DTA measure 1pb3 Date: 202535:916 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.51 s Mass = 958.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1478 -0.3542 221.1981 221.5523 261.5590 1.9103 -0.3485 221.3812 221.7297 261.5517 2.7320 -0.3445 221.5426 221.8870 261.5228 3.5245 -0.3440 221.6800 222.0239 261.5227 4.3158 -0.3418 221.8538 222.1956 261.5288 5.1380 -0.3358 222.0391 222.3749 261.5492 5.9298 -0.3322 222.1928 222.5250 261.5543 6.7518 -0.3286 222.3457 222.6743 261.5477 7.5440 -0.3282 222.5130 222.8412 261.5831 8.3355 -0.3219 222.6886 223.0105 261.6085 9.1580 -0.3225 222.8362 223.1587 261.6434 9.9498 -0.3185 222.9968 223.3153 261.6917 10.7725 -0.3120 223.1772 223.4892 261.7441 11.5650 -0.3104 223.3482 223.6586 261.7594 12.3565 -0.3097 223.5117 223.8214 261.8145 13.1790 -0.3052 223.6602 223.9654 261.8686 13.9705 -0.3042 223.8117 224.1159 261.9278 14.7928 -0.3010 223.9798 224.2809 262.0150 15.5850 -0.2986 224.1572 224.4558 262.0880 16.3775 -0.2981 224.3055 224.6036 262.1919 17.2000 -0.2948 224.4739 224.7687 262.2950 17.9598 -0.2917 224.6206 224.9123 262.3840 18.8080 -0.2878 224.8017 225.0895 262.4900 19.5970 -0.2814 224.9434 225.2248 262.5926 20.3850 -0.2804 225.1237 225.4042 262.7194 21.2033 -0.2775 225.2961 225.5736 262.8497 21.9610 -0.2776 225.4330 225.7106 262.9830 22.8090 -0.2742 225.5908 225.8650 263.1350 23.5973 -0.2695 225.7457 226.0152 263.2680 24.3860 -0.2695 225.9040 226.1735 263.4163 25.2050 -0.2683 226.0763 226.3446 263.5920 25.9640 -0.2677 226.2235 226.4912 263.7421 26.8130 -0.2669 226.3787 226.6456 263.8933 27.6010 -0.2632 226.5238 226.7870 264.0430 28.3900 -0.2583 226.6755 226.9338 264.2182 29.2083 -0.2576 226.8654 227.1230 264.4084 29.9970 -0.2607 227.0064 227.2672 264.5959 30.8163 -0.2568 227.1870 227.4438 264.7755 31.6050 -0.2600 227.3240 227.5840 264.9588 32.3953 -0.2617 227.5015 227.7632 265.1426 33.2165 -0.2590 227.6633 227.9223 265.3308 34.0063 -0.2601 227.8073 228.0674 265.5234 34.8273 -0.2605 227.9557 228.2162 265.7048 35.6185 -0.2634 228.1074 228.3709 265.8984 36.4098 -0.2649 228.2738 228.5387 266.0769 37.2315 -0.2662 228.4426 228.7088 266.2818 38.0235 -0.2642 228.5975 228.8617 266.4548 38.8455 -0.2648 228.7580 229.0228 266.6443 39.6375 -0.2681 228.9086 229.1767 266.8342 40.4295 -0.2671 229.0657 229.3328 267.0210 41.2515 -0.2667 229.2385 229.5052 267.2165 42.0135 -0.2654 229.3900 229.6554 267.3859 42.8655 -0.2638 229.5292 229.7931 267.5775 43.6575 -0.2590 229.6844 229.9434 267.7573 44.4495 -0.2625 229.8542 230.1167 267.9145 45.2715 -0.2629 230.0470 230.3099 268.1018 46.0335 -0.2634 230.1864 230.4498 268.2675 46.8855 -0.2675 230.3561 230.6236 268.4688 47.6775 -0.2664 230.4860 230.7524 268.6117 48.4695 -0.2691 230.6407 230.9097 268.7601 49.2915 -0.2685 230.8206 231.0892 268.9195 50.0533 -0.2699 230.9586 231.2285 269.0695 50.9053 -0.2681 