DTA measure 1Olom1 Date: 20251119:912 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.59 s Mass = 1367.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2615 -4.5244 184.6327 189.1571 246.6456 2.0483 -4.5197 184.8769 189.3967 246.5544 2.8448 -4.5098 185.1176 189.6273 246.4614 3.6728 -4.4973 185.3845 189.8819 246.3905 4.4388 -4.4898 185.6293 190.1191 246.3330 5.2970 -4.4779 185.8972 190.3750 246.2540 6.0533 -4.4679 186.1524 190.6203 246.1896 6.8810 -4.4596 186.4125 190.8722 246.1093 7.6468 -4.4464 186.6549 191.1013 246.0401 8.4645 -4.4334 186.8834 191.3169 245.9505 9.2615 -4.4199 187.1038 191.5237 245.9007 10.0580 -4.4074 187.3165 191.7239 245.8205 10.8758 -4.3956 187.5641 191.9598 245.7152 11.6523 -4.3876 187.7924 192.1800 245.6878 12.5000 -4.3756 188.0896 192.4652 245.6346 13.2665 -4.3627 188.3416 192.7043 245.5746 14.0940 -4.3503 188.5865 192.9368 245.5379 14.8805 -4.3429 188.8236 193.1665 245.5137 15.6778 -4.3352 189.0624 193.3976 245.4819 16.5053 -4.3249 189.2897 193.6146 245.4912 17.2713 -4.3134 189.5011 193.8145 245.4932 18.1300 -4.3050 189.7593 194.0643 245.4542 18.8855 -4.2918 189.9767 194.2685 245.4438 19.7235 -4.2775 190.2230 194.5005 245.4081 20.5105 -4.2700 190.4441 194.7141 245.3884 21.3073 -4.2585 190.6811 194.9396 245.3665 22.1348 -4.2448 190.9083 195.1531 245.3460 22.9013 -4.2348 191.1087 195.3435 245.3672 23.7593 -4.2202 191.3743 195.5946 245.3777 24.5153 -4.2107 191.5965 195.8072 245.4070 25.3535 -4.2021 191.8521 196.0543 245.4525 26.1400 -4.1927 192.0793 196.2720 245.4956 26.9470 -4.1797 192.3029 196.4826 245.4866 27.7648 -4.1680 192.5422 196.7102 245.5113 28.5413 -4.1575 192.7743 196.9318 245.5441 29.3890 -4.1417 193.0326 197.1743 245.5991 30.1555 -4.1212 193.2344 197.3556 245.6426 30.9830 -4.1046 193.4535 197.5581 245.6918 31.7798 -4.0880 193.6956 197.7836 245.7581 32.5770 -4.0737 193.8872 197.9609 245.8257 33.3943 -4.0628 194.1269 198.1897 245.9229 34.1705 -4.0509 194.3431 198.3941 246.0146 35.0190 -4.0451 194.5892 198.6342 246.1538 35.7850 -4.0378 194.8126 198.8503 246.2771 36.6125 -4.0331 195.0148 199.0479 246.4075 37.4098 -4.0214 195.2002 199.2217 246.5299 38.2068 -4.0050 195.4321 199.4371 246.6412 39.0238 -3.9913 195.6792 199.6705 246.7448 39.7903 -3.9795 195.8765 199.8560 246.8354 40.6388 -3.9646 196.1362 200.1008 246.9705 41.4043 -3.9519 196.3443 200.2962 247.1275 42.2220 -3.9363 196.5737 200.5100 247.2544 43.0193 -3.9276 196.7909 200.7185 247.3994 43.8155 -3.9145 197.0143 200.9288 247.5364 44.6435 -3.9064 197.2415 201.1479 247.6983 45.4100 -3.9013 197.4650 201.3663 247.8535 46.2270 -3.8922 197.6846 201.5767 248.0233 46.9933 -3.8765 197.8965 201.7729 248.1459 47.8520 -3.8644 198.1087 201.9731 248.3298 48.6073 -3.8549 198.3201 202.1750 248.4972 49.4455 -3.8486 198.5352 202.3838 248.6519 50.2325 -3.8442 198.7186 202.5627 248.8547 51.0288 -3.8288 198.9348 202.7636 249.0603 51.8568 -3.8168 199.1299 202.9467 249.2836 52.6230 -3.8001 199.3675 203.1677 249.5039 53.4810 -3.7881 199.5892 203.3773 249.6959 54.2373 -3.7797 199.7612 203.5409 249.8872 