794 219.0694 220.2489 248.3518 12.4130 -1.1751 219.1467 220.3218 248.2956 13.2315 -1.1716 219.2226 220.3942 248.2492 14.0390 -1.1720 219.2954 220.4674 248.2396 14.8253 -1.1686 219.3729 220.5415 248.1847 15.6533 -1.1669 219.4754 220.6422 248.1495 16.4195 -1.1655 219.5937 220.7592 248.0757 17.2688 -1.1638 219.7038 220.8675 248.0389 18.0350 -1.1658 219.8436 221.0094 248.0090 18.8630 -1.1662 219.9798 221.1461 247.9876 19.6603 -1.1672 220.0763 221.2435 247.9677 20.4570 -1.1665 220.1703 221.3368 247.9586 21.2753 -1.1656 220.2933 221.4588 247.9314 22.0515 -1.1647 220.3828 221.5475 247.8960 22.9000 -1.1636 220.4866 221.6503 247.8532 23.6665 -1.1606 220.5771 221.7377 247.8223 24.4945 -1.1600 220.6842 221.8441 247.8168 25.2923 -1.1599 220.7761 221.9360 247.7910 26.0890 -1.1558 220.8640 222.0198 247.8027 26.9075 -1.1570 220.9760 222.1330 247.8310 27.6845 -1.1562 221.0770 222.2332 247.8594 28.5330 -1.1551 221.1791 222.3342 247.8065 29.2995 -1.1528 221.2823 222.4351 247.8753 30.1275 -1.1506 221.3732 222.5238 247.9355 30.9248 -1.1479 221.4978 222.6457 247.9792 31.7220 -1.1447 221.6280 222.7728 248.0026 32.5398 -1.1415 221.7489 222.8903 248.0546 33.3165 -1.1403 221.8350 222.9753 248.1149 34.1650 -1.1400 221.8931 223.0330 248.1572 34.9110 -1.1405 221.9841 223.1246 248.2415 35.7595 -1.1369 222.0775 223.2144 248.3267 36.5363 -1.1339 222.1874 223.3214 248.3712 37.3540 -1.1333 222.3140 223.4473 248.4350 38.1513 -1.1308 222.4059 223.5367 248.4902 38.9485 -1.1312 222.5133 223.6445 248.5657 39.7765 -1.1301 222.6066 223.7367 248.6772 40.5430 -1.1322 222.6871 223.8193 248.7198 41.3925 -1.1283 222.8138 223.9421 248.8946 42.1683 -1.1251 222.9076 224.0327 249.0167 42.9863 -1.1237 222.9901 224.1138 249.1184 43.7835 -1.1238 223.0948 224.2187 249.1867 44.5808 -1.1209 223.1783 224.2992 249.2860 45.4088 -1.1186 223.2819 224.4005 249.4056 46.1755 -1.1208 223.3635 224.4843 249.5130 47.0245 -1.1214 223.4604 224.5818 249.6533 47.8013 -1.1187 223.5814 224.7001 249.7433 48.6190 -1.1177 223.6805 224.7982 249.8524 49.4163 -1.1135 223.8010 224.9145 249.9640 50.2135 -1.1117 223.8949 225.0066 250.0647 51.0415 -1.1078 223.9845 225.0924 250.1872 51.8080 -1.1063 224.0638 225.1701 250.3172 52.6565 -1.1011 224.1811 225.2822 250.4544 53.4333 -1.1000 224.2696 225.3697 250.5468 54.2613 -1.0960 224.3965 225.4924 250.6808 55.0585 -1.0925 224.5306 225.6231 250.7994 55.8455 -1.0927 224.6073 225.7000 250.9289 56.6838 -1.0919 224.7131 225.8050 251.0786 57.4400 -1.0906 224.8031 225.8938 251.1978 58.2988 -1.0982 224.8841 225.9823 251.3601 59.0655 -1.1007 224.9579 226.0586 251.5055 59.8935 -1.0998 224.9938 226.0935 251.6528 60.6498 -1.0999 225.0611 226.1609 251.7820 61.4785 -1.0992 225.1346 226.2338 251.9211 62.2758 -1.1001 225.2602 226.3603 252.0376 63.0628 -1.1028 225.3566 226.4594 252.1593 63.8908 -1.1020 225.4879 226.5899 252.2655 64.6470 -1.1005 225.5998 226.7003 252.3990 65.5058 -1.1009 