DTA measure 1pb4 Date: 202535:1026 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.77 s Mass = 958.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2936 0.9330 207.6732 206.7401 206.8477 3.8885 0.9334 207.6704 206.7370 206.8080 5.4981 0.9326 207.6417 206.7091 206.7707 7.0966 0.9313 207.6401 206.7088 206.7357 8.7244 0.9308 207.6188 206.6880 206.7004 10.3229 0.9283 207.6128 206.6845 206.6821 11.9218 0.9295 207.6107 206.6812 206.6576 13.5208 0.9333 207.6081 206.6748 206.6328 15.1198 0.9290 207.6009 206.6718 206.6392 16.7489 0.9270 207.5796 206.6526 206.6576 18.3479 0.9282 207.5727 206.6445 206.6681 19.9468 0.9256 207.5740 206.6484 206.6933 21.5608 0.9259 207.5578 206.6319 206.7322 23.1598 0.9233 207.5494 206.6260 206.7845 24.7605 0.9232 207.5265 206.6032 206.8563 26.3866 0.9263 207.5348 206.6085 206.9381 28.0006 0.9223 207.5501 206.6279 207.0311 29.5995 0.9189 207.5200 206.6011 207.1458 31.1985 0.9202 207.5132 206.5930 207.2812 32.8125 0.9159 207.5093 206.5934 207.4117 34.4265 0.9159 207.4893 206.5734 207.5768 36.0394 0.9134 207.4854 206.5719 207.7540 37.6405 0.9098 207.4863 206.5765 207.9421 39.2548 0.9080 207.4822 206.5743 208.1096 40.8543 0.9069 207.4884 206.5815 208.3050 42.4680 0.9038 207.4719 206.5681 208.5262 44.0828 0.8993 207.4714 206.5721 208.7514 45.6818 0.8925 207.4774 206.5848 208.9824 47.2958 0.8924 207.4984 206.6060 209.1976 48.8948 0.8851 207.4847 206.5996 209.4389 50.5246 0.8780 207.4887 206.6107 209.6873 52.1229 0.8751 207.4898 206.6147 209.9317 53.7310 0.8737 207.4846 206.6109 210.1707 55.3221 0.8690 207.4986 206.6296 210.4195 56.9218 0.8652 207.5079 206.6427 210.6855 58.5281 0.8625 207.5008 206.6383 210.9352 60.1340 0.8577 207.5188 206.6612 211.1712 61.7403 0.8556 207.5214 206.6658 211.4226 63.3326 0.8496 207.5394 206.6898 211.6787 64.9396 0.8437 207.5612 206.7175 211.9367 66.5628 0.8415 207.5730 206.7315 212.1958 68.1566 0.8328 207.5784 206.7456 212.4488 69.7529 0.8269 207.6016 206.7747 212.7051 71.3648 0.8244 207.6223 206.7979 212.9306 72.9766 0.8179 207.6443 206.8264 213.1573 74.5906 0.8149 207.6512 206.8363 213.3895 76.1895 0.8121 207.6741 206.8620 213.5913 77.7885 0.8071 207.7026 206.8955 213.8234 79.4025 0.7986 207.7199 206.9213 214.0420 81.0015 0.7970 207.7555 206.9585 214.2460 82.6305 0.7936 207.7779 206.9843 214.4565 84.2295 0.7873 207.8092 207.0219 214.6603 85.8285 0.7855 207.8371 207.0516 214.8648 87.4425 0.7796 207.8505 207.0708 215.0557 89.0413 0.7761 207.8845 207.1084 215.2510 90.6551 0.7694 207.9222 207.1528 215.4613 92.2690 0.7683 207.9554 207.1871 215.6455 93.8679 0.7629 207.9935 207.2305 215.8263 95.4668 0.7583 208.0166 207.2583 216.0218 97.0839 0.7566 208.0583 207.3017 216.2096 98.6998 0.7548 208.1050 207.3501 216.3946 100.2989 0.7474 208.1361 207.3887 216.5527 101.9126 0.7433 208.1732 207.4299 216.7344 103.5116 0.7423 208.2297 207.4874 216.9072 105.1105 0.7361 