231.1139 231.3820 269.2440 51.6973 -0.2696 231.2783 231.5478 269.3900 52.4885 -0.2718 231.4330 231.7048 269.5544 53.3113 -0.2723 231.5963 231.8686 269.7197 54.1028 -0.2722 231.7317 232.0038 269.8722 54.9250 -0.2751 231.9031 232.1782 270.0061 55.7170 -0.2734 232.0595 232.3329 270.1463 56.5085 -0.2779 232.2086 232.4866 270.2769 57.3310 -0.2782 232.3756 232.6538 270.4128 58.1228 -0.2815 232.5179 232.7994 270.5540 58.9448 -0.2826 232.7009 232.9834 270.6813 59.7370 -0.2834 232.8564 233.1398 270.8098 60.5285 -0.2841 232.9887 233.2728 270.9134 61.3810 -0.2801 233.1798 233.4599 271.0719 62.1428 -0.2796 233.3060 233.5856 271.1815 62.9648 -0.2804 233.4750 233.7553 271.3206 63.7570 -0.2863 233.6400 233.9263 271.4348 64.5485 -0.2874 233.7662 234.0536 271.5458 65.4008 -0.2879 233.9524 234.2403 271.6823 66.1625 -0.2886 234.1063 234.3949 271.7945 66.9848 -0.2885 234.2411 234.5296 271.9134 67.8070 -0.2880 234.3985 234.6865 272.0261 68.5695 -0.2896 234.5602 234.8498 272.1395 69.4215 -0.2915 234.7069 234.9984 272.2726 70.2135 -0.2910 234.8578 235.1488 272.3866 71.0055 -0.2930 235.0184 235.3113 272.5221 71.8275 -0.2959 235.1894 235.4853 272.6201 72.5895 -0.2956 235.3438 235.6394 272.7440 73.4418 -0.2932 235.4953 235.7885 272.8184 74.2335 -0.2937 235.6510 235.9447 272.9262 75.0255 -0.2980 235.8061 236.1042 273.0544 75.8475 -0.2997 235.9586 236.2583 273.1723 76.6395 -0.2970 236.1127 236.4096 273.2640 77.4623 -0.3012 236.2791 236.5802 273.4059 78.2545 -0.3008 236.4191 236.7199 273.5090 79.0465 -0.2996 236.5774 236.8770 273.6420 79.8988 -0.3012 236.7549 237.0560 273.7601 80.6615 -0.2997 236.8876 237.1873 273.8556 81.4830 -0.3004 237.0354 237.3358 273.9738 82.2753 -0.2994 237.1780 237.4774 274.0840 83.0833 -0.3047 237.3478 237.6524 274.1970 83.9023 -0.3054 237.4869 237.7924 274.3077 84.6600 -0.3022 237.6380 237.9402 274.4141 85.5085 -0.3077 237.8103 238.1180 274.5305 86.2663 -0.3088 237.9591 238.2679 274.6498 87.0855 -0.3096 238.0813 238.3909 274.7656 87.8733 -0.3092 238.2457 238.5549 274.8656 88.6613 -0.3098 238.3857 238.6955 274.9843 89.5095 -0.3095 238.5475 238.8569 275.1201 90.2673 -0.3126 238.7182 239.0309 275.2385 91.0853 -0.3142 238.8746 239.1889 275.3527 91.8738 -0.3147 239.0213 239.3360 275.4582 92.6625 -0.3164 239.1470 239.4635 275.5851 93.5113 -0.3178 239.3088 239.6267 275.7066 94.2693 -0.3177 239.4591 239.7767 275.8136 95.0890 -0.3214 239.6120 239.9334 275.9468 95.9080 -0.3221 239.7579 240.0800 276.0753 96.6670 -0.3205 239.9142 240.2347 276.2026 97.5165 -0.3215 240.0792 240.4007 276.3456 98.2760 -0.3259 240.2258 240.5516 276.4600 99.0968 -0.3262 240.3649 240.6911 276.5992 99.8870 -0.3256 240.5128 240.8383 276.7364 100.6768 -0.3290 240.6790 241.0080 276.8721 101.5280 -0.3306 240.8389 241.1695 277.0056 102.2893 -0.3305 240.9674 241.2980 277.1421 103.1108 -0.3340 241.1093 241.4433 277.2874 103.9030 -0.3361 241.2675 241.6036 277.4306 104.6945 -0.3406 241.4341 241.7748 277.5472 105.5170 -0.3400 241.5932 241.9333 277.7175 106.2785 -0.3378 241.7350 242.0728 277.8506 107.1310 -0.3438 241.8814 242.2252 278.0061 107.8928 -0.3466 242.0251 242.3716 278.1451 108.7148 -0.3481 242.1840 242.5321 278.2806 109.5370 -0.3482 242.3401 242.6883 278.4412 110.2985 -0.3523 242.4761 242.8284 278.5600 111.1508 -0.3544 242.6302 242.9846 278.7204 111.9125 -0.3566 242.7834 243.1400 278.8612 112.7348 -0.3572 242.9132 243.2704 279.0075 113.5268 -0.3612 243.0846 243.4458 279.1333 114.3185 -0.3618 243.2388 243.6005 279.2926 115.1408 -0.3634 243.3706 243.7340 279.4496 115.9325 -0.3641 243.5225 243.8866 279.5861 116.7548 -0.3629 243.6867 244.0496 279.7378 117.5468 -0.3644 243.8499 244.2143 279.8868 118.3385 -0.3695 244.0020 244.3714 280.0200 119.1608 -0.3711 244.1521 244.5232 280.1531 119.9225 -0.3744 244.2675 244.6419 280.2912 120.7745 -0.3784 244.4054 244.7838 280.4620 121.5665 -0.3775 244.5467 244.9243 280.5923 122.3585 -0.3809 244.7078 245.0886 280.7355 123.1805 -0.3816 244.8604 245.2420 280.8697 123.9425 -0.3818 245.0082 245.3901 280.9927 124.7945 -0.3856 245.1637 245.5493 281.1284 125.5865 -0.3851 245.3163 245.7014 281.2771 126.3785 -0.3869 245.4547 245.8416 281.4167 127.2005 -0.3887 245.6175 246.0062 281.5393 127.9625 -0.3906 245.7742 246.1648 281.6707 128.8145 -0.3926 245.9341 246.3267 281.8060 129.6070 -0.3952 246.0873 246.4825 281.9463 130.3990 -0.4024 246.2239 246.6262 282.0556 131.2215 -0.4032 246.3738 246.7770 282.1776 131.9830 -0.4017 246.5221 246.9238 282.2988 132.8353 -0.4024 246.6627 247.0651 282.4392 133.6270 -0.4066 246.8144 247.2210 282.5712 134.4185 -0.4072 246.9656 247.3729 282.6811 135.2410 -0.4121 247.1385 247.5505 282.8163 136.0025 -0.4140 247.2683 247.6823 282.9169 136.8550 -0.4114 247.4145 247.8259 283.0592 137.6470 -0.4130 247.5623 247.9754 283.1854 138.4395 -0.4145 247.7000 248.1144 283.2947 139.2623 -0.4196 247.8457 248.2653 283.4152 140.0245 -0.4182 247.9871 248.4053 283.5213 140.8770 -0.4159 248.1516 248.5675 283.6457 141.6690 -0.4232 248.3066 248.7297 283.7656 142.4615 -0.4254 248.4613 248.8867 283.8995 143.2838 -0.4279 248.5926 249.0204 284.0083 144.0455 -0.4280 248.7256 249.1537 284.1304 144.8983 -0.4273 248.8936 249.3209 284.2744 145.6908 -0.4303 249.0515 249.4818 284.3862 146.4825 -0.4354 249.1693 249.6046 284.5078 147.3010 -0.4387 249.3141 249.7528 284.6510 148.0600 -0.4403 249.4634 249.9037 284.7637 148.9080 -0.4398 249.6387 250.0785 284.9106 149.6965 -0.4417 249.7893 250.2310 285.0193 150.4850 -0.4394 249.9340 250.3734 285.1637 151.3020 -0.4429 250.0663 250.5092 285.2952 152.0610 -0.4448 250.2070 250.6518 285.4398 152.9090 -0.4447 250.3678 250.8125 285.5824 153.6970 -0.4476 250.5123 250.9599 285.7037 154.4955 -0.4503 250.6302 251.0806 285.8332 155.2935 -0.4519 