225.6863 226.7872 252.5559 66.2723 -1.1023 225.7930 226.8953 252.7301 67.0900 -1.1075 225.9209 227.0285 252.9365 67.8565 -1.1080 226.0530 227.1610 253.1180 68.6845 -1.1071 226.1491 227.2562 253.2668 69.4715 -1.1077 226.2507 227.3584 253.4004 70.2688 -1.1068 226.3561 227.4629 253.5137 71.0968 -1.1061 226.4500 227.5561 253.6666 71.8530 -1.1076 226.5472 227.6548 253.7896 72.7118 -1.1056 226.6505 227.7561 253.9419 73.4475 -1.1051 226.7405 227.8456 254.0391 74.3063 -1.1084 226.8854 227.9938 254.2063 75.0625 -1.1056 226.9422 228.0479 254.3395 75.8905 -1.1045 227.0246 228.1291 254.4948 76.6878 -1.1013 227.1016 228.2029 254.6165 77.4850 -1.1035 227.1916 228.2951 254.6948 78.3035 -1.1082 227.2590 228.3673 254.7971 79.0805 -1.1060 227.3285 228.4345 254.9957 79.9290 -1.1057 227.4301 228.5358 255.1770 80.6955 -1.1073 227.5397 228.6470 255.3070 81.5235 -1.1058 227.6384 228.7442 255.4680 82.2798 -1.1031 227.7656 228.8687 255.6210 83.1078 -1.1034 227.8712 228.9746 255.7321 83.9050 -1.1064 227.9853 229.0916 255.8760 84.6920 -1.1078 228.0727 229.1805 255.9914 85.5200 -1.1088 228.1495 229.2584 256.1187 86.2865 -1.1087 228.2318 229.3406 256.2453 87.1555 -1.1095 228.3550 229.4644 256.3998 87.9118 -1.1102 228.4419 229.5520 256.5718 88.7398 -1.1133 228.5569 229.6702 256.6984 89.5063 -1.1124 228.6768 229.7892 256.8437 90.3343 -1.1132 228.7667 229.8799 256.9590 91.1315 -1.1152 228.8733 229.9885 257.0930 91.9185 -1.1152 228.9818 230.0969 257.2494 92.7568 -1.1130 229.0973 230.2103 257.3659 93.5130 -1.1165 229.2135 230.3300 257.4753 94.3718 -1.1176 229.3331 230.4506 257.5853 95.1383 -1.1142 229.4379 230.5520 257.7058 95.9663 -1.1159 229.5297 230.6456 257.8199 96.7635 -1.1228 229.6307 230.7535 257.9411 97.5505 -1.1268 229.7118 230.8386 258.0795 98.3888 -1.1269 229.7918 230.9186 258.2098 99.1450 -1.1219 229.9193 231.0412 258.3087 100.0038 -1.1213 230.0183 231.1396 258.4168 100.7703 -1.1240 230.1303 231.2543 258.5192 101.5983 -1.1247 230.2419 231.3666 258.6449 102.3955 -1.1254 230.3182 231.4437 258.7518 103.1825 -1.1272 230.4166 231.5437 258.8574 104.0208 -1.1285 230.5446 231.6732 258.9711 104.7770 -1.1306 230.6308 231.7614 259.0632 105.6358 -1.1334 230.7426 231.8761 259.2107 106.3715 -1.1356 230.8261 231.9617 259.2885 107.2405 -1.1351 230.9530 232.0881 259.4239 107.9968 -1.1346 231.0317 232.1663 259.4898 108.8248 -1.1401 231.1231 232.2632 259.5931 109.6220 -1.1454 231.2301 232.3755 259.7025 110.4193 -1.1506 231.3267 232.4773 259.8056 111.2473 -1.1477 231.4866 232.6342 259.9385 112.0035 -1.1473 231.5907 232.7380 260.0417 112.8725 -1.1497 231.6695 232.8192 260.1499 113.6288 -1.1458 231.7452 232.8910 260.2270 114.4568 -1.1464 231.8636 233.0100 260.3185 115.2540 -1.1506 231.9458 233.0964 260.4007 116.0513 -1.1551 232.0696 233.2247 260.4779 116.8793 -1.1531 232.1699 233.3231 260.5824 117.6355 -1.1514 232.2548 233.4063 260.6905 118.5045 -1.1483 232.4001 233.5484 260.7775 