208.2632 207.5271 217.0708 106.7396 0.7287 208.2939 207.5652 217.2815 108.3385 0.7266 208.3374 207.6108 217.4426 109.9529 0.7209 208.3852 207.6643 217.6197 111.5529 0.7184 208.4445 207.7261 217.7882 113.1530 0.7174 208.4895 207.7722 217.9771 114.7675 0.7130 208.5475 207.8345 218.1559 116.3808 0.7092 208.6041 207.8949 218.3528 117.9730 0.7046 208.6384 207.9338 218.5294 119.5645 0.7035 208.6786 207.9751 218.7235 121.1708 0.6993 208.7380 208.0387 218.9172 122.7618 0.6958 208.7862 208.0904 219.0811 124.3830 0.6940 208.8443 208.1503 219.2927 125.9751 0.6864 208.8906 208.2043 219.4856 127.5824 0.6812 208.9622 208.2810 219.6747 129.1754 0.6798 209.0244 208.3446 219.8844 130.7988 0.6755 209.0889 208.4134 220.0809 132.3934 0.6704 209.1426 208.4721 220.2753 134.0044 0.6686 209.2008 208.5322 220.4990 135.6011 0.6625 209.2617 208.5993 220.7068 137.2000 0.6626 209.3158 208.6532 220.9179 138.8290 0.6611 209.3892 208.7282 221.1342 140.4280 0.6570 209.4406 208.7836 221.3386 142.0268 0.6518 209.5308 208.8789 221.5468 143.6408 0.6448 209.5837 208.9388 221.7652 145.2398 0.6412 209.6574 209.0161 221.9796 146.8539 0.6397 209.7371 209.0974 222.2046 148.4679 0.6350 209.7977 209.1627 222.3949 150.0668 0.6265 209.8669 209.2403 222.6200 151.6806 0.6240 209.9329 209.3089 222.8314 153.2796 0.6181 210.0190 209.4009 223.0324 154.9086 0.6144 210.0906 209.4762 223.2544 156.5076 0.6092 210.1792 209.5700 223.4768 158.1215 0.6033 210.2341 209.6309 223.6747 159.7205 0.5959 210.3291 209.7332 223.8873 161.3345 0.5951 210.3996 209.8045 224.1007 162.9485 0.5903 210.4831 209.8927 224.3258 164.5625 0.5838 210.5630 209.9792 224.5185 166.1615 0.5797 210.6328 210.0531 224.7360 167.7755 0.5756 210.7285 210.1529 224.9451 169.3895 0.5741 210.8157 210.2416 225.1441 171.0038 0.5685 210.9030 210.3345 225.3508 172.6028 0.5635 210.9912 210.4277 225.5447 174.2168 0.5616 211.0780 210.5165 225.7349 175.8158 0.5593 211.1701 210.6108 225.9491 177.4305 0.5607 211.2641 210.7034 226.1400 179.0449 0.5557 211.3442 210.7885 226.3408 180.6596 0.5479 211.4344 210.8865 226.5573 182.2541 0.5547 211.5391 210.9844 226.7710 183.8450 0.5603 211.6350 211.0747 226.9520 185.4361 0.5589 211.7264 211.1675 227.1339 187.0571 0.5557 211.8162 211.2604 227.3368 188.6483 0.5536 211.9128 211.3592 227.5138 190.2405 0.5561 212.0203 211.4642 227.7161 191.8470 0.5546 212.1061 211.5515 227.9089 193.4539 0.5482 212.2179 211.6696 228.0918 195.0619 0.5288 212.3046 211.7758 228.3123 196.6561 0.5215 212.4287 211.9072 228.5163 198.2536 0.5188 212.5151 211.9963 228.7202 199.8503 0.5188 212.6109 212.0922 228.9166 201.4676 0.5122 212.7165 212.2043 229.1326 203.0665 0.5080 212.8226 212.3146 229.3359 204.6806 0.5075 212.9352 212.4276 229.5579 206.2945 0.5036 213.0193 212.5158 229.7534 207.8935 0.5010 213.1445 212.6435 229.9572 209.4971 0.5012 213.2434 212.7422 230.1623 211.1005 0.4970 213.3519 212.8549 