55.0753 -3.7677 200.0130 203.7807 250.1255 55.8615 -3.7561 200.2202 203.9764 250.3309 56.6588 -3.7443 200.4585 204.2028 250.5063 57.4865 -3.7294 200.6751 204.4045 250.7129 58.2523 -3.7210 200.8516 204.5726 250.8966 59.1110 -3.7130 201.1035 204.8165 251.0948 59.8670 -3.7009 201.2921 204.9930 251.2592 60.7045 -3.6867 201.4941 205.1808 251.4479 61.5018 -3.6769 201.6978 205.3747 251.6354 62.2985 -3.6629 201.9027 205.5657 251.8262 63.1158 -3.6550 202.1213 205.7763 252.0325 63.8925 -3.6469 202.3163 205.9632 252.2442 64.7403 -3.6336 202.5444 206.1779 252.4311 65.5065 -3.6259 202.7624 206.3883 252.6050 66.3345 -3.6196 203.0028 206.6224 252.8124 67.1310 -3.6102 203.2409 206.8512 253.0131 67.9280 -3.6063 203.3984 207.0046 253.1983 68.7560 -3.5971 203.6016 207.1987 253.4050 69.5218 -3.5865 203.8125 207.3989 253.5768 70.3495 -3.5779 204.0290 207.6068 253.7751 71.1058 -3.5727 204.2215 207.7942 253.8939 71.9635 -3.5613 204.3839 207.9453 254.1166 72.7198 -3.5535 204.5806 208.1340 254.3086 73.5478 -3.5518 204.8226 208.3744 254.4946 74.3443 -3.5467 205.0235 208.5702 254.7014 75.1310 -3.5484 205.1906 208.7390 254.9003 75.9590 -3.5488 205.3985 208.9474 255.1198 76.7245 -3.5480 205.5819 209.1299 255.2708 77.5525 -3.5470 205.7765 209.3235 255.4459 78.3190 -3.5488 205.9722 209.5210 255.6029 79.1668 -3.5466 206.1531 209.6997 255.7984 79.9433 -3.5403 206.3044 209.8447 255.9544 80.7610 -3.5321 206.5310 210.0631 256.1381 81.5473 -3.5342 206.7765 210.3107 256.3131 82.3545 -3.5265 206.9392 210.4657 256.4823 83.1723 -3.5225 207.1652 210.6877 256.6594 83.9385 -3.5220 207.3555 210.8776 256.8137 84.7965 -3.5152 207.6031 211.1183 256.9642 85.5425 -3.5007 207.8070 211.3078 257.0949 86.3905 -3.4871 208.0221 211.5092 257.2691 87.1565 -3.4747 208.2302 211.7048 257.4260 87.9845 -3.4605 208.4310 211.8915 257.5677 88.7815 -3.4509 208.6136 212.0645 257.7055 89.5780 -3.4438 208.7999 212.2437 257.8406 90.3958 -3.4415 209.0063 212.4478 257.9915 91.1720 -3.4360 209.1976 212.6336 258.1433 92.0200 -3.4328 209.4005 212.8333 258.2674 92.7660 -3.4260 209.5693 212.9953 258.3710 93.6143 -3.4192 209.7728 213.1920 258.4853 94.3903 -3.4126 209.9292 213.3419 258.5849 95.2080 -3.4047 210.1218 213.5265 258.7061 96.0153 -3.4008 210.3338 213.7346 258.8378 96.8015 -3.4026 210.5386 213.9412 258.9848 97.6398 -3.4030 210.7531 214.1561 259.1169 98.3958 -3.3945 210.9059 214.3004 259.2682 99.2640 -3.3852 211.1115 214.4967 259.4454 100.0203 -3.3803 211.2719 214.6522 259.5552 100.8583 -3.3772 211.4522 214.8294 259.6696 101.6445 -3.3681 211.6247 214.9928 259.7682 102.4418 -3.3649 211.8086 215.1735 259.8940 103.2390 -3.3537 211.9770 215.3307 260.0109 104.0253 -3.3465 212.1360 215.4825 260.1468 104.8428 -3.3423 212.3409 215.6832 260.2702 105.6195 -3.3369 212.5323 215.8693 260.3833 106.4670 -3.3362 212.7377 216.0739 260.5170 107.2540 -3.3304 212.9304 216.2608 260.6249 108.0613 -3.3221 213.1449 216.4670 260.7318 108.8475 -3.3177 213.3219 216.6396 260.8413 109.6345 -3.3176 213.5422 216.8599 260.9199 110.4728 -3.3158 213.7456 217.0613 261.0350 