119.2608 -1.1487 232.5041 233.6528 260.8664 120.0888 -1.1490 232.5839 233.7328 260.9879 120.8860 -1.1515 232.6572 233.8087 261.0876 121.6833 -1.1522 232.7509 233.9031 261.1801 122.5113 -1.1515 232.8938 234.0453 261.2383 123.2675 -1.1545 233.0084 234.1629 261.3181 124.1365 -1.1608 233.1177 234.2785 261.4194 124.8928 -1.1618 233.1796 234.3414 261.5105 125.7105 -1.1660 233.2858 234.4518 261.6104 126.5078 -1.1668 233.4046 234.5714 261.7114 127.3050 -1.1690 233.5167 234.6856 261.7756 128.1228 -1.1683 233.6022 234.7705 261.8390 128.8893 -1.1681 233.6969 234.8651 261.9159 129.7378 -1.1659 233.8084 234.9742 262.0050 130.5043 -1.1707 233.9001 235.0708 262.0917 131.3220 -1.1751 233.9873 235.1624 262.1802 132.1193 -1.1734 234.1033 235.2766 262.2875 132.9165 -1.1722 234.2022 235.3744 262.3790 133.7445 -1.1648 234.2999 235.4647 262.4279 134.5008 -1.1633 234.4167 235.5800 262.5183 135.3595 -1.1754 234.5765 235.7518 262.6194 136.0850 -1.1790 234.6864 235.8655 262.7054 136.9438 -1.1760 234.7887 235.9647 262.7831 137.7103 -1.1735 234.8829 236.0564 262.8678 138.5280 -1.1752 234.9746 236.1499 262.9406 139.3253 -1.1741 235.0464 236.2206 263.0284 140.1225 -1.1764 235.1332 236.3096 263.1063 140.9505 -1.1755 235.2306 236.4061 263.1816 141.7170 -1.1778 235.3297 236.5075 263.2711 142.5655 -1.1767 235.4750 236.6516 263.3156 143.3423 -1.1774 235.5852 236.7627 263.4016 144.1600 -1.1780 235.6932 236.8712 263.4574 144.9573 -1.1767 235.7935 236.9702 263.5425 145.7545 -1.1784 235.9215 237.0999 263.6348 146.5825 -1.1776 236.0384 237.2160 263.7265 147.3490 -1.1767 236.1664 237.3431 263.8200 148.1975 -1.1764 236.3055 237.4820 263.9619 148.9640 -1.1754 236.4240 237.5994 264.0373 149.7920 -1.1754 236.4875 237.6629 264.1298 150.5790 -1.1767 236.5507 237.7273 264.2311 151.3865 -1.1823 236.6349 237.8172 264.3364 152.2043 -1.1864 236.6858 237.8722 264.4297 152.9708 -1.1849 236.7539 237.9388 264.5298 153.8295 -1.1823 236.8549 238.0372 264.6124 154.5960 -1.1777 236.9567 238.1344 264.7110 155.4240 -1.1752 237.0741 238.2493 264.8309 156.2110 -1.1714 237.1751 238.3465 264.9086 157.0185 -1.1705 237.2880 238.4585 264.9840 157.8363 -1.1736 237.4176 238.5912 265.0756 158.6028 -1.1786 237.5473 238.7259 265.1791 159.4615 -1.1833 237.6488 238.8321 265.2746 160.1973 -1.1861 237.7478 238.9338 265.3885 161.0560 -1.1846 237.8267 239.0113 265.4765 161.8123 -1.1876 237.9276 239.1152 265.5500 162.6505 -1.1889 238.0633 239.2522 265.6377 163.4375 -1.1881 238.1574 239.3456 265.7149 164.2450 -1.1856 238.2696 239.4553 265.8042 165.0628 -1.1845 238.3800 239.5645 265.9097 165.8395 -1.1799 238.4805 239.6604 266.0471 166.6880 -1.1797 238.6058 239.7855 266.1611 167.4545 -1.1830 238.6721 239.8552 266.2653 168.2825 -1.1921 238.7761 239.9683 266.3268 169.0798 -1.1967 238.8538 240.0505 266.4201 169.8770 -1.2010 238.9566 240.1575 266.5403 170.6948 -1.1996 239.0589 240.2585 266.6568 171.4715 -1.1987 