230.3834 212.6995 0.4892 213.4741 212.9849 230.5862 214.3135 0.4879 213.5829 213.0949 230.8012 215.9275 0.4849 213.6997 213.2148 231.0246 217.5263 0.4829 213.8075 213.3246 231.2250 219.1250 0.4807 213.9117 213.4309 231.4290 220.7389 0.4763 214.0519 213.5756 231.6627 222.3529 0.4725 214.1481 213.6756 231.8648 223.9669 0.4691 214.2694 213.8003 232.0502 225.5658 0.4671 214.3933 213.9262 232.2595 227.1648 0.4647 214.4941 214.0294 232.4612 228.7788 0.4624 214.6150 214.1526 232.6939 230.3909 0.4601 214.7320 214.2719 232.9133 232.0099 0.4526 214.8525 214.3999 233.1174 233.6089 0.4480 214.9845 214.5365 233.2902 235.2086 0.4428 215.1046 214.6618 233.4981 236.8225 0.4375 215.2242 214.7867 233.7148 238.4215 0.4372 215.3291 214.8918 233.9218 240.0505 0.4322 215.4778 215.0455 234.1202 241.6495 0.4293 215.5942 215.1649 234.3332 243.2639 0.4259 215.7205 215.2946 234.5204 244.8634 0.4226 215.8480 215.4254 234.7351 246.4716 0.4207 215.9780 215.5573 234.9378 248.0769 0.4186 216.1170 215.6983 235.1289 249.6689 0.4155 216.2252 215.8097 235.3035 251.2761 0.4098 216.3533 215.9435 235.4994 252.8680 0.4047 216.4941 216.0894 235.6889 254.4900 0.4031 216.6009 216.1978 235.8841 256.0971 0.3975 216.7433 216.3458 236.1026 257.6894 0.3960 216.8890 216.4930 236.2887 259.2978 0.3926 217.0150 216.6224 236.4990 260.9069 0.3850 217.1506 216.7655 236.7108 262.5181 0.3848 217.2856 216.9008 236.9269 264.1161 0.3834 217.4308 217.0474 237.1560 265.7149 0.3835 217.5671 217.1836 237.3464 267.3288 0.3779 217.6973 217.3195 237.5750 268.9278 0.3769 217.8282 217.4513 237.7807 270.5570 0.3749 217.9656 217.5907 238.0155 272.1558 0.3730 218.1175 217.7445 238.2263 273.7548 0.3661 218.2549 217.8888 238.4401 275.3688 0.3632 218.3923 218.0291 238.6658 276.9678 0.3592 218.5360 218.1768 238.8786 278.5970 0.3543 218.6682 218.3140 239.1108 280.1956 0.3509 218.8063 218.4554 239.3183 281.8128 0.3495 218.9522 218.6027 239.5510 283.4146 0.3451 219.0895 218.7443 239.7531 285.0135 0.3425 219.2579 218.9154 239.9673 286.6426 0.3394 219.4211 219.0817 240.1892 288.2415 0.3332 219.5446 219.2114 240.3932 289.8563 0.3321 219.6796 219.3475 240.5976 291.4565 0.3303 219.8199 219.4897 240.8175 293.0561 0.3301 219.9729 219.6427 241.0344 294.6855 0.3285 220.1294 219.8009 241.2471 296.2845 0.3254 220.2849 219.9594 241.4729 297.8984 0.3219 220.4381 220.1162 241.6631 299.4978 0.3183 220.5629 220.2445 241.8655 301.0999 0.3532 220.7361 220.3830 242.0846 302.7039 0.3268 220.8831 220.5563 242.3032 304.3335 0.3152 221.0397 220.7246 242.5009 305.9328 0.3114 221.1879 220.8764 242.7000 307.5466 0.3123 221.3243 221.0120 242.9127 309.1454 0.3078 221.5029 221.1951 243.1179 310.7388 0.3078 221.6382 221.3303 243.3204 312.3366 0.3068 221.7879 221.4811 243.4945 313.9451 0.3051 221.9486 221.6434 243.6996 315.5511 0.3046 222.1123 221.8077 243.9003 317.1430 0.2974 222.2718 221.9744 244.1012 318.7340 0.2958 