111.2280 -3.3091 213.9128 217.2219 261.1752 112.0868 -3.2990 214.0909 217.3899 261.3091 112.8533 -3.2927 214.2808 217.5736 261.4340 113.6805 -3.2872 214.4870 217.7742 261.5530 114.4775 -3.2862 214.6877 217.9739 261.6564 115.2645 -3.2882 214.8880 218.1762 261.7251 116.1020 -3.2802 215.1259 218.4061 261.8244 116.8580 -3.2729 215.3323 218.6052 261.8750 117.7168 -3.2679 215.5135 218.7815 262.0167 118.4825 -3.2622 215.6722 218.9344 262.1498 119.3103 -3.2608 215.8489 219.1097 262.2244 120.1075 -3.2585 216.0258 219.2843 262.3441 120.8935 -3.2513 216.1933 219.4446 262.4547 121.7318 -3.2470 216.3872 219.6341 262.5644 122.4880 -3.2432 216.5641 219.8073 262.6868 123.3463 -3.2428 216.7987 220.0415 262.8080 124.1123 -3.2391 217.0150 220.2541 262.9502 124.9403 -3.2346 217.1928 220.4274 263.0656 125.7063 -3.2307 217.3717 220.6023 263.1720 126.5440 -3.2275 217.5267 220.7542 263.3019 127.3310 -3.2245 217.6950 220.9195 263.4301 128.1383 -3.2188 217.9201 221.1388 263.5519 128.9553 -3.2133 218.1052 221.3185 263.6433 129.7218 -3.2087 218.2754 221.4842 263.7319 130.5805 -3.2078 218.5082 221.7160 263.8318 131.3463 -3.2025 218.6891 221.8916 263.9505 132.1740 -3.1999 218.8728 222.0727 264.1039 132.9713 -3.1981 219.0482 222.2463 264.2386 133.7680 -3.1912 219.2344 222.4256 264.3545 134.5853 -3.1878 219.4016 222.5894 264.4855 135.3415 -3.1817 219.5569 222.7386 264.5927 136.1998 -3.1704 219.7536 222.9240 264.7047 136.9658 -3.1636 219.9522 223.1157 264.8050 137.7835 -3.1612 220.1470 223.3083 264.8985 138.5800 -3.1551 220.3299 223.4850 265.0128 139.3770 -3.1486 220.5104 223.6590 265.1438 140.1948 -3.1479 220.6867 223.8346 265.2768 140.9705 -3.1423 220.8713 224.0136 265.3755 141.8190 -3.1393 221.0575 224.1968 265.5117 142.5855 -3.1374 221.2240 224.3614 265.6653 143.4125 -3.1338 221.3503 224.4841 265.8211 144.2098 -3.1283 221.5631 224.6915 265.9323 145.0070 -3.1238 221.7504 224.8742 266.0858 145.8238 -3.1214 221.9425 225.0639 266.2133 146.6005 -3.1147 222.1282 225.2429 266.3185 147.4490 -3.1076 222.3134 225.4211 266.4605 148.2145 -3.1017 222.4674 225.5691 266.5736 149.0425 -3.0961 222.6573 225.7534 266.7014 149.8398 -3.0942 222.8329 225.9270 266.8152 150.6360 -3.0942 223.0149 226.1091 266.9449 151.4538 -3.0890 223.2143 226.3032 267.0547 152.2305 -3.0835 223.3711 226.4546 267.1561 153.0780 -3.0804 223.5399 226.6203 267.3142 153.8445 -3.0736 223.6942 226.7677 267.4465 154.6725 -3.0704 223.9080 226.9784 267.5559 155.4488 -3.0674 224.0791 227.1464 267.6386 156.2660 -3.0643 224.2416 227.3059 267.7573 157.0633 -3.0625 224.4292 227.4917 267.9077 157.8598 -3.0582 224.6166 227.6749 268.0579 158.6875 -3.0507 224.7852 227.8359 268.2098 159.4540 -3.0481 224.9509 227.9990 268.3413 160.3020 -3.0487 225.1302 228.1789 268.4926 161.0783 -3.0509 225.3027 228.3536 268.6531 161.9063 -3.0501 225.4782 228.5283 268.8038 162.7028 -3.0420 225.6591 228.7011 268.9467 163.4895 -3.0385 225.8296 228.8680 269.0759 164.3278 -3.0340 226.0093 229.0433 269.2316 165.0833 -3.0266 226.1497 229.1763 269.3476 165.9520 -3.0244 226.4007 229.4251 269.4541 