250.8012 251.2531 285.9535 156.0830 -0.4533 250.9495 251.4028 286.0874 156.9315 -0.4540 251.0946 251.5486 286.2194 157.6900 -0.4588 251.2390 251.6978 286.3433 158.5088 -0.4600 251.3881 251.8482 286.5025 159.3273 -0.4583 251.5329 251.9912 286.6348 160.0870 -0.4609 251.6818 252.1427 286.7479 160.9363 -0.4654 251.8278 252.2931 286.9117 161.7260 -0.4642 251.9702 252.4344 287.0493 162.5158 -0.4653 252.1109 252.5761 287.1974 163.3355 -0.4690 252.2847 252.7537 287.3192 164.0953 -0.4689 252.4110 252.8800 287.4502 164.9463 -0.4731 252.5547 253.0278 287.6115 165.7363 -0.4770 252.6892 253.1663 287.7393 166.5270 -0.4809 252.8326 253.3135 287.8772 167.3485 -0.4814 252.9978 253.4792 288.0393 168.1105 -0.4855 253.1469 253.6324 288.1444 168.9625 -0.4879 253.3378 253.8257 288.3116 169.7545 -0.4904 253.4504 253.9408 288.4554 170.5465 -0.4930 253.5829 254.0758 288.5856 171.3685 -0.4913 253.7446 254.2359 288.7099 172.1305 -0.4937 253.8546 254.3483 288.8196 172.9825 -0.4981 254.0136 254.5117 288.9584 173.7745 -0.4976 254.1593 254.6569 289.1008 174.5665 -0.4986 254.3105 254.8091 289.2515 175.3885 -0.5002 254.4540 254.9542 289.3812 176.1505 -0.5033 254.5800 255.0833 289.4991 177.0025 -0.5033 254.7498 255.2531 289.6297 177.7945 -0.5045 254.9076 255.4122 289.7756 178.5865 -0.5106 255.0559 255.5665 289.9293 179.4085 -0.5105 255.2110 255.7215 290.0548 180.1703 -0.5155 255.3349 255.8504 290.1948 181.0220 -0.5161 255.4921 256.0081 290.3457 181.8143 -0.5196 255.6526 256.1722 290.4842 182.6055 -0.5217 255.7877 256.3093 290.6217 183.4283 -0.5222 255.9180 256.4401 290.7541 184.2200 -0.5251 256.0512 256.5763 290.8832 185.0418 -0.5256 256.2103 256.7359 291.0225 185.8340 -0.5252 256.3659 256.8912 291.1456 186.6255 -0.5300 256.5069 257.0369 291.2736 187.4480 -0.5295 256.6564 257.1859 291.4272 188.2398 -0.5319 256.8231 257.3549 291.5660 189.0618 -0.5321 256.9608 257.4929 291.6841 189.8540 -0.5335 257.0848 257.6184 291.8156 190.6455 -0.5399 257.2182 257.7581 291.9380 191.4978 -0.5424 257.3935 257.9358 292.1188 192.2598 -0.5462 257.5336 258.0798 292.2312 193.0818 -0.5450 257.6805 258.2254 292.3524 193.8738 -0.5501 257.8229 258.3730 292.4870 194.6655 -0.5508 257.9699 258.5207 292.6124 195.5178 -0.5538 258.1311 258.6849 292.7636 196.2795 -0.5564 258.2689 258.8253 292.8918 197.1018 -0.5554 258.4186 258.9740 293.0284 197.9240 -0.5585 258.5438 259.1023 293.1585 198.6865 -0.5608 258.7020 259.2628 293.2781 199.5388 -0.5603 258.8474 259.4076 293.4300 200.3005 -0.5640 258.9748 259.5387 293.5579 201.1225 -0.5656 259.1275 259.6931 293.7075 201.9445 -0.5689 259.2877 259.8565 293.8529 202.7065 -0.5692 259.4369 260.0060 293.9482 203.5585 -0.5744 259.5661 260.1404 294.0794 204.3205 -0.5760 259.7130 260.2890 294.2147 205.1425 -0.5802 259.8532 260.4334 294.3501 205.9493 -0.5827 260.0186 260.6013 294.4790 206.7455 -0.5814 260.1610 260.7424 