222.4192 222.1234 244.2867 320.3405 0.2916 222.5843 222.2928 244.4781 321.9440 0.2895 222.7463 222.4568 244.6988 323.5549 0.2871 222.9133 222.6262 244.8816 325.1634 0.2804 223.0651 222.7846 245.0966 326.7590 0.2817 223.2270 222.9453 245.2955 328.3565 0.2782 223.3903 223.1121 245.4808 329.9705 0.2797 223.5521 223.2724 245.6772 331.5845 0.2755 223.7199 223.4445 245.8591 333.1835 0.2706 223.8527 223.5821 246.0587 334.7975 0.2706 224.0221 223.7515 246.2468 336.3965 0.2648 224.1791 223.9143 246.4349 337.9955 0.2654 224.3561 224.0907 246.6414 339.6095 0.2617 224.5189 224.2572 246.8550 341.2235 0.2551 224.6846 224.4295 247.0702 342.8225 0.2534 224.8499 224.5965 247.2733 344.4360 0.2519 225.0105 224.7586 247.4725 346.0350 0.2473 225.1860 224.9387 247.6981 347.6493 0.2473 225.3495 225.1022 247.9228 349.2629 0.2447 225.5204 225.2757 248.1335 350.8618 0.2388 225.6890 225.4502 248.3492 352.4758 0.2433 225.8415 225.5983 248.5646 354.0748 0.2401 226.0080 225.7679 248.7706 355.6889 0.2418 226.1762 225.9345 248.9897 357.3028 0.2309 226.3356 226.1047 249.2232 358.9026 0.2319 226.5153 226.2834 249.4452 360.5166 0.2255 226.6880 226.4625 249.6474 362.1156 0.2067 226.8620 226.6552 249.8687 363.7445 0.2011 227.0401 226.8389 250.0962 365.3435 0.1955 227.2023 227.0068 250.3022 366.9575 0.1953 227.3826 227.1873 250.5207 368.5565 0.1912 227.5581 227.3669 250.7429 370.1705 0.1858 227.7168 227.5310 250.9658 371.7995 0.1835 227.8804 227.6969 251.1910 373.3976 0.1805 228.0595 227.8790 251.3908 374.9894 0.1774 228.2345 228.0571 251.6260 376.5954 0.1732 228.4187 228.2454 251.8361 378.1865 0.1718 228.5922 228.4204 252.0451 379.8078 0.1709 228.7615 228.5906 252.2671 381.3990 0.1666 228.9344 228.7678 252.4802 382.9911 0.1629 229.1191 228.9563 252.7020 384.5991 0.1601 229.3090 229.1489 252.9032 386.2079 0.1559 229.4800 229.3241 253.1273 387.8180 0.1531 229.6542 229.5011 253.3358 389.4138 0.1478 229.8271 229.6793 253.5387 391.0251 0.1446 230.0216 229.8770 253.7429 392.6238 0.1429 230.2042 230.0612 253.9565 394.2374 0.1408 230.3788 230.2380 254.1613 395.8509 0.1352 230.5486 230.4135 254.3869 397.4498 0.1332 230.7174 230.5842 254.5861 399.0638 0.1316 230.8986 230.7670 254.8064 400.6628 0.1304 231.0949 230.9645 255.0053 402.2768 0.1241 231.2634 231.1393 255.2059 403.8909 0.1160 231.4348 231.3187 255.4262 405.4916 0.1136 231.6273 231.5137 255.6080 407.1056 0.1112 231.8135 231.7023 255.8133 408.7045 0.1061 231.9992 231.8931 256.0151 410.3185 0.1037 232.1601 232.0564 256.2278 411.9326 0.0969 232.3629 232.2660 256.4155 413.5315 0.0962 232.5364 232.4402 256.6352 415.1459 0.0962 232.7310 232.6348 256.8269 416.7455 0.0930 232.9144 232.8214 257.0251 418.3745 0.0916 233.1027 233.0111 257.2350 419.9744 0.0872 233.2758 233.1886 257.4153 421.5884 0.0873 233.4620 233.3748 257.6176 423.1875 0.0857 233.6358 233.5502 257.8066 424.7869 0.0793 233.8379 233.7586 