166.7083 -3.0214 226.5569 229.5783 269.5973 167.5358 -3.0207 226.7441 229.7648 269.6958 168.3223 -3.0208 226.9253 229.9461 269.8580 169.1195 -3.0145 227.0977 230.1121 270.0017 169.9470 -3.0080 227.2771 230.2851 270.1366 170.7028 -3.0053 227.4512 230.4565 270.2620 171.5308 -3.0003 227.6052 230.6055 270.4056 172.2865 -2.9964 227.7670 230.7634 270.5144 173.1448 -2.9929 227.9747 230.9676 270.6894 173.9113 -2.9924 228.1461 231.1386 270.8071 174.7288 -2.9922 228.2998 231.2920 270.9244 175.5253 -2.9897 228.5038 231.4936 271.0666 176.3225 -2.9850 228.6477 231.6327 271.1998 177.1300 -2.9828 228.8227 231.8055 271.3599 177.9365 -2.9823 228.9768 231.9591 271.4827 178.7543 -2.9771 229.1594 232.1365 271.5921 179.5205 -2.9734 229.3028 232.2762 271.7462 180.3785 -2.9694 229.5012 232.4706 271.8850 181.1450 -2.9669 229.6488 232.6157 271.9977 181.9728 -2.9577 229.8487 232.8064 272.1134 182.7283 -2.9512 230.0654 233.0167 272.2402 183.5665 -2.9564 230.2412 233.1977 272.3666 184.3533 -2.9550 230.4127 233.3677 272.4906 185.1498 -2.9531 230.5810 233.5341 272.6446 185.9778 -2.9492 230.7084 233.6576 272.8145 186.7440 -2.9417 230.8303 233.7720 272.9702 187.6020 -2.9380 231.0149 233.9528 273.1285 188.3583 -2.9335 231.1945 234.1280 273.2587 189.1960 -2.9304 231.3562 234.2867 273.3903 189.9825 -2.9326 231.5617 234.4944 273.5112 190.7798 -2.9285 231.7153 234.6438 273.6233 191.6075 -2.9229 231.8731 234.7960 273.7754 192.3733 -2.9170 232.0501 234.9671 273.8886 193.2320 -2.9147 232.2156 235.1302 273.9432 193.9883 -2.9126 232.3657 235.2783 274.0524 194.8255 -2.9106 232.5800 235.4906 274.1925 195.5920 -2.9085 232.7584 235.6669 274.3124 196.4200 -2.9042 232.9226 235.8268 274.4556 197.2060 -2.9024 233.0627 235.9652 274.6031 198.0135 -2.8999 233.2365 236.1365 274.7730 198.8313 -2.8951 233.4254 236.3206 274.9227 199.5868 -2.8949 233.5837 236.4786 275.0335 200.4453 -2.8924 233.7550 236.6475 275.1541 201.2118 -2.8921 233.8987 236.7908 275.2355 202.0288 -2.8900 234.0471 236.9371 275.3607 202.8258 -2.8882 234.1708 237.0590 275.5067 203.6230 -2.8858 234.3551 237.2408 275.6201 204.4093 -2.8847 234.5459 237.4305 275.7457 205.2165 -2.8873 234.7152 237.6026 275.9054 206.0343 -2.8899 234.9154 237.8052 276.0330 206.8003 -2.8887 235.0599 237.9486 276.1569 207.6585 -2.8802 235.2553 238.1356 276.3063 208.4250 -2.8715 235.4541 238.3256 276.4300 209.2530 -2.8661 235.6285 238.4946 276.5637 210.0390 -2.8655 235.8074 238.6729 276.6850 210.8465 -2.8644 235.9606 238.8250 276.8004 211.6333 -2.8631 236.1256 238.9887 276.9296 212.4400 -2.8644 236.2967 239.1611 277.1033 213.2578 -2.8645 236.4633 239.3278 277.2088 214.0340 -2.8630 236.6211 239.4841 277.3116 214.8820 -2.8592 236.7604 239.6195 277.4287 215.6483 -2.8616 236.8988 239.7604 277.5593 216.4755 -2.8586 237.0607 239.9193 277.7381 217.2728 -2.8508 237.2219 240.0727 277.8829 218.0700 -2.8507 237.3583 240.2090 278.0272 218.8663 -2.8471 237.4859 240.3330 278.1704 219.6635 -2.8471 237.6330 240.4800 278.2748 220.4915 -2.8461 237.8448 240.6909 278.4003 221.2573 -2.8482 238.0116 240.8597 