239.1592 240.3579 266.7490 172.2995 -1.1935 239.2654 240.4589 266.8454 173.0660 -1.1877 239.3684 240.5560 266.9510 173.9145 -1.1836 239.4716 240.6552 267.0562 174.6913 -1.1849 239.5347 240.7196 267.1606 175.5090 -1.1820 239.6394 240.8214 267.2669 176.3063 -1.1846 239.7462 240.9308 267.3676 177.1035 -1.1849 239.8362 241.0210 267.4768 177.9315 -1.1841 239.9516 241.1358 267.5901 178.6980 -1.1838 240.0616 241.2455 267.6851 179.5568 -1.1835 240.1843 241.3678 267.8263 180.2925 -1.1835 240.2842 241.4677 267.9440 181.1513 -1.1829 240.3785 241.5613 268.0542 181.9178 -1.1856 240.4690 241.6547 268.1429 182.7355 -1.1875 240.5933 241.7807 268.2710 183.5430 -1.1870 240.6916 241.8787 268.3901 184.3300 -1.1842 240.7854 241.9695 268.5063 185.1683 -1.1845 240.8787 242.0632 268.6409 185.9245 -1.1854 240.9831 242.1684 268.7403 186.7935 -1.1921 241.1654 242.3575 268.8675 187.5498 -1.1973 241.2594 242.4566 268.9835 188.3778 -1.2001 241.3710 242.5711 269.1280 189.1443 -1.2024 241.4433 242.6457 269.2431 189.9723 -1.1999 241.5215 242.7215 269.3544 190.7593 -1.1990 241.6260 242.8250 269.4666 191.5565 -1.2009 241.7076 242.9086 269.5643 192.3743 -1.2014 241.8382 243.0396 269.6462 193.1305 -1.2042 241.9508 243.1550 269.7619 193.9893 -1.2011 242.0551 243.2562 269.9337 194.7455 -1.1985 242.1907 243.3892 270.0249 195.5735 -1.1976 242.2855 243.4831 270.1432 196.3400 -1.1986 242.3935 243.5921 270.2842 197.1578 -1.1992 242.5007 243.7000 270.4028 197.9550 -1.2043 242.5843 243.7887 270.4966 198.7523 -1.2063 242.7085 243.9149 270.6463 199.5803 -1.2080 242.7912 243.9992 270.7813 200.3365 -1.2102 242.8631 244.0733 270.8751 201.2055 -1.2110 242.9550 244.1660 271.0127 201.9310 -1.2172 243.0615 244.2787 271.1115 202.7795 -1.2189 243.1769 244.3958 271.2214 203.5563 -1.2189 243.2797 244.4986 271.3330 204.3740 -1.2173 243.3963 244.6136 271.4535 205.1713 -1.2156 243.4961 244.7116 271.5722 205.9685 -1.2139 243.5733 244.7871 271.6797 206.7965 -1.2101 243.6866 244.8968 271.8087 207.5528 -1.2107 243.8007 245.0114 271.9244 208.4115 -1.2123 243.9256 245.1378 272.0375 209.1780 -1.2140 244.0498 245.2637 272.1540 210.0060 -1.2175 244.1669 245.3845 272.2723 210.7930 -1.2181 244.2514 245.4695 272.3731 211.5903 -1.2164 244.3527 245.5691 272.5013 212.4183 -1.2169 244.4598 245.6766 272.6286 213.1745 -1.2172 244.5380 245.7553 272.7521 214.0435 -1.2187 244.6369 245.8555 272.8458 214.7998 -1.2215 244.7573 245.9788 272.9409 215.6175 -1.2220 244.8724 246.0944 273.0265 216.4250 -1.2288 245.0020 246.2309 273.1350 217.2120 -1.2307 245.1225 246.3531 273.2096 218.0400 -1.2331 245.2010 246.4340 273.3127 218.8065 -1.2386 245.2676 246.5062 273.4089 219.6653 -1.2401 245.3751 246.6152 273.5062 220.4010 -1.2395 245.4592 246.6987 273.5941 221.2495 -1.2372 245.5845 246.8217 273.7050 222.0570 -1.2388 245.6855 246.9243 273.7968 222.8440 -1.2394 245.8082 247.0477 273.8649 223.6413 -1.2407 245.9389 247.1796 273.9949 