258.0132 426.4159 0.0742 234.0243 233.9501 258.2080 428.0299 0.0733 234.2071 234.1339 258.3813 429.6288 0.0717 234.3888 234.3171 258.5971 431.2278 0.0709 234.5780 234.5071 258.7761 432.8418 0.0680 234.7583 234.6903 258.9532 434.4708 0.0653 234.9732 234.9079 259.1692 436.0709 0.0641 235.1298 235.0657 259.3584 437.6706 0.0617 235.3264 235.2647 259.5476 439.2800 0.0593 235.5032 235.4439 259.7579 440.8710 0.0555 235.7012 235.6457 259.9842 442.4930 0.0543 235.8910 235.8367 260.1794 444.0854 0.0504 236.0840 236.0336 260.3797 445.6930 0.0475 236.2734 236.2258 260.5925 447.2844 0.0437 236.4566 236.4129 260.8230 448.8918 0.0431 236.6568 236.6137 261.0462 450.5004 0.0401 236.8496 236.8095 261.2500 452.1103 0.0375 237.0319 236.9944 261.4814 453.7044 0.0325 237.2171 237.1846 261.7232 455.3133 0.0304 237.4066 237.3762 261.9315 456.9255 0.0270 237.6010 237.5740 262.1471 458.5380 0.0237 237.7905 237.7668 262.3773 460.1358 0.0208 237.9723 237.9515 262.5909 461.7345 0.0184 238.1759 238.1575 262.8226 463.3485 0.0149 238.3567 238.3418 263.0599 464.9625 0.0137 238.5570 238.5433 263.2858 466.5765 0.0104 238.7595 238.7491 263.5097 468.1755 0.0095 238.9558 238.9463 263.7413 469.7744 0.0019 239.1371 239.1352 263.9663 471.3885 -0.0013 239.3374 239.3387 264.1978 473.0023 -0.0023 239.5332 239.5355 264.4185 474.6159 -0.0071 239.7127 239.7198 264.6316 476.2151 -0.0083 239.9008 239.9091 264.8708 477.8148 -0.0114 240.1041 240.1155 265.0657 479.4288 -0.0162 240.3062 240.3224 265.2993 481.0580 -0.0198 240.5068 240.5266 265.5098 482.6566 -0.0248 240.7048 240.7296 265.7274 484.2559 -0.0281 240.9057 240.9338 265.9252 485.8698 -0.0306 241.0980 241.1286 266.1194 487.4686 -0.0341 241.2840 241.3180 266.3040 489.0978 -0.0378 241.4802 241.5181 266.4865 490.6966 -0.0417 241.6859 241.7276 266.6735 492.3105 -0.0444 241.8790 241.9234 266.8643 493.9100 -0.0483 242.0711 242.1194 267.0399 495.5395 -0.0497 242.2842 242.3339 267.2251 497.1385 -0.0527 242.4705 242.5232 267.4357 498.7525 -0.0546 242.6714 242.7260 267.6243 500.3518 -0.0587 242.8746 242.9333 267.8240 501.9656 -0.0618 243.0795 243.1413 267.9990 503.5745 -0.0651 243.2826 243.3477 268.2107 505.1821 -0.0697 243.4680 243.5377 268.3950 506.7765 -0.0695 243.6814 243.7509 268.6088 508.3703 -0.0678 243.8706 243.9384 268.7858 509.9621 -0.0713 244.0707 244.1420 268.9845 511.5850 -0.0756 244.2761 244.3517 269.1837 513.1785 -0.0823 244.4667 244.5490 269.3875 514.7869 -0.0858 244.6494 244.7353 269.5796 516.3819 -0.0902 244.8590 244.9491 269.7766 517.9919 -0.0937 245.0577 245.1514 269.9587 519.6173 -0.0965 245.2523 245.3488 270.1793 521.2148 -0.1010 245.4691 245.5701 270.3741 522.8130 -0.1017 245.6630 245.7647 270.5875 524.4268 -0.1082 245.8600 245.9682 270.8034 526.0258 -0.1114 246.0568 246.1682 271.0277 527.6549 -0.1153 246.2565 246.3718 271.2603 529.2538 -0.1187 246.4689 246.5876 271.4752 530.8528 -0.1201 