278.5050 222.1055 -2.8501 238.1758 241.0259 278.6295 222.8823 -2.8475 238.3434 241.1909 278.7603 223.6993 -2.8474 238.5240 241.3714 278.9202 224.5065 -2.8425 238.6714 241.5139 279.0679 225.2935 -2.8378 238.8273 241.6651 279.2077 226.1308 -2.8302 238.9758 241.8060 279.3426 226.8870 -2.8276 239.1240 241.9516 279.4709 227.7455 -2.8242 239.2702 242.0944 279.6407 228.5113 -2.8220 239.4511 242.2731 279.7376 229.3495 -2.8246 239.6393 242.4638 279.9065 230.1363 -2.8227 239.7794 242.6021 280.0412 230.9328 -2.8211 239.9405 242.7616 280.1945 231.7608 -2.8234 240.1201 242.9434 280.3441 232.5168 -2.8222 240.2835 243.1056 280.4507 233.3645 -2.8177 240.4221 243.2398 280.5664 234.1413 -2.8136 240.6081 243.4217 280.7433 234.9590 -2.8177 240.7550 243.5727 280.8738 235.7450 -2.8179 240.9359 243.7538 281.0474 236.5423 -2.8142 241.0985 243.9127 281.1831 237.3703 -2.8106 241.2797 244.0903 281.2973 238.1258 -2.8084 241.4239 244.2322 281.4024 238.9945 -2.8079 241.6034 244.4113 281.5754 239.7508 -2.8053 241.7672 244.5724 281.7071 240.5680 -2.8026 241.9366 244.7393 281.8362 241.3750 -2.7988 242.1204 244.9191 282.0036 242.1620 -2.7977 242.2827 245.0805 282.1328 242.9893 -2.7976 242.4428 245.2405 282.2597 243.7555 -2.7951 242.5673 245.3624 282.3777 244.6143 -2.7903 242.7025 245.4928 282.5566 245.3490 -2.7897 242.8382 245.6280 282.7523 246.1975 -2.7945 242.9943 245.7888 282.8892 246.9738 -2.7912 243.1493 245.9405 282.9925 247.7910 -2.7950 243.3218 246.1168 283.1658 248.5985 -2.7940 243.4795 246.2734 283.3408 249.3853 -2.7950 243.6522 246.4472 283.5027 250.2228 -2.7963 243.8381 246.6343 283.6694 250.9790 -2.7890 243.9662 246.7552 283.8190 251.8375 -2.7840 244.1283 246.9124 283.9453 252.6033 -2.7840 244.3006 247.0846 284.0731 253.4313 -2.7827 244.4604 247.2431 284.1833 254.2283 -2.7815 244.6250 247.4065 284.3119 255.0145 -2.7795 244.7981 247.5776 284.4751 255.8528 -2.7800 244.9514 247.7313 284.5710 256.6190 -2.7784 245.1124 247.8907 284.6954 257.4770 -2.7763 245.2790 248.0552 284.8391 258.2333 -2.7796 245.4271 248.2068 284.9771 259.0710 -2.7817 245.6074 248.3891 285.1330 259.8575 -2.7815 245.7414 248.5229 285.2629 260.6548 -2.7817 245.8912 248.6729 285.3524 261.4825 -2.7803 246.0405 248.8208 285.4984 262.2483 -2.7750 246.1899 248.9650 285.6568 263.1070 -2.7711 246.2854 249.0566 285.7930 263.8628 -2.7715 246.4275 249.1990 285.9271 264.6903 -2.7709 246.6213 249.3922 286.0689 265.4773 -2.7674 246.7871 249.5545 286.1959 266.2740 -2.7662 246.9519 249.7181 286.3485 267.1015 -2.7694 247.0879 249.8573 286.5114 267.8578 -2.7710 247.2327 250.0037 286.5993 268.7160 -2.7730 247.4433 250.2163 286.7053 269.4820 -2.7758 247.6049 250.3807 286.8342 270.3100 -2.7731 247.7757 250.5488 286.9774 271.0658 -2.7719 247.9487 250.7205 287.1083 271.8933 -2.7707 248.1291 250.8999 287.2444 272.6905 -2.7706 248.2915 251.0621 287.3472 273.4773 -2.7737 248.4409 251.2146 287.4633 274.3148 -2.7775 248.5720 251.3495 287.5968 275.0710 -2.7740 248.6813 251.4553 287.7048 275.9295 -2.7683 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