294.6197 207.5678 -0.5847 260.2991 260.8838 294.7453 208.3305 -0.5874 260.4368 261.0241 294.8856 209.1825 -0.5856 260.6112 261.1968 295.0080 209.9443 -0.5890 260.7401 261.3291 295.1083 210.7653 -0.5922 260.8829 261.4751 295.2314 211.5833 -0.5911 261.0504 261.6415 295.3740 212.3410 -0.5886 261.1940 261.7826 295.5060 213.1893 -0.5944 261.3327 261.9271 295.6560 213.9473 -0.5979 261.4607 262.0586 295.7781 214.7653 -0.6000 261.6060 262.2059 295.8876 215.5523 -0.6018 261.7437 262.3455 296.0193 216.3413 -0.6060 261.8889 262.4949 296.1448 217.1903 -0.6043 262.0580 262.6623 296.2731 217.9485 -0.6088 262.1980 262.8068 296.3854 218.7663 -0.6156 262.3317 262.9473 296.5189 219.5548 -0.6193 262.4636 263.0829 296.6715 220.3435 -0.6219 262.5980 263.2199 296.7923 221.1918 -0.6212 262.7581 263.3792 296.9089 221.9493 -0.6207 262.9006 263.5214 297.0564 222.7680 -0.6236 263.0603 263.6840 297.1706 223.5870 -0.6283 263.1980 263.8263 297.2962 224.3463 -0.6276 263.3138 263.9414 297.4089 225.1968 -0.6320 263.4833 264.1152 297.5420 225.9568 -0.6351 263.6344 264.2695 297.6607 226.7760 -0.6390 263.7801 264.4191 297.7820 227.5950 -0.6406 263.9456 264.5863 297.9322 228.3548 -0.6422 264.0730 264.7153 298.0613 229.2045 -0.6432 264.2383 264.8815 298.1624 229.9658 -0.6470 264.3645 265.0115 298.2928 230.7878 -0.6489 264.5070 265.1560 298.4286 231.5790 -0.6481 264.6368 265.2849 298.5336 232.3705 -0.6511 264.7932 265.4443 298.6408 233.2230 -0.6514 264.9520 265.6034 298.7918 233.9848 -0.6559 265.0768 265.7327 298.8995 234.8068 -0.6575 265.2315 265.8890 299.0217 235.5993 -0.6577 265.3641 266.0218 299.1472 236.3905 -0.6583 265.4953 266.1536 299.2969 237.2130 -0.6602 265.6322 266.2925 299.4132 238.0048 -0.6656 265.7691 266.4346 299.5293 238.8268 -0.6672 265.9385 266.6057 299.6388 239.6190 -0.6678 266.0838 266.7516 299.7502 240.4105 -0.6689 266.2279 266.8968 299.8704 241.2330 -0.6698 266.3611 267.0309 299.9986 241.9945 -0.6731 266.5017 267.1748 300.1378 242.8470 -0.6762 266.6512 267.3274 300.2994 243.6388 -0.6771 266.8204 267.4975 300.3971 244.4305 -0.6779 266.9489 267.6268 300.5196 245.2528 -0.6789 267.0982 267.7771 300.6549 246.0145 -0.6835 267.2443 267.9278 300.8071 246.8668 -0.6851 267.3822 268.0673 300.9303 247.6585 -0.6875 267.5270 268.2145 301.0388 248.4505 -0.6882 267.6728 268.3610 301.1738 249.2725 -0.6915 267.8044 268.4959 301.3146 250.0345 -0.6940 267.9344 268.6284 301.4471 250.8865 -0.6937 268.0861 268.7798 301.5804 251.6785 -0.6966 268.2459 268.9426 301.7279 252.4705 -0.6996 268.3879 269.0875 301.8687 253.2925 -0.7018 268.5258 269.2276 302.0037 254.0545 -0.7038 268.6832 269.3871 302.1398 254.9065 -0.7053 268.8184 269.5237 302.2784 255.6985 -0.7078 268.9462 269.6540 302.4284 256.4905 -0.7113 269.1006 269.8119 302.5706 257.3125 -0.7109 269.2443 269.9551 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