246.6614 246.7815 271.6850 532.4666 -0.1253 246.8600 246.9853 271.9152 534.0658 -0.1297 247.0670 247.1967 272.1742 535.6948 -0.1347 247.2725 247.4073 272.3910 537.2936 -0.1355 247.4648 247.6003 272.6324 538.9076 -0.1384 247.6827 247.8211 272.8659 540.5065 -0.1405 247.8729 248.0134 273.1060 542.1205 -0.1467 248.0739 248.2206 273.3386 543.7345 -0.1474 248.2713 248.4187 273.5564 545.3485 -0.1504 248.4804 248.6308 273.7766 546.9475 -0.1531 248.7026 248.8557 273.9862 548.5465 -0.1588 248.8826 249.0414 274.2050 550.1754 -0.1595 249.0983 249.2578 274.4234 551.7891 -0.1641 249.3031 249.4673 274.6273 553.3880 -0.1684 249.5154 249.6838 274.8164 554.9878 -0.1709 249.7092 249.8801 275.0356 556.6024 -0.1741 249.9186 250.0927 275.2466 558.2320 -0.1779 250.1176 250.2956 275.4532 559.8308 -0.1823 250.3153 250.4977 275.6398 561.4308 -0.1858 250.5360 250.7218 275.8280 563.0448 -0.1848 250.7505 250.9352 276.0240 564.6586 -0.1889 250.9503 251.1392 276.2049 566.2719 -0.1935 251.1569 251.3503 276.4239 567.8641 -0.1943 251.3442 251.5385 276.5983 569.4550 -0.1992 251.5706 251.7698 276.7895 571.0610 -0.2021 251.7797 251.9817 276.9663 572.6676 -0.2050 251.9921 252.1970 277.1793 574.2740 -0.2086 252.1769 252.3854 277.3717 575.8655 -0.2128 252.3711 252.5839 277.5785 577.4734 -0.2166 252.5733 252.7899 277.7736 579.0669 -0.2169 252.7864 253.0033 277.9820 580.6916 -0.2233 253.0113 253.2347 278.1999 582.2859 -0.2247 253.2138 253.4384 278.3967 583.8958 -0.2311 253.4164 253.6474 278.6211 585.4928 -0.2350 253.6116 253.8466 278.8281 587.0915 -0.2384 253.8107 254.0491 279.0384 588.7205 -0.2432 254.0338 254.2770 279.2630 590.3195 -0.2467 254.2277 254.4745 279.4527 591.9185 -0.2489 254.4443 254.6932 279.6761 593.5325 -0.2545 254.6639 254.9184 279.8980 595.1315 -0.2553 254.8687 255.1240 280.0958 596.7455 -0.2532 255.0655 255.3187 280.3164 598.3594 -0.2565 255.2814 255.5379 280.5286 599.9581 -0.2607 255.4830 255.7436 280.7312 601.5593 -0.2642 255.6694 255.9337 280.9483 603.1759 -0.2674 255.8934 256.1608 281.1690 604.7748 -0.2708 256.1029 256.3737 281.3664 606.4040 -0.2723 256.3177 256.5899 281.5790 608.0028 -0.2745 256.5323 256.8068 281.7803 609.6018 -0.2794 256.7448 257.0242 281.9979 611.2156 -0.2849 256.9441 257.2289 282.2040 612.8146 -0.2878 257.1537 257.4415 282.4315 614.4436 -0.2898 257.3730 257.6628 282.6134 616.0428 -0.2957 257.5671 257.8628 282.8285 617.6429 -0.2988 257.7742 258.0730 283.0255 619.2575 -0.3034 257.9802 258.2835 283.2247 620.8565 -0.3082 258.1814 258.4896 283.4510 622.4880 -0.3102 258.4144 258.7246 283.6488 624.0876 -0.3112 258.6221 258.9332 283.8562 625.6876 -0.3181 258.8286 259.1467 284.0481 627.3021 -0.3213 259.0401 259.3615 284.2598 628.9015 -0.3242 259.2618 259.5861 284.4566 630.5296 -0.3262 259.4620 259.7883 284.6601 632.1208 -0.3312 259.6684 259.9996 284.8651 633.7125 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