224.4385 -1.2442 246.0357 247.2799 274.0797 225.2665 -1.2436 246.1579 247.4015 274.1621 226.0330 -1.2449 246.2419 247.4868 274.2810 226.8815 -1.2484 246.3439 247.5923 274.3760 227.6583 -1.2478 246.4624 247.7102 274.4489 228.4760 -1.2473 246.5734 247.8207 274.5486 229.2733 -1.2460 246.6686 247.9146 274.6352 230.0705 -1.2473 246.7776 248.0249 274.7132 230.8985 -1.2483 246.9009 248.1492 274.8028 231.6650 -1.2483 246.9747 248.2230 274.9305 232.5135 -1.2492 247.0729 248.3221 275.0396 233.2903 -1.2467 247.1884 248.4351 275.1200 234.1080 -1.2438 247.3152 248.5590 275.2529 234.9053 -1.2461 247.4125 248.6585 275.3543 235.7025 -1.2510 247.5092 248.7602 275.4536 236.5305 -1.2540 247.6168 248.8708 275.5393 237.2970 -1.2596 247.6927 248.9523 275.6008 238.1455 -1.2634 247.8132 249.0765 275.6440 238.9223 -1.2639 247.8891 249.1531 275.7254 239.7400 -1.2599 248.0238 249.2838 275.8018 240.5373 -1.2631 248.1565 249.4196 275.8560 241.3345 -1.2660 248.2444 249.5104 275.9753 242.1625 -1.2694 248.3322 249.6016 276.0944 242.9290 -1.2684 248.4265 249.6949 276.1902 243.7775 -1.2693 248.5807 249.8500 276.2949 244.5543 -1.2710 248.6800 249.9510 276.3791 245.3823 -1.2740 248.7936 250.0676 276.4473 246.1795 -1.2738 248.8713 250.1451 276.5355 246.9665 -1.2725 248.9545 250.2271 276.6392 247.8048 -1.2774 249.0576 250.3350 276.7455 248.5610 -1.2783 249.1313 250.4096 276.8407 249.4198 -1.2753 249.2389 250.5142 276.9645 250.1863 -1.2731 249.3360 250.6091 277.0522 251.0143 -1.2719 249.4272 250.6991 277.1766 251.8115 -1.2704 249.5577 250.8281 277.2601 252.5985 -1.2719 249.6708 250.9428 277.3503 253.4368 -1.2718 249.7776 251.0494 277.4657 254.1930 -1.2725 249.8732 251.1457 277.6014 255.0415 -1.2659 249.9839 251.2497 277.7044 255.8080 -1.2681 250.0774 251.3456 277.7910 256.6360 -1.2692 250.1906 251.4598 277.8794 257.4230 -1.2682 250.3194 251.5876 277.9608 258.2203 -1.2724 250.4392 251.7116 278.0531 259.0380 -1.2693 250.5376 251.8068 278.1305 259.8045 -1.2707 250.6602 251.9309 278.2313 260.6633 -1.2735 250.7937 252.0672 278.3244 261.3990 -1.2709 250.8542 252.1250 278.4243 262.2475 -1.2737 250.9392 252.2129 278.5527 263.0243 -1.2804 251.0689 252.3493 278.6350 263.8420 -1.2798 251.1832 252.4630 278.7173 264.6290 -1.2852 251.2977 252.5828 278.7848 265.4365 -1.2878 251.3860 252.6738 278.9101 266.2543 -1.2865 251.4939 252.7804 279.0153 267.0105 -1.2880 251.5775 252.8655 279.1268 267.8795 -1.2920 251.6784 252.9704 279.2539 268.6358 -1.2914 251.7873 253.0787 279.3243 269.4638 -1.2888 251.9460 253.2348 279.4065 270.2610 -1.2895 252.0566 253.3461 279.5092 271.0480 -1.2920 252.1686 253.4605 279.6361 271.8453 -1.2945 252.2913 253.5859 279.7481 272.6425 -1.2930 252.3770 253.6700 279.8687 273.4705 -1.2905 252.4936 253.7841 279.9478 274.2370 -1.2904 252.5999 253.8903 280.0335 275.0855 -1.2902 252.6973 253.9875 280